CN113951335A - Rice germ oil composition and microcapsule product and preparation method thereof - Google Patents
Rice germ oil composition and microcapsule product and preparation method thereof Download PDFInfo
- Publication number
- CN113951335A CN113951335A CN202111310737.XA CN202111310737A CN113951335A CN 113951335 A CN113951335 A CN 113951335A CN 202111310737 A CN202111310737 A CN 202111310737A CN 113951335 A CN113951335 A CN 113951335A
- Authority
- CN
- China
- Prior art keywords
- rice germ
- germ oil
- oil composition
- rice
- raw materials
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 235000007164 Oryza sativa Nutrition 0.000 title claims abstract description 77
- 235000009566 rice Nutrition 0.000 title claims abstract description 77
- 239000000203 mixture Substances 0.000 title claims abstract description 69
- 239000003094 microcapsule Substances 0.000 title claims abstract description 18
- 238000002360 preparation method Methods 0.000 title abstract description 9
- 238000004519 manufacturing process Methods 0.000 title description 2
- 240000007594 Oryza sativa Species 0.000 title 1
- 239000003921 oil Substances 0.000 claims abstract description 86
- 235000019198 oils Nutrition 0.000 claims abstract description 86
- 241000209094 Oryza Species 0.000 claims abstract description 76
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 claims abstract description 40
- 238000003756 stirring Methods 0.000 claims abstract description 24
- 238000002156 mixing Methods 0.000 claims abstract description 20
- 235000016709 nutrition Nutrition 0.000 claims abstract description 18
- 229930003427 Vitamin E Natural products 0.000 claims abstract description 17
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 claims abstract description 17
- 235000019165 vitamin E Nutrition 0.000 claims abstract description 17
- 239000011709 vitamin E Substances 0.000 claims abstract description 17
- 229940046009 vitamin E Drugs 0.000 claims abstract description 17
- 239000002994 raw material Substances 0.000 claims abstract description 14
- 238000001694 spray drying Methods 0.000 claims abstract description 14
- 238000010438 heat treatment Methods 0.000 claims abstract description 10
- 239000000463 material Substances 0.000 claims abstract description 10
- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 claims abstract description 9
- 239000000787 lecithin Substances 0.000 claims abstract description 9
- 229940067606 lecithin Drugs 0.000 claims abstract description 9
- 235000010445 lecithin Nutrition 0.000 claims abstract description 9
- 230000035764 nutrition Effects 0.000 claims abstract description 8
- 239000000944 linseed oil Substances 0.000 claims abstract description 7
- 235000021388 linseed oil Nutrition 0.000 claims abstract description 7
- 230000001804 emulsifying effect Effects 0.000 claims abstract description 6
- 239000000843 powder Substances 0.000 claims description 16
- JLPULHDHAOZNQI-ZTIMHPMXSA-N 1-hexadecanoyl-2-(9Z,12Z-octadecadienoyl)-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCCCCCC\C=C/C\C=C/CCCCC JLPULHDHAOZNQI-ZTIMHPMXSA-N 0.000 claims description 12
- 239000011162 core material Substances 0.000 claims description 12
- 239000003995 emulsifying agent Substances 0.000 claims description 10
- 239000005913 Maltodextrin Substances 0.000 claims description 9
- 229920002774 Maltodextrin Polymers 0.000 claims description 9
- 229940035034 maltodextrin Drugs 0.000 claims description 9
- 229940083466 soybean lecithin Drugs 0.000 claims description 8
- 238000005303 weighing Methods 0.000 claims description 8
- LDVVTQMJQSCDMK-UHFFFAOYSA-N 1,3-dihydroxypropan-2-yl formate Chemical compound OCC(CO)OC=O LDVVTQMJQSCDMK-UHFFFAOYSA-N 0.000 claims description 7
- -1 ferulic acid ester Chemical class 0.000 claims description 7
- 108010073771 Soybean Proteins Proteins 0.000 claims description 6
- 235000019710 soybean protein Nutrition 0.000 claims description 6
- 235000020183 skimmed milk Nutrition 0.000 claims description 5
- 239000008347 soybean phospholipid Substances 0.000 claims description 5
- 235000019774 Rice Bran oil Nutrition 0.000 claims description 4
- 108010046377 Whey Proteins Proteins 0.000 claims description 4
- 102000007544 Whey Proteins Human genes 0.000 claims description 4
- LGJMUZUPVCAVPU-UHFFFAOYSA-N beta-Sitostanol Natural products C1CC2CC(O)CCC2(C)C2C1C1CCC(C(C)CCC(CC)C(C)C)C1(C)CC2 LGJMUZUPVCAVPU-UHFFFAOYSA-N 0.000 claims description 4
- NJKOMDUNNDKEAI-UHFFFAOYSA-N beta-sitosterol Natural products CCC(CCC(C)C1CCC2(C)C3CC=C4CC(O)CCC4C3CCC12C)C(C)C NJKOMDUNNDKEAI-UHFFFAOYSA-N 0.000 claims description 4
- 238000000034 method Methods 0.000 claims description 4
- 239000008165 rice bran oil Substances 0.000 claims description 4
- KZJWDPNRJALLNS-VJSFXXLFSA-N sitosterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CC[C@@H](CC)C(C)C)[C@@]1(C)CC2 KZJWDPNRJALLNS-VJSFXXLFSA-N 0.000 claims description 4
- 229950005143 sitosterol Drugs 0.000 claims description 4
- 229930003799 tocopherol Natural products 0.000 claims description 4
- 239000011732 tocopherol Substances 0.000 claims description 4
- 235000010384 tocopherol Nutrition 0.000 claims description 4
- 229960001295 tocopherol Drugs 0.000 claims description 4
- 235000021119 whey protein Nutrition 0.000 claims description 4
- GVJHHUAWPYXKBD-IEOSBIPESA-N α-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-IEOSBIPESA-N 0.000 claims description 4
- SGNBVLSWZMBQTH-FGAXOLDCSA-N Campesterol Natural products O[C@@H]1CC=2[C@@](C)([C@@H]3[C@H]([C@H]4[C@@](C)([C@H]([C@H](CC[C@H](C(C)C)C)C)CC4)CC3)CC=2)CC1 SGNBVLSWZMBQTH-FGAXOLDCSA-N 0.000 claims description 3
- BTEISVKTSQLKST-UHFFFAOYSA-N Haliclonasterol Natural products CC(C=CC(C)C(C)(C)C)C1CCC2C3=CC=C4CC(O)CCC4(C)C3CCC12C BTEISVKTSQLKST-UHFFFAOYSA-N 0.000 claims description 3
- 229940076810 beta sitosterol Drugs 0.000 claims description 3
- SGNBVLSWZMBQTH-PODYLUTMSA-N campesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CC[C@@H](C)C(C)C)[C@@]1(C)CC2 SGNBVLSWZMBQTH-PODYLUTMSA-N 0.000 claims description 3
- 235000000431 campesterol Nutrition 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 239000001335 perilla frutescens leaf extract Substances 0.000 claims description 3
- KSEBMYQBYZTDHS-HWKANZROSA-M (E)-Ferulic acid Natural products COC1=CC(\C=C\C([O-])=O)=CC=C1O KSEBMYQBYZTDHS-HWKANZROSA-M 0.000 claims description 2
- BBTIMXAYZRWPNG-UHFFFAOYSA-N 3beta,Delta4-stigmasten-3-ol Natural products C1CC2=CC(O)CCC2(C)C2C1C1CCC(C(C)CCC(CC)C(C)C)C1(C)CC2 BBTIMXAYZRWPNG-UHFFFAOYSA-N 0.000 claims description 2
- 235000001815 DL-alpha-tocopherol Nutrition 0.000 claims description 2
- 239000011627 DL-alpha-tocopherol Substances 0.000 claims description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 2
- 244000068988 Glycine max Species 0.000 claims description 2
- 235000010469 Glycine max Nutrition 0.000 claims description 2
- 150000001336 alkenes Chemical class 0.000 claims description 2
- QADVIPISOOQJMJ-WLKYTNTRSA-N beta-stigmasterol Natural products CCC(CC)C=C[C@@H](C)[C@H]1CC[C@@H]2[C@@H]1CC[C@H]3[C@H]2CC=C4C[C@@H](O)CC[C@]34C QADVIPISOOQJMJ-WLKYTNTRSA-N 0.000 claims description 2
- 239000005018 casein Substances 0.000 claims description 2
- BECPQYXYKAMYBN-UHFFFAOYSA-N casein, tech. Chemical compound NCCCCC(C(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(CC(C)C)N=C(O)C(CCC(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(C(C)O)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(COP(O)(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(N)CC1=CC=CC=C1 BECPQYXYKAMYBN-UHFFFAOYSA-N 0.000 claims description 2
- 235000021240 caseins Nutrition 0.000 claims description 2
- 235000013339 cereals Nutrition 0.000 claims description 2
- 150000001875 compounds Chemical class 0.000 claims description 2
- 210000002969 egg yolk Anatomy 0.000 claims description 2
- 229940114124 ferulic acid Drugs 0.000 claims description 2
- KSEBMYQBYZTDHS-UHFFFAOYSA-N ferulic acid Natural products COC1=CC(C=CC(O)=O)=CC=C1O KSEBMYQBYZTDHS-UHFFFAOYSA-N 0.000 claims description 2
- 235000001785 ferulic acid Nutrition 0.000 claims description 2
- 150000003904 phospholipids Chemical class 0.000 claims description 2
- 229940075999 phytosterol ester Drugs 0.000 claims description 2
- HCXVJBMSMIARIN-UHFFFAOYSA-N stigmasterol Chemical compound C1C=C2CC(O)CCC2(C)C2C1C1CCC(C(C)C=CC(CC)C(C)C)C1(C)CC2 HCXVJBMSMIARIN-UHFFFAOYSA-N 0.000 claims description 2
- 229940032091 stigmasterol Drugs 0.000 claims description 2
- 235000016831 stigmasterol Nutrition 0.000 claims description 2
- BFDNMXAIBMJLBB-UHFFFAOYSA-N stigmasterol Natural products CCC(C=CC(C)C1CCCC2C3CC=C4CC(O)CCC4(C)C3CCC12C)C(C)C BFDNMXAIBMJLBB-UHFFFAOYSA-N 0.000 claims description 2
- QURCVMIEKCOAJU-UHFFFAOYSA-N trans-isoferulic acid Natural products COC1=CC=C(C=CC(O)=O)C=C1O QURCVMIEKCOAJU-UHFFFAOYSA-N 0.000 claims description 2
- 150000003648 triterpenes Chemical class 0.000 claims description 2
- 150000002632 lipids Chemical class 0.000 abstract description 6
- 235000013376 functional food Nutrition 0.000 abstract description 4
- 238000010411 cooking Methods 0.000 abstract description 3
- 235000021186 dishes Nutrition 0.000 abstract description 3
- 239000004480 active ingredient Substances 0.000 abstract description 2
- 235000020661 alpha-linolenic acid Nutrition 0.000 description 8
- DTOSIQBPPRVQHS-PDBXOOCHSA-N alpha-linolenic acid Chemical compound CC\C=C/C\C=C/C\C=C/CCCCCCCC(O)=O DTOSIQBPPRVQHS-PDBXOOCHSA-N 0.000 description 8
- 235000019197 fats Nutrition 0.000 description 8
- 229960004488 linolenic acid Drugs 0.000 description 8
- KQQKGWQCNNTQJW-UHFFFAOYSA-N linolenic acid Natural products CC=CCCC=CCC=CCCCCCCCC(O)=O KQQKGWQCNNTQJW-UHFFFAOYSA-N 0.000 description 8
- 102000011632 Caseins Human genes 0.000 description 7
- 108010076119 Caseins Proteins 0.000 description 7
- OYHQOLUKZRVURQ-HZJYTTRNSA-N Linoleic acid Chemical compound CCCCC\C=C/C\C=C/CCCCCCCC(O)=O OYHQOLUKZRVURQ-HZJYTTRNSA-N 0.000 description 7
- 239000000839 emulsion Substances 0.000 description 7
- 235000020778 linoleic acid Nutrition 0.000 description 7
- OYHQOLUKZRVURQ-IXWMQOLASA-N linoleic acid Natural products CCCCC\C=C/C\C=C\CCCCCCCC(O)=O OYHQOLUKZRVURQ-IXWMQOLASA-N 0.000 description 7
- 239000007764 o/w emulsion Substances 0.000 description 7
- 239000008213 purified water Substances 0.000 description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
- MBMBGCFOFBJSGT-KUBAVDMBSA-N all-cis-docosa-4,7,10,13,16,19-hexaenoic acid Chemical compound CC\C=C/C\C=C/C\C=C/C\C=C/C\C=C/C\C=C/CCC(O)=O MBMBGCFOFBJSGT-KUBAVDMBSA-N 0.000 description 6
- 239000000498 cooling water Substances 0.000 description 6
- 239000008157 edible vegetable oil Substances 0.000 description 6
- 230000036541 health Effects 0.000 description 6
- 229940080237 sodium caseinate Drugs 0.000 description 6
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 5
- 238000000605 extraction Methods 0.000 description 5
- 235000013305 food Nutrition 0.000 description 5
- 238000007670 refining Methods 0.000 description 5
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 238000004945 emulsification Methods 0.000 description 4
- 235000015112 vegetable and seed oil Nutrition 0.000 description 4
- 244000170916 Paeonia officinalis Species 0.000 description 3
- 235000006484 Paeonia officinalis Nutrition 0.000 description 3
- JAZBEHYOTPTENJ-JLNKQSITSA-N all-cis-5,8,11,14,17-icosapentaenoic acid Chemical compound CC\C=C/C\C=C/C\C=C/C\C=C/C\C=C/CCCC(O)=O JAZBEHYOTPTENJ-JLNKQSITSA-N 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 230000018109 developmental process Effects 0.000 description 3
- 201000010099 disease Diseases 0.000 description 3
- 235000020669 docosahexaenoic acid Nutrition 0.000 description 3
- 229940090949 docosahexaenoic acid Drugs 0.000 description 3
- 235000020673 eicosapentaenoic acid Nutrition 0.000 description 3
- 229960005135 eicosapentaenoic acid Drugs 0.000 description 3
- JAZBEHYOTPTENJ-UHFFFAOYSA-N eicosapentaenoic acid Natural products CCC=CCC=CCC=CCC=CCC=CCCCC(O)=O JAZBEHYOTPTENJ-UHFFFAOYSA-N 0.000 description 3
- 230000006870 function Effects 0.000 description 3
- 238000005728 strengthening Methods 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- GJJVAFUKOBZPCB-UHFFFAOYSA-N 2-methyl-2-(4,8,12-trimethyltrideca-3,7,11-trienyl)-3,4-dihydrochromen-6-ol Chemical compound OC1=CC=C2OC(CCC=C(C)CCC=C(C)CCC=C(C)C)(C)CCC2=C1 GJJVAFUKOBZPCB-UHFFFAOYSA-N 0.000 description 2
- 206010003210 Arteriosclerosis Diseases 0.000 description 2
- 208000007443 Neurasthenia Diseases 0.000 description 2
- 208000008589 Obesity Diseases 0.000 description 2
- 229930003448 Vitamin K Natural products 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 230000032683 aging Effects 0.000 description 2
- 208000011775 arteriosclerosis disease Diseases 0.000 description 2
- 206010003549 asthenia Diseases 0.000 description 2
- 210000004369 blood Anatomy 0.000 description 2
- 239000008280 blood Substances 0.000 description 2
- 235000012000 cholesterol Nutrition 0.000 description 2
- 208000029078 coronary artery disease Diseases 0.000 description 2
- 230000029087 digestion Effects 0.000 description 2
- 235000004626 essential fatty acids Nutrition 0.000 description 2
- 235000013402 health food Nutrition 0.000 description 2
- 230000037356 lipid metabolism Effects 0.000 description 2
- 210000005229 liver cell Anatomy 0.000 description 2
- 230000007246 mechanism Effects 0.000 description 2
- 235000020824 obesity Nutrition 0.000 description 2
- SHUZOJHMOBOZST-UHFFFAOYSA-N phylloquinone Natural products CC(C)CCCCC(C)CCC(C)CCCC(=CCC1=C(C)C(=O)c2ccccc2C1=O)C SHUZOJHMOBOZST-UHFFFAOYSA-N 0.000 description 2
- 208000020016 psychiatric disease Diseases 0.000 description 2
- 229930003802 tocotrienol Natural products 0.000 description 2
- 239000011731 tocotrienol Substances 0.000 description 2
- 235000019148 tocotrienols Nutrition 0.000 description 2
- UFTFJSFQGQCHQW-UHFFFAOYSA-N triformin Chemical compound O=COCC(OC=O)COC=O UFTFJSFQGQCHQW-UHFFFAOYSA-N 0.000 description 2
- 235000018648 unbalanced nutrition Nutrition 0.000 description 2
- 235000019168 vitamin K Nutrition 0.000 description 2
- 239000011712 vitamin K Substances 0.000 description 2
- 150000003721 vitamin K derivatives Chemical class 0.000 description 2
- 229940046010 vitamin k Drugs 0.000 description 2
- KZJWDPNRJALLNS-VPUBHVLGSA-N (-)-beta-Sitosterol Natural products O[C@@H]1CC=2[C@@](C)([C@@H]3[C@H]([C@H]4[C@@](C)([C@H]([C@H](CC[C@@H](C(C)C)CC)C)CC4)CC3)CC=2)CC1 KZJWDPNRJALLNS-VPUBHVLGSA-N 0.000 description 1
- CSVWWLUMXNHWSU-UHFFFAOYSA-N (22E)-(24xi)-24-ethyl-5alpha-cholest-22-en-3beta-ol Natural products C1CC2CC(O)CCC2(C)C2C1C1CCC(C(C)C=CC(CC)C(C)C)C1(C)CC2 CSVWWLUMXNHWSU-UHFFFAOYSA-N 0.000 description 1
- KLEXDBGYSOIREE-UHFFFAOYSA-N 24xi-n-propylcholesterol Natural products C1C=C2CC(O)CCC2(C)C2C1C1CCC(C(C)CCC(CCC)C(C)C)C1(C)CC2 KLEXDBGYSOIREE-UHFFFAOYSA-N 0.000 description 1
- 235000019737 Animal fat Nutrition 0.000 description 1
- 208000019901 Anxiety disease Diseases 0.000 description 1
- 206010003178 Arterial thrombosis Diseases 0.000 description 1
- 206010003211 Arteriosclerosis coronary artery Diseases 0.000 description 1
- 208000007333 Brain Concussion Diseases 0.000 description 1
- LPZCCMIISIBREI-MTFRKTCUSA-N Citrostadienol Natural products CC=C(CC[C@@H](C)[C@H]1CC[C@H]2C3=CC[C@H]4[C@H](C)[C@@H](O)CC[C@]4(C)[C@H]3CC[C@]12C)C(C)C LPZCCMIISIBREI-MTFRKTCUSA-N 0.000 description 1
- 229920000858 Cyclodextrin Polymers 0.000 description 1
- ARVGMISWLZPBCH-UHFFFAOYSA-N Dehydro-beta-sitosterol Natural products C1C(O)CCC2(C)C(CCC3(C(C(C)CCC(CC)C(C)C)CCC33)C)C3=CC=C21 ARVGMISWLZPBCH-UHFFFAOYSA-N 0.000 description 1
- 241000208688 Eucommia Species 0.000 description 1
- 239000001116 FEMA 4028 Substances 0.000 description 1
- 102000007330 LDL Lipoproteins Human genes 0.000 description 1
- 108010007622 LDL Lipoproteins Proteins 0.000 description 1
- 206010029333 Neurosis Diseases 0.000 description 1
- 229930006000 Sucrose Natural products 0.000 description 1
- 208000007536 Thrombosis Diseases 0.000 description 1
- 208000025865 Ulcer Diseases 0.000 description 1
- 235000019498 Walnut oil Nutrition 0.000 description 1
- 230000004913 activation Effects 0.000 description 1
- 238000009098 adjuvant therapy Methods 0.000 description 1
- 239000010775 animal oil Substances 0.000 description 1
- 229940121363 anti-inflammatory agent Drugs 0.000 description 1
- 239000002260 anti-inflammatory agent Substances 0.000 description 1
- 230000036506 anxiety Effects 0.000 description 1
- 244000052616 bacterial pathogen Species 0.000 description 1
- MJVXAPPOFPTTCA-UHFFFAOYSA-N beta-Sistosterol Natural products CCC(CCC(C)C1CCC2C3CC=C4C(C)C(O)CCC4(C)C3CCC12C)C(C)C MJVXAPPOFPTTCA-UHFFFAOYSA-N 0.000 description 1
- WHGYBXFWUBPSRW-FOUAGVGXSA-N beta-cyclodextrin Chemical compound OC[C@H]([C@H]([C@@H]([C@H]1O)O)O[C@H]2O[C@@H]([C@@H](O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O3)[C@H](O)[C@H]2O)CO)O[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@@H]3O[C@@H]1CO WHGYBXFWUBPSRW-FOUAGVGXSA-N 0.000 description 1
- 235000011175 beta-cyclodextrine Nutrition 0.000 description 1
- 229960004853 betadex Drugs 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 210000001772 blood platelet Anatomy 0.000 description 1
- 230000036772 blood pressure Effects 0.000 description 1
- 210000004958 brain cell Anatomy 0.000 description 1
- 230000004641 brain development Effects 0.000 description 1
- 230000003925 brain function Effects 0.000 description 1
- 239000002775 capsule Substances 0.000 description 1
- 210000000170 cell membrane Anatomy 0.000 description 1
- 230000019522 cellular metabolic process Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 208000026758 coronary atherosclerosis Diseases 0.000 description 1
- 210000003792 cranial nerve Anatomy 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 235000019007 dietary guidelines Nutrition 0.000 description 1
- 208000035475 disorder Diseases 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000002500 effect on skin Effects 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 201000005577 familial hyperlipidemia Diseases 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 230000001605 fetal effect Effects 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000013355 food flavoring agent Nutrition 0.000 description 1
- 125000002642 gamma-glutamyl group Chemical group 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 238000000265 homogenisation Methods 0.000 description 1
- 208000000509 infertility Diseases 0.000 description 1
- 230000036512 infertility Effects 0.000 description 1
- 231100000535 infertility Toxicity 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 235000001705 insufficient nutrition Nutrition 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 230000003908 liver function Effects 0.000 description 1
- 210000003141 lower extremity Anatomy 0.000 description 1
- 210000001161 mammalian embryo Anatomy 0.000 description 1
- 235000013310 margarine Nutrition 0.000 description 1
- 239000003264 margarine Substances 0.000 description 1
- 230000036651 mood Effects 0.000 description 1
- 208000010125 myocardial infarction Diseases 0.000 description 1
- 210000005036 nerve Anatomy 0.000 description 1
- 208000015238 neurotic disease Diseases 0.000 description 1
- 231100000957 no side effect Toxicity 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 230000035790 physiological processes and functions Effects 0.000 description 1
- 229940068065 phytosterols Drugs 0.000 description 1
- 230000006584 pituitary dysfunction Effects 0.000 description 1
- 235000008476 powdered milk Nutrition 0.000 description 1
- 108090000765 processed proteins & peptides Proteins 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 235000018102 proteins Nutrition 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 239000008171 pumpkin seed oil Substances 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 210000001525 retina Anatomy 0.000 description 1
- 235000015500 sitosterol Nutrition 0.000 description 1
- NLQLSVXGSXCXFE-UHFFFAOYSA-N sitosterol Natural products CC=C(/CCC(C)C1CC2C3=CCC4C(C)C(O)CCC4(C)C3CCC2(C)C1)C(C)C NLQLSVXGSXCXFE-UHFFFAOYSA-N 0.000 description 1
- 208000010110 spontaneous platelet aggregation Diseases 0.000 description 1
- 206010041823 squamous cell carcinoma Diseases 0.000 description 1
- 230000035882 stress Effects 0.000 description 1
- 239000005720 sucrose Substances 0.000 description 1
- 208000024891 symptom Diseases 0.000 description 1
- 208000011580 syndromic disease Diseases 0.000 description 1
- 231100000397 ulcer Toxicity 0.000 description 1
- 235000019871 vegetable fat Nutrition 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 239000008170 walnut oil Substances 0.000 description 1
- 239000003357 wound healing promoting agent Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/007—Other edible oils or fats, e.g. shortenings, cooking oils characterised by ingredients other than fatty acid triglycerides
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/007—Other edible oils or fats, e.g. shortenings, cooking oils characterised by ingredients other than fatty acid triglycerides
- A23D9/013—Other fatty acid esters, e.g. phosphatides
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/02—Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
- A23D9/04—Working-up
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
- A23L33/11—Plant sterols or derivatives thereof, e.g. phytosterols
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/115—Fatty acids or derivatives thereof; Fats or oils
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/115—Fatty acids or derivatives thereof; Fats or oils
- A23L33/12—Fatty acids or derivatives thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
- A23P10/00—Shaping or working of foodstuffs characterised by the products
- A23P10/30—Encapsulation of particles, e.g. foodstuff additives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The invention discloses a rice germ oil composition and a microcapsule product and a preparation method thereof, wherein the composition is prepared from the following raw materials: 65-92% of rice germ oil, 1.0-20.0% of linseed oil, 0.1-3.5% of oryzanol, 0.05-2.5% of vitamin E and 0.1-3.5% of phytosterol; 0.0 to 10 percent of lecithin; adding the above materials into a blending tank, respectively, heating under vacuum, stirring, mixing, and homogenizing to obtain rice germ oil composition; or mixing with wall material, emulsifying, homogenizing, and spray drying to obtain microcapsule rice germ oil composition product. The rice germ oil composition and the microcapsule product prepared by the invention are rich in various balanced lipid physiological active ingredients, have higher nutrition and edible value, and can be widely applied to the aspects of cooking, cold dishes, drinks, functional foods and the like of common people and middle-aged and elderly people.
Description
Technical Field
The invention relates to a rice germ oil (rice oil) composition, a microcapsule product and a preparation method thereof, belonging to the technical field of functional food processing.
Background
With the development of human material civilization and the popularization of nutrition knowledge, people have also made profound changes in the concept of oil selection in order to pursue healthy life. The edible nutritional healthy oil is gradually changed from the animal oil and fat as the main material. The nutritional and healthy edible oil not only can cook delicious dishes and provide essential fatty acid and multiple vitamins for a human body, but also has physiological functions and nutrition, and the key point of maintaining health is to intake healthy oil reasonably.
In the early nineties, developed countries used rice germ oil as a functional nutrient to improve health in the food industry and the health food industry. For example, rice germ oil is made into capsule with high nutritive value in Japan to prevent cholesterol increase, and rice germ oil is added into margarine and flavoring agent, and rice germ oil is used as athlete strengthening food and senile strengthening body-building agent in America and Japan to improve memory and energy of the elderly.
The domestic research on rice germ oil and compositions is reported less. For example, patent application 200910033283.9 provides a method for preparing rice germ oil; patent application No.: 202080009408.9 edible oil and fat composition and its preparation method, provide a method for improving the rich taste of gamma-glutamyl peptide and endow effects; CN110089581A discloses an oil and fat composition containing an oil and fat composition such as 1-oleic acid-2-palmitic acid-3-linoleic acid triglyceride (OPL) and 1, 3-dioleic acid-2-palmitic acid (OPO), wherein the triglyceride is composed of fatty acids of C14 to C18; the invention of patent No. CN110200086A provides a fat composition, which comprises vegetable fat/animal fat and artificial structure fat, and fat-soluble vitamin K, wherein the digestion and absorption of vitamin K promote the digestion and absorption of fat; CN110169464A, a peony seed oil grease composition and a preparation method thereof. The preparation raw materials of the peony seed oil and fat composition comprise: peony seed oil, pumpkin seed oil, eucommia seed oil, etc.
At present, most edible oil products have the problems of insufficient functional components, unbalanced nutrition, easy obesity and sub-health of people and the like: based on meeting the requirements of people on nutritional and healthy oil, according to theoretical knowledge of oil chemistry, modern nutrition, lipid metabolism, diseases and the like, the rice germ oil produced by rice germs containing various nutritional functional components in Dabie mountain areas is used as a raw material, functional lipid substances such as linoleic acid/linolenic acid balance, tocopherol, tocotrienol, phytosterol, lecithin, oryzanol and the like are enhanced, a rice germ oil composition is produced, and the microcapsule rice germ oil composition food is further processed and prepared in a deep mode, wherein the lipid substances contained in the product are essential substances for human bodies and are used as functional nutritional edible oil and health-care food, and the living and nutritional and healthy levels of people can be obviously improved.
Disclosure of Invention
The technical problem to be solved by the invention is as follows: aiming at the problems that the most of edible oil products in the current market have insufficient and unbalanced nutrition of linoleic acid/linolenic acid, oryzanol, vitamin E, phytosterol and other physiologically active components: the rice germ oil composition with the nutrition and health care functions is produced by adopting the rice germ oil prepared by the subcritical extraction technology as a raw material, strengthening and adding nutritional ingredients such as linolenic acid, oryzanol, sitosterol, vitamin E and the like into the rice germ oil according to theories of modern nutriology, lipid metabolism and diseases, nutrition and health and the like, and adopting methods of mixing, homogenizing and the like under the vacuum condition, and the edible rice germ oil composition with the nutrition and health care functions is used as edible oil for cooking, frying, cold mixing and the like;
the purpose of the invention is realized by the following technical scheme:
the rice germ oil composition is prepared from the following raw materials in percentage by mass:
65-92% of rice germ oil,
1.0 to 20.0 percent of linseed oil,
0.1 to 3.5 percent of oryzanol,
0.05 to 2.5 percent of vitamin E,
phytosterol 0.1-3.5%;
0.0 to 10 percent of lecithin.
The rice germ oil can be replaced by rice bran oil.
The oleum Lini can be replaced by Perilla seed oil and oleum Juglandis.
The phytosterol is any one or combination of more of phytosterol, phytosterol ester, beta-sitosterol, stigmasterol and campesterol.
The oryzanol is ferulic acid ester mixture mainly containing triterpene (alkene) alcohol extracted from rice oil and grain oil.
The vitamin E is one or more of compound tocopherol, vitamin E (dl-a-tocopherol) and natural vitamin E.
The lecithin is one or more of soybean lecithin (PC 35-70), powdered soybean lecithin, yolk lecithin and soybean concentrated phospholipid.
The preparation method of the rice germ oil composition comprises the following steps: weighing the raw materials according to the proportion requirement, adding the raw materials into a stirring tank, heating to 50-90 ℃ under a vacuum condition, stirring for 60-120 min, uniformly mixing, homogenizing by a homogenizer, and cooling to 25-35 ℃ to obtain the rice germ oil composition.
In addition, the rice germ oil composition is used as a core material, and is further processed deeply and mixed with wall materials such as soybean protein powder, whey protein powder, skim milk powder, maltodextrin, emulsifier sodium caseinate, soybean lecithin, monoglyceride and the like, emulsified, homogenized and spray-dried to prepare the microcapsule rice germ oil composition product.
The preparation method of the microcapsule rice germ oil composition product comprises the following steps: heating and dissolving wall materials such as soybean protein powder, maltodextrin and emulsifier and purified water at a certain temperature, adding a certain amount of core material (rice germ oil composition) under stirring, uniformly mixing, and homogenizing and emulsifying under the pressure of 0.5-60 Mpa to obtain an oil-in-water (O/W) emulsion; the amount of the protein powder is 1.0-50.0% of the total mass of the reaction system, the amount of the maltodextrin is 1.0-60.0% of the total mass of the reaction system, and the amount of the emulsifier is 0.1-10.0% of the total mass of the reaction system; and (3) carrying out spray drying on the emulsion, wherein the temperature of an air inlet of the spray drying is 170-230 ℃, and the temperature of an air outlet of the spray drying is 75-120 ℃, so as to obtain the microcapsule rice germ oil composition product.
The invention has the following development mechanism and outstanding advantages:
the prepared rice germ oil composition is rich in tocopherol and tocotrienol, can inhibit the generation of lipid peroxide in human body, and has important functions of delaying human mechanism aging, maintaining normal metabolism of cell membrane, resisting aging, regulating infertility caused by pituitary dysfunction, and protecting human cranial nerves, especially fetal brain development.
Oryzanol in rice germ oil composition can prevent neurasthenia caused by vegetative nerve disorder, improve mental disorder, stabilize mood, relieve anxiety and stress, and improve sleep, and can be used for adjuvant treatment of climacteric syndrome, neurosis, and cerebral concussion sequelae.
Phytosterols, which has been recommended by the U.S. food and drug administration as a new raw material for natural health food "to reduce blood lipid and prevent arteriosclerosis". Has good curative effect on reducing serum cholesterol of human body and preventing coronary atherosclerosis, and also has good curative effect on skin squamous carcinoma, ulcer of lower limb and other diseases. Is used as skin tissue promoter, anti-inflammatory agent, wound healing agent, etc.
Lecithin in the embryo oil composition can fully protect liver cells, enhance liver functions, promote the activation and regeneration of the liver cells and reduce the prevalence rate of the liver. It also can effectively reduce cholesterol, hyperlipemia and coronary heart disease incidence, thereby protecting heart and preventing arteriosclerosis.
The rice germ oil composition contains linoleic acid/linolenic acid which are essential fatty acids for human bodies in a balanced proportion, and meets the standard recommended by WHO and Chinese resident dietary guidelines, wherein the linoleic acid/linolenic acid = 5-10/l, and the linoleic acid/linolenic acid =4-6/l, and the linoleic acid can inhibit the formation of arterial thrombosis and prevent the occurrence of myocardial infarction; linolenic acid can be converted into EPA (eicosapentaenoic acid) and DHA (docosahexaenoic acid) in human body, EPA has effects of inhibiting blood platelet aggregation and preventing thrombosis, reducing blood lipid, low density lipoprotein, blood pressure, etc., and DHA has effects of promoting normal development of infant brain cell and retina and enhancing brain function. If linoleic acid is taken into human body excessively, linolenic acid cannot be absorbed, and the health of people is seriously affected.
The rice germ oil composition and the microencapsulated rice germ oil composition product prepared by the invention have no side effect after being eaten, and are ideal nutritional health-care oil and functional food. The nutritional health-care food is rich in various balanced lipid physiological active ingredients, has higher nutritional and edible values, can solve the problem of auxiliary treatment of people with sub-health, obesity, neurasthenia and mental disorder symptoms, and is suitable for cooking, cold dishes, drinks, functional food auxiliary materials and the like of common people and middle-aged and old people.
Detailed Description
The present invention is further illustrated in detail by the following examples, which are provided only for illustrating the present invention and are not intended to limit the scope of the present invention.
Example 1
Weighing 92.0kg of rice germ oil processed by subcritical extraction and refining in a stirring and heating tank, and respectively adding 8kg of linseed oil and oryzanol: 0.65kg, total phytosterol: 0.5kg, vitamin E: 0.10kg under vacuum,Mixing at 70 deg.C for 90min and stirring at 400 r/min, and cooling with cooling water at 30 deg.C to obtain rice germ oil composition.
Mixing rice germ oil composition 15.0kg and soybean lecithin (PC 35) 0.4kg to obtain core material; then 10.0kg of soybean protein powder and 30.0kg of maltodextrin are weighed and added into 250.0kg of purified water at 70 ℃ to be uniformly stirred, 1.0kg of emulsifier (casein: monoglyceride, 1:1, W/W) is added, core materials are gradually added, the mixture is homogenized and emulsified for 6.0min at the emulsification temperature of 75 ℃ and the rotation speed of 8500r/min and the pressure of 25Mpa by a homogenizer to prepare oil-in-water (O/W) emulsion, and the emulsion is subjected to spray drying: the inlet air temperature is 195 ℃ and the outlet air temperature is 90 ℃, and 56.0kg of microcapsule rice germ oil composition product is obtained.
Example 2
Weighing 45.0kg of rice germ oil processed by subcritical extraction and refining in a stirring and heating tank, and respectively adding 5.5kg of linseed oil and oryzanol: 0.5kg, total phytosterol: 0.4kg, vitamin E: 0.5kg of the rice germ oil composition, uniformly mixing under the vacuum condition at the temperature of 75 ℃ for 120min and the stirring speed of 450 r/min, and introducing cooling water to cool to 30 ℃ for later use.
Mixing rice germ oil composition 15.0kg and powdered soybean phospholipids 0.5 kg; then 8.0kg of whey protein powder and 15.0kg of maltodextrin are respectively weighed and added into 150.0kg of purified water with the temperature of 55 ℃ to be uniformly stirred, 0.7kg of emulsifier (sodium caseinate: sucrose ester: monoglyceride, 1.0:0.5: 0.5W/W) is added, core materials are gradually added, and the mixture is homogenized and emulsified for 10.0min at the rotation speed of 8500r/min and 10Mpa by a homogenizer at the emulsification temperature of 80 ℃ to prepare the oil-in-water (O/W) emulsion. Then the emulsion is subjected to spray drying, and the spray drying conditions are controlled such that the air inlet temperature is 210 ℃ and the air outlet temperature is 90 ℃, so as to obtain 38.5kg of microcapsule rice germ oil composition product.
Example 3
Weighing 200.0kg of rice bran oil subjected to subcritical extraction refining processing in a stirring heating tank, and respectively adding 16kg of linseed oil and oryzanol: 1.80kg, beta-sitosterol: 1.0kg, vitamin E: 0.3kg of the rice germ oil composition, uniformly mixing under the vacuum condition at the temperature of 70 ℃ for 90min and the stirring speed of 500r/min, and introducing cooling water to cool to 30 ℃ for later use.
Mixing rice germ oil composition 25.0kg and soybean lecithin (PC 35) 1.0 kg; then 10.0kg of skimmed milk powder and 35.0kg of maltodextrin are weighed and added into 400.0kg of purified water at 75 ℃ to be uniformly stirred, 1.6kg of emulsifier (sodium caseinate: monoglyceride, 2:1, W/W) is added, then the core material is gradually added under the stirring condition, and the homogenization is carried out for 8.0min at the rotation speed of 8500r/min and 25Mpa by a homogenizer at the emulsification temperature of 90 ℃ to prepare the oil-in-water (O/W) emulsion. Then the emulsion is subjected to spray drying, the spray drying conditions are controlled such that the air inlet temperature is 205 ℃ and the air outlet temperature is 90 ℃, and 68.0kg of microcapsule rice germ oil composition product is obtained.
Example 4
Weighing 120.0kg of rice germ oil subjected to refining processing in a stirring and heating tank, and respectively adding 10kg of perilla seed oil and oryzanol: 1.5kg, total phytosterol: 0.8kg, vitamin E: 0.30kg of soybean lecithin (PC 35) and 0.5kg of the rice germ oil composition are uniformly mixed under the vacuum condition at the temperature of 70 ℃ for 90min and the stirring speed of 650 r/min, and cooled by introducing cooling water at the temperature of 30 ℃ for later use.
Mixing 40.0kg of rice germ oil composition; then 30kg of skimmed milk powder and 10kg of soybean protein isolate powder are weighed and dissolved in 600.0kg of purified water, the mixture is heated to 80 ℃ under the condition of stirring, 2.0kg of sodium caseinate and 1kg of powdered soybean phospholipid emulsifier are added, then core materials are gradually added under the condition of stirring for emulsification and stirring for 90min, and then the mixture is homogenized and emulsified for 12.0min under the conditions of the rotating speed of 7000r/min and 20Mpa by a mass machine to prepare the oil-in-water (O/W) emulsion. And then carrying out spray drying on the emulsion under the conditions that the air inlet temperature is 205 ℃ and the air outlet temperature is 95 ℃ to obtain 82.5kg of microcapsule rice germ oil composition products.
Example 5
Weighing 80.0kg of refined rice bran oil in a stirring heating tank, and respectively adding 6.5kg of linseed oil and oryzanol: 0.75kg, campesterol: 0.5kg, vitamin E: 0.08kg of the rice germ oil composition, uniformly mixing under the vacuum condition at the temperature of 70 ℃ for 90min at the stirring speed of 550 r/min, and introducing cooling water to cool to 30 ℃ for later use.
Mixing 50.0kg of rice germ oil composition and 2.0kg of concentrated soybean phospholipid (PC 35) uniformly; then 50.0kg of maltodextrin and 10.0kg of whey protein powder are weighed and added into 600.0kg of purified water at 75 ℃ to be uniformly stirred, 1.5kg of emulsifier (sodium caseinate: monoglyceride; 7: 3W/W) is added, then the core material is gradually added under the stirring condition, and the emulsifying temperature is 75 ℃, and then the core material is homogenized and emulsified for 10.0min under the conditions of the rotating speed of 8200r/min and 15Mpa by a homogenizer to prepare the oil-in-water (O/W) emulsion. And then the emulsion is subjected to spray drying, and the spray drying conditions are controlled such that the air inlet temperature is 195 ℃ and the air outlet temperature is 88 ℃, so as to obtain 113.0kg of microcapsule rice germ oil composition product.
Example 6
Weighing 100.0kg of rice germ oil subjected to subcritical extraction refining processing, putting the rice germ oil into a stirring and heating tank, and respectively adding 8kg of walnut oil and oryzanol: 1.20kg, total phytosterol: 0.55kg, vitamin E: 0.11kg of the rice germ oil composition, uniformly mixing under the vacuum condition at the temperature of 70 ℃ for 90min and the stirring speed of 600 r/min, and introducing cooling water to cool to 30 ℃ for later use.
Mixing rice germ oil composition 20.0kg and powdered soybean phospholipid 1.5 kg; then 15.0kg of maltodextrin was weighed: beta-cyclodextrin (7: 3W/W), 30.0kg of soybean protein powder and skim milk powder (6W/W), adding 450.0kg of purified water at 60 ℃, stirring uniformly, adding 0.8kg of emulsifier (sodium caseinate: monoglyceride, 8: 2W/W), gradually adding core material, homogenizing and emulsifying at the emulsifying temperature of 82 ℃ by a homogenizer at the rotating speed of 7500r/min and under the condition of 30Mpa for 6.0min, and preparing the oil-in-water (O/W) emulsion. And then the emulsion is subjected to spray drying under the conditions that the air inlet temperature is 210 ℃ and the air outlet temperature is 95 ℃, so as to obtain 66.5kg of microcapsule rice germ oil composition product.
Claims (10)
1. A rice germ oil composition characterized by: the material is prepared from the following raw materials in percentage by mass:
65-92% of rice germ oil,
1.0 to 20.0 percent of linseed oil,
0.1 to 3.5 percent of oryzanol,
0.05 to 2.5 percent of vitamin E,
phytosterol 0.1-3.5%;
0.0 to 10 percent of lecithin.
2. The rice germ oil composition of claim 1, wherein: the rice germ oil can be replaced by rice bran oil.
3. The rice germ oil composition of claim 1, wherein: the oleum Lini can be replaced by Perilla seed oil and oleum Juglandis.
4. The rice germ oil composition of claim 1, wherein: the phytosterol is any one or combination of more of phytosterol, phytosterol ester, beta-sitosterol, stigmasterol and campesterol.
5. The rice germ oil composition of claim 1, wherein: the oryzanol is ferulic acid ester mixture mainly containing triterpene (alkene) alcohol extracted from rice oil and grain oil.
6. The rice germ oil composition of claim 1, wherein: the vitamin E is one or more of compound tocopherol, vitamin E (dl-a-tocopherol) and natural vitamin E.
7. The rice germ oil composition of claim 1, wherein: the lecithin is one or more of soybean lecithin (PC 35-70), powdered soybean lecithin, yolk lecithin and soybean concentrated phospholipid.
8. A method for preparing the rice germ oil composition of claims 1 to 7, wherein: weighing the raw materials according to the proportion requirement, adding the raw materials into a stirring tank, heating to 50-90 ℃ under a vacuum condition, stirring for 60-120 min, uniformly mixing, homogenizing by a homogenizer, and cooling to 25-35 ℃ to obtain the rice germ oil composition.
9. A microcapsule rice germ oil composition product is characterized in that: the microcapsule rice germ oil composition product with the nutrition function is prepared by taking the raw materials as the core materials in the claims 1 to 7 and mixing the core materials with wall material raw materials, emulsifying, homogenizing and spray drying.
10. The microencapsulated rice germ oil composition product of claim 1 wherein: the wall material raw materials comprise soybean protein powder, whey protein powder, skim milk powder, maltodextrin, emulsifier soybean phospholipid, monoglyceride and casein.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202111310737.XA CN113951335A (en) | 2021-11-08 | 2021-11-08 | Rice germ oil composition and microcapsule product and preparation method thereof |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202111310737.XA CN113951335A (en) | 2021-11-08 | 2021-11-08 | Rice germ oil composition and microcapsule product and preparation method thereof |
Publications (1)
Publication Number | Publication Date |
---|---|
CN113951335A true CN113951335A (en) | 2022-01-21 |
Family
ID=79469596
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN202111310737.XA Pending CN113951335A (en) | 2021-11-08 | 2021-11-08 | Rice germ oil composition and microcapsule product and preparation method thereof |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN113951335A (en) |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102228249A (en) * | 2011-07-07 | 2011-11-02 | 合肥工业大学 | Method for manufacturing wheat germ oil microcapsule |
-
2021
- 2021-11-08 CN CN202111310737.XA patent/CN113951335A/en active Pending
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102228249A (en) * | 2011-07-07 | 2011-11-02 | 合肥工业大学 | Method for manufacturing wheat germ oil microcapsule |
Non-Patent Citations (3)
Title |
---|
赵贵兴: "高维生素E含量大豆胚芽油的制备及其微胶囊化研究", 农业工程, vol. 02, no. 04, pages 34 - 41 * |
金增辉 等: "米胚芽油制取技术试验报告", 粮食加工, no. 02, pages 7 - 11 * |
金增辉: "功能性粉末米胚芽油生产技术", 粮食与油脂, no. 08, pages 41 - 42 * |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN101156679B (en) | Rice bran nutrition stock solution and its preparation method | |
JP2005508621A (en) | Blood cholesterol reducing composition | |
CN1160990A (en) | Food composition containing balancing agent for 'omega'-6 and 'omega'-3 unsaturated fatty acids | |
CN103997901B (en) | Fat based food products | |
CN107969506A (en) | A kind of high stability fish oil breast for improving glycometabolism and preparation method thereof | |
WO2022016773A1 (en) | Composition conducive to nourishing and protecting stomach and preparation method therefor | |
AU2001244269B2 (en) | Natural vegetable oil concentrated in unsaponifiable matters as food ingredient | |
CN113660867B (en) | Nutritional composition exhibiting phase separation under gastric conditions and method of making the same | |
CN105533721B (en) | Samara oil oral emulsion and preparation method thereof | |
WO2014183550A1 (en) | Phosphatidyl sterol and/or phosphatidyl stanol containing polyunsaturated fatty acyl and preparation method and use thereof | |
CN112205557A (en) | Hypolipidemic solid food beverage and preparation method thereof | |
CN112137109A (en) | Compound vegetable oil microcapsule powder for controlling weight | |
CN113951335A (en) | Rice germ oil composition and microcapsule product and preparation method thereof | |
CN106387916A (en) | Oral microencapsulated porcupine oil and preparation method thereof | |
CN106070650A (en) | A kind of instant soybeen milk powder of the reduced hypertension of Surface coating lecithin | |
RU2524821C1 (en) | Mayonnaise | |
EP2744355B1 (en) | Edible composition comprising sterol | |
CN112262960A (en) | Preparation method of functional soybean milk powder containing OPO structure fat | |
CN102077981A (en) | Method for producing sauce | |
AU2004262864A1 (en) | Food product comprising phytosterols | |
CN112806562B (en) | Weight-losing composition, weight-losing preparation and application | |
CN107874254A (en) | A kind of health care oral liquid for alleviating physical fatigue | |
CN107821536A (en) | It is a kind of to be adapted to cake designed for old people and preparation method thereof | |
CN106259965A (en) | A kind of instant soybeen milk powder of the Surface coating lecithin rich in vitamin | |
CN106212698A (en) | A kind of instant soybeen milk powder of Surface coating lecithin |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination |