CN113605090B - 一种羽绒服除味清新喷雾及其制备方法 - Google Patents
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Abstract
本发明涉及羽绒服除味技术领域，具体公开了一种羽绒服除味清新喷雾及其制备方法，喷雾的制备原料包括：除味活性剂、细菌抑制剂、有机溶剂、清新剂、芳香剂和稳定剂，除味活性剂由香豆素和木酚素按5:1‑2的质量比混合而成，细菌抑制剂为异噻唑啉酮和/或对羟基苯甲酸乙酯，清新剂为薄荷提取物、蒲公英提取物、野菊花提取物中的一种或多种。本发明喷雾中采用了香豆素和木酚素作为除味活性剂，能起到良好的除味作用，尤其是针对羽绒角蛋白纤维的腥味，同时还能配合细菌抑制剂，起到良好的抗菌作用，从源头上避免腥味的产生；喷雾中采用了薄荷提取物、蒲公英提取物或野菊花提取物作为清新剂，配合精油类芳香剂，能在使用后使羽绒服长久散发清新香味。
Description
技术领域
本发明涉及羽绒除味技术领域，具体涉及一种羽绒服除味清新喷雾及其制备方法。
背景技术
羽绒是一种绿色天然蛋白质纤维，也是宝贵的生物质资源，其具有轻盈、柔软，保暖性能好、资源丰富，性价比极高等特性。随着人们生活水平的提高，对羽绒的品质要求也越来越高。
但是羽绒属于一种角蛋白纤维，其耐碱性较差，在人们日常使用中用肥皂或一般洗衣粉清洗，较强的碱性会破坏其表面的脂肪膜，加上存放不当，极易滋生细菌，并产生腥味。人的皮肤每时每刻都在新陈代谢，分泌皮脂、汗液、角质、废气等代谢废物，成为了细菌生长的养分，同时影响和皮肤接触的纺织品，使其发臭、发腥，尤其在我国南方湿气重的环境下更容易这样。那么无论是保护人体不受环境中有害细菌和气味的侵害，还是防止细菌在羽绒制品上的生长和散发腥味，对其进行抗菌除腥味处理都是有必要的。
目前，市面上出现一些羽绒服用的除味清新喷雾，这些喷雾能起到一定的遮蔽异味的作用，但是不能从根本上解决羽绒服异味的问题，需要反复使用。
发明内容
本发明的目的在于提供一种羽绒服除味清新喷雾及其制备方法，其解决了现有市面上的除味清新喷雾不能从根本上解决羽绒服异味的问题。
本发明通过以下技术方案来实现上述目的：
一种羽绒服除味清新喷雾，所述喷雾的制备原料包括：除味活性剂、细菌抑制剂、有机溶剂、清新剂、芳香剂和稳定剂，其中，所述除味活性剂由香豆素和木酚素按5:1-2的质量比混合而成，所述细菌抑制剂为异噻唑啉酮和/或对羟基苯甲酸乙酯，所述清新剂为薄荷提取物、蒲公英提取物、野菊花提取物中的一种或多种。
进一步改进在于，所述喷雾的制备原料按重量份数包括：2-10份除味活性剂、1-5份细菌抑制剂、20-40份有机溶剂、2-4份清新剂、0.1-0.5份芳香剂和0.2-0.6份稳定剂。
进一步改进在于，所述有机溶剂选自乙醇、乙醚、丙酮、苯、氯仿、乙酸乙酯中的一种或多种。
进一步改进在于，所述芳香剂为经过高磁化处理的天然精油，在磁场作用下使精油分子团变小，实现微米化，且活性和渗透性提升，而粘性降低，从而有利于精油效果的发挥。
进一步改进在于，所述天然精油选自薰衣草精油、茉莉精油、茶树油、橄榄精油、薄荷精油、肉桂精油、茴香油、百合精油、玫瑰精油中的一种或多种。
进一步改进在于，所述高磁化处理的磁场强度为8000-20000GS，处理时间为20-80min。
进一步改进在于，所述稳定剂选自荼多酚、羧甲基纤维素钠、1，4-丁二醇、二苯酮-4中的一种或多种。
本发明还提供了一种羽绒服除味清新喷雾的制备方法，步骤包括：
步骤一、取香豆素和木酚素按比例混合后加入到有机溶剂中，在温度为35-55℃、以300-500r/min的转速搅拌提取5-7h，过滤得除味活性剂备用；
步骤二、取薄荷、蒲公英和/或野菊花新鲜的有效植物体，将植物体粉碎后用乙醇溶液室温浸泡8-15h，过滤取滤液，然后再重复一次，合并两次滤液得到混合滤液，将该混合滤液与同体积的水混合后，减压浓缩去除乙醇，得到所需清新剂；
步骤三、取异噻唑啉酮和/或对羟基苯甲酸乙酯作为细菌抑制剂，将所述除味活性剂、细菌抑制剂溶于有机溶剂中，再加入清新剂、芳香剂和稳定剂，搅拌均匀，精滤后压缩至罐中，即得羽绒服除味清新喷雾。
本发明的有益效果在于：
(1)本发明喷雾中采用了香豆素和木酚素作为除味活性剂，其中香豆素自身属于天然的香料，在与木酚素配合使用时能起到了良好的除味作用，尤其是针对羽绒角蛋白纤维的腥味，同时还能配合细菌抑制剂，起到良好的抗菌作用，从源头上避免腥味的产生；
(2)本发明喷雾中采用了薄荷提取物、蒲公英提取物或野菊花提取物作为清新剂，配合精油类芳香剂，能在使用后使羽绒服长久散发清新香味。
具体实施方式
下面结合实施例对本申请作进一步详细描述，有必要在此指出的是，以下具体实施方式只用于对本申请进行进一步的说明，不能理解为对本申请保护范围的限制，该领域的技术人员可以根据上述申请内容对本申请作出一些非本质的改进和调整。
实施例1
一种羽绒服除味清新喷雾，所述喷雾的制备原料按重量份数包括：2份除味活性剂、1份细菌抑制剂、20份有机溶剂、2份清新剂、0.1份芳香剂和0.2份稳定剂，其中，所述除味活性剂由香豆素和木酚素按5:1的质量比混合而成，所述细菌抑制剂为异噻唑啉酮，所述清新剂为薄荷提取物；所述机溶剂为乙醇；所述芳香剂为经过高磁化处理(磁场强度为8000GS，处理时间为80min)的薰衣草精油；所述稳定剂为荼多酚。
上述羽绒服除味清新喷雾的制备方法，步骤包括：
步骤一、取香豆素和木酚素按比例混合后加入到有机溶剂中，在温度为35℃、以300r/min的转速搅拌提取7h，过滤得除味活性剂备用；
步骤二、取薄荷新鲜的薄荷叶，将薄荷叶粉碎后用乙醇溶液室温浸泡8h，过滤取滤液，然后再重复一次，合并两次滤液得到混合滤液，将该混合滤液与同体积的水混合后，减压浓缩去除乙醇，得到所需清新剂；
步骤三、取异噻唑啉酮作为细菌抑制剂，将所述除味活性剂、细菌抑制剂溶于有机溶剂中，再加入清新剂、芳香剂和稳定剂，搅拌均匀，精滤后压缩至罐中，即得羽绒服除味清新喷雾。
实施例2
一种羽绒服除味清新喷雾，所述喷雾的制备原料按重量份数包括：8份除味活性剂、3份细菌抑制剂、30份有机溶剂、3份清新剂、0.3份芳香剂和0.4份稳定剂，其中，所述除味活性剂由香豆素和木酚素按5:1.5的质量比混合而成，所述细菌抑制剂为对羟基苯甲酸乙酯，所述清新剂为野菊花提取物；所述机溶剂为乙酸乙酯；所述芳香剂为经过高磁化处理(磁场强度为14000GS，处理时间为50min)的百合精油；所述稳定剂为二苯酮-4。
上述羽绒服除味清新喷雾的制备方法，步骤包括：
步骤一、取香豆素和木酚素按比例混合后加入到有机溶剂中，在温度为45℃、以400r/min的转速搅拌提取6h，过滤得除味活性剂备用；
步骤二、取野菊花新鲜的花瓣，将花瓣粉碎后用乙醇溶液室温浸泡12h，过滤取滤液，然后再重复一次，合并两次滤液得到混合滤液，将该混合滤液与同体积的水混合后，减压浓缩去除乙醇，得到所需清新剂；
步骤三、取对羟基苯甲酸乙酯作为细菌抑制剂，将所述除味活性剂、细菌抑制剂溶于有机溶剂中，再加入清新剂、芳香剂和稳定剂，搅拌均匀，精滤后压缩至罐中，即得羽绒服除味清新喷雾。
实施例3
一种羽绒服除味清新喷雾，所述喷雾的制备原料按重量份数包括：10份除味活性剂、5份细菌抑制剂、40份有机溶剂、4份清新剂、0.5份芳香剂和0.6份稳定剂，其中，所述除味活性剂由香豆素和木酚素按5:2的质量比混合而成，所述细菌抑制剂为异噻唑啉酮和对羟基苯甲酸乙酯1:1质量比混合，所述清新剂为薄荷提取物；所述机溶剂为丙酮；所述芳香剂为经过高磁化处理(磁场强度为20000GS，处理时间为20min)的玫瑰精油；所述稳定剂为羧甲基纤维素钠。
上述羽绒服除味清新喷雾的制备方法，步骤包括：
步骤一、取香豆素和木酚素按比例混合后加入到有机溶剂中，在温度为55℃、以500r/min的转速搅拌提取5h，过滤得除味活性剂备用；
步骤二、取薄荷新鲜的薄荷叶，将薄荷叶粉碎后用乙醇溶液室温浸泡15h，过滤取滤液，然后再重复一次，合并两次滤液得到混合滤液，将该混合滤液与同体积的水混合后，减压浓缩去除乙醇，得到所需清新剂；
步骤三、取异噻唑啉酮和对羟基苯甲酸乙酯作为细菌抑制剂，将所述除味活性剂、细菌抑制剂溶于有机溶剂中，再加入清新剂、芳香剂和稳定剂，搅拌均匀，精滤后压缩至罐中，即得羽绒服除味清新喷雾。
对比例1
一种羽绒服除味清新喷雾，其原料和制备方法与实施例2基本相同，唯一区别在于：除味活性剂为8份香豆素。
对比例2
一种羽绒服除味清新喷雾，其原料和制备方法与实施例2基本相同，唯一区别在于：除味活性剂为8份木酚素。
对比例3
一种羽绒服除味清新喷雾，其原料和制备方法与实施例2基本相同，唯一区别在于：去除除味活性剂，替换为8份细菌抑制剂。
对上述实施例2以及对比例1-3制得的羽绒服除味清新喷雾进行除味效果以及抗菌性能测试，具体测试方式为：取同一批次的鹅绒以及同一批次的鸭绒制成羽绒服，参照《GB/T14272-2011羽绒服装标准》检测其沙门氏菌含量、粪链球菌含量，再取各羽绒服除味清新喷雾，对鹅绒以及鸭绒羽绒服分别进行喷雾除味处理，喷雾采用完全覆盖、均匀喷雾的方式，且用量控制在1mL/m2，处理完成后将羽绒服放置在无菌环境中静置8h，再以同样的方式再次检测羽绒服的沙门氏菌含量、粪链球菌含量，并计算除菌率，同时由专业感官检测人员检测其腥味程度和清新芳香程度，分为1-5五个等级，等级越高说明腥味越重、清新芳香味越重。所有结果统计得到下表：
从上表可以看出，本发明实施例2制得的除味清新喷雾的除味效果突出，针对鹅绒和鸭绒羽绒服均只有1级，且清新芳香程度达到了4级以上，同时除菌效果突出，达到了99.88％以上；而对比例1因除味活性剂仅采用了香豆素，对比例2仅采用了木酚素，均导致除味效果明显下降，且除菌率也有所下降，由此说明香豆素和木酚素需要同时使用，才能发挥良好的除菌、除味作用；而对比例3因去除了除味活性剂，腥味严重，同时该实施例中相应增加了等量的细菌抑制剂，细菌抑制剂具有杀菌、杀病毒作用，然而结果表明其除菌率并没有提升，反而略微下降，这说明本发明除味活性剂能配合细菌抑制剂，起到更好的抗菌作用。
以上所述实施例仅表达了本发明的几种实施方式，其描述较为具体和详细，但并不能因此而理解为对本发明专利范围的限制。应当指出的是，对于本领域的普通技术人员来说，在不脱离本发明构思的前提下，还可以做出若干变形和改进，这些都属于本发明的保护范围。
Claims (1)
1.一种羽绒服除味清新喷雾，其特征在于，所述喷雾的制备原料按重量份数包括：8份除味活性剂、3份细菌抑制剂、30份有机溶剂、3份清新剂、0.3份芳香剂和0.4份稳定剂，其中，所述除味活性剂由香豆素和木酚素按5:1.5的质量比混合而成，所述细菌抑制剂为对羟基苯甲酸乙酯，所述清新剂为野菊花提取物；所述机溶剂为乙酸乙酯；所述芳香剂为经过高磁化处理的百合精油，磁场强度为14000GS，处理时间为50min；所述稳定剂为二苯酮-4；
上述羽绒服除味清新喷雾的制备方法，步骤包括：
步骤一、取香豆素和木酚素按比例混合后加入到有机溶剂中，在温度为45℃、以400r/min的转速搅拌提取6h，过滤得除味活性剂备用；
步骤二、取野菊花新鲜的花瓣，将花瓣粉碎后用乙醇溶液室温浸泡12h，过滤取滤液，然后再重复一次，合并两次滤液得到混合滤液，将该混合滤液与同体积的水混合后，减压浓缩去除乙醇，得到所需清新剂；
步骤三、取对羟基苯甲酸乙酯作为细菌抑制剂，将所述除味活性剂、细菌抑制剂溶于有机溶剂中，再加入清新剂、芳香剂和稳定剂，搅拌均匀，精滤后压缩至罐中，即得羽绒服除味清新喷雾。
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH05317396A (ja) * | 1992-05-25 | 1993-12-03 | Toppan Printing Co Ltd | 消臭剤 |
| CN102051276A (zh) * | 2011-01-24 | 2011-05-11 | 北京洛娃日化有限公司 | 羽绒服清洗剂 |
| CN110327763A (zh) * | 2019-07-16 | 2019-10-15 | 上海逸族环保科技有限公司 | 环保型室内空气净化剂 |
| CN111471534A (zh) * | 2020-04-30 | 2020-07-31 | 中山榄菊日化实业有限公司 | 一种快干不留痕高效羽绒服喷雾清洁剂及其制备方法 |
| CN113062119A (zh) * | 2021-03-29 | 2021-07-02 | 安徽高梵电子商务有限公司 | 一种具有芳香气味的羽绒服加工生产方法 |
| WO2021160049A1 (zh) * | 2020-02-12 | 2021-08-19 | 深圳优丽康生物技术有限公司 | 抑菌组合物及其制备方法和用途 |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8563754B2 (en) * | 2010-01-28 | 2013-10-22 | New York University | Compounds, compositions and methods for preventing skin darkening |
| CN111789133A (zh) * | 2019-04-05 | 2020-10-20 | 张海苓 | 一种新型除霉剂 |
-
2021
- 2021-09-06 CN CN202111037222.7A patent/CN113605090B/zh active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH05317396A (ja) * | 1992-05-25 | 1993-12-03 | Toppan Printing Co Ltd | 消臭剤 |
| CN102051276A (zh) * | 2011-01-24 | 2011-05-11 | 北京洛娃日化有限公司 | 羽绒服清洗剂 |
| CN110327763A (zh) * | 2019-07-16 | 2019-10-15 | 上海逸族环保科技有限公司 | 环保型室内空气净化剂 |
| WO2021160049A1 (zh) * | 2020-02-12 | 2021-08-19 | 深圳优丽康生物技术有限公司 | 抑菌组合物及其制备方法和用途 |
| CN111471534A (zh) * | 2020-04-30 | 2020-07-31 | 中山榄菊日化实业有限公司 | 一种快干不留痕高效羽绒服喷雾清洁剂及其制备方法 |
| CN113062119A (zh) * | 2021-03-29 | 2021-07-02 | 安徽高梵电子商务有限公司 | 一种具有芳香气味的羽绒服加工生产方法 |
Non-Patent Citations (2)
| Title |
|---|
| 植物提取物抑菌活性及作用机理;刘旺景等;《动物营养学报》;20160831;第28卷(第8期);第2344-2452页 * |
| 植物源抑菌活性成分研究新进展;吴传万等;《西北农业学报》;20040910(第03期);第81-88页 * |
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