CN113604282A - Preparation method and application product of essence base of top note and lasting note of daily chemical essence - Google Patents
Preparation method and application product of essence base of top note and lasting note of daily chemical essence Download PDFInfo
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- CN113604282A CN113604282A CN202110940933.9A CN202110940933A CN113604282A CN 113604282 A CN113604282 A CN 113604282A CN 202110940933 A CN202110940933 A CN 202110940933A CN 113604282 A CN113604282 A CN 113604282A
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- essence
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- helional
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
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- Life Sciences & Earth Sciences (AREA)
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- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention discloses a preparation method of a base of top note and left note of daily chemical essence, which comprises the following steps: white rosin molecules and ethyl ether are mixed according to the mass ratio of 1: 1, mixing; mixing with kestone and ambrotone, and adding lilial and methyl anthranilate to react naturally for 24 hr to produce lilacin; the method comprises the following steps of (1) naturally reacting the naringenin, the helional and methyl o-aminotoluate, and reacting for 15 days at a constant temperature of 48 ℃ to obtain helional spilanthol and water; and drying the mixture in an oven at the temperature of between 48 and 55 ℃ for 8 hours, and drying the water to obtain the completely dried helional spipe. The invention relates to a preparation method of a base of top and left fragrances of a daily chemical essence and an application product thereof, which have the advantages of strengthening performance, and endowing the essence with the extraordinary performance of amber, natural fragrance, musk and ambergris, and are almost suitable for all essences.
Description
Technical Field
The invention relates to the technical field of essence, in particular to a preparation method of a fragrance base of top note and top note of daily chemical essence and an application product thereof.
Background
At present, the spice is widely applied to various daily necessities, food and other industries of people life, but the spice has the defects of easy volatilization, difficult storage, unstable property and the like. In recent years, the textile industry is gradually developing multifunctional cloth such as fragrant cloth, but the fragrant cloth prepared by using the traditional method such as the method of directly adding essence for daily use on the cloth has the advantages of fast fragrance emission and short fragrance retention time, and the fragrant material prepared by the traditional method can not meet the requirements of people on high standards.
Disclosure of Invention
Aiming at the defects of the existing essence, the invention provides a preparation method of a base of a first fragrance and a second fragrance of a daily chemical essence and an application product thereof, wherein the base has enhanced performance, and the fragrance of the first fragrance and the second fragrance is amber, natural fragrance, musk and ambergris, which endows the essence with extraordinary performance, and is almost suitable for all essences.
The invention provides a preparation method of a base of top note and left note of daily chemical essence, which comprises the following steps:
white rosin molecules and ethyl ether are mixed according to the mass ratio of 1: 1, mixing;
mixing with kestone and ambrotone, and adding lilial and methyl anthranilate to react naturally for 24 hr to produce lilacin;
the method comprises the following steps of (1) naturally reacting the naringenin, the helional and methyl o-aminotoluate, and reacting for 15 days at a constant temperature of 48 ℃ to obtain helional spilanthol and water;
and drying the mixture in an oven at the temperature of between 48 and 55 ℃ for 8 hours, and drying the water to obtain the completely dried helional spipe.
The method further comprises the following steps:
adding duplicative pelargonide into the dried helional spilanthol base, wherein the pelargonide accounts for 0.5-1.5% of the total mass ratio.
Correspondingly, the invention also provides daily chemical essence perfume, and the obtained perfume base is mixed in the daily chemical essence perfume.
Correspondingly, the invention also provides a washing and caring liquid, which is prepared by mixing the obtained essence base in the washing and caring liquid.
Correspondingly, the invention also provides a fabric care solution, and the obtained perfume base is mixed in the fabric care solution.
Correspondingly, the invention also provides the household care solution, and the obtained incense base is mixed in the household care solution.
Correspondingly, the invention also provides a candle, and the obtained incense base is mixed in the candle.
The essence base can generate ultra-strong, strong and fragrant amber fragrance, and based on mutual reaction of the components in the embodiment of the invention, a brand-new staged characteristic capable of improving the essence order can be prepared, the essence is suitable for all types of daily chemical essences, the key index requirements of the essence, such as top aroma, body aroma, fragrance retention and the like, which are important in the prior art can be met, meanwhile, the essence can be proportionally added into the essence and products according to the cost requirements of customers, and the performance of all the daily chemical essences can be enhanced.
Drawings
In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings used in the description of the embodiments or the prior art will be briefly described below, it is obvious that the drawings in the following description are only some embodiments of the present invention, and for those skilled in the art, other drawings can be obtained according to the drawings without creative efforts.
Fig. 1 is a flow chart of a method for preparing a base of top note and top note of a daily chemical essence in the embodiment of the invention.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Fig. 1 shows a flow chart of a method for preparing a fragrance base of top notes and top notes of a daily chemical essence in an embodiment of the invention, wherein the method comprises the following steps:
s11, mixing white rosin molecules and diethyl ether according to the mass ratio of 1: 1, mixing;
white rosin essential oil is useful for inflammation, swelling, wounds and abscesses, especially those skin conditions that are otherwise unresponsive to other drugs, and has long been used to treat persistent infections of the lungs, particularly to remove mucus and relieve coughing in humans.
The ether is an organic substance, has a structural formula of C2H5OC2H5, is colorless transparent liquid in appearance, has special pungent smell, has sweet taste, is very volatile, and has vapor heavier than air. Oxidized to peroxides, aldehydes and acetic acid under the action of air, and the oxidation of which is promoted by exposure to light, are used here as solvents for the white rosin molecules.
Here, a strong amber fragrance can be generated by mixing the white pine essential oil and the diethyl ether.
S12, mixing with kestone and ambrotone, and adding convallaria aldehyde and methyl anthranilate to naturally react for 24 hours to generate convallaria;
it should be noted that, here, the reference reactant of kestone is proportioned and mixed with 3% to 5% of the total mass ratio, the reference reactant of ambrotone is proportioned and mixed with 5% to 10% of the total mass ratio, the reference reactant of Convallaria aldehyde is proportioned and mixed with 2% to 4% of the total mass ratio, and the reference reactant of methyl anthranilate is proportioned and mixed with 10% to 20% of the total mass ratio.
Kestominone is an organic substance with chemical formula of C14H22O, is a light yellow liquid, has strong, lasting and sweet fragrance of Moschus and radix aucklandiae, and has strong fragrance.
The ambrotone can be used in the essence of cologne, perfumed soap and detergent, and its dosage can be up to 30%. Plays a role in fixing fragrance in the essence and can provide vivid and continuous harmonious fragrance.
Lilial, colorless transparent liquid, soluble in ethanol and oil, and insoluble in water. The product has sweet fragrance of Bulbus Lilii, and has low irritation to skin and alkali stability. Is widely used for lily, clove, magnolia, camellia, vegetarian orchid and oriental type fragrant essence for daily use. It is commonly used as perfume for soap and detergent, and also used as perfume for floral type cosmetics.
Methyl anthranilate is an organic compound having the formula C8H9NO2, a colorless crystalline or pale yellow liquid, with a grape-like odor. The color change can be achieved after long-term exposure, and the color change can be volatilized along with water vapor. It is easily soluble in ethanol and diethyl ether, the ethanol solution has blue fluorescence, is soluble in most of the fixed oil and propylene glycol, is slightly soluble in mineral oil, is slightly soluble in water, and is insoluble in glycerol. Used for synthesizing perfume, medicine, etc.
S13, enabling the naringenin, the helional and methyl o-aminotoluate to naturally react, and reacting for 15 days at the constant temperature of 48 ℃ to obtain helional spicebush and water;
helional, a chemical molecular name, foreign name Helonal, molecular formula C11H12O 3.
S14, drying the mixture in an oven at the temperature of 48-55 ℃ for 8 hours, and drying the water to obtain the dried helional spicebush;
s15, adding duplicative pelargonide in the dried heliotropin clomazone, wherein the pelargonide accounts for 0.5-1.5% of the total mass ratio.
Correspondingly, the invention also provides daily chemical essence perfume, and the obtained perfume base is mixed in the daily chemical essence perfume.
Correspondingly, the invention also provides a washing and caring liquid, which is prepared by mixing the obtained essence base in the washing and caring liquid.
Correspondingly, the invention also provides a fabric care solution, and the obtained perfume base is mixed in the fabric care solution.
Correspondingly, the invention also provides the household care solution, and the obtained incense base is mixed in the household care solution.
Correspondingly, the invention also provides a candle, and the obtained incense base is mixed in the candle.
Description of the aromas involved in the examples of the invention: amber, Benxiang, musk and ambergris, which endow the perfume with extraordinary performance, and are almost suitable for all essences.
The application thereof comprises the following steps: essence and perfume for daily use, fabric care, washing and protecting liquid, household care and candle
The fragrance base appearance description: colorless to pale yellow liquid
Standard practice is to use 5% (essence) flash point with fragrance retention at 128 ℃ for more than 2 weeks.
The essence base in the embodiment of the invention can generate ultra-strong, strong and fragrant amber fragrance, and based on mutual reaction of the components in the embodiment of the invention, a brand-new staged characteristic capable of improving the essence order can be prepared, the essence is suitable for all types of daily chemical essences, the key index requirements of the essence, such as top aroma, body aroma, fragrance retention and the like, which are important in the prior art can be met, meanwhile, the essence can be added into the used essence and products according to the cost requirement of customers in proportion, and the performance of the essence can be enhanced for all the daily chemical essences.
The foregoing detailed description is provided for the embodiments of the present invention, and the principles and embodiments of the present invention are described herein using specific examples, which are provided only for the purpose of assisting understanding of the method and the core concepts thereof; meanwhile, for a person skilled in the art, according to the idea of the present invention, there may be variations in the specific embodiments and the application scope, and in summary, the content of the present specification should not be construed as a limitation to the present invention.
Claims (7)
1. A preparation method of a base of top note and left note of daily chemical essence is characterized by comprising the following steps:
white rosin molecules and ethyl ether are mixed according to the mass ratio of 1: 1, mixing;
mixing with kestone and ambrotone, and adding lilial and methyl anthranilate to react naturally for 24 hr to produce lilacin;
the method comprises the following steps of (1) naturally reacting the naringenin, the helional and methyl o-aminotoluate, and reacting for 15 days at a constant temperature of 48 ℃ to obtain helional spilanthol and water;
and drying the mixture in an oven at the temperature of between 48 and 55 ℃ for 8 hours, and drying the water to obtain the completely dried helional spipe.
2. The method for preparing the essence base of the first and the last essence of daily chemical essence according to claim 1, which further comprises the following steps:
adding duplicative pelargonide into the dried helional spilanthol base, wherein the pelargonide accounts for 0.5-1.5% of the total mass ratio.
3. A daily use chemical perfume wherein the base obtained according to claim 1 or 2 is mixed in a daily use chemical perfume.
4. A lotion characterized by the fact that the perfume base obtained according to claim 1 or 2 is mixed in a lotion.
5. A fabric care solution characterized by being mixed in a fabric care solution with the fragrance base obtained according to claim 1 or 2.
6. A home care liquid characterized in that the fragrance base obtained in claim 1 or 2 is mixed in the home care liquid.
7. A candle, characterized in that the fragrance base obtained according to claim 1 or 2 is mixed in a candle.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110940933.9A CN113604282A (en) | 2021-08-17 | 2021-08-17 | Preparation method and application product of essence base of top note and lasting note of daily chemical essence |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110940933.9A CN113604282A (en) | 2021-08-17 | 2021-08-17 | Preparation method and application product of essence base of top note and lasting note of daily chemical essence |
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| Publication Number | Publication Date |
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| CN113604282A true CN113604282A (en) | 2021-11-05 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN202110940933.9A Pending CN113604282A (en) | 2021-08-17 | 2021-08-17 | Preparation method and application product of essence base of top note and lasting note of daily chemical essence |
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2158896A2 (en) * | 2009-11-02 | 2010-03-03 | Symrise GmbH & Co. KG | Materials containing aromas incorporating neopentyl glycol isononanoate |
| CN106221911A (en) * | 2016-08-03 | 2016-12-14 | 广州爱普香精香料有限公司 | A kind of perfume compositions and application thereof |
-
2021
- 2021-08-17 CN CN202110940933.9A patent/CN113604282A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2158896A2 (en) * | 2009-11-02 | 2010-03-03 | Symrise GmbH & Co. KG | Materials containing aromas incorporating neopentyl glycol isononanoate |
| CN106221911A (en) * | 2016-08-03 | 2016-12-14 | 广州爱普香精香料有限公司 | A kind of perfume compositions and application thereof |
Non-Patent Citations (2)
| Title |
|---|
| M.V.COOK ET AL: "调香扎记(一)", 上海日用化工, pages 66 - 67 * |
| 林翔云: "定香机理及定香基的配制", 香料香精化妆品, pages 47 - 50 * |
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