CN113603454B - High-light-transmittance silicon-rich white porcelain tea set and manufacturing process thereof - Google Patents
High-light-transmittance silicon-rich white porcelain tea set and manufacturing process thereof Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/04—Clay; Kaolin
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
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- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
- C04B33/1305—Organic additives
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- C—CHEMISTRY; METALLURGY
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- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/24—Manufacture of porcelain or white ware
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/96—Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/96—Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance
- C04B2235/9646—Optical properties
- C04B2235/9653—Translucent or transparent ceramics other than alumina
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/60—Production of ceramic materials or ceramic elements, e.g. substitution of clay or shale by alternative raw materials, e.g. ashes
Abstract
The invention discloses a high-light-transmission silicon-rich white porcelain tea set and a manufacturing process thereof, belonging to the technical field of white porcelain; the Bai Ci element embryo comprises the following components in parts by weight: 20-35 parts of kaolin, 10-25 parts of synthetic fluorophlogopite powder, 10-20 parts of cordierite, 5-15 parts of talcum, 3-10 parts of zirconia, 3-10 parts of synthetic diopside, 1-8 parts of titanium oxide and 1-8 parts of molybdenum oxide; the high-light-transmittance silicon-rich white porcelain glaze comprises the following components: 10-20 parts of organosilicon polymer, 10-20 parts of albite, 8-12 parts of silicon oxide, 8-12 parts of aluminum oxide, 4-7 parts of cosolvent and 1-5 parts of synthetic diopside; wherein the cosolvent is a mixture of potassium oxide, sodium oxide and barium oxide in a weight ratio of 3:2:3; the embryo prepared by the invention has extremely high transparency and transmittance in the embryo; meanwhile, the heat-resistant rubber has the advantages of good heat stability and excellent impact strength; after the organosilicon polymer is added into the glaze water and is formed by subsequent firing, the crosslinking degree is high, the hardness is high, and the wear resistance is good.
Description
Technical Field
The invention belongs to the technical field of white porcelain, and particularly relates to a high-light-transmission silicon-rich white porcelain tea set and a manufacturing process thereof.
Background
Chinese white porcelain is also called Chinese white. The white porcelain has long history, and the chen kiln is the earliest white porcelain kiln site in China. One of the seven kilns of Tang dynasty has the chen kiln of the nose ancestor of China. The chen kiln burns in the late north and fades into the Tang dynasty stage after the rapid development of the inert dynasty, and becomes the center for early production of white porcelain in China in the final five-generation stage of Tang dynasty. Over 1500 years of history exist, the exquisite fine white porcelain is used as tribute to the palace, and tens of countries and regions are also sold overseas and overseas. White porcelain is usually made by firing porcelain blanks after pure transparent glaze is applied, but the existing white porcelain paint has lower light transmittance and insufficient strength.
Disclosure of Invention
First, the technical problem to be solved
The preparation method is provided for improving the light transmittance and strength of the white porcelain.
(II) technical scheme
The invention is realized by the following technical scheme: a high-light-transmission silicon-rich white porcelain tea set comprises a white porcelain biscuit and a high-light-transmission silicon-rich white porcelain glaze;
the Bai Ci element embryo comprises the following components in parts by weight: 20-35 parts of kaolin, 10-25 parts of synthetic fluorophlogopite powder, 10-20 parts of cordierite, 5-15 parts of talcum, 3-10 parts of zirconia, 3-10 parts of synthetic diopside, 1-8 parts of titanium oxide and 1-8 parts of molybdenum oxide;
the high-light-transmittance silicon-rich white porcelain glaze comprises the following components: 10-20 parts of organosilicon polymer, 10-20 parts of albite, 8-12 parts of silicon oxide, 8-12 parts of aluminum oxide, 4-7 parts of cosolvent and 1-5 parts of synthetic diopside; wherein the cosolvent is a mixture of potassium oxide, sodium oxide and barium oxide in a weight ratio of 3:2:3.
As a further explanation of the above scheme, the Bai Ci green body comprises the following components by weight: 30 parts of kaolin, 17 parts of synthetic fluorophlogopite powder, 14 parts of cordierite, 13 parts of talcum, 7 parts of zirconia, 8 parts of synthetic diopside, 3 parts of titanium oxide and 3 parts of molybdenum oxide
The high-light-transmittance silicon-rich white porcelain glaze comprises the following components: 15 parts of organosilicon polymer, 12 parts of albite, 9 parts of silicon oxide, 11 parts of aluminum oxide, 6 parts of cosolvent and 4 parts of synthetic diopside; wherein the cosolvent is a mixture of potassium oxide, sodium oxide and barium oxide in a weight ratio of 3:2:3.
As a further explanation of the scheme, the high-light-transmittance silicon-rich white enamel further comprises 1-3 parts of suspending agent.
As a further explanation of the scheme, the high-light-transmittance silicon-rich white enamel further comprises 1-3 parts of calcium oxide.
As a further explanation of the scheme, the high-light-transmittance silicon-rich white enamel further comprises 1-3 parts of magnesium oxide.
The invention also provides a manufacturing process of the high-light-transmission silicon-rich white porcelain tea set,
step 100: weighing raw materials according to the components to prepare a white porcelain biscuit;
step 200: preparing a liquid organosilicon polymer;
step 300: raw materials are weighed according to the components to prepare the high-light-transmittance silicon-rich white porcelain glaze;
step 400: the surface Shi Gao of the white porcelain biscuit is made of light-transmitting silicon-rich white porcelain glaze and is sintered and formed.
As a further explanation of the above scheme, in step 100, the raw materials are specifically mixed, added with water, ball-milled, pressed, pugging, slip casting, embryo forming, embryo washing and air drying to obtain the white porcelain biscuit.
As a further explanation of the above scheme, in step 200, the vinyl silicone resin, the hydrogen-containing silicone oil and the tetramethyl tetra-vinyl cyclotetrasiloxane are added into a container and mechanically stirred, a platinum catalyst is added during stirring, and the colorless and transparent liquid organosilicon polymer is obtained after uniform mixing.
As a further explanation of the above scheme, in step 300, the components of the other high-transmittance silicon-rich white enamel raw materials except the liquid organosilicon polymer are weighed, mixed with water according to the weight ratio of 1:0.7-1.3, and ball-milled after mixing; and weighing liquid organosilicon polymer according to the components, and mixing with the ball-milled raw materials to obtain the high-light-transmittance silicon-rich white enamel.
As a further explanation of the above scheme, in step 400, the high-transmittance silicon-rich white enamel prepared in step 300 is specifically glazed by spraying; after glazing, placing the ceramic material into a kiln, controlling the temperature of a furnace chamber to rise to 1000-1250 ℃ at a speed of 12-20 ℃/min through a high-temperature furnace temperature control system, and then preserving heat for 8-12 hours; and (5) after heat preservation, cooling to room temperature along with furnace temperature.
(III) beneficial effects
Compared with the prior art, the invention has the following beneficial effects: the embryo prepared by the invention has extremely high transparency and light transmittance in the embryo; meanwhile, the heat-resistant rubber has the advantages of good heat stability and excellent impact strength; after the organosilicon polymer is added into the glaze water and is formed by subsequent firing, the crosslinking degree is high, the hardness is high, and the wear resistance is good.
Detailed Description
A high-light-transmission silicon-rich white porcelain tea set comprises a white porcelain biscuit and a high-light-transmission silicon-rich white porcelain glaze;
the Bai Ci element embryo comprises the following components in parts by weight: 20-35 parts of kaolin, 10-25 parts of synthetic fluorophlogopite powder, 10-20 parts of cordierite, 5-15 parts of talcum, 3-10 parts of zirconia, 3-10 parts of synthetic diopside, 1-8 parts of titanium oxide and 1-8 parts of molybdenum oxide;
the high-light-transmittance silicon-rich white porcelain glaze comprises the following components: 10-20 parts of organosilicon polymer, 10-20 parts of albite, 8-12 parts of silicon oxide, 8-12 parts of aluminum oxide, 4-7 parts of cosolvent and 1-5 parts of synthetic diopside; wherein the cosolvent is a mixture of potassium oxide, sodium oxide and barium oxide in a weight ratio of 3:2:3.
Wherein the Bai Ci element embryo comprises the following components in parts by weight: 30 parts of kaolin, 17 parts of synthetic fluorophlogopite powder, 14 parts of cordierite, 13 parts of talcum, 7 parts of zirconia, 8 parts of synthetic diopside, 3 parts of titanium oxide and 3 parts of molybdenum oxide
The high-light-transmittance silicon-rich white porcelain glaze comprises the following components: 15 parts of organosilicon polymer, 12 parts of albite, 9 parts of silicon oxide, 11 parts of aluminum oxide, 6 parts of cosolvent and 4 parts of synthetic diopside; wherein the cosolvent is a mixture of potassium oxide, sodium oxide and barium oxide in a weight ratio of 3:2:3.
Wherein the high-light-transmittance silicon-rich white porcelain glaze also comprises 1-3 parts of suspending agent.
Wherein the high-light-transmittance silicon-rich white porcelain glaze also comprises 1-3 parts of calcium oxide.
Wherein the high-light-transmittance silicon-rich white porcelain glaze also comprises 1-3 parts of magnesium oxide.
The invention also provides a manufacturing process of the high-light-transmission silicon-rich white porcelain tea set,
step 100: weighing raw materials according to the components to prepare a white porcelain biscuit;
step 200: preparing a liquid organosilicon polymer;
step 300: raw materials are weighed according to the components to prepare the high-light-transmittance silicon-rich white porcelain glaze;
step 400: the surface Shi Gao of the white porcelain biscuit is made of light-transmitting silicon-rich white porcelain glaze and is sintered and formed.
The method comprises the following steps of step 100, specifically, mixing the raw materials, adding water, performing ball milling, squeezing, pugging, slip casting, embryo forming, embryo washing and air drying to obtain the white porcelain biscuit.
And step 200, specifically adding vinyl silicone resin, hydrogen-containing silicone oil and tetramethyl tetravinyl cyclotetrasiloxane into a container, mechanically stirring, adding a platinum catalyst in the stirring process, and uniformly mixing to obtain a colorless and transparent liquid organosilicon polymer.
The method comprises the following steps of (300) weighing other high-light-transmittance silicon-rich white enamel raw materials except for liquid organosilicon polymer according to the components, mixing the raw materials with water according to the weight ratio of 1:0.7-1.3, and ball milling after mixing; and weighing liquid organosilicon polymer according to the components, and mixing with the ball-milled raw materials to obtain the high-light-transmittance silicon-rich white enamel.
The step 400 is to apply the high-transmittance silicon-rich white enamel prepared in the step 300 by a spraying method; after glazing, placing the ceramic material into a kiln, controlling the temperature of a furnace chamber to rise to 1000-1250 ℃ at a speed of 12-20 ℃/min through a high-temperature furnace temperature control system, and then preserving heat for 8-12 hours; and (5) after heat preservation, cooling to room temperature along with furnace temperature.
Examples
Firstly, preparing a white porcelain biscuit; weighing 30 parts of kaolin, 17 parts of synthetic fluorophlogopite powder, 14 parts of cordierite, 13 parts of talcum, 7 parts of zirconia, 8 parts of synthetic diopside, 3 parts of titanium oxide and 3 parts of molybdenum oxide according to the components; the whiteness of the blank can be improved by adding the synthetic fluorophlogopite powder into the components of the blank; the embryo prepared by synthesizing diopside has extremely high transparency and light transmittance; the cordierite is prepared into a green body and has the characteristics of good thermal stability and excellent impact strength; the addition of the three oxides of zirconium oxide, titanium oxide and molybdenum oxide can improve the strength of the blank and the performance of the blank, and the blank prepared by the components has the characteristics of high permeability and high strength. The method comprises the steps of specifically grinding all components by using a ball mill, putting the ground components into a slurry tank for stirring, vibrating and sieving to remove impurities after stirring, preparing slurry into a mud cake by using a squeezer, exhausting air by using a pugging machine, and preparing the mud cake into tea embryo by using a roller press molding process or a slip casting process; after the tea set embryo is formed, washing the embryo and brushing the embryo, and keeping the embryo for standby;
secondly, preparing a liquid organosilicon polymer, and preparing high-light-transmittance silicon-rich white porcelain glaze by weighing raw materials according to the components; specifically, the raw materials with the following components by weight are weighed to prepare the underglaze: 15 parts of organosilicon polymer, 12 parts of albite, 9 parts of silicon oxide, 11 parts of aluminum oxide, 6 parts of cosolvent and 4 parts of synthetic diopside; 1-3 parts of suspending agent, 1-3 parts of calcium oxide and 1-3 parts of magnesium oxide. Wherein the cosolvent is a mixture of potassium oxide, sodium oxide and barium oxide in a weight ratio of 3:2:3. Weighing other high-light-transmittance silicon-rich white enamel raw materials except for liquid organosilicon polymers according to the components, mixing the raw materials, mixing with water according to the weight ratio of 1:0.7-1.3, and ball milling after mixing; weighing liquid organosilicon polymer according to the components, and mixing with the ball-milled raw materials to obtain the high-light-transmittance silicon-rich white enamel; wherein the ball milling medium adopts alumina balls, the weight ratio of the balls to water is 1:2:0.7, and the ball milling time is 12 hours;
to further improve the performance and strength of the glaze; according to the invention, the organosilicon polymer is added into glaze water, specifically, vinyl silicone resin, hydrogen-containing silicone oil and tetramethyl tetra-vinyl cyclotetrasiloxane are added into a container for mechanical stirring, a platinum catalyst is added during stirring, and the colorless and transparent liquid organosilicon polymer is obtained after uniform mixing. The organosilicon polymer has high crosslinking degree, high hardness and good wear resistance after being formed by subsequent firing, and the appearance is like glass, so that the addition of the organosilicon polymer does not influence the property of the glaze, but improves the transparency and the mechanical property of the glaze.
And finally, the surface Shi Gao of the white porcelain biscuit is light-transmitting silicon-rich white porcelain glaze and is sintered and molded. Regulating the water content of the glaze to 60%; after the glaze water is blended, a glaze swinging method is adopted to apply a bottom layer, and after the preparation of the bottom layer is finished, a dryer is used to control the water content of the bottom layer to 8%; the high-light-transmittance silicon-rich white porcelain glaze is glazed by adopting a spraying method; after glazing, placing the ceramic material into a kiln, controlling the temperature of a furnace chamber to rise to 1000-1250 ℃ at a speed of 12-20 ℃/min through a high-temperature furnace temperature control system, and then preserving heat for 8-12 hours; and (5) after heat preservation, cooling to room temperature along with furnace temperature.
While the fundamental and principal features of the invention and advantages of the invention have been shown and described, it will be apparent to those skilled in the art that the invention is not limited to the details of the foregoing exemplary embodiments, but may be embodied in other specific forms without departing from the spirit or essential characteristics thereof. The present embodiments are, therefore, to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein.
Furthermore, it should be understood that although the present disclosure describes embodiments, not every embodiment is provided with a separate embodiment, and that this description is provided for clarity only, and that the embodiments of the disclosure may be suitably combined to form other embodiments as will be understood by those skilled in the art.
Claims (6)
1. A high-light-transmission silicon-rich white porcelain tea set comprises a white porcelain biscuit and a high-light-transmission silicon-rich white porcelain glaze; the method is characterized in that:
the Bai Ci element embryo comprises the following components in parts by weight: 20-35 parts of kaolin, 10-25 parts of synthetic fluorophlogopite powder, 10-20 parts of cordierite, 5-15 parts of talcum, 3-10 parts of zirconia, 3-10 parts of synthetic diopside, 1-8 parts of titanium oxide and 1-8 parts of molybdenum oxide;
the high-light-transmittance silicon-rich white porcelain glaze comprises the following components: 10-20 parts of organosilicon polymer, 10-20 parts of albite, 8-12 parts of silicon oxide, 8-12 parts of aluminum oxide, 4-7 parts of cosolvent and 1-5 parts of synthetic diopside; wherein the cosolvent is a mixture of potassium oxide, sodium oxide and barium oxide in a weight ratio of 3:2:3;
the organic silicon polymer is prepared by adding vinyl silicone resin, hydrogen-containing silicone oil and tetramethyl tetra-vinyl cyclotetrasiloxane into a container, mechanically stirring, adding a platinum catalyst in the stirring process, and uniformly mixing to obtain a colorless and transparent liquid organic silicon polymer.
2. The high-transmittance silicon-rich white porcelain tea set according to claim 1, wherein:
the Bai Ci element embryo comprises the following components in parts by weight: 30 parts of kaolin, 17 parts of synthetic fluorophlogopite powder, 14 parts of cordierite, 13 parts of talcum, 7 parts of zirconia, 8 parts of synthetic diopside, 3 parts of titanium oxide and 3 parts of molybdenum oxide
The high-light-transmittance silicon-rich white porcelain glaze comprises the following components: 15 parts of organosilicon polymer, 12 parts of albite, 9 parts of silicon oxide, 11 parts of aluminum oxide, 6 parts of cosolvent and 4 parts of synthetic diopside; wherein the cosolvent is a mixture of potassium oxide, sodium oxide and barium oxide in a weight ratio of 3:2:3.
3. The high-transmittance silicon-rich white porcelain tea set according to claim 1, wherein: the high-light-transmittance silicon-rich white porcelain glaze also comprises 1-3 parts of suspending agent.
4. The high-transmittance silicon-rich white porcelain tea set according to claim 1, wherein: the high-light-transmittance silicon-rich white porcelain glaze also comprises 1-3 parts of calcium oxide.
5. The high-transmittance silicon-rich white porcelain tea set according to claim 1, wherein: the high-light-transmittance silicon-rich white porcelain glaze also comprises 1-3 parts of magnesium oxide.
6. A high light transmission silicon-rich white porcelain tea set according to any one of claims 1 to 5, characterised in that: the manufacturing process of the high-light-transmittance silicon-rich white porcelain tea set also comprises the following steps of;
step 100: weighing raw materials according to the components to prepare a white porcelain biscuit;
step 200: preparing a liquid organosilicon polymer;
step 300: raw materials are weighed according to the components to prepare the high-light-transmittance silicon-rich white porcelain glaze;
step 400: the surface Shi Gao of the white porcelain biscuit is light-transmitting silicon-rich white porcelain glaze and is sintered and molded;
step 100 is to mix the raw materials, add water to ball mill, squeeze, pugging, slip casting, embryo forming, embryo washing and air drying to obtain white porcelain biscuit;
step 200 is to add vinyl silicone resin, hydrogen-containing silicone oil and tetramethyl tetravinyl cyclotetrasiloxane into a container, mechanically stir, add platinum catalyst in the stirring process, and uniformly mix to obtain colorless transparent liquid organosilicon polymer;
step 300 is to weigh other high-light-transmittance silicon-rich white enamel raw materials except liquid organosilicon polymer according to the components, mix the raw materials with water according to the weight ratio of 1:0.7-1.3, and ball mill after mixing; weighing liquid organosilicon polymer according to the components, and mixing with the ball-milled raw materials to obtain the high-light-transmittance silicon-rich white enamel;
the step 400 is to apply the high-light-transmittance silicon-rich white porcelain glaze prepared in the step 300 by adopting a spraying method; after glazing, placing the ceramic material into a kiln, controlling the temperature of a furnace chamber to rise to 1000-1250 ℃ at a speed of 12-20 ℃/min through a high-temperature furnace temperature control system, and then preserving heat for 8-12 hours; and (5) after heat preservation, cooling to room temperature along with furnace temperature.
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| CN108033768A (en) * | 2017-12-08 | 2018-05-15 | 泉州市德化县恒峰陶瓷有限公司 | Ceramic whiteware pot and preparation method thereof with high temperature resistant, explosion-proof glaze paint |
| CN111574211A (en) * | 2020-05-19 | 2020-08-25 | 福建省德化县中国白陶瓷有限责任公司 | White ceramic product for open fire and preparation method thereof |
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