CN113786374A - Blocky freeze-dried soft membrane, preparation method and use method - Google Patents
Blocky freeze-dried soft membrane, preparation method and use method Download PDFInfo
- Publication number
- CN113786374A CN113786374A CN202111024117.XA CN202111024117A CN113786374A CN 113786374 A CN113786374 A CN 113786374A CN 202111024117 A CN202111024117 A CN 202111024117A CN 113786374 A CN113786374 A CN 113786374A
- Authority
- CN
- China
- Prior art keywords
- freeze
- parts
- block
- soft membrane
- dried soft
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
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- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 28
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- Cosmetics (AREA)
Abstract
The application relates to the technical field of membrane powder, and discloses a blocky freeze-dried soft membrane, a preparation method and a use method. The freeze-dried soft membrane is a massive solid prepared from the following raw materials, by mass, 50-70 parts of diatomite, 10-30 parts of maltodextrin, 5-10 parts of sodium alginate, 5-10 parts of calcium sulfate, 0.3-1 part of tetrasodium pyrophosphate, 0.3-1 part of sodium chloride, 1.5-3 parts of a skin conditioner, 0.3-1 part of a humectant and 0-0.05 part of essence through a vacuum freeze-drying process. The block freeze-dried soft membrane is prepared by a vacuum freeze-drying process, so that the original performance of the soft membrane powder is reserved; and the mask is convenient to carry, the usage amount is strictly calculated and controlled, the normal mask requirements of all facial shapes can be met, and the problems that the freeze-dried soft mask is wasted or the facial skin cannot be covered in the using process and the like cannot be caused.
Description
Technical Field
The application relates to the technical field of membrane powder, in particular to a blocky freeze-dried soft membrane, a preparation method and a use method.
Background
The film powder is generally divided into soft film, hard film and water washing film powder. The soft film powder can be formed into a film and lifted, and the film powder cannot be formed into a film when washed by water, and the film powder is wiped off by a wet towel after use. The soft mask powder is a removable mask, and can soften, moisturize and clean the stratum corneum of skin.
In the process of using the soft film powder in practice at present, the soft film powder is inconvenient to carry and take when traveling, for example, the powder can be scattered on the surfaces of other objects, the ground, the table top and other places due to carelessness in taking, and little trouble is brought to the actual life; meanwhile, the dosage is not well controlled, unnecessary waste is caused by too much dosage, and the facial skin cannot be covered by too little dosage, so that improvement is needed.
Disclosure of Invention
Aiming at the defects in the prior art, the application provides a block-shaped freeze-dried soft membrane, a preparation method and a use method.
In a first aspect, the present application provides a block-shaped lyophilized soft membrane, which adopts the following technical scheme:
a block freeze-dried soft membrane is prepared by preparing raw materials with the following mass parts into a block solid through a vacuum freeze-drying process,
50-70 parts of diatomite;
10-30 parts of maltodextrin;
5-10 parts of sodium alginate;
5-10 parts of calcium sulfate;
0.3-1 part of tetrasodium pyrophosphate;
0.3-1 part of sodium chloride;
1.5-3 parts of a skin conditioner;
0.3-1 part of humectant;
0-0.05 part of essence.
By adopting the technical scheme, the soft membrane powder raw material is prepared into a block solid (namely a freeze-dried soft membrane) through a vacuum freeze drying process, so that the original performance of the soft membrane powder is kept (the soft membrane powder can be pasted after being added with an aqueous solution, and can be formed into a membrane after being dried); and convenient to carry, the use amount is through strict calculation control, can satisfy the normal facial mask demand of all types of face, and the in-process of use can not cause the waste of freeze-drying mantle or can not apply facial skin scheduling problem, has improved the convenient degree when the mantle uses.
Preferably, the feed additive is prepared from the following raw materials in parts by mass:
60-70 parts of diatomite;
20-22 parts of maltodextrin;
8-10 parts of sodium alginate;
8-9 parts of calcium sulfate;
0.4-0.6 part of tetrasodium pyrophosphate;
0.4-0.6 part of sodium chloride;
2-2.3 parts of a skin conditioner;
0.3-0.5 part of humectant;
0.01-0.02 part of essence.
Preferably, the mass ratio of the diatomite, the maltodextrin, the sodium alginate, the calcium sulfate, the tetrasodium pyrophosphate and the sodium chloride is (110-) -130 (35-40): (17-18): (15-16):1: 1.
By adopting the technical scheme, the dosage proportion of the diatomite, the maltodextrin, the sodium alginate, the calcium sulfate, the tetrasodium pyrophosphate and the sodium chloride is controlled, the quality of the solidified block of the soft membrane powder can be effectively improved on the basis of keeping the good skin cleaning and skin care capability of the membrane powder, and the block freeze-dried membrane powder basically has no obvious deformation, looseness and breakage after falling of a falling platform of about 1 meter.
Preferably, the skin conditioner is at least one selected from the group consisting of rose extract, bletilla striata root powder, ascorbic acid, collagen, tranexamic acid, niacinamide, zinc oxide, magnesium oxide, pearl powder and oligopeptide-1.
Preferably, the skin conditioner consists of rose extract, bletilla root powder, ascorbic acid, collagen, tranexamic acid, nicotinamide, zinc oxide, magnesium oxide, pearl powder and oligopeptide-1, wherein the mass ratio of the sodium chloride, the rose extract, the bletilla root powder, the ascorbic acid, the collagen, the tranexamic acid, the nicotinamide, the zinc oxide, the magnesium oxide, the pearl powder and the oligopeptide-1 is (2-3) to 1.
By adopting the technical scheme, the rose extract, the rhizoma bletillae root powder, the ascorbic acid, the pearl powder and other animal and plant source active substances are added, so that the antioxidation and whitening effects on skin can be effectively improved, and the natural skin whitening cream is natural and has no stimulation. The addition of chemical components such as zinc oxide, magnesium oxide and the like can improve the absorption promoting and repairing effects on skin, and the combined action of the components can achieve good effects of cleaning, nursing and repairing skin.
Preferably, the moisturizer is selected from at least one of aloe vera extract and arbutin.
Preferably, the moisturizer consists of aloe extract and arbutin, and the mass ratio of the aloe extract to the arbutin is 1: 1.
Preferably, the ALOE extract is selected from ALOE vera (ALOE BARBADENSIS) extract.
By adopting the technical scheme, after the aloe extract and the arbutin are added, the moisture-keeping and water-locking effects are good, the skin can be repaired, and the generation of melanin is prevented by inhibiting the activity of tyrosinase in vivo, so that the skin pigmentation is reduced, color spots and freckles are removed, and the effects of sterilization and inflammation diminishing are achieved. In addition, the aloe gel in the aloe extract can be combined with calcium sulfate and tetrasodium pyrophosphate to form a film on the surface of the facial skin more easily under the dispersion action of maltodextrin, and the brittleness of the formed film of the calcium sulfate can be improved under the action of the diatomite, the tetrasodium pyrophosphate of the aloe extract and the maltodextrin, so that the formed film has certain elasticity (namely deformability), an operator can completely tear the whole facial mask from the face without tearing and pulling the skin, and the hard damage of the soft film to the skin is reduced.
In a second aspect, the present application provides a method for preparing a block-shaped lyophilized soft membrane, which adopts the following technical scheme:
a preparation method of a block freeze-dried soft membrane comprises the following steps:
1) adding diatomite, maltodextrin, sodium alginate, calcium sulfate, tetrasodium pyrophosphate, sodium chloride, a humectant and a skin conditioner according to the proportion, stirring for 20-40min, adding essence, continuously stirring for 20-25 min, filtering, discharging and standing for 10-15 h;
2) filling the powder filtered in the step 1) into a mold, and carrying out vacuum freeze drying for 20-30 h at the temperature of-35 to-40 ℃ and under the pressure of 3-4 MPa to obtain the blocky freeze-dried soft membrane.
By adopting the technical scheme, the operation is simple, the performance of the product can be kept (namely the product can be pasted after being added with aqueous solution and can be formed into a film after being dried), the block-shaped freeze-dried soft film prepared by the vacuum freeze-drying process still keeps the graininess similar to frosting, but the hardness after the block-shaped freeze-dried soft film can meet the normal storage and transportation requirements, and the product is verified to fall at a height of about 1 meter, and the appearance of the product basically has no deformation, looseness and breakage.
In a third aspect, the application provides a use method of a block-shaped freeze-dried soft membrane, which adopts the following technical scheme:
a use method of a block freeze-dried soft membrane comprises the following operations: putting the block-shaped freeze-dried soft membrane into a container, adding the aqueous solution, and stirring within 1min to obtain pasty facial mask paste; applying the pasty facial mask paste on cleaned skin surface, curing at room temperature for 3-8min to form a film, and taking off the whole face after 15-20 min.
Preferably, the mass ratio of the aqueous solution to the freeze-dried soft membrane is 1: 1.
preferably, the aqueous solution is one or more of purified water, mineral water, cosmetic water and essence.
Through adopting above-mentioned technical scheme, easy operation, convenient to use can arrange the aqueous solution wantonly according to operator's demand and dissolve and stir into the paste, and the stable performance that becomes the paste does not receive the nature influence of temperature, water yield and water, can solidify the membrane after skin surface drying at last, and the convenience of using ten minutes, and can not cause the damage of powerful tear (similar plucking) to skin like the dura mater.
In summary, the present application has the following beneficial effects:
1. the block freeze-dried soft membrane is prepared by a vacuum freeze-drying process, so that the original performance of the soft membrane powder is reserved; and convenient to carry, the use amount is through strict calculation control, can satisfy the normal facial mask demand of all types of face, and the in-process of use can not cause the waste of freeze-drying mantle or can not apply facial skin scheduling problem, has improved the convenient degree when the mantle uses.
2. According to the aloe extract, the aloe gel in the aloe extract can be combined with calcium sulfate and tetrasodium pyrophosphate to form a film on the surface of facial skin more easily under the dispersion effect of maltodextrin, and the brittleness of the formed film of calcium sulfate can be improved under the effects of diatomite, the tetrasodium pyrophosphate of the aloe extract and the maltodextrin, so that the formed film has certain elasticity (namely deformability), an operator can completely tear the whole facial mask from the face without tearing and pulling the skin, and the hard damage of the soft film to the skin is reduced.
3. The preparation method is simple to operate, the product can be pasted after being added into the water solution, meanwhile, the characteristic of film forming can be realized after drying, the blocky freeze-dried soft film prepared by the vacuum freeze-drying process still keeps the graininess similar to frosting, but the hardness after the blocky freeze-dried soft film can meet the normal storage and transportation requirements, and the product basically has no deformation, looseness and breakage after falling at the height of about 1 meter.
4. This application convenient to use can arrange the aqueous solution wantonly according to operator's demand and dissolve and stir into the paste, and the stable performance that becomes the paste does not receive the nature influence of temperature, water yield and water, can solidify the membrane after skin surface drying simultaneously, uses convenience very, and can not cause the damage of powerful tear (similar plucking) to skin like the dura mater.
Drawings
FIG. 1 is a schematic representation of a block-shaped lyophilized soft film prior to tempering with water in example 1 of the present application.
FIG. 2 is a schematic diagram of a block-shaped lyophilized soft film obtained by blending water in example 1 of the present application.
FIG. 3 is a schematic representation of the bulk film prior to the addition of water and tempering in comparative example 3 of the present application.
FIG. 4 is a schematic representation of the block-shaped soft film after water blending of comparative example 3 in this application.
Detailed Description
The present application is described in further detail below with reference to figures 1-4 and examples.
The raw materials used in the examples of the present application are commercially available products unless otherwise specified.
The flos Rosae Rugosae (Rosa Rugosa) extract is selected from flos Rosae Rugosae extract of Feng source commercial Limited in Guangzhou city.
Oligopeptide-1 is selected from oligopeptide-1 (lyophilized powder) from Feng Source commerce, Inc., Guangzhou city.
The rhizoma Bletillae (BLETILLA STRATA) root powder is selected from rhizoma Bletillae root powder of ANO QIAN pharmaceutical industry Limited.
Examples
Example 1
A block-shaped freeze-dried soft membrane is prepared by using the raw materials and the dosage of the freeze-dried soft membrane in the following table 1.
The preparation method comprises the following steps:
1) sequentially adding diatomite, maltodextrin, sodium alginate, calcium sulfate, tetrasodium pyrophosphate, sodium chloride, rose (ROSA RUGOSA) flower extract, ALOE vera (Aloe Barbadensis) extract, rhizoma bletillae (BLETILLA STRATA) root powder, ascorbic acid (vitamin C), collagen, arbutin, tranexamic acid, nicotinamide, zinc oxide, magnesium oxide and oligopeptide-1 according to the proportion, stirring for 20min, adding daily chemical essence, continuously stirring for 25min, filtering, discharging, and standing for 15 h.
2) Filling the powder filtered in the step 1) into a mould, and carrying out vacuum freeze drying for 20h at the temperature of-35 ℃ and under the pressure of 3MPa to obtain a blocky freeze-dried soft membrane (see figure 1).
Example 2
A block-shaped freeze-dried soft membrane is prepared by using the raw materials and the dosage of the freeze-dried soft membrane in the following table 1.
1) Sequentially adding diatomite, maltodextrin, sodium alginate, calcium sulfate, tetrasodium pyrophosphate, sodium chloride, rose (ROSA RUGOSA) flower extract, ALOE vera (Aloe Barbadensis) extract, rhizoma bletillae (BLETILLA STRATA) root powder, ascorbic acid (vitamin C), collagen, arbutin, tranexamic acid, nicotinamide, zinc oxide, magnesium oxide and oligopeptide-1 according to the proportion, stirring for 20-40min, adding daily chemical essence, continuously stirring for 20min, filtering, discharging and standing for 10 h.
2) Filling the powder filtered in the step 1) into a mould, and carrying out vacuum freeze drying for 30h at the temperature of minus 40 ℃ and under the pressure of 4MPa to obtain the blocky freeze-dried soft membrane.
Examples 3 to 7: a block-shaped lyophilized soft film, which is different from example 1 in that: the raw materials and the dosage of the freeze-dried soft membrane are different, and the specific reference is made in table 1.
TABLE 1 composition and amount (kg) of lyophilized block film of examples 1-7
Example 8
A block-shaped lyophilized soft film, which is different from example 7 in that: 55kg of diatomite, 17.5kg of maltodextrin, 8.5kg of sodium alginate, 7.5kg of calcium sulfate, 0.5kg of tetrasodium pyrophosphate and 0.5kg of sodium chloride. At this time, the mass ratio of diatomaceous earth, maltodextrin, sodium alginate, calcium sulfate, tetrasodium pyrophosphate, and sodium chloride was 110:35:17:15:1: 1.
Example 9
A block-shaped lyophilized soft film, which is different from example 7 in that: 65kg of diatomite, 20kg of maltodextrin, 9kg of sodium alginate, 8kg of calcium sulfate, 0.5kg of tetrasodium pyrophosphate and 0.5kg of sodium chloride. At this time, the mass ratio of diatomaceous earth, maltodextrin, sodium alginate, calcium sulfate, tetrasodium pyrophosphate, and sodium chloride was 130:40:18:16:1: 1.
Application example 1
A use method of a block freeze-dried soft membrane comprises the following operations: putting the block-shaped freeze-dried soft membrane prepared in the example 7 into a membrane mixing bowl, adding purified water, and stirring within 1min to obtain pasty mask paste; adjusting the mask in a clockwise stirring and pressing manner, applying the pasty facial mask paste on the cleaned skin surface, curing at room temperature for 3min to form a film, and taking off the whole face after 15 min.
Application example 2
A use method of a block freeze-dried soft membrane comprises the following operations: putting the block freeze-dried soft membrane prepared in the example 8 into a mask bowl, adding mineral water and about 3 drops of essence (a small white bottle of magnolia oil olay) and stirring into pasty mask cream within 1 min; manually adjusting the mask in a manner of stirring and pressing anticlockwise, applying pasty mask cream on the surface of cleaned skin, curing to form a film after 5min at normal temperature, taking off the whole face after 20min, dipping a flat circle of a wet lower film when peeling off the film, and then slowly peeling off the film.
Comparative example
Comparative example 1
A soft film powder, which is different from example 7 in that: the soft membrane powder comprises 30kg of glucose, 0.05kg of sodium hyaluronate, 10kg of diatomite, 0.5kg of microcrystalline cellulose, 0.2kg of extract flower of sphenoides, 0.1kg of apple seed extract, 3kg of sodium alginate and 15kg of silica, wherein the filler is glucose, the dispersing agent is silica, the molecular weight of the sodium alginate is 20-30 ten thousand, the molecular weight of the sodium hyaluronate is 100-120 ten thousand, and the average particle size of the diatomite is 70 microns.
The preparation method comprises adding glucose, sodium hyaluronate, diatomaceous earth, microcrystalline cellulose, herba Clerodendranthi Spicati extract, sodium alginate and silica into a stirring pot, stirring at 80r/min, reversing every 5min, and stirring for 20min to obtain soft membrane powder.
Comparative example 2
A bulk film, which is different from comparative example 1 in that: the block soft film powder is prepared by pressing raw materials into a block structure under the pressure of 4MPa by an experimental powder pressing machine (aerospace chemical machinery factory of Gaoyou city) with the product number of YHJX-YF-J.
Comparative example 3
A bulk film, which is different from comparative example 1 in that: the block soft film powder is prepared by pressing the raw material with experimental type powder press (aerospace chemical machinery factory, Gaoypost) with the product number of YHJX-YF-J under the pressure of 8MPa to form a block structure (see FIG. 3).
Performance detection analysis
Test one: product basic performance test subjects: the block-shaped lyophilized films prepared in examples 1 to 9 were used as test samples 1 to 9, and the film powders of comparative examples 1 to 3 were used as control samples 1 to 3.
The test method comprises the following steps:
1) the appearance state of the product was observed, the product was manually picked up and shaken left and right for 5 to 6 times, and then put down to observe the condition of the product, and the observed condition was registered in table 2.
2) A total of 6 pieces of each group of test products were placed on 0.5m, 1m, 2m, 3m, 4m, 5m and 6m high stands, respectively, and dropped onto the ground, and if it was observed that significant deformation and breakage occurred on the surface of the product, the corresponding drop heights were registered in table 2.
3) The product was placed on a test bed 1m from the ground, the height of the product dropping was strictly controlled, the block-shaped products (examples 1 to 9, comparative examples 2 to 3, total 11 groups, each group 10 times) were horizontally dropped onto the ground, the appearance state of the block-shaped product dropped at high altitude was observed for the presence of deformation, loosening, and occurrence of breakage, and the results after the detection were averaged and registered in table 2.
TABLE 2
As can be seen by combining examples 1 to 9, comparative examples 1 to 3 and commercially available products 1 to 2 and by combining Table 2, comparative example 1 and commercially available products 1 to 2 were each a powdery substance. Referring to fig. 1 and 3, examples 1 to 9 and comparative examples 2 to 3 of the present application each had a block structure (fig. 1 shows the block freeze-dried soft membrane before water blending in example 1, and fig. 3 shows the block soft membrane before water blending in comparative example 3).
As can be seen by combining examples 1-9, comparative examples 2-3 and Table 2, the products of examples 1-9 have no deformation, looseness and breakage when dropped at a height of 1 m; there was significant deformation and breakage when dropped at a height of 2 meters. Comparative example 2 dropped at a height of 0.5m and was pulverized into a powder without an intact shape. While comparative example 3 had essentially no deformation, loosening and breakage of the product appearance when dropped at a height of 1 meter, whereas the product appearance had essentially significant deformation and breakage up to a drop at a height of 4 meters. It can be seen that the products of examples 1-9 can meet normal transportation, damage from accidental dropping at a height of about 1m and do not affect normal use of the products.
As can be seen by combining examples 1-9, comparative examples 1-3 and commercial products 1-2 and by combining Table 2, examples 1-9, comparative example 1 and commercial products 1-2 all dissolved and stirred normally into a paste within 1min (see FIG. 2), and the peeled mask was film-formed intact and could be peeled off together with the whole sheet. The product in comparative example 3 is stable in lumping, but difficult to dissolve, still can not be pasted within 2min, has obvious solid-liquid layering, and can not be formed into a film for practical use. From this, it is understood that the product of comparative example 3 has improved the stability of the product in the form of a lump by pressurization (8MPa), but the agglomerated product cannot be dissolved in an aqueous solution (see fig. 4), and thus the normal use of the product is affected, and the product is a failed product. The product of comparative example 2 can be dissolved in the aqueous solution and can be pasted by stirring, but the stirring time (pasting within 1.5 min) of pasting is obviously longer than that of the stirring time (pasting within 1 min) of the examples 1-9, the stability of the pressed blocks under the pressure of 4MPa is poor, the crushing is serious, and the bumping and bumping in the transportation process can influence the aesthetic degree of the sale, so the product of comparative example 2 is not suitable for being pressed into blocks for sale.
Test two test subjects: the block-shaped lyophilized films prepared in examples 1 to 9 were used as test samples 1 to 9, and the film powders of comparative examples 1 to 3 were used as control samples 1 to 3, and 12 groups were added, and 3 samples were counted for each group.
The test method comprises the following steps: the subjects were randomly selected 36, all ages 18-45 years old, male and female. After 36 subjects had cleaned their skin, the corresponding swatches (examples 1-9 and test samples 1-9) were used once a day in the morning and once a day in the evening, and the initial skin condition of 18 subjects was recorded in table 4 as blank control 1, and the initial skin condition of another 18 subjects was recorded in table 4 as blank control 2; the average values of the skin condition of the subjects after using the corresponding pellicles were then registered in table 4.
The skin is used for one time in the morning and at night, and then different items are respectively graded (0-100 points) according to the absorption degree, cleanliness, water wettability, skin elasticity, wrinkle change, repairing effect, skin brightening change and use feeling of the skin.
TABLE 3
TABLE 4
As can be seen by combining examples 1-9, comparative examples 1-2 and blank controls 1-2, and by combining tables 2 and 3, the changes in skin absorbency, cleanliness, moisturization, skin elasticity, wrinkle changes, rejuvenation, and skin lightening obtained in examples 1-9 of the present application are superior to those of comparative examples 1-2 and blank controls 1-2. Therefore, the effects of effectively improving the skin moisturizing, brightening and repairing after the freeze-dried soft filming water film is prepared by matching the diatomite, the maltodextrin, the sodium alginate, the calcium sulfate, the tetrasodium pyrophosphate, the sodium chloride, the skin conditioner, the humectant and the essence.
The specific embodiments are merely illustrative of the present application and are not restrictive of the present application, and those skilled in the art can make modifications of the embodiments as required without any inventive contribution thereto after reading the present specification, but only protected by the patent laws within the scope of the claims of the present application.
Claims (10)
1. The block freeze-dried soft membrane is characterized in that the freeze-dried soft membrane is prepared into a block solid by a vacuum freeze-drying process from the following raw materials in parts by mass,
50-70 parts of diatomite;
10-30 parts of maltodextrin;
5-10 parts of sodium alginate;
5-10 parts of calcium sulfate;
0.3-1 part of tetrasodium pyrophosphate;
0.3-1 part of sodium chloride;
1.5-3 parts of a skin conditioner;
0.3-1 part of humectant;
0-0.05 part of essence.
2. The block freeze-dried soft membrane as claimed in claim 1, which is prepared from the following raw materials in parts by mass:
60-70 parts of diatomite;
20-22 parts of maltodextrin;
8-10 parts of sodium alginate;
8-9 parts of calcium sulfate;
0.4-0.6 part of tetrasodium pyrophosphate;
0.4-0.6 part of sodium chloride;
2-2.3 parts of a skin conditioner;
0.3-0.5 part of humectant;
0.01-0.02 part of essence.
3. The block freeze-dried soft membrane as claimed in claim 1, wherein the mass ratio of the diatomite, the maltodextrin, the sodium alginate, the calcium sulfate, the tetrasodium pyrophosphate and the sodium chloride is (110-130): (35-40): (17-18): (15-16):1: 1.
4. The block-shaped freeze-dried soft membrane as claimed in claim 1, wherein the skin conditioner is at least one selected from rose extract, rhizoma bletillae root powder, ascorbic acid, collagen, tranexamic acid, nicotinamide, zinc oxide, magnesium oxide, pearl powder and oligopeptide-1.
5. The block-shaped freeze-dried soft membrane as claimed in claim 4, wherein the skin conditioner comprises rose extract, rhizoma bletillae root powder, ascorbic acid, collagen, tranexamic acid, nicotinamide, zinc oxide, magnesium oxide, pearl powder and oligopeptide-1, and the mass ratio of the sodium chloride, the rose extract, the rhizoma bletillae root powder, the ascorbic acid, the collagen, the tranexamic acid, the nicotinamide, the zinc oxide, the magnesium oxide, the pearl powder and the oligopeptide-1 is (2-3) to 1:1:1:1:1:1:1:1: 1.
6. The block-shaped lyophilized soft film according to claim 1, wherein the humectant is at least one selected from aloe vera extract and arbutin.
7. The block freeze-dried soft film according to claim 6, wherein the moisturizer is composed of aloe extract and arbutin, and the mass ratio of the aloe extract to the arbutin is 1: 1.
8. The method for preparing a block-shaped lyophilized soft membrane according to any one of claims 1 to 7, comprising the steps of:
1) adding diatomite, maltodextrin, sodium alginate, calcium sulfate, tetrasodium pyrophosphate, sodium chloride, a humectant and a skin conditioner according to the proportion, stirring for 20-40min, adding essence, continuously stirring for 20-25 min, filtering, discharging and standing for 10-15 h;
2) filling the powder filtered in the step 1) into a mold, and carrying out vacuum freeze drying at the temperature of minus 35 to minus 40 ℃ and under the pressure of 3 to 4MPa for 20 to 30 hours to obtain the blocky freeze-dried soft membrane.
9. The method for using a block-shaped freeze-dried soft membrane as claimed in any one of claims 1 to 7, which comprises the following operations: putting the block-shaped freeze-dried soft membrane into a container, adding the aqueous solution, and stirring within 1min to obtain pasty facial mask paste; applying the pasty facial mask paste on cleaned skin surface, curing at room temperature for 3-8min to form a film, and taking off the whole face after 15-20 min.
10. The use method of the block-shaped freeze-dried soft membrane as claimed in claim 9, wherein the aqueous solution is one or more selected from purified water, mineral water, cosmetic water and essence.
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| CN114099395A (en) * | 2022-01-05 | 2022-03-01 | 广州辰沐生物科技有限公司 | Multifunctional removable mask and preparation method thereof |
| CN115607457A (en) * | 2022-08-15 | 2023-01-17 | 星智豫美(上海)生物科技有限公司 | Soft mask powder mask suitable for sensitive muscles and preparation method thereof |
| WO2024182500A1 (en) * | 2023-02-28 | 2024-09-06 | Onelogy Inc. | Dried cosmetic preparation for rehydration and use |
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| CN111632005A (en) * | 2020-06-09 | 2020-09-08 | 科丽思化妆品（上海）有限公司 | Polypeptide freeze-dried powder mask composition and preparation and use methods thereof |
| CN112716868A (en) * | 2021-03-06 | 2021-04-30 | 广州相宜化妆品有限公司 | Multifunctional microcrystalline soft film powder and preparation method thereof |
| CN113018216A (en) * | 2021-03-12 | 2021-06-25 | 广州相宜化妆品有限公司 | Water-nourishing ice-moistening soft film powder and preparation method thereof |
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| CN114099395A (en) * | 2022-01-05 | 2022-03-01 | 广州辰沐生物科技有限公司 | Multifunctional removable mask and preparation method thereof |
| CN115607457A (en) * | 2022-08-15 | 2023-01-17 | 星智豫美(上海)生物科技有限公司 | Soft mask powder mask suitable for sensitive muscles and preparation method thereof |
| WO2024182500A1 (en) * | 2023-02-28 | 2024-09-06 | Onelogy Inc. | Dried cosmetic preparation for rehydration and use |
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| CN113786374B (en) | 2023-06-09 |
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Effective date of registration: 20240527 Address after: Room 201 and 301, Building 9, No. 7 Chuangye Road, Guangfo Industrial Park, Tangtang Town, Fogang County, Qingyuan City, Guangdong Province, 511500 (multiple photos of one site) Patentee after: Guangdong Xiangyi Cosmetics Co.,Ltd. Country or region after: China Address before: 510000 No. 88, Miaoling, Shishe, shatinggang, Taihe Town, Baiyun District, Guangzhou City, Guangdong Province Patentee before: Guangzhou Suitable Cosmetics Co.,Ltd. Country or region before: China |