CN113940439A - Sweetening agent suitable for sucking electronic cigarette atomized liquid with multiple mouths and electronic cigarette atomized liquid - Google Patents

Sweetening agent suitable for sucking electronic cigarette atomized liquid with multiple mouths and electronic cigarette atomized liquid Download PDF

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Publication number
CN113940439A
CN113940439A CN202111166651.4A CN202111166651A CN113940439A CN 113940439 A CN113940439 A CN 113940439A CN 202111166651 A CN202111166651 A CN 202111166651A CN 113940439 A CN113940439 A CN 113940439A
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China
Prior art keywords
electronic cigarette
sweetener
atomized liquid
smoking
sweetening agent
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CN202111166651.4A
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CN113940439B (en
Inventor
邹阳
邹军
刘梅森
陈慧
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Shenzhen Zinwi Biotech Co Ltd
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Shenzhen Zinwi Biotech Co Ltd
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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00Preparing tobacco in the factory
    • A24B3/12Steaming, curing, or flavouring tobacco
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/16Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • A24B15/167Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacture Of Tobacco Products (AREA)
  • Seasonings (AREA)

Abstract

The invention relates to the technical field of electronic cigarette atomized liquid, in particular to a sweetener suitable for sucking electronic cigarette atomized liquid in multiple mouths and the electronic cigarette atomized liquid. The sweetener provided by the invention has better high temperature resistance, and when the sweetener is applied to the electronic cigarette atomization liquid, 500 mouths are sucked at the atomization temperature of 230-250 ℃, so that the sweetener is not easy to generate the phenomenon of carbon deposit paste core on a heating wire or a ceramic core of an electronic cigarette.

Description

Sweetening agent suitable for sucking electronic cigarette atomized liquid with multiple mouths and electronic cigarette atomized liquid
Technical Field
The invention relates to the technical field of electronic cigarette atomized liquid, in particular to a sweetening agent suitable for sucking electronic cigarette atomized liquid with multiple mouths and the electronic cigarette atomized liquid.
Background
The electronic cigarette aerosol generally contains a sweetener in addition to glycerin and propylene glycol as main components. The sweetener endows the electronic cigarette with richer taste experience, can increase fruit flavor and can also increase the verisimilitude of the fruit flavor, so that the sweetener is widely available in the electronic cigarette atomized liquid. However, the existence of the sweetener brings the potential risk of smoking peculiar smell, after all, all the sweeteners for food are not high-temperature resistant, and at the electronic cigarette atomization temperature of 230-.
Disclosure of Invention
The invention aims to overcome the defects of the prior art and provide a sweetener suitable for sucking electronic cigarette atomized liquid with multiple mouths so as to solve the problem that a carbon paste core is easily deposited on a heating wire or a ceramic core by the sweetener of the conventional electronic cigarette atomized liquid.
The invention also provides the electronic cigarette atomized liquid suitable for multi-opening suction, and the problem that the existing electronic cigarette atomized liquid is easy to generate burnt odor during long-time suction is solved.
In order to solve the technical problems, the invention adopts the following technical scheme:
a sweetening agent suitable for multi-mouth smoking of electronic cigarette atomized liquid comprises, by weight, 1 part of neotame and 2.5-3 parts of sucralose, and is used for smoking cotton-cored smoking sets with more than 500 mouths.
According to the invention, the neotame with high sweetness and high temperature resistance and the sucralose with natural sweet feeling and good high temperature resistance are compounded, and the proportion is strictly controlled, so that the prepared sweetener has better high temperature resistance, when the sweetener is applied to the electronic cigarette atomized liquid, 500 mouths are sucked at the atomizing temperature of 230 plus one of the materials, the sweetener is not easy to generate the phenomenon of carbon accumulation and paste core on the heating wire or ceramic core of the electronic cigarette, further burnt taste can not be generated, and the smoking experience is favorably improved.
Wherein, at least one of the Edwardsient and the alitame is also included.
Wherein the weight portion of the Edwardsient is 0.01-0.2.
Wherein the part by weight of the alitame is 0.1-1.0.
Wherein, the composition also comprises 9 to 11 weight portions of propylene glycol.
According to the invention, the sweetening agent is compounded by adding propylene glycol as a solvent, the carbonization temperature of neotame in propylene glycol can reach 180-plus 190 ℃, sucralose is carbonized at 180 ℃, when neotame, sucralose and propylene glycol are compounded and the proportion of the neotame, sucralose and propylene glycol is strictly controlled to prepare the sweetening agent, the high temperature resistance of the sweetening agent is better, when the sweetening agent is applied to an electronic cigarette atomization liquid, the sweetening agent is not easy to generate the condition of carbon deposit paste core after being sucked for 500 mouths at the atomization temperature of 230-plus 250 ℃, and the high temperature resistance is better than that of a single sweetening agent.
Wherein the adding amount of the sweetening agent in the atomized liquid is 0.2-0.7%.
The preparation method of the sweetener comprises the following steps: mixing and stirring the components according to the parts by weight, controlling the stirring speed to be 100-200r/min, controlling the temperature to be 25-40 ℃, and stirring for 5-15 minutes, and obtaining the sweetener after the stirring is finished.
The preparation method of the sweetener is simple in steps, high in controllability and suitable for industrial production, the prepared sweetener is natural and pleasant in sweet taste and has high temperature resistance, the carbonized paste core is not easy to occur when the sweetener is sucked for 500 mouths at the atomizing temperature of 230-.
The invention also provides an atomized liquid suitable for multi-mouth electronic cigarette smoking, which comprises the following components: glycerin, propylene glycol, nicotine, a sweetening agent and essence, wherein the sweetening agent is the sweetening agent.
Wherein, the electronics smog spinning disk atomiser is used for sucking the cotton core smoking set that is greater than 500 mouths.
According to the electronic cigarette atomizing agent, the sweetening agent is added into the electronic cigarette atomizing liquid, so that the electronic cigarette atomizing liquid is natural and pleasant in sweet taste and better in high temperature resistance, and when 500 mouths are smoked at the atomizing temperature of 230-250 ℃, the phenomenon of carbon accumulation on a heating wire or a ceramic core of an electronic cigarette using the electronic cigarette atomizing agent is avoided, and the smoking taste experience is prevented from being influenced due to the burnt taste caused by the phenomenon of carbon accumulation on the heating wire or the ceramic core.
The essence comprises but is not limited to edible essences such as watermelon essence, tobacco essence, strawberry essence, apple essence, orange essence and the like, and one or more of the tobacco essences.
The invention has the beneficial effects that: according to the invention, the sweetening agent is compounded by adding propylene glycol as a solvent, the carbonization temperature of neotame in propylene glycol can reach 180-plus 190 ℃, sucralose is carbonized at 180 ℃, when neotame, sucralose and propylene glycol are compounded and the proportion of the neotame, sucralose and propylene glycol is strictly controlled to prepare the sweetening agent, the high temperature resistance of the sweetening agent is better, when the sweetening agent is applied to an electronic cigarette atomization liquid, the sweetening agent is not easy to generate the condition of carbon deposit paste core after being sucked for 500 mouths at the atomization temperature of 230-plus 250 ℃, and the high temperature resistance is better than that of a single sweetening agent.
Drawings
In order to more clearly illustrate the technical solutions and technical effects of the embodiments of the present invention, the following figures show the test results related to the specific embodiments.
Fig. 1 shows the state of a paste core of an electronic cigarette atomized liquid prepared by the sweetening agent of the invention when the electronic cigarette atomized liquid is sucked for 200 mouths;
FIG. 2 is a core paste situation of an electronic cigarette aerosol prepared by a sweetener of a comparative example when the electronic cigarette aerosol is sucked for 200 mouths;
fig. 3 is a paste core situation of an electronic cigarette atomized liquid prepared by the sweetening agent of the invention when the electronic cigarette atomized liquid is sucked by 500 mouths;
figure 4 is a core paste situation of an electronic cigarette aerosol prepared by the sweetener of the comparative example when sucking 500 mouths;
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are some, not all, embodiments of the present invention. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
It will be understood that the terms "comprises" and/or "comprising," when used in this specification and the appended claims, specify the presence of stated features, integers, steps, operations, elements, and/or components, but do not preclude the presence or addition of one or more other features, integers, steps, operations, elements, components, and/or groups thereof.
It is also to be understood that the terminology used in the description of the invention herein is for the purpose of describing particular embodiments only and is not intended to be limiting of the invention. As used in the specification of the present invention and the appended claims, the singular forms "a," "an," and "the" are intended to include the plural forms as well, unless the context clearly indicates otherwise.
It should be further understood that the term "and/or" as used in this specification and the appended claims refers to and includes any and all possible combinations of one or more of the associated listed items.
Example 1
A sweetening agent suitable for multi-mouth smoking of electronic cigarette atomized liquid comprises, by weight, 1 part of neotame, 3 parts of sucralose and 10 parts of propylene glycol, and is used for smoking cotton-cored smoking set with more than 500 mouths.
The preparation method of the sweetener comprises the following steps: weighing 1 weight part of neotame and 3 weight parts of sucralose in sequence, mixing, adding 10 weight parts of propylene glycol, stirring at the stirring speed of 100r/min and the temperature of 30 ℃ for 10 minutes, and obtaining the sweetener after stirring.
The electronic cigarette aerosol suitable for multi-mouth-number smoking comprises 30% of glycerol, 54% of propylene glycol, 2% of nicotine, a sweetener diluted by the propylene glycol and 7.5% of watermelon essence, wherein the sweetener is the sweetener. The adding amount of the sweetening agent actually accounts for 0.7% of the total mass of the electronic cigarette atomized liquid.
Wherein, the electronics smog spinning disk atomiser is used for sucking the cotton core smoking set that is greater than 500 mouths.
The preparation method of the atomized liquid comprises the following steps: adding 30% glycerol, 54% propylene glycol, 2% nicotine, sweetener diluted with propylene glycol, and 7.5% watermelon essence into a blending tank, mixing and stirring for 10min to uniformly mix the components, filling, sealing, and inspecting the final product.
Example 2
A sweetening agent suitable for multi-mouth smoking of electronic cigarette atomized liquid comprises, by weight, 1 part of neotame, 2.5 parts of sucralose and 9 parts of propylene glycol, and is used for smoking cotton-core smoking sets with more than 500 mouths.
The preparation method of the sweetener comprises the following steps: weighing 1 weight part of neotame and 2.5 weight parts of sucralose in sequence, mixing, adding 9 weight parts of propylene glycol, stirring at the stirring speed of 150r/min and the temperature of 35 ℃ for 10 minutes, and after stirring, obtaining the sweetener.
The electronic cigarette aerosol suitable for multi-mouth-number smoking comprises 40% of glycerol, 46% of propylene glycol, 3% of nicotine, a sweetener diluted by propylene glycol and 5.5% of tobacco essence, wherein the sweetener is the sweetener in the embodiment 2. The adding amount of the sweetening agent actually accounts for 0.45% of the total mass of the electronic cigarette atomized liquid.
Wherein, the electronics smog spinning disk atomiser is used for sucking the cotton core smoking set that is greater than 500 mouths.
The preparation method of the atomized liquid comprises the following steps: adding 40% glycerol, 46% propylene glycol, 3% nicotine, 5.5% sweetener, and tobacco essence diluted with propylene glycol into a blending tank, mixing and stirring for 10min to uniformly mix the components, filling, sealing, and inspecting the final product.
Example 3
A sweetening agent suitable for multi-mouth smoking of electronic cigarette atomized liquid comprises, by weight, 1 part of neotame, 2.75 parts of sucralose and 11 parts of propylene glycol, and is used for smoking cotton-core smoking sets with more than 500 mouths.
The preparation method of the sweetener comprises the following steps: weighing 1 weight part of neotame and 2.75 weight parts of sucralose in sequence, mixing, adding 11 weight parts of propylene glycol, stirring at the stirring speed of 200r/min and the temperature of 25 ℃ for 5min, and after stirring, obtaining the sweetener.
The electronic cigarette aerosol suitable for multi-mouth-number smoking comprises 45% of glycerol, 40% of propylene glycol, 5% of nicotine, a sweetener diluted by propylene glycol and 5.5% of strawberry essence, wherein the sweetener is the sweetener in the embodiment 3. The adding amount of the sweetening agent actually accounts for 0.45% of the total mass of the electronic cigarette atomized liquid.
Wherein, the electronics smog spinning disk atomiser is used for sucking the cotton core smoking set that is greater than 500 mouths.
The preparation method of the atomized liquid comprises the following steps: adding 45% glycerol, 40% propylene glycol, 5% nicotine, sweetener diluted with propylene glycol, and 5.5% strawberry essence into a blending tank, mixing and stirring for 5min to uniformly mix the components, filling, sealing, and inspecting the final product.
Example 4
Example 4 is different from example 1 in that the sweetener in example 4 further includes 0.05 parts by weight of edmuntin, and the other formulation and preparation method of example 4 are the same as those of example 1.
Example 5
Example 5 is different from example 1 in that the sweetener of the electronic aerosolization liquid in example 5 further includes 0.5 parts by weight of alitame, and other conditions are the same as example 1 and are not described herein again.
Example 6
The difference between example 6 and example 1 is that the essence of the electronic cigarette aerosol in example 6 is a mixture of strawberry essence and cantaloupe essence, and other conditions are the same as those in example 1 and are not described herein again.
Comparative example
2 parts of sucralose, 50 parts of propylene glycol and 6 parts of neotame, wherein the preparation method of the sweetener is the same as that of the electronic cigarette atomization liquid in the example 1, the sweetener in the electronic cigarette atomization liquid in the example 1 is replaced by the sweetener in a pair proportion, and other components are consistent with those in the example 1 to prepare the new electronic cigarette atomization liquid.
Performance testing
The core pasting conditions of the electronic cigarette aerosol of examples 1 to 6 and the core pasting conditions of the electronic cigarette aerosol of the comparative example at 200-500-mouth pumping and 500-mouth pumping were tested by setting the volume of 55mL and the flow rate of 27.5mL/s according to the rule of 2-mouth pumping and 8-second stopping by using a smoke extractor.
Through tests, the core pasting degree of the electronic cigarette atomizing liquid is shown in figure 1 under the condition of sucking 200 mouths, and the core pasting degree is shown in figure 3 under the condition of sucking 500 mouths; the core pasting degree of the electronic cigarette aerosol of the comparative example is shown in fig. 2 in the case of sucking 200 orifices, and the core pasting degree is shown in fig. 4 in the case of sucking 500 orifices.
Comparing fig. 1 and 2, fig. 3 and 4, it can be seen that the sweetener of the present invention has better high temperature resistance, and is not easy to generate carbonization paste core phenomenon at the atomization temperature of 230-250 ℃, while the sweetener of the comparative example has poorer high temperature resistance, and generates serious carbonization paste core phenomenon at the same atomization temperature. The neotame, the sucralose and the propylene glycol are compounded, and the proportion of the neotame, the sucralose and the propylene glycol is strictly controlled, so that the components are mutually cooperated, the high-temperature resistance of the sweetener is improved, the core pasting phenomenon of the sweetener is not easy to occur at the atomization temperature, and the sweetener is moderate in sweet taste, natural and pleasant and is favorable for improving the smoking taste.
While the invention has been described with reference to specific embodiments, the invention is not limited thereto, and various equivalent modifications and substitutions can be easily made by those skilled in the art within the technical scope of the invention. Therefore, the protection scope of the present invention shall be subject to the protection scope of the claims.

Claims (8)

1. The sweetener suitable for multi-mouth smoking of electronic cigarette atomized liquid is characterized by comprising 1 weight part of neotame, 2.5-3 weight parts of sucralose and a solvent, and is used for smoking a cotton core smoking set with more than 500 mouths.
2. The sweetener suitable for use in a multiple puff e-cigarette aerosol of claim 1, further comprising at least one of edmuntin and alitame.
3. The sweetener suitable for electronic cigarette aerosol with multiple mouthfuls of smoking according to claim 2, wherein the weight portion of the edmuntin is 0.01-0.2.
4. The sweetener suitable for electronic cigarette aerosol with multiple puffs according to claim 2, wherein the alitame is present in an amount of 0.1 to 1.0 parts by weight.
5. A sweetener suitable for use in an electronic smoking solution according to any one of claims 1 to 4, wherein the solvent is 9 to 11 parts by weight propylene glycol.
6. The sweetener suitable for the electronic cigarette aerosol with multiple puffs of claim 5, wherein the sweetener is added to the aerosol in an amount of 0.2% to 0.7%.
7. An electronic cigarette atomized liquid suitable for multi-mouth smoking, which is characterized by comprising glycerol, propylene glycol, nicotine, a sweetener and essence, wherein the sweetener is the sweetener in any one of claims 1 to 5.
8. The electronic cigarette aerosol suitable for multi-puff smoking according to claim 7, wherein the electronic cigarette aerosol is used for smoking a cotton core smoking set with more than 500 puffs.
CN202111166651.4A 2021-10-01 2021-10-01 Sweetener suitable for sucking electronic cigarette atomized liquid with multiple openings and electronic cigarette atomized liquid Active CN113940439B (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115918951A (en) * 2022-12-30 2023-04-07 东莞市吉纯生物技术有限公司 Compound sweetener for electronic cigarette liquid and preparation method thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110506978A (en) * 2019-09-11 2019-11-29 深圳多客技术有限公司 A kind of electronic cigarette oil solvent, electronic cigarette tobacco tar and preparation method comprising it
CN112401293A (en) * 2020-09-17 2021-02-26 深圳雪雾科技有限公司 Bitter inhibitor, application, electronic atomized liquid and preparation method thereof
CN113197330A (en) * 2021-04-28 2021-08-03 深圳市博睿生物科技有限公司 Novel sweetener for electronic cigarettes, preparation method and application

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110506978A (en) * 2019-09-11 2019-11-29 深圳多客技术有限公司 A kind of electronic cigarette oil solvent, electronic cigarette tobacco tar and preparation method comprising it
CN112401293A (en) * 2020-09-17 2021-02-26 深圳雪雾科技有限公司 Bitter inhibitor, application, electronic atomized liquid and preparation method thereof
CN113197330A (en) * 2021-04-28 2021-08-03 深圳市博睿生物科技有限公司 Novel sweetener for electronic cigarettes, preparation method and application

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115918951A (en) * 2022-12-30 2023-04-07 东莞市吉纯生物技术有限公司 Compound sweetener for electronic cigarette liquid and preparation method thereof

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