CN113756104A - Perfume composition for textiles - Google Patents
Perfume composition for textiles Download PDFInfo
- Publication number
- CN113756104A CN113756104A CN202111130096.XA CN202111130096A CN113756104A CN 113756104 A CN113756104 A CN 113756104A CN 202111130096 A CN202111130096 A CN 202111130096A CN 113756104 A CN113756104 A CN 113756104A
- Authority
- CN
- China
- Prior art keywords
- solution
- stirring
- perfume composition
- silk
- constant speed
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000203 mixture Substances 0.000 title claims abstract description 35
- 239000002304 perfume Substances 0.000 title claims abstract description 28
- 239000004753 textile Substances 0.000 title claims abstract description 26
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 54
- 238000003756 stirring Methods 0.000 claims abstract description 40
- 239000000243 solution Substances 0.000 claims abstract description 34
- 239000003205 fragrance Substances 0.000 claims abstract description 28
- AMXOYNBUYSYVKV-UHFFFAOYSA-M lithium bromide Chemical compound [Li+].[Br-] AMXOYNBUYSYVKV-UHFFFAOYSA-M 0.000 claims abstract description 26
- 238000000502 dialysis Methods 0.000 claims abstract description 25
- 239000001926 citrus aurantium l. subsp. bergamia wright et arn. oil Substances 0.000 claims abstract description 22
- 239000000725 suspension Substances 0.000 claims abstract description 22
- 239000011259 mixed solution Substances 0.000 claims abstract description 20
- 239000008367 deionised water Substances 0.000 claims abstract description 19
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 19
- UZFLPKAIBPNNCA-BQYQJAHWSA-N alpha-ionone Chemical compound CC(=O)\C=C\C1C(C)=CCCC1(C)C UZFLPKAIBPNNCA-BQYQJAHWSA-N 0.000 claims abstract description 16
- UZFLPKAIBPNNCA-UHFFFAOYSA-N alpha-ionone Natural products CC(=O)C=CC1C(C)=CCCC1(C)C UZFLPKAIBPNNCA-UHFFFAOYSA-N 0.000 claims abstract description 16
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 claims abstract description 15
- 229920000053 polysorbate 80 Polymers 0.000 claims abstract description 15
- 239000012460 protein solution Substances 0.000 claims abstract description 15
- 239000004005 microsphere Substances 0.000 claims abstract description 12
- 239000012535 impurity Substances 0.000 claims abstract description 7
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 36
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 18
- 238000000034 method Methods 0.000 claims description 17
- 238000009835 boiling Methods 0.000 claims description 12
- 108010013296 Sericins Proteins 0.000 claims description 6
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 claims description 6
- 229910052921 ammonium sulfate Inorganic materials 0.000 claims description 6
- 235000011130 ammonium sulphate Nutrition 0.000 claims description 6
- 239000007864 aqueous solution Substances 0.000 claims description 6
- 229920006395 saturated elastomer Polymers 0.000 claims description 6
- 238000010025 steaming Methods 0.000 claims description 6
- 241000220317 Rosa Species 0.000 claims description 4
- 241000207199 Citrus Species 0.000 claims description 3
- 235000020971 citrus fruits Nutrition 0.000 claims description 3
- 239000004744 fabric Substances 0.000 abstract description 8
- 239000002245 particle Substances 0.000 abstract description 6
- 238000003860 storage Methods 0.000 abstract description 3
- 235000013599 spices Nutrition 0.000 description 7
- 230000000052 comparative effect Effects 0.000 description 5
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- 108010022355 Fibroins Proteins 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000004094 surface-active agent Substances 0.000 description 2
- 229920000049 Carbon (fiber) Polymers 0.000 description 1
- 244000178870 Lavandula angustifolia Species 0.000 description 1
- 235000010663 Lavandula angustifolia Nutrition 0.000 description 1
- 238000007792 addition Methods 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 239000001102 lavandula vera Substances 0.000 description 1
- 235000018219 lavender Nutrition 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000012466 permeate Substances 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 238000005185 salting out Methods 0.000 description 1
- 238000009958 sewing Methods 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M23/00—Treatment of fibres, threads, yarns, fabrics or fibrous goods made from such materials, characterised by the process
- D06M23/12—Processes in which the treating agent is incorporated in microcapsules
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
- B01J13/02—Making microcapsules or microballoons
- B01J13/06—Making microcapsules or microballoons by phase separation
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/005—Compositions containing perfumes; Compositions containing deodorants
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/12—Aldehydes; Ketones
- D06M13/13—Unsaturated aldehydes, e.g. acrolein; Unsaturated ketones; Ketenes ; Diketenes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/144—Alcohols; Metal alcoholates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/15—Proteins or derivatives thereof
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention relates to a textile perfume composition, which is prepared by the following steps: step S1, adding degummed silk into a lithium bromide solution with the mass fraction of 80% to prepare a protein solution, dialyzing, separating impurities, and preparing a purified protein solution, namely a solution a; step S2, adding bergamot oil, rhodinol and alpha-ionone into deionized water respectively, stirring at a constant speed, adding Tween-80, and stirring at a rotating speed of 350r/min for 2h to obtain a suspension; step S3, adding the suspension into the solution a, stirring at a constant speed for 15min to obtain a mixed solution, transferring the mixed solution into a dialysis bag, and dialyzing for 1h to form microspheres, thus obtaining the perfume composition for textiles; the microsphere particles have small particle size, can be easily attached to the surface of the fabric, and slowly release the fragrance, so that the fragrance storage time of the fabric is longer.
Description
Technical Field
The invention belongs to the technical field of spices, and particularly relates to a spice composition for textiles.
Background
In order to meet the increasing demands of aromatic textiles, a plurality of essence production enterprises are continuously developing post-finishing technologies of perfuming, fragrance soaking and fragrance coating. From the beginning of spraying incense powder and perfume on clothes or sewing an incense bag on the clothes, the prior incense method is developed, the perfumed soap with large fragrance or the incense bag filled with lavender are sealed in a clothes box, the fragrance volatilizes and permeates into fiber pores, and the clothes can keep the fragrance in a short time. In order to improve the capability of the fabric for absorbing the aroma, a method for attaching activated carbon fibers to clothes and a method for attaching the aroma to the fabric through washing liquid are also adopted, but the aroma adding agents are volatile, have poor stability and short aroma storage time, and cannot store the aroma on the textile for a long time.
Disclosure of Invention
In order to solve the above-mentioned problems, an object of the present invention is to provide a perfume composition for textiles.
The purpose of the invention can be realized by the following technical scheme:
a perfume composition for textiles, the composition comprising the steps of:
step S1, adding degummed silk into a lithium bromide solution with the mass fraction of 80%, completely immersing, placing in an oven with the temperature of 50-60 ℃ for dissolving, shaking for 1 time every 1 hour to prepare a protein solution, dialyzing, centrifuging for 2 times at the rotating speed of 10000r/min, separating impurities for 10min every time, preparing a purified protein solution, namely a solution a, and controlling the dosage ratio of the degummed silk to the lithium bromide to be 25 g: 80 g;
step S2, adding bergamot oil, rhodinol and alpha-ionone into deionized water respectively, stirring at a constant speed, adding Tween-80, stirring at a rotating speed of 350r/min for 2h to prepare suspension, and controlling the dosage ratio of the bergamot oil, the rhodinol, the alpha-ionone and the deionized water to be 5 mg: 10mL, wherein the dosage of the Tween-80 is 1-1.5% of that of the bergamot oil;
in step S2, bergamot oil, rhodinol, alpha-ionone, and the like as perfume components are added to water, tween-80 as a surfactant is added, and the mixture is stirred to prepare a suspension.
And step S3, adding the suspension into the solution a, stirring at a constant speed for 15min to obtain a mixed solution, transferring the mixed solution into a dialysis bag, dialyzing the mixed solution in a saturated aqueous solution of ammonium sulfate for 1h, stirring at a constant speed in the dialysis process to form microspheres to obtain the perfume composition for the textile, and controlling the volume ratio of the suspension to the solution a to be 1: 10-15.
Further: the degummed silk is prepared by the following steps:
adding sodium carbonate into boiling water, stirring at constant speed until the sodium carbonate is dissolved, adding silk, completely immersing in the solution, steaming for 50min, stirring once every 15min, taking out the steamed silk, rubbing with deionized water for three times, removing residual sericin to obtain degummed silk, and controlling the dosage ratio of sodium carbonate, boiling water and silk to be 24.65 g: 10L: 30 g.
Further: the dialysis time in the step S1 is 36h, the water is changed for 6 times in the dialysis process, the water is changed for every 3h in the first two times, and the water is changed for every 6h in the last four times.
Further: the perfume composition has citrus fragrance and rose fragrance.
The invention has the beneficial effects that:
the spice composition of the invention has citrus fragrance and rose fragrance, and during the preparation process, the protein solution is prepared by degumming silk, and then bergamot oil, rhodinol, alpha-ionone and the like are taken as spice components and added into water, adding Tween-80 as surfactant, stirring to obtain suspension, mixing, dialyzing, preparing microsphere particles by salting out method, namely the spice composition of the invention, the microsphere particles are silk fibroin microspheres embedded with spice components, the structure of the silk fibroin has controllability, and has high-content folding mechanism and crystal structure, so that the acting force between spice and protein molecules can be increased, the microsphere particles have small particle size, can be easily attached to the surface of the fabric, slowly release the fragrance, and prolong the fragrance storage time of the fabric.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
A perfume composition for textiles, the composition comprising the steps of:
step S1, adding degummed silk into a lithium bromide solution with the mass fraction of 80%, completely immersing, placing in a 50 ℃ oven for dissolving, shaking for 1 time every 1 hour to prepare a protein solution, dialyzing, wherein the dialysis time is 36h, water is changed for 6 times in the dialysis process, water is changed for 3 hours in the first two times, water is changed for 6 hours in the last four times, centrifuging for 2 times at the rotating speed of 10000r/min, and separating impurities every 10 minutes to prepare a purified protein solution, namely a solution a, wherein the dosage ratio of the degummed silk to the lithium bromide is controlled to be 25 g: 80 g;
adding sodium carbonate into boiling water, stirring at constant speed until the sodium carbonate is dissolved, adding silk, completely immersing in the solution, steaming for 50min, stirring once every 15min, taking out the steamed silk, rubbing with deionized water for three times, removing residual sericin to obtain degummed silk, and controlling the dosage ratio of sodium carbonate, boiling water and silk to be 24.65 g: 10L: 30 g.
Step S2, adding bergamot oil, rhodinol and alpha-ionone into deionized water respectively, stirring at a constant speed, adding Tween-80, stirring at a rotating speed of 350r/min for 2h to prepare suspension, and controlling the dosage ratio of the bergamot oil, the rhodinol, the alpha-ionone and the deionized water to be 5 mg: 10mL, wherein the dosage of the Tween-80 is 1% of that of the bergamot oil;
and step S3, adding the suspension into the solution a, stirring at a constant speed for 15min to obtain a mixed solution, transferring the mixed solution into a dialysis bag, dialyzing the mixed solution in a saturated aqueous solution of ammonium sulfate for 1h, stirring at a constant speed in the dialysis process to form microspheres to obtain the perfume composition for the textile, and controlling the volume ratio of the suspension to the solution a to be 1: 10.
Example 2
A perfume composition for textiles, the composition comprising the steps of:
step S1, adding degummed silk into a lithium bromide solution with the mass fraction of 80%, completely immersing, placing in a 55 ℃ oven for dissolving, shaking for 1 time every 1 hour to prepare a protein solution, dialyzing, wherein the dialysis time is 36h, water is changed for 6 times in the dialysis process, water is changed for 3 hours in the first two times, water is changed for 6 hours in the last four times, centrifuging for 2 times at the rotating speed of 10000r/min, and separating impurities every 10 minutes to prepare a purified protein solution, namely a solution a, wherein the dosage ratio of the degummed silk to the lithium bromide is controlled to be 25 g: 80 g;
adding sodium carbonate into boiling water, stirring at constant speed until the sodium carbonate is dissolved, adding silk, completely immersing in the solution, steaming for 50min, stirring once every 15min, taking out the steamed silk, rubbing with deionized water for three times, removing residual sericin to obtain degummed silk, and controlling the dosage ratio of sodium carbonate, boiling water and silk to be 24.65 g: 10L: 30 g.
Step S2, adding bergamot oil, rhodinol and alpha-ionone into deionized water respectively, stirring at a constant speed, adding Tween-80, stirring at a rotating speed of 350r/min for 2h to prepare suspension, and controlling the dosage ratio of the bergamot oil, the rhodinol, the alpha-ionone and the deionized water to be 5 mg: 10mL, wherein the dosage of the Tween-80 is 1.2% of that of the bergamot oil;
and step S3, adding the suspension into the solution a, stirring at a constant speed for 15min to obtain a mixed solution, transferring the mixed solution into a dialysis bag, dialyzing the mixed solution in a saturated aqueous solution of ammonium sulfate for 1h, stirring at a constant speed in the dialysis process to form microspheres to obtain the perfume composition for the textile, and controlling the volume ratio of the suspension to the solution a to be 1: 12.
Example 3
A perfume composition for textiles, the composition comprising the steps of:
step S1, adding degummed silk into a lithium bromide solution with the mass fraction of 80%, completely immersing, placing in a 60 ℃ oven for dissolving, shaking for 1 time every 1 hour to prepare a protein solution, dialyzing, wherein the dialysis time is 36h, water is changed for 6 times in the dialysis process, water is changed for 3 hours in the first two times, water is changed for 6 hours in the last four times, centrifuging for 2 times at the rotating speed of 10000r/min, and separating impurities every 10 minutes to prepare a purified protein solution, namely a solution a, wherein the dosage ratio of the degummed silk to the lithium bromide is controlled to be 25 g: 80 g;
adding sodium carbonate into boiling water, stirring at constant speed until the sodium carbonate is dissolved, adding silk, completely immersing in the solution, steaming for 50min, stirring once every 15min, taking out the steamed silk, rubbing with deionized water for three times, removing residual sericin to obtain degummed silk, and controlling the dosage ratio of sodium carbonate, boiling water and silk to be 24.65 g: 10L: 30 g.
Step S2, adding bergamot oil, rhodinol and alpha-ionone into deionized water respectively, stirring at a constant speed, adding Tween-80, stirring at a rotating speed of 350r/min for 2h to prepare suspension, and controlling the dosage ratio of the bergamot oil, the rhodinol, the alpha-ionone and the deionized water to be 5 mg: 10mL, wherein the dosage of the Tween-80 is 1.4% of that of the bergamot oil;
and step S3, adding the suspension into the solution a, stirring at a constant speed for 15min to obtain a mixed solution, transferring the mixed solution into a dialysis bag, dialyzing the mixed solution in a saturated aqueous solution of ammonium sulfate for 1h, stirring at a constant speed in the dialysis process to form microspheres to obtain the perfume composition for the textile, and controlling the volume ratio of the suspension to the solution a to be 1: 14.
Example 4
A perfume composition for textiles, the composition comprising the steps of:
step S1, adding degummed silk into a lithium bromide solution with the mass fraction of 80%, completely immersing, placing in a 60 ℃ oven for dissolving, shaking for 1 time every 1 hour to prepare a protein solution, dialyzing, wherein the dialysis time is 36h, water is changed for 6 times in the dialysis process, water is changed for 3 hours in the first two times, water is changed for 6 hours in the last four times, centrifuging for 2 times at the rotating speed of 10000r/min, and separating impurities every 10 minutes to prepare a purified protein solution, namely a solution a, wherein the dosage ratio of the degummed silk to the lithium bromide is controlled to be 25 g: 80 g;
adding sodium carbonate into boiling water, stirring at constant speed until the sodium carbonate is dissolved, adding silk, completely immersing in the solution, steaming for 50min, stirring once every 15min, taking out the steamed silk, rubbing with deionized water for three times, removing residual sericin to obtain degummed silk, and controlling the dosage ratio of sodium carbonate, boiling water and silk to be 24.65 g: 10L: 30 g.
Step S2, adding bergamot oil, rhodinol and alpha-ionone into deionized water respectively, stirring at a constant speed, adding Tween-80, stirring at a rotating speed of 350r/min for 2h to prepare suspension, and controlling the dosage ratio of the bergamot oil, the rhodinol, the alpha-ionone and the deionized water to be 5 mg: 10mL, wherein the dosage of the Tween-80 is 1.5% of that of the bergamot oil;
and step S3, adding the suspension into the solution a, stirring at a constant speed for 15min to obtain a mixed solution, transferring the mixed solution into a dialysis bag, dialyzing the mixed solution in a saturated aqueous solution of ammonium sulfate for 1h, stirring at a constant speed in the dialysis process to form microspheres to obtain the perfume composition for the textile, and controlling the volume ratio of the suspension to the solution a to be 1: 15.
Comparative example 1
This comparative example compares to example 1, where bergamot oil, rhodinol and alpha-ionone were sprayed directly onto the textile.
Comparative example 2
This comparative example is a commercially available rose fragrance.
The perfume compositions prepared in examples 1 to 4 and comparative examples 1 and 2 were added to water at a weight ratio of 1: 1000, the fabric was soaked in water after being uniformly stirred, soaked for 30min, and then washed with clean water, air-dried, 10 fragrance smellers were found, the retention time of fragrance on the fabric was tested, and the data of 2h, 10h and 24h were recorded, respectively, and the results are shown in table 1 below, wherein the scores are according to the following table 2:
TABLE 1
TABLE 2 scoring basis
| Standard of merit | Rank and score |
| If the fragrance is similar to the original one at 20cm, the fragrance is smelled at 10cm | Level 1 |
| If the fragrance is similar to that at 10cm, smelling the fragrance at 5cm | Stage 2 |
| If the fragrance is similar to the fragrance at the position of 5cm, smelling the fragrance at the nose end | Grade 3 |
| The nose part has similar or no fragrance | 4 stage |
| Without fragrance | Grade 5 |
It can be seen from table 1 above that the perfume compositions of examples 1-4 have a longer lasting fragrance preserving effect.
In the description herein, references to the description of "one embodiment," "an example," "a specific example" or the like are intended to mean that a particular feature, structure, material, or characteristic described in connection with the embodiment or example is included in at least one embodiment or example of the invention. In this specification, the schematic representations of the terms used above do not necessarily refer to the same embodiment or example. Furthermore, the particular features, structures, materials, or characteristics described may be combined in any suitable manner in any one or more embodiments or examples.
The foregoing is illustrative and explanatory only and is not intended to be exhaustive or to limit the invention to the precise embodiments described, and various modifications, additions, and substitutions may be made by those skilled in the art without departing from the scope of the invention or exceeding the scope of the claims.
Claims (6)
1. A perfume composition for textiles, characterized in that: the method comprises the following steps:
step S1, adding degummed silk into a lithium bromide solution with the mass fraction of 80%, completely immersing, placing in an oven with the temperature of 50-60 ℃ for dissolving, shaking for 1 time every 1 hour to prepare a protein solution, dialyzing, centrifuging for 2 times at the rotating speed of 10000r/min for 10min every time, separating impurities, and preparing a purified protein solution, namely a solution a;
step S2, adding bergamot oil, rhodinol and alpha-ionone into deionized water respectively, stirring at a constant speed, adding Tween-80, and stirring at a rotating speed of 350r/min for 2h to obtain a suspension;
and step S3, adding the suspension into the solution a, stirring at a constant speed for 15min to obtain a mixed solution, transferring the mixed solution into a dialysis bag, dialyzing the mixed solution in a saturated aqueous solution of ammonium sulfate for 1h, stirring at a constant speed in the dialysis process to form microspheres to obtain the perfume composition for the textile, and controlling the volume ratio of the suspension to the solution a to be 1: 10-15.
2. A perfume composition for textile use according to claim 1, wherein: in step S1, the dosage ratio of degummed silk and lithium bromide is controlled to be 25 g: 80 g.
3. A perfume composition for textile use according to claim 1, wherein: in step S2, the dosage ratio of bergamot oil, rhodinol, alpha-ionone and deionized water is controlled to be 5 mg: 10mL, and the dosage of Tween-80 is 1-1.5% of that of the bergamot oil.
4. A perfume composition for textile use according to claim 1, wherein: the degummed silk is prepared by the following steps:
adding sodium carbonate into boiling water, stirring at constant speed until the sodium carbonate is dissolved, adding silk, completely immersing in the solution, steaming for 50min, stirring once every 15min, taking out the steamed silk, rubbing with deionized water for three times, removing residual sericin to obtain degummed silk, and controlling the dosage ratio of sodium carbonate, boiling water and silk to be 24.65 g: 10L: 30 g.
5. A perfume composition for textile use according to claim 1, wherein: the dialysis time in the step S1 is 36h, the water is changed for 6 times in the dialysis process, the water is changed for every 3h in the first two times, and the water is changed for every 6h in the last four times.
6. A perfume composition for textile use according to claim 1, wherein: the perfume composition has citrus fragrance and rose fragrance.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202111130096.XA CN113756104B (en) | 2021-09-26 | 2021-09-26 | Perfume composition for textiles |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202111130096.XA CN113756104B (en) | 2021-09-26 | 2021-09-26 | Perfume composition for textiles |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN113756104A true CN113756104A (en) | 2021-12-07 |
| CN113756104B CN113756104B (en) | 2023-11-10 |
Family
ID=78797535
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202111130096.XA Active CN113756104B (en) | 2021-09-26 | 2021-09-26 | Perfume composition for textiles |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN113756104B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114748671A (en) * | 2022-03-22 | 2022-07-15 | 德晟康(苏州)生物科技有限公司 | Compound protein slow-release hydrocolloid patch and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104822366A (en) * | 2012-07-13 | 2015-08-05 | 塔夫茨大学 | Encapsulation of fragrance and/or flavors in silk fibroin biomaterials |
| CN105544210A (en) * | 2016-01-21 | 2016-05-04 | 苏州印丝特纺织数码科技有限公司 | Fabric post-finishing agent based on modified silk fibroin solution and preparation method of fabric post-finishing agent |
| CN107405277A (en) * | 2014-12-02 | 2017-11-28 | 丝绸医疗公司 | Silk performance clothes and product and preparation method thereof |
| CN108316018A (en) * | 2018-03-15 | 2018-07-24 | 南通纺织丝绸产业技术研究院 | A kind of preparation method of fibroin albumen/chitosan functional solution |
-
2021
- 2021-09-26 CN CN202111130096.XA patent/CN113756104B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104822366A (en) * | 2012-07-13 | 2015-08-05 | 塔夫茨大学 | Encapsulation of fragrance and/or flavors in silk fibroin biomaterials |
| CN107405277A (en) * | 2014-12-02 | 2017-11-28 | 丝绸医疗公司 | Silk performance clothes and product and preparation method thereof |
| CN105544210A (en) * | 2016-01-21 | 2016-05-04 | 苏州印丝特纺织数码科技有限公司 | Fabric post-finishing agent based on modified silk fibroin solution and preparation method of fabric post-finishing agent |
| CN108316018A (en) * | 2018-03-15 | 2018-07-24 | 南通纺织丝绸产业技术研究院 | A kind of preparation method of fibroin albumen/chitosan functional solution |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114748671A (en) * | 2022-03-22 | 2022-07-15 | 德晟康(苏州)生物科技有限公司 | Compound protein slow-release hydrocolloid patch and preparation method thereof |
| CN115737888A (en) * | 2022-03-22 | 2023-03-07 | 德晟康(苏州)生物科技有限公司 | Compound protein slow-release hydrocolloid application |
| CN115737888B (en) * | 2022-03-22 | 2023-12-15 | 德晟康(苏州)生物科技有限公司 | Composite protein slow-release hydrocolloid application |
Also Published As
| Publication number | Publication date |
|---|---|
| CN113756104B (en) | 2023-11-10 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN107988652B (en) | Composite fiber containing lotus leaf extract and lotus seed extract and preparation method thereof | |
| CN108690223A (en) | A kind of layered double hydroxide/fibrination hole composite material and preparation method thereof | |
| CN103484961A (en) | Sustained release aramid nano-microcapsule cellulosic fiber and production method thereof | |
| CN105369639B (en) | A kind of bactericidal deodorant and its method of removal natural feather and chemical fiber plus material peculiar smell | |
| CN113756104A (en) | Perfume composition for textiles | |
| CN105200802A (en) | Preparation method of fragrant light-weight thin wool fabric with health function | |
| CN103343455B (en) | A kind of production method of aromatic fabrics | |
| CN111088695A (en) | Agilawood-flavor finishing fabric and preparation method thereof | |
| CN112011847A (en) | Lotus leaf, isatis root or aloe modified polyester fiber and preparation method thereof | |
| CN108035154A (en) | A kind of degerming technique of white duck down degreasing based on bioenzyme washing method | |
| CN1978779A (en) | Feather-down clothing care agent | |
| CN110144730A (en) | A kind of preparation method of fragrance flannel man textile fabric | |
| CN110747650B (en) | Finishing process of moisture-absorbing and sweat-releasing aromatic chemical fiber wig | |
| CN109183439A (en) | A kind of textile production technique | |
| CN112030261A (en) | Dacron fiber containing dandelion and preparation method thereof | |
| CN106750502A (en) | A kind of Longaacting fragrance-aretaining regenerated celulose fibre | |
| CN110616568A (en) | Plant functional down feather and preparation method thereof | |
| CN105064046A (en) | Preparation method and application of fragrant microcapsule compounded organic silicone softener for cotton fabric | |
| KR102252198B1 (en) | Fabric softener composition manufacturing method for dryer | |
| KR20230147814A (en) | Sheet type fabric softener and manufacturing method | |
| CN114575150A (en) | Fragrant durable pure cotton cloth for hat decoration and preparation method thereof | |
| CN104963002B (en) | Ring spun flax-cotton blended yarn pretreatment method | |
| CN103174034A (en) | Fragrant finishing process of woolen sweater and wool blend ready-made clothes | |
| KR20160131246A (en) | Soap composition | |
| CN108642876A (en) | A kind of fragrant softening agent for textile fabric |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |