CN110747650B - Finishing process of moisture-absorbing and sweat-releasing aromatic chemical fiber wig - Google Patents
Finishing process of moisture-absorbing and sweat-releasing aromatic chemical fiber wig Download PDFInfo
- Publication number
- CN110747650B CN110747650B CN201911126361.XA CN201911126361A CN110747650B CN 110747650 B CN110747650 B CN 110747650B CN 201911126361 A CN201911126361 A CN 201911126361A CN 110747650 B CN110747650 B CN 110747650B
- Authority
- CN
- China
- Prior art keywords
- finishing
- wig
- chemical fiber
- microcapsule
- aromatic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
- D06M16/003—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic with enzymes or microorganisms
-
- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41G—ARTIFICIAL FLOWERS; WIGS; MASKS; FEATHERS
- A41G3/00—Wigs
- A41G3/0091—Sweat absorbing means or deodorants
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
- D06M13/248—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing sulfur
- D06M13/256—Sulfonated compounds esters thereof, e.g. sultones
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/402—Amides imides, sulfamic acids
- D06M13/41—Amides derived from unsaturated carboxylic acids, e.g. acrylamide
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/15—Proteins or derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/55—Epoxy resins
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/564—Polyureas, polyurethanes or other polymers having ureide or urethane links; Precondensation products forming them
- D06M15/568—Reaction products of isocyanates with polyethers
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M23/00—Treatment of fibres, threads, yarns, fabrics or fibrous goods made from such materials, characterised by the process
- D06M23/12—Processes in which the treating agent is incorporated in microcapsules
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/32—Polyesters
Abstract
The invention relates to the field of textile fibers, and discloses a finishing process of a moisture-absorbing and sweat-releasing aromatic chemical fiber wig, which comprises the following steps: cleaning chemical fiber wig with a cleaning agent, washing with water, drying, soaking in a cutinase finishing liquid for hydrophilic finishing, and soaking in a moisture-absorbing and sweat-releasing finishing agent for moisture-absorbing and sweat-releasing finishing; adding the microcapsule aromatic into the capsule wall liquid to obtain microcapsule suspension; and finally, adding a cross-linking agent into the microcapsule suspension, and soaking the chemical fiber wig subjected to moisture absorption and sweat releasing finishing in the microcapsule suspension for aromatic finishing. The chemical fiber wig obtained by the finishing process has excellent moisture absorption and sweat releasing performance and good fragrance durability.
Description
Technical Field
The invention relates to the field of textile fibers, in particular to a finishing process of a moisture-absorbing and sweat-releasing aromatized fibril wig.
Background
The materials of the wig at present mainly comprise chemical fiber, chemical fiber and natural hair. The wig made of real hair has better moisture absorption and air permeability than other two types, but has high price and lower application range. And two kinds of wigs of chemical fibre silk class, chemical fiber silk and real hair mixture, the price is moderate, and the effect is lifelike relatively, but is less ventilative after wearing, and moisture absorption perspire nature is relatively poor, if wear for a long time and make the scalp generate heat, impels the scalp metabolism to accelerate for the scalp perspiration volume increases, and can secrete more grease, and then can block up the hair follicle and arouse that partly allergic people appear rash or even can lose hair, and the wig still can produce the foul smell simultaneously. Therefore, the chemical fiber wig is not breathable and has unpleasant smell, which is a technical problem to be solved in wig preparation.
Disclosure of Invention
The invention aims to provide a finishing process of a moisture-absorbing and sweat-releasing aromatic chemical fiber wig, and the chemical fiber wig obtained by finishing the finishing process has excellent moisture-absorbing and sweat-releasing performance and good fragrance durability.
In order to solve the technical problem, the invention provides a finishing process of a moisture-absorbing and sweat-releasing aromatic fibril wig, which comprises the following steps:
1) cleaning the chemical fiber wig with a cleaning agent, washing with water, and drying;
2) soaking the chemical fiber wig obtained by the treatment of the step 1) in a cutinase finishing liquid at the temperature of 40-70 ℃ and under the condition that the pH value is 6-8, adding a nonionic surfactant, and continuously stirring for 1-2 hours, wherein the concentration of the cutinase finishing liquid is 50-200U/mL;
3) dipping the chemical fiber filament wig obtained by the treatment of the step 2) in a moisture absorption and sweat releasing finishing agent at the temperature of 60-100 ℃, wherein the dipping time is 15-35 min, and then drying, wherein the concentration of the moisture absorption and sweat releasing finishing agent is 10-30 g/L;
4) mixing the aromatic essential oil, the gelatin and the emulsifier, adding distilled water, and stirring at 40-80 ℃ to obtain a microcapsule aromatic;
5) mixing chitosan and gelatin, adding distilled water, heating and stirring at 40-80 ℃ to completely dissolve the chitosan and the gelatin, then adding an emulsifier under high-speed stirring, and uniformly mixing to obtain a capsule wall liquid; wherein the mass ratio of the chitosan, the gelatin, the emulsifier and the distilled water is (1-4) to (1-10) to (1-5): 100.
6) slowly adding the microcapsule aromatic into the capsule wall liquid obtained in the step 5) while stirring, and continuously stirring for 30-60 min to obtain a microcapsule suspension;
7) adding a cross-linking agent into the microcapsule suspension to obtain a mixed solution of microcapsules and the cross-linking agent, soaking the chemical fiber wig obtained by the treatment of the step 3) in the mixed solution of the microcapsules and the cross-linking agent according to a bath ratio of 1 (10-30) for treatment, and then taking out and drying.
Preferably, the chemical fiber silk wig is a polyester silk wig.
Preferably, the cleaning agent is a condensate of fatty alcohol and ethylene oxide.
Preferably, the amount of the nonionic surfactant in step 2) is 2g per 1L of the cutinase finishing liquor, and the nonionic surfactant is peregal O.
Preferably, the drying temperature in the step 3) is 50-80 ℃, and the drying time is 10-30 min.
Preferably, the moisture absorption and sweat releasing finishing agent in the step 3) is a mixture of sulfonate, acrylamide and epoxy resin.
Preferably, the mass ratio of the aromatic essential oil, the gelatin, the emulsifier and the distilled water in the step 4) is (0.2-1.0): (1.5-2): (0.5-0.75): 50-100).
Preferably, the crosslinking agent in step 7) is a crosslinking agent which is synthesized by polyether polyol, lactide and isophorone diisocyanate and is blocked by diisocyanate groups.
Preferably, the dipping temperature in the step 7) is 30-60 ℃, the time is 30-60 min, the drying temperature is 60-80 ℃, and the drying time is 10-20 min.
Preferably, the concentration of the microcapsule in the mixed solution of the microcapsule and the cross-linking agent in the step 7) is 30-70 g/L, and the concentration of the cross-linking agent is 10-30 g/L.
Compared with the prior art, the invention has the following beneficial effects:
(1) the chemical fiber yarn is subjected to hydrophilic treatment by using cutinase finishing liquid, so that the moisture absorption and sweat releasing finishing agent in the later period can be better adsorbed on the chemical fiber yarn, the finishing effect of the moisture absorption and sweat releasing finishing agent is enhanced, and the chemical fiber yarn wig prepared by the method has good moisture absorption and sweat releasing performance.
(2) The invention uses microcapsule technology to carry out aromatic finishing, greatly reduces the consumption of various chemicals compared with the conventional process, has convenient operation, less treatment process harmful to human bodies, low chemical residue and good fragrance retention. Meanwhile, the cross-linking agent used in the aromatic finishing can be biologically degraded, and can not generate larger burden on the environment.
(3) The microcapsule prepared by taking chitosan as a capsule core and gelatin as a capsule material can slowly release chitosan for a long time, so that the wig has an antibacterial effect for a long time, and the microcapsule aromatic prepared by the aromatic essential oil, the gelatin and the emulsifier can slowly release the aromatic essential oil for a long time, so that the problem of acid odor of the wig after long-time use can be effectively solved, and the practicability of the wig is enhanced.
Detailed Description
For a further understanding of the invention, reference will now be made to the preferred embodiments of the present invention by way of example, and it is to be understood that the description is intended to further illustrate features and advantages of the present invention and is not intended to limit the scope of the claims which follow.
All of the starting materials of the present invention, without particular limitation as to their source, may be purchased commercially or prepared according to conventional methods well known to those skilled in the art.
The invention provides a finishing process of a moisture absorption and sweat releasing aromatic fibril wig, which comprises the following steps:
1) cleaning the chemical fiber wig with a cleaning agent, washing with water, and drying;
2) soaking the chemical fiber wig obtained by the treatment of the step 1) in a cutinase finishing liquid at the temperature of 40-70 ℃ and under the condition that the pH value is 6-8, adding a nonionic surfactant, and continuously stirring for 1-2 hours, wherein the concentration of the cutinase finishing liquid is 50-200U/mL;
3) dipping the chemical fiber hairpiece obtained by the step 2) in a moisture absorption and sweat releasing finishing agent at the temperature of 60-130 ℃, wherein the dipping time is 15-35 min, and then drying, wherein the concentration of the moisture absorption and sweat releasing finishing agent is 10-30 g/L;
4) mixing the aromatic essential oil, the gelatin and the emulsifier, adding distilled water, and stirring at 40-80 ℃ to obtain a microcapsule aromatic;
5) mixing chitosan and gelatin, adding distilled water, heating and stirring at 40-80 ℃ to completely dissolve the chitosan and the gelatin, then adding an emulsifier under high-speed stirring, and uniformly mixing to obtain a capsule wall liquid; wherein the mass ratio of the chitosan, the gelatin, the emulsifier and the distilled water is (1-4) to (1-10) to (1-5): 100.
6) slowly adding the microcapsule aromatic into the capsule wall liquid obtained in the step 5) while stirring, and continuously stirring for 30-60 min to obtain a microcapsule suspension;
7) adding a cross-linking agent into the microcapsule suspension to obtain a mixed solution of microcapsules and the cross-linking agent, soaking the chemical fiber wig obtained by the treatment of the step 3) in the mixed solution of the microcapsules and the cross-linking agent according to a bath ratio of 1 (10-30) for treatment, and then taking out and drying.
Specifically, firstly, the chemical fiber wig is washed with a detergent, and then washed with water and dried to obtain a clean chemical fiber wig. Since the chemical fiber wig may have some impurities, in order to improve the cleaning effect, the wig may be washed with water until the wig is free from impurities and then cleaned with a cleaning agent. The chemical fiber hairpiece is preferably selected from a polyester filament hairpiece, the adopted cleaning agent is preferably a condensation product of fatty alcohol and ethylene oxide, and is further preferably one or more of an emulsifier MOA-7, an emulsifier MOA-9, an emulsifier MOA-15, an emulsifier MOA-18 and an emulsifier MOA-20, and is more preferably one or more of an emulsifier MOA-7, an emulsifier MOA-9, an emulsifier MOA-15 and an emulsifier MOA-18; in the invention, the dosage of the nonionic surfactant in each 1L of cutinase finishing liquid is 2g, and the nonionic surfactant preferably adopts peregal O.
After the clean chemical fiber hairpiece is obtained, soaking the clean chemical fiber hairpiece in cutinase finishing liquid with the temperature of 40-70 ℃ and the pH value of 6-8, adding a nonionic surfactant, continuously stirring for 1-2 h, and carrying out hydrophilic finishing, so that the subsequently used moisture absorption and sweat releasing finishing agent can be uniformly adsorbed onto the chemical fiber hairpiece, wherein the concentration of the cutinase finishing liquid is 50-200U/mL.
After hydrophilic finishing is carried out by cutinase finishing liquid, the obtained hydrophilic chemical fiber wig is soaked in a moisture absorption and sweat releasing finishing agent at the temperature of 60-130 ℃ for moisture absorption and sweat releasing finishing, the soaking time is 15-35 min, and then drying is carried out, wherein the concentration of the moisture absorption and sweat releasing finishing agent is 10-30 g/L. In the invention, the drying temperature is preferably 50-80 ℃, the drying time is preferably 10-30 min, the adopted moisture-absorbing and sweat-releasing finishing agent is preferably a mixture of sulfonate, acrylamide and epoxy resin, the moisture-absorbing and sweat-releasing finishing agent used in the invention is a commercial product, and the preferred type is one or more of ZLJ-2, ZLJ-6, ZLJ-9, ZLJ-12 and ZLJ-17, and more preferably one or more of ZLJ-2, ZLJ-6, ZLJ-9 and ZLJ-12.
In addition, the microcapsule aromatic is obtained by mixing the aromatic essential oil, the gelatin and the emulsifier, adding distilled water, and stirring at 40-80 ℃, wherein the mass ratio of the aromatic essential oil, the gelatin, the emulsifier and the distilled water is preferably (0.2-1.0): (1.5-2): (0.5-0.75): 50-100). Mixing chitosan and gelatin, adding distilled water, heating and stirring at the temperature of 40-80 ℃ to completely dissolve the chitosan and the gelatin, then adding an emulsifier under high-speed stirring, and uniformly mixing to obtain capsule wall liquid with chitosan as a capsule core and gelatin as a capsule wall material; wherein the mass ratio of the chitosan, the gelatin, the emulsifier and the distilled water is (1-4) to (1-10) to (1-5): 100. and finally, slowly adding the microcapsule aromatic into the capsule wall liquid while stirring, and continuously stirring for 30-60 min after the microcapsule aromatic is added to obtain the microcapsule suspension. The aromatic essential oil used in some embodiments of the invention is in particular lavender essential oil or rose essential oil.
In order to obtain the chemical fiber wig with aromatic odor, the cross-linking agent is added into the microcapsule suspension to obtain a mixed solution of the microcapsule and the cross-linking agent, the chemical fiber wig subjected to moisture absorption and sweat releasing finishing is soaked in the mixed solution for treatment according to the bath ratio of 1 (10-30), and then the chemical fiber wig is taken out and dried. In the invention, the cross-linking agent is preferably a cross-linking agent which is synthesized by polyether polyol, lactide and isophorone diisocyanate and is blocked by a diisocyanate group, and specifically is a biodegradable cross-linking agent which is blocked by a diisocyanate group and is synthesized by polyether polyol as a soft segment, lactide as a hard segment and isophorone diisocyanate as a blocking agent. In the invention, the dipping temperature is preferably 30-60 ℃, the dipping time is preferably 30-60 min, the drying temperature is preferably 60-80 ℃, and the drying time is preferably 10-20 min; the concentration of the microcapsule in the mixed solution of the microcapsule and the cross-linking agent is preferably 30-70 g/L, and the concentration of the cross-linking agent is preferably 10-30 g/L.
In order to further illustrate the invention, the finishing process of the moisture absorption and sweat releasing aromatic filament wig provided by the invention is described in detail with reference to the following examples.
Example 1
(1) Weighing 1g of polyester yarn wig, fully washing with water, and naturally drying.
(2) And (2) putting the polyester silk wig treated in the step (1) into 50ml of an emulsifying agent MOA-7 solution (the concentration of the solution is 5g/L) for further cleaning for 90min, fully washing with water after the cleaning is finished, and naturally drying.
(3) Carrying out hydrophilic finishing on the polyester silk wig by using cutinase finishing liquid: the polyester silk wig is soaked in 100mL of cutinase finishing liquid with the concentration of 50U/mL under the condition of 40 ℃ and the pH value of 6, 200mg of peregal O is added, and the mixture is continuously stirred for 1 h.
(4) Carrying out moisture absorption and sweat releasing finishing on the polyester yarn wig by using a dipping method: soaking the polyester silk wig subjected to hydrophilic finishing in the step (3) in 10g/L ZLJ-2 at 60 ℃ for 15min, and drying at 50 ℃ for 30 min.
(5) 0.2g of rose essential oil, 1.5g of gelatin and 0.5g of emulsifier were added to a beaker, and 50mL of distilled water was added thereto, followed by stirring at 40 ℃ to obtain a microcapsule fragrance.
(6) Mixing chitosan with capsule core weight of 0.5g and gelatin with capsule wall weight of 2g, adding 50mL distilled water, heating at 40 deg.C and stirring to dissolve completely; and finally, adding 0.5g of emulsifier under high-speed stirring, and uniformly mixing to obtain the capsule wall liquid.
(7) And (3) slowly adding the microcapsule aromatic prepared in the step (5) into the capsule wall liquid obtained in the step (6) while stirring, and continuously stirring for 30min after the addition is finished to obtain a microcapsule suspension.
(8) Carrying out aromatic finishing on the polyester yarn wig by using a microcapsule technology: and (3) taking 100mL of the microcapsule suspension prepared in the step (7), adding 1g of a cross-linking agent to obtain a mixed solution of the microcapsules and the cross-linking agent, soaking the polyester silk wig obtained by the step (4) in the mixed solution of the microcapsules and the cross-linking agent at a bath ratio of 1:10 at 30 ℃ for treatment for 30min, and taking out and drying at 60 ℃ for 10 min.
(9) The moisture-absorbing and sweat-releasing aromatic fibril wig obtained in this example was subjected to water washing several times, and the fragrance retaining performance after water washing was evaluated, and the evaluation results are shown in table 1.
Example 2
(1) Weighing 2g of polyester yarn wig, fully washing with water, and naturally drying.
(2) And (2) putting the polyester silk wig treated in the step (1) into 80ml of an emulsifying agent MOA-9 solution (the concentration of the solution is 3g/L) for further cleaning for 100min, fully washing with water after the cleaning is finished, and naturally drying.
(3) Carrying out hydrophilic finishing on the polyester silk wig by using cutinase finishing liquid: the polyester silk wig is soaked in 100mL of cutinase finishing liquid with the concentration of 100U/mL under the condition of 50 ℃ and pH 7, 200mg of peregal O is added, and the mixture is continuously stirred for 1 h.
(4) Carrying out moisture absorption and sweat releasing finishing on the polyester yarn wig by using a dipping method: soaking the polyester silk wig subjected to hydrophilic finishing in the step (3) in 15g/L ZLJ-6 for 20min at 70 ℃, and drying for 20min at 60 ℃.
(5) 0.4g of rose essential oil, 1.6g of gelatin and 0.55g of emulsifier were added to a beaker, and 80mL of distilled water was added thereto, followed by stirring at 50 ℃ to obtain a microcapsule fragrance.
(6) Mixing chitosan with capsule core weight of 1g and gelatin with capsule wall weight of 4g, adding 80mL distilled water, heating at 40 deg.C and stirring to dissolve completely; and finally, adding 0.6g of emulsifier under high-speed stirring, and uniformly mixing to obtain the capsule wall liquid.
(7) And (3) slowly adding the microcapsule aromatic prepared in the step (5) into the capsule wall liquid obtained in the step (6) while stirring, and continuously stirring for 40min after the addition is finished to obtain a microcapsule suspension.
(8) Carrying out aromatic finishing on the polyester yarn wig by using a microcapsule technology: and (3) taking 100mL of the microcapsule suspension prepared in the step (7), adding 1.5g of a cross-linking agent to obtain a mixed solution of the microcapsule and the cross-linking agent, soaking the polyester silk wig obtained by the step (4) in the mixed solution of the microcapsule and the cross-linking agent at a bath ratio of 1:20 at 40 ℃ for treatment for 40min, and taking out and drying at 65 ℃ for 10 min.
Example 3
(1) Weighing 5g of polyester yarn wig, fully washing with water, and naturally drying.
(2) And (2) putting the polyester silk wig treated in the step (1) into 100ml of an emulsifying agent MOA-15 solution (the concentration of the solution is 8g/L) for further cleaning for 120min, fully washing with water after the cleaning is finished, and naturally drying.
(3) Carrying out hydrophilic finishing on the polyester silk wig by using cutinase finishing liquid: the polyester silk wig is soaked in 100mL of cutinase finishing liquid with the concentration of 150U/mL under the condition of 60 ℃ and the pH value of 8, 200mg of peregal O is added, and the mixture is continuously stirred for 1 h.
(4) Carrying out moisture absorption and sweat releasing finishing on the polyester yarn wig by using a dipping method: soaking the polyester silk wig subjected to hydrophilic finishing in the step (3) in 20g/L ZLJ-9 at 80 ℃ for 25min, and drying at 70 ℃ for 15 min.
(5) 0.6g of rose essential oil, 1.7g of gelatin and 0.6g of emulsifier were added to a beaker, and 90mL of distilled water was added thereto, followed by stirring at 60 ℃ to obtain a microcapsule fragrance.
(6) Mixing chitosan with capsule core weight of 1.2g and gelatin with capsule wall weight of 4.5g, adding 90mL distilled water, heating at 40 deg.C and stirring to dissolve completely; and finally, adding 0.65g of emulsifier under high-speed stirring, and uniformly mixing to obtain the capsule wall liquid.
(7) And (3) slowly adding the microcapsule aromatic prepared in the step (5) into the capsule wall liquid obtained in the step (6) while stirring, and continuously stirring for 50min after the addition is finished to obtain a microcapsule suspension.
(8) Carrying out aromatic finishing on the polyester yarn wig by using a microcapsule technology: and (3) taking 100mL of the microcapsule suspension prepared in the step (7), adding 2g of a cross-linking agent to obtain a mixed solution of microcapsules and the cross-linking agent, soaking the polyester silk wig obtained by the step (4) in the mixed solution of the microcapsules and the cross-linking agent at a bath ratio of 1:30 at 50 ℃ for treatment for 40min, and taking out and drying at 70 ℃ for 15 min.
Example 4
(1) Weighing 10g of polyester yarn wig, fully washing with water, and naturally drying.
(2) And (2) putting the polyester silk wig treated in the step (1) into 150ml of an emulsifying agent MOA-18 solution (the concentration of the solution is 8g/L) for further cleaning for 120min, fully washing with water after the cleaning is finished, and naturally drying.
(3) Carrying out hydrophilic finishing on the polyester silk wig by using cutinase finishing liquid: the polyester silk wig is soaked in 100mL of cutinase finishing liquid with the concentration of 200U/mL under the condition of 70 ℃ and the pH value of 8, 200mg of peregal O is added, and the mixture is continuously stirred for 1.5 h.
(4) Carrying out moisture absorption and sweat releasing finishing on the polyester yarn wig by using a dipping method: soaking the polyester silk wig subjected to hydrophilic finishing in the step (3) in 30g/L ZLJ-9 at 90 ℃ for 35min, and drying at 80 ℃ for 10 min.
(5) 0.8g of rose essential oil, 1.8g of gelatin and 0.65g of emulsifier were added to a beaker, and 100mL of distilled water was added thereto, followed by stirring at 80 ℃ to obtain a microcapsule fragrance.
(6) Mixing chitosan with capsule core weight of 2g and gelatin with capsule wall weight of 5g, adding 100mL distilled water, heating at 40 deg.C and stirring to dissolve completely; and finally, adding 0.65g of emulsifier under high-speed stirring, and uniformly mixing to obtain the capsule wall liquid.
(7) And (3) slowly adding the microcapsule aromatic prepared in the step (5) into the capsule wall liquid obtained in the step (6) while stirring, and continuously stirring for 60min after the addition is finished to obtain a microcapsule suspension.
(8) Carrying out aromatic finishing on the polyester yarn wig by using a microcapsule technology: and (3) adding 3g of cross-linking agent into 100mL of microcapsule suspension prepared in the step (7) to obtain a mixed solution of microcapsules and the cross-linking agent, then soaking the polyester silk wig treated in the step (4) in the mixed solution of the microcapsules and the cross-linking agent at a bath ratio of 1:30 at 60 ℃ for treating for 60min, and then taking out and drying at 80 ℃ for 20 min.
Taking example 1 as an example, the evaluation results of the fragrance retention of the treated wig are shown in table 1:
TABLE 1 evaluation table for fragrance-retaining performance of wig
Table 1 shows that the wig obtained by the finishing process has good fragrance durability.
While there have been shown and described what are at present considered the fundamental principles and essential features of the invention and its advantages, it will be apparent to those skilled in the art that the invention is not limited to the details of the foregoing exemplary embodiments, but is capable of other specific forms without departing from the spirit or essential characteristics thereof. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein. Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (5)
1. A finishing process of a moisture absorption and sweat releasing aromatic chemical fiber wig is characterized in that the chemical fiber wig is a polyester fiber wig and comprises the following steps:
1) cleaning the chemical fiber wig with a cleaning agent, washing with water, and drying;
2) soaking the chemical fiber wig obtained by the treatment of the step 1) in a cutinase finishing liquid at the temperature of 40-70 ℃ and under the condition that the pH value is 6-8, adding a nonionic surfactant, and continuously stirring for 1-2 hours, wherein the concentration of the cutinase finishing liquid is 50-200U/mL; the dosage of the nonionic surfactant in each 1L of cutinase finishing liquid is 2g, and the nonionic surfactant is peregal O;
3) dipping the chemical fiber filament wig obtained by the treatment of the step 2) in a moisture absorption and sweat releasing finishing agent at the temperature of 60-100 ℃, wherein the dipping time is 15-35 min, and then drying, wherein the concentration of the moisture absorption and sweat releasing finishing agent is 10-30 g/L; the moisture-absorbing and sweat-releasing finishing agent is a mixture of sulfonate, acrylamide and epoxy resin;
4) mixing the aromatic essential oil, the gelatin and the emulsifier, adding distilled water, and stirring at 40-80 ℃ to obtain a microcapsule aromatic; the mass ratio of the aromatic essential oil, the gelatin, the emulsifier and the distilled water is (0.2-1.0): 1.5-2): 0.5-0.75): 50-100;
5) mixing chitosan and gelatin, adding distilled water, heating and stirring at 40-80 ℃ to completely dissolve the chitosan and the gelatin, then adding an emulsifier under high-speed stirring, and uniformly mixing to obtain a capsule wall liquid; wherein the mass ratio of the chitosan to the gelatin to the emulsifier to the distilled water is (1-4) to (1-10) to (1-5): 100, respectively;
6) slowly adding the microcapsule aromatic into the capsule wall liquid obtained in the step 5) while stirring, and continuously stirring for 30-60 min to obtain a microcapsule suspension;
7) adding a cross-linking agent into the microcapsule suspension to obtain a mixed solution of microcapsules and the cross-linking agent, soaking the chemical fiber wig obtained by the treatment of the step 3) in the mixed solution of the microcapsules and the cross-linking agent according to a bath ratio of 1 (10-30) for treatment, and then taking out and drying; the concentration of the microcapsule in the mixed solution of the microcapsule and the cross-linking agent is 30-70 g/L, and the concentration of the cross-linking agent is 10-30 g/L.
2. The finishing process of claim 1, wherein the cleaning agent is a condensate of an aliphatic alcohol and ethylene oxide.
3. The finishing process according to claim 1, wherein the drying temperature in the step 3) is 50-80 ℃, and the drying time is 10-30 min.
4. The finishing process according to claim 1, characterized in that the crosslinker in step 7) is a crosslinker blocked with diisocyanate groups synthesized from polyether polyols, lactide and isophorone diisocyanate.
5. The finishing process according to claim 1, wherein the dipping temperature in the step 7) is 30-60 ℃ and the time is 30-60 min, the drying temperature is 60-80 ℃ and the drying time is 10-20 min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911126361.XA CN110747650B (en) | 2019-11-18 | 2019-11-18 | Finishing process of moisture-absorbing and sweat-releasing aromatic chemical fiber wig |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911126361.XA CN110747650B (en) | 2019-11-18 | 2019-11-18 | Finishing process of moisture-absorbing and sweat-releasing aromatic chemical fiber wig |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN110747650A CN110747650A (en) | 2020-02-04 |
| CN110747650B true CN110747650B (en) | 2022-05-17 |
Family
ID=69283510
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201911126361.XA Active CN110747650B (en) | 2019-11-18 | 2019-11-18 | Finishing process of moisture-absorbing and sweat-releasing aromatic chemical fiber wig |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN110747650B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116270264B (en) * | 2023-04-14 | 2023-09-05 | 青岛凯利辰星化妆品有限公司 | Aromatic microcapsule, aromatic chemical fiber false eyelash and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103437192A (en) * | 2013-08-13 | 2013-12-11 | 江苏金太阳纺织科技有限公司 | Preparation method and application of pure-natural fragrant microcapsule textile finishing agent |
| CN103668548A (en) * | 2012-09-21 | 2014-03-26 | 江苏蓝品纤维科技发展有限公司 | Lukens fiber and functional fiber prepared therefrom |
| CN104420203A (en) * | 2013-09-11 | 2015-03-18 | 青岛三秀新科技复合面料有限公司 | Moisture-absorbing sweat-releasing hydrophilic finishing process of polyester fabrics |
| CN106884334A (en) * | 2017-03-08 | 2017-06-23 | 江苏大同宝富纺织科技有限公司 | A kind of method for carrying out dacron Aroma finishing based on grafting microcapsules |
| CN107557960A (en) * | 2017-10-13 | 2018-01-09 | 江苏美恒纺织实业有限公司 | A kind of ventilation and perspiration function fabric and its manufacture method |
-
2019
- 2019-11-18 CN CN201911126361.XA patent/CN110747650B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103668548A (en) * | 2012-09-21 | 2014-03-26 | 江苏蓝品纤维科技发展有限公司 | Lukens fiber and functional fiber prepared therefrom |
| CN103437192A (en) * | 2013-08-13 | 2013-12-11 | 江苏金太阳纺织科技有限公司 | Preparation method and application of pure-natural fragrant microcapsule textile finishing agent |
| CN104420203A (en) * | 2013-09-11 | 2015-03-18 | 青岛三秀新科技复合面料有限公司 | Moisture-absorbing sweat-releasing hydrophilic finishing process of polyester fabrics |
| CN106884334A (en) * | 2017-03-08 | 2017-06-23 | 江苏大同宝富纺织科技有限公司 | A kind of method for carrying out dacron Aroma finishing based on grafting microcapsules |
| CN107557960A (en) * | 2017-10-13 | 2018-01-09 | 江苏美恒纺织实业有限公司 | A kind of ventilation and perspiration function fabric and its manufacture method |
Also Published As
| Publication number | Publication date |
|---|---|
| CN110747650A (en) | 2020-02-04 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105648771B (en) | The antibacterial deodourizing and anti-crease finishing technique of cotton/silk blend fabric | |
| CN105200802A (en) | Preparation method of fragrant light-weight thin wool fabric with health function | |
| CN102312342A (en) | Multifunctional thermal underwear fabric and processing method thereof | |
| KR20190086600A (en) | Plant fiber blend skin-friendly fabric and its processing method | |
| CN110747650B (en) | Finishing process of moisture-absorbing and sweat-releasing aromatic chemical fiber wig | |
| CN110592938A (en) | Antibacterial modified silk fiber and preparation method thereof | |
| JPH0949171A (en) | Polyurethane fiber-containing textile product with modified absorbed sweat releasability and its production | |
| CN107059142A (en) | A kind of overlength cattle-hide collagen fibers and its preparation method and application | |
| CN101193620A (en) | Method and composition for obtaining odor-suppressing textile product and textile product garment, thus obtained | |
| WO2020206989A1 (en) | Preparation method for aromatic flannel household textile fabric | |
| US3625811A (en) | Method of preparing yarn and the like from animal hide | |
| CN105220485A (en) | A kind of infant based on ionic liquid is with new modified cotton fiber and preparation method thereof | |
| CN111719310A (en) | Preparation method of fiber containing Chinese herbal medicine effective components | |
| CN110607685A (en) | Antibacterial natural silk fiber product and preparation method thereof | |
| CN111235879A (en) | Preparation method of silk-woven fabric for Hunan embroidery | |
| CN113756104A (en) | Perfume composition for textiles | |
| CN113652870A (en) | Preparation method of multifunctional fibroin finishing agent and application of multifunctional fibroin finishing agent to polyester fabric | |
| CN111118879B (en) | Modified cotton production method and method for producing fragrant yarn | |
| CN112080834A (en) | Preparation method of super-hydrophobic cotton-linen textile fabric | |
| CN109695150A (en) | A kind of preparation method of pro-skin type uvioresistant silk fabric | |
| CN107287880A (en) | A kind of summer clothing special fabric of pants and its handling process | |
| CN117051581B (en) | Antibacterial finishing process for polyester fabric | |
| CN111379162B (en) | Softening method of ramie fibers | |
| JP3481383B2 (en) | Polyurethane fiber-containing fiber product excellent in sweat-absorbing property and method for producing the same | |
| CN117721560A (en) | Preparation method of washable antibacterial nylon composite fabric |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20220915 Address after: Room 4001, Building 3, No. 6, Shandong Road, Shinan District, Qingdao City, Shandong Province, 266000 Patentee after: Qingdao Huaruimei Import & Export Co.,Ltd. Address before: 226019 Jiangsu city of Nantong province sik Road No. 9 Patentee before: NANTONG University |
|
| TR01 | Transfer of patent right |