CN113712050A - Eucalyptus oil-containing plant protection additive and preparation method thereof - Google Patents
Eucalyptus oil-containing plant protection additive and preparation method thereof Download PDFInfo
- Publication number
- CN113712050A CN113712050A CN202111179161.8A CN202111179161A CN113712050A CN 113712050 A CN113712050 A CN 113712050A CN 202111179161 A CN202111179161 A CN 202111179161A CN 113712050 A CN113712050 A CN 113712050A
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- CN
- China
- Prior art keywords
- eucalyptus oil
- plant protection
- containing plant
- parts
- weight
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000010642 eucalyptus oil Substances 0.000 title claims abstract description 35
- 229940044949 eucalyptus oil Drugs 0.000 title claims abstract description 35
- 241000196324 Embryophyta Species 0.000 title claims abstract description 25
- 238000002360 preparation method Methods 0.000 title claims abstract description 8
- 239000000654 additive Substances 0.000 title claims abstract description 4
- 230000000996 additive effect Effects 0.000 title claims abstract description 4
- 239000005884 Beta-Cyfluthrin Substances 0.000 claims abstract description 13
- QQODLKZGRKWIFG-RUTXASTPSA-N [(R)-cyano-(4-fluoro-3-phenoxyphenyl)methyl] (1S)-3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropane-1-carboxylate Chemical compound CC1(C)C(C=C(Cl)Cl)[C@@H]1C(=O)O[C@@H](C#N)C1=CC=C(F)C(OC=2C=CC=CC=2)=C1 QQODLKZGRKWIFG-RUTXASTPSA-N 0.000 claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 11
- 239000000203 mixture Substances 0.000 claims description 13
- 239000002202 Polyethylene glycol Substances 0.000 claims description 12
- 229920001223 polyethylene glycol Polymers 0.000 claims description 12
- 238000002156 mixing Methods 0.000 claims description 10
- 235000007688 Lycopersicon esculentum Nutrition 0.000 claims description 7
- 239000002270 dispersing agent Substances 0.000 claims description 6
- 238000000034 method Methods 0.000 claims description 5
- 239000002671 adjuvant Substances 0.000 claims description 4
- 240000003768 Solanum lycopersicum Species 0.000 claims description 2
- 239000010672 sassafras oil Substances 0.000 claims 1
- 239000012752 auxiliary agent Substances 0.000 abstract description 6
- DSSYKIVIOFKYAU-XCBNKYQSSA-N (R)-camphor Chemical compound C1C[C@@]2(C)C(=O)C[C@@H]1C2(C)C DSSYKIVIOFKYAU-XCBNKYQSSA-N 0.000 description 6
- 241000723346 Cinnamomum camphora Species 0.000 description 6
- 241000227653 Lycopersicon Species 0.000 description 5
- 238000003756 stirring Methods 0.000 description 4
- 229960000411 camphor oil Drugs 0.000 description 3
- 239000010624 camphor oil Substances 0.000 description 3
- 238000000605 extraction Methods 0.000 description 3
- 239000003921 oil Substances 0.000 description 3
- 235000013399 edible fruits Nutrition 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000010899 nucleation Methods 0.000 description 2
- 238000009331 sowing Methods 0.000 description 2
- 206010011224 Cough Diseases 0.000 description 1
- 241000218195 Lauraceae Species 0.000 description 1
- 244000227633 Ocotea pretiosa Species 0.000 description 1
- 235000004263 Ocotea pretiosa Nutrition 0.000 description 1
- 241001518143 Polypodium <fern> Species 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- -1 beta-cyfluthrin) Chemical compound 0.000 description 1
- 210000000481 breast Anatomy 0.000 description 1
- 239000012459 cleaning agent Substances 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 210000001672 ovary Anatomy 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 238000000194 supercritical-fluid extraction Methods 0.000 description 1
- 229940034610 toothpaste Drugs 0.000 description 1
- 239000000606 toothpaste Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N53/00—Biocides, pest repellants or attractants, or plant growth regulators containing cyclopropane carboxylic acids or derivatives thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/24—Lauraceae [Laurel family], e.g. laurel, avocado, sassafras, cinnamon or camphor
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Zoology (AREA)
- Agronomy & Crop Science (AREA)
- Plant Pathology (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Environmental Sciences (AREA)
- Biotechnology (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Pest Control & Pesticides (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a plant protection additive containing eucalyptus oil and a preparation method thereof, wherein the preparation method comprises the following steps: 0.1-10 parts of beta-cyfluthrin; 0.1-10 parts of eucalyptus oil; and 1000 parts by weight of water. The eucalyptus oil-containing plant protection auxiliary agent can improve the emergence rate of plants.
Description
Technical Field
The invention relates to the field of cinnamomum camphora application, and particularly relates to a eucalyptus oil-containing plant protection auxiliary agent and a preparation method thereof.
Background
Cinnamomum camphora (with the academic name of Camphorum longipaniticulatum (Gamble) N. Chao ex H.W.Li) is evergreen arbor of Lauraceae, with height of 20 m and diameter at breast height of 50 cm; the bark is gray, the branch is cylindrical, hairless, the young branch is fine, the leaves are intergrowth, oval or elliptical, the tip is suddenly short and gradually sharp to long and gradually sharp, the upper surface is dark green, bright, the lower surface is grey green, dark, the two surfaces are hairless, the leaf stalk is flat and back convex, light green, the cone inflorescence axillary, is fine, the branch is fine and weak, each branch is 3-7 flowers of the polypodium, the shaft is hairless, the flower is light yellow, fragrance is provided, the stalk is fine, the flower quilt is cone-shaped, the flower quilt is oval, the filament is white and soft, the filament is glandless, the anther is long round, the ovary is oval, the young fruit is spherical, the flower is in 5-6 months, and the fruit is yielded in 7-9 months.
Yibin is the primary resource of the cinnamomum camphora, and by the end of 2018, 47 ten thousand mu of cinnamomum camphora forest base in the whole market has the crude cinnamomum camphora oil yield of over 70 percent of the whole country, the yibin crude cinnamomum camphora has high oil yield and good oil quality, and belongs to a non-inspection product in the international market.
At present, the main methods for extracting the crude camphor oil comprise a CO2 supercritical extraction method, a water vapor extraction method, an extraction method and the like, and target products are extracted from the crude camphor oil through the extraction methods, wherein the eucalyptus oil is one of the target products.
The existing eucalyptus oil is generally used as cough drops, gum candies, gargles, toothpaste and air cleaning agents, and other purposes are not reported.
Disclosure of Invention
In view of the above problems, in one aspect, the present invention provides a plant protection aid containing eucalyptus oil, which can improve the rate of emergence of plants.
A eucalyptus oil-containing plant protection aid comprising:
0.1-10 parts of beta-cyfluthrin;
0.1-10 parts of eucalyptus oil; and
1000 parts of water.
In one or more specific embodiments herein, the eucalyptus oil-containing plant protection adjuvant further comprises a dispersant in an amount of 0.001 to 0.1 parts by weight.
In one or more specific embodiments herein, the dispersant is 0.01 to 0.1 parts by weight.
In one or more specific embodiments herein, the dispersant is polyethylene glycol. After the polyethylene glycol is added, the dispersion of the plant protection auxiliary agent is promoted, and the seedling emergence amount is uniformly distributed under the same experiment conditions in a field experiment.
In one or more specific embodiments herein, the beta-cyhalothrin is 1 to 10 parts by weight.
In one or more specific embodiments of the present application, the plant comprises tomato.
In one or more specific embodiments of the present application, the eucalyptus oil is prepared from sassafras.
On one hand, the invention also provides a preparation method of the eucalyptus oil-containing plant protection auxiliary agent.
A preparation method of the eucalyptus oil-containing plant protection auxiliary agent comprises the following steps:
firstly, mixing beta-cyfluthrin and eucalyptus oil.
And adding polyethylene glycol into the mixture of the first step, and uniformly mixing.
Thirdly, water is added into the mixture of the second step.
The invention principle and the beneficial effects of the application are as follows:
the invention mixes beta-cyfluthrin, eucalyptus oil and polyethylene glycol as the plant protection auxiliary agent, thereby improving the rate of emergence.
Detailed Description
The present invention will be further explained below.
The examples provided herein are merely to further illustrate the invention and should not be construed as limiting the invention in any way.
It will be apparent to those skilled in the art that the materials and methods of operation used in the present invention are well known in the art, unless otherwise specified, in the following.
In the present invention, parts by weight means measured in units of weight, such as 1 part by weight means: when the weight is Kg, 1 part by weight means 1 Kg; when the weight is g, 1 part by weight means 1g, and the like, and is not limited to a specific Kg or g.
In the following examples 1-3, beta-cyfluthrin (i.e., beta-cyfluthrin), polyethylene glycol, and eucalyptus oil, which is prepared by extracting crude camphor oil, are commercially available.
Example 1
Firstly, 1 part by weight of beta-cyfluthrin and 1 part by weight of eucalyptus oil are taken and mixed evenly.
② adding 0.01 weight portion of polyethylene glycol into the mixture of the first step, and mixing uniformly.
And thirdly, adding 1000 parts by weight of water into the mixture of the second step, and uniformly stirring for later use.
Example 2
Firstly, 5 parts by weight of beta-cyfluthrin and 1 part by weight of eucalyptus oil are uniformly mixed.
② adding 0.05 weight part of polyethylene glycol into the mixture of the first step, and mixing evenly.
Thirdly, 1000 parts by weight of water is added into the mixture of the second step, and the mixture is stirred uniformly.
Example 3
Taking 10 parts by weight of beta-cyfluthrin and 1 part by weight of eucalyptus oil, and uniformly mixing.
② adding 0.1 weight part of polyethylene glycol into the mixture of the first step, and mixing uniformly.
And thirdly, adding 1000 parts by weight of water into the mixture of the second step, and uniformly stirring for later use.
Example 4
Taking 2 parts of beta-cyfluthrin by weight.
② adding 0.01 weight part of polyethylene glycol into beta-cyfluthrin of the first step, and mixing uniformly.
And thirdly, adding 1000 parts by weight of water into the mixture of the second step, and uniformly stirring for later use.
Example 5
Taking 2 parts by weight of eucalyptus oil.
② adding 0.01 weight part of polyethylene glycol into the eucalyptus oil of the first step, and uniformly mixing.
And thirdly, adding 1000 parts by weight of water into the mixture of the second step, and uniformly stirring for later use.
Example 6
The test specimens prepared in each of example 1, example 4 and example 5 were subjected to field tests for tomato emergence.
Tomato seeds are purchased from the market and comprise three types, namely, parents (fine variety), hybrid seeds (first-grade) and conventional seeds (fine variety).
The experimental land of the field test is the same ground source, and the same ground source is divided into 36 small plots with equal areas. Wherein, in example 1, there are three small plots corresponding to the parent (improved variety), three small plots corresponding to the hybrid (first-grade), and three small plots corresponding to the conventional variety (improved variety); example 4 there were three small plots corresponding to the parent (elite), three small plots corresponding to the hybrid (first-grade), and three small plots corresponding to the conventional (elite); example 5 three small plots corresponding to the parent (elite), three small plots corresponding to the hybrid (first-grade), and three small plots corresponding to the conventional (elite); the other 9 small plots are blank control plots, wherein the parent (fine variety) corresponds to three small plots, the hybrid (first grade) corresponds to three small plots, and the conventional variety (fine variety) corresponds to three small plots.
Before sowing, except the tomato seeds corresponding to the blank control plots, the tomato seeds corresponding to each small plot are treated by the corresponding samples, and the treatment methods are the same. And directly sowing the tomato seeds corresponding to the blank control plot, and treating without a sample.
When in seeding, the number of the seeds sowed in each small plot is the same, and the field management after seeding is the same.
And observing and recording the number of seedlings, and calculating the rate of emergence, wherein the rate of emergence is 100% of the number of seedlings/seed number.
Table 1 below is a table comparing the emergence rates of the samples of example 1, example 4 and example 5 with the blank control.
Table 1 table for comparison of emergence rates of samples of example 1, example 4 and example 5 with blank control
Remarking: in table 1, the values in each bin are the average values after removing the suspicious data according to the grassbs criterion, except the average value. The average value is the average value of the emergence rate of the parent, the emergence rate of the hybrid and the emergence rate of the conventional seed.
As can be seen from Table 1, the emergence rates of the hybrids were higher than those of the parent and the conventional species for the samples of example 1, example 4 and example 5, the higher emergence rates were obtained for the samples of example 1 than for the samples of example 4 and example 5, and the higher emergence rates were obtained for the samples of example 4 and example 5 relative to the blank control, wherein the emergence rates of example 4 and example 5 were substantially the same.
The above description is only a preferred embodiment of the present invention and is not intended to limit the present invention, and various modifications and changes may be made by those skilled in the art. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (8)
1. A eucalyptus oil-containing plant protection aid comprising:
0.1-10 parts of beta-cyfluthrin;
0.1-10 parts of eucalyptus oil; and
1000 parts of water.
2. The eucalyptus oil-containing plant protection auxiliary according to claim 1, wherein the eucalyptus oil-containing plant protection auxiliary further comprises a dispersant in an amount of 0.001 to 0.1 parts by weight.
3. The eucalyptus oil-containing plant protection adjuvant according to claim 2, wherein the dispersant is 0.01 to 0.1 part by weight.
4. The eucalyptus oil-containing plant protection adjuvant according to claim 2 or 3, wherein the dispersant is polyethylene glycol.
5. The eucalyptus oil-containing plant protection auxiliary according to any one of claims 1 to 4, wherein the beta-cyhalothrin is 1 to 10 parts by weight.
6. The eucalyptus oil-containing plant protection aid according to any one of claims 1 to 5, wherein the plant comprises a tomato.
7. The eucalyptus oil-containing plant protection additive according to any one of claims 1 to 6, wherein the eucalyptus oil is prepared from sassafras oil.
8. A process for the preparation of a eucalyptus oil containing plant protection adjuvant as claimed in any of claims 1 to 7, comprising the steps of:
firstly, mixing beta-cyfluthrin and eucalyptus oil;
adding polyethylene glycol into the mixture of the first step, and uniformly mixing;
thirdly, water is added into the mixture of the second step.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202111179161.8A CN113712050A (en) | 2021-10-09 | 2021-10-09 | Eucalyptus oil-containing plant protection additive and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202111179161.8A CN113712050A (en) | 2021-10-09 | 2021-10-09 | Eucalyptus oil-containing plant protection additive and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN113712050A true CN113712050A (en) | 2021-11-30 |
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| CN202111179161.8A Pending CN113712050A (en) | 2021-10-09 | 2021-10-09 | Eucalyptus oil-containing plant protection additive and preparation method thereof |
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1107293A (en) * | 1994-02-23 | 1995-08-30 | 郑树勤 | Multifunctional emulsified insecticide |
| CA2769005A1 (en) * | 2009-07-28 | 2011-02-03 | The Energy And Resources Institute (Teri) | Novel biopesticide compositions and method for isolation and characterization of same |
| CN102805115A (en) * | 2012-08-30 | 2012-12-05 | 白静 | Plant-source natural fungicide for preventing and controlling botrytis cinerea and preparation method thereof |
| CN104770406A (en) * | 2014-01-15 | 2015-07-15 | 馥稷生物科技发展（上海）有限公司 | Botanical herbicide based on eucalyptus leaf oil |
| CN108308188A (en) * | 2018-04-18 | 2018-07-24 | 中国人民解放军海军军医大学海军医学研究所 | A kind of water-base pesticide emulsion |
| CN111134146A (en) * | 2019-12-26 | 2020-05-12 | 山西奇星农药有限公司 | Synergistic granule and preparation method and application thereof |
-
2021
- 2021-10-09 CN CN202111179161.8A patent/CN113712050A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1107293A (en) * | 1994-02-23 | 1995-08-30 | 郑树勤 | Multifunctional emulsified insecticide |
| CA2769005A1 (en) * | 2009-07-28 | 2011-02-03 | The Energy And Resources Institute (Teri) | Novel biopesticide compositions and method for isolation and characterization of same |
| CN102805115A (en) * | 2012-08-30 | 2012-12-05 | 白静 | Plant-source natural fungicide for preventing and controlling botrytis cinerea and preparation method thereof |
| CN104770406A (en) * | 2014-01-15 | 2015-07-15 | 馥稷生物科技发展（上海）有限公司 | Botanical herbicide based on eucalyptus leaf oil |
| CN108308188A (en) * | 2018-04-18 | 2018-07-24 | 中国人民解放军海军军医大学海军医学研究所 | A kind of water-base pesticide emulsion |
| CN111134146A (en) * | 2019-12-26 | 2020-05-12 | 山西奇星农药有限公司 | Synergistic granule and preparation method and application thereof |
Non-Patent Citations (1)
| Title |
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| 马安民等: "《园林植物杀虫剂应用技术》", 31 October 2017, 河南科学技术出版社 * |
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Application publication date: 20211130 |