CN113564753A - Fiber dispersing and collecting device and method based on airflow impact and static electricity - Google Patents

Fiber dispersing and collecting device and method based on airflow impact and static electricity Download PDF

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Publication number
CN113564753A
CN113564753A CN202110755726.6A CN202110755726A CN113564753A CN 113564753 A CN113564753 A CN 113564753A CN 202110755726 A CN202110755726 A CN 202110755726A CN 113564753 A CN113564753 A CN 113564753A
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pressure
static electricity
fiber
unit
dispersion
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CN113564753B (en
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李树然
沈星
闫克平
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Zhejiang University ZJU
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Zhejiang University ZJU
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    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01GPRELIMINARY TREATMENT OF FIBRES, e.g. FOR SPINNING
    • D01G99/00Subject matter not provided for in other groups of this subclass

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Abstract

The invention discloses a fiber dispersing and collecting device and method based on airflow impact and static electricity, wherein the fiber dispersing and collecting device comprises an impact dispersing unit and a static electricity collecting unit which are sequentially connected; the impact dispersion unit comprises a pressure storage container, a pressure release device and a fiber cluster container which are sequentially connected; the static electricity collecting unit comprises a collecting high-potential pole, a collecting low-potential pole and a corresponding first high-voltage power supply. The invention can solve the problems of dispersion and collection of the fibers in the gas phase, can not cause damage and structural damage of the carbon fibers, can keep the dispersion state of the carbon fibers and is beneficial to subsequent reutilization.

Description

Fiber dispersing and collecting device and method based on airflow impact and static electricity
Technical Field
The invention belongs to the technical field of fiber preparation, and particularly relates to a fiber dispersing and collecting device and method based on airflow impact and static electricity.
Background
The fiber reinforced thermoplastic composite material is widely applied to the fields of automobiles, buildings, aerospace and the like, and has low density, corrosion resistance and excellent mechanical properties. Due to the advantages of low manufacturing cost, diversity of processable shapes, high specific strength and the like, the composite material of the chopped fiber has excellent performance in the application fields of common black body materials, super capacitors, high-performance heat dissipation materials and the like.
Most fibers cause an inevitable agglomeration phenomenon due to high length-diameter ratio and strong van der waals attraction, and the dispersibility of the fibers is a key for ensuring the performance of the fiber reinforced thermoplastic composite material.
Numerous fiber dispersion techniques in the liquid phase have been developed, such as addition of liquid phase dispersants, rotor/stator centrifugal dispersion, high compression ratio fluids due to extreme pressure drop, and the like.
For example, patent application publication No. CN105818398A discloses a liquid phase dispersion method using a bio-based surface modifier, dopamine, and a bio-based thickener, which is environmentally friendly, but has problems of long treatment time and easy damage to the fiber surface.
In addition to the liquid phase dispersion method, there are also many methods for dispersing fiber in gas phase, for example, chinese patent publication No. CN110963779A discloses a dispersion method for adding mullite fiber cotton into purple sand pug, which uses purple sand pug and mullite fiber cotton as raw materials, and uses SD-JR08D type small rotary blade crusher, UBE-V0.4L type planetary ball mill, JJ-1 type timing electric mixer, double rotary blade mixer, and ZLDL1400-4T-6K type medium temperature furnace, through crushing, dispersing, stirring, suction filtering, mixing, molding, and firing, the purple sand pottery with mullite fiber uniformly existing inside is obtained.
However, in the gas phase, the conventional ball milling process can completely disperse the 2mm fiber aggregates into 300 μm single fibers, which causes the breakage of long fibers. Therefore, it is necessary to develop a simple and fast dispersion collection method without damaging the fiber surface and changing the original size of the fiber.
Disclosure of Invention
The invention provides a fiber dispersion and collection device and method based on airflow impact and static electricity, which solve the problems of dispersion and collection of fibers in a gas phase by airflow impact dispersion and static electricity collection.
A fiber dispersing and collecting device based on airflow impact and static electricity comprises an impact dispersing unit and a static electricity collecting unit which are connected in sequence;
the impact dispersion unit comprises a pressure storage container, a pressure release device and a fiber cluster container which are sequentially connected;
the static electricity collecting unit comprises a collecting high-potential pole, a collecting low-potential pole and a corresponding first high-voltage power supply.
Further, the pressure storage container includes, but is not limited to, one or a combination of a positive displacement compressor, a piston compressor, a rotary compressor, a centrifugal compressor, a screw compressor, and a gas cylinder.
Furthermore, an impact baffle is arranged in the fiber cluster container, and the dispersion degree is improved through the impact baffle.
Further, the pressure release device comprises a pressure release shutdown device and a pressure release port;
the pressure release stopping device is used for starting and stopping pressure release in unit time and comprises one or a combination of a pressure limiting valve, a pressure reducing valve, a solenoid valve and the like; the pressure relief port is used for forming high-pressure impact airflow, and the shape of the pressure relief port comprises one or a combination of, but is not limited to, a circle, a square and a mesh; the ratio of the storage pressure of the pressure storage container to the area of the pressure release opening is not less than 8 x 106kPa/m2
The collecting high-potential electrode and the collecting low-potential electrode in the static collecting unit can be made of conductive materials, and insulating medium layers can also be covered on the surfaces of the conductive materials.
Further, the tail part of the static electricity collecting unit is connected with a cyclone dust collector.
Optionally, a charging unit is further arranged between the impact dispersion unit and the static electricity collection unit, and the charging unit comprises a charging high-voltage electrode, a charging low-potential electrode and a corresponding second high-voltage power supply.
Alternatively, the charging unit and the static electricity collecting unit are arranged in the same module, and in this case, the first high-voltage power supply and the second high-voltage power supply can be replaced by the same power supply.
The invention also provides a fiber dispersion and collection method based on airflow impact and static electricity, which adopts the fiber dispersion and collection device without the charging unit and comprises the following steps:
(1) accumulating gas pressure in the pressure storage container, releasing pressure to the fiber clusters through a pressure release device in unit time, and realizing deagglomeration and dispersion of the fiber clusters through high-pressure airflow impact;
(2) the fibers after the de-agglomeration and dispersion enter a static collecting unit along with airflow, high voltage is applied to the static collecting unit, and the surfaces of the fibers are collected by a low-potential electrode after being charged.
In the invention, the fiber to be dispersed comprises one or more of carbon fiber, glass fiber, aramid fiber, nylon fiber and ultrahigh molecular weight fiber in combination, and the fiber can be in any length combination between 0.1mm and 20 mm.
In the step (1), the pressure range accumulated in the pressure storage container is 100-800 kPa; the unit time range of pressure release is 0.1 ms-10 s.
In the step (2), a high voltage including but not limited to one or a combination of direct current, alternating current and pulse is applied to the electrostatic collecting unit, the polarity of the high voltage may be one of positive polarity or negative polarity, and the difference between the high voltage and the zero potential ranges from 1 kV to 80 kV.
The invention also provides another fiber dispersion and collection method based on airflow impact and static electricity, which adopts the fiber dispersion and collection device with the charging unit and comprises the following steps:
(1) accumulating gas pressure in the pressure storage container, releasing pressure to the fiber clusters through a pressure release device in unit time, and realizing deagglomeration and dispersion of the fiber clusters through high-pressure airflow impact;
(2) the fibers after the de-agglomeration and dispersion enter a charge unit along with airflow, positive direct-current high-voltage electricity is applied between a charge high-voltage electrode and a charge low-potential electrode, and the fibers are charged on the charge unit;
(3) the fiber passing through the charging unit enters the electrostatic collecting unit, high voltage is applied between the collecting high-potential electrode and the collecting low-potential electrode, and the fiber surface is charged and then collected by the collecting low-potential electrode.
Compared with the prior art, the invention has the following beneficial effects:
1. the invention realizes the gas phase dispersion of the fiber by releasing high-pressure fluid to the fiber cluster in a short time, and obviously improves the fiber dispersion efficiency.
2. The air flow and the high voltage electricity adopted by the invention can not cause the damage and the structural damage of the carbon fiber.
3. The invention collects the carbon fiber in a high-voltage electrostatic manner, can keep the dispersion state of the carbon fiber and is beneficial to subsequent reutilization.
Drawings
FIG. 1 is a schematic view of a fiber dispersion collection apparatus with a charging unit according to an embodiment of the present invention;
FIG. 2 is a view showing the construction of a fiber dispersion collection apparatus without a charging unit according to an embodiment of the present invention;
FIG. 3 is a structural view of a fiber dispersion collection device with an integrated charging unit and an integrated static electricity collection unit according to an embodiment of the present invention;
FIG. 4 is a diagram illustrating the effect of scattering and collecting according to an embodiment of the present invention.
Detailed Description
The invention will be described in further detail below with reference to the drawings and examples, which are intended to facilitate the understanding of the invention without limiting it in any way.
Example 1
As shown in fig. 1, a fiber dispersion and collection device based on airflow impact and static electricity comprises an impact dispersion unit, a charge unit and a static electricity collection unit which are sequentially connected; the tail of the electrostatic collection unit is connected with a cyclone dust collector 9.
The impact dispersion unit comprises a pressure storage container 1, a pressure release device and a fiber cluster container 4 which are connected in sequence; wherein the pressure relief means comprises a pressure relief shut-off device 2 and a pressure relief port 3. In this embodiment, the pressure storage container 1 is a positive displacement compressor, the pressure release shutdown device 2 is a pressure limiting valve, and the pressure release port 3 is circular.
The charging unit comprises a charging high-voltage electrode 5, a charging low-potential electrode 6 and a corresponding second high-voltage power supply. Wherein, the charged low-potential electrode 6 is arranged on the upper end surface and the lower end surface, and the charged high-voltage electrode 5 is arranged in the middle position.
The static electricity collecting unit includes a collecting high potential pole 8, a collecting low potential pole 7, and a corresponding first high voltage power supply. Wherein, the collecting low-potential electrode 7 is arranged on the upper end surface and the lower end surface, and the high-potential electrode 8 is arranged in the middle position.
The method for collecting and dispersing fibers by using the device for collecting and dispersing fibers of the embodiment comprises the following steps:
s01, accumulating 100kPa gas pressure in the pressure storage container 1, releasing the pressure to the 3mm carbon fiber cluster in the fiber cluster container 4 through the pressure release shutoff device 2 and the pressure release port 3 within 0.1ms, and realizing deagglomeration and dispersion of the fiber cluster by high-pressure air impact.
And S02, the fibers after de-agglomeration and dispersion enter a charging unit along with airflow, 30kV positive direct-current high-voltage electricity is applied between the charging high-voltage electrode 5 and the charging low-potential electrode 6, and the fibers are charged in the charging unit.
And S03, the fibers passing through the charging unit enter a static collecting unit, pulse negative polarity high voltage of 20kV is applied between a collecting high potential pole 8 and a collecting low potential pole 7 of the static collecting unit, and the fibers are collected by the low potential pole.
And S04, the fibers which are not collected are subjected to tail gas treatment by the cyclone separator 9 of the tail gas treatment unit, so that the environment is ensured not to be polluted.
S05, the collected dispersed fibers can be reused by applying a negative DC voltage of 10kV between the high potential pole and the low potential pole.
Example 2
Different from the embodiment 1, in this embodiment, the fiber dispersion collection device is not provided with the cyclone 9, the pressure storage container 1 is a gas cylinder, the pressure release shutdown device 2 is a pressure reducing valve, and the pressure release port 3 is square.
The method for collecting and dispersing fibers by using the device for collecting and dispersing fibers of the embodiment comprises the following steps:
and S01, accumulating gas pressure of 200kPa in the pressure storage container 1, releasing pressure to the aramid fiber clusters of 20mm in the fiber cluster container 4 through the pressure release shutdown device 2 and the pressure release port 3 within 1S, and realizing deagglomeration and dispersion of the fiber clusters through high-pressure air flow impact.
And S02, the fibers after de-agglomeration and dispersion enter a charging unit along with airflow, 10kV negative polarity alternating current high voltage is applied between the charging high voltage electrode 5 and the charging low potential electrode 6, and the fibers are charged in the charging unit.
And S03, the fibers passing through the charging unit enter a static collecting unit, a direct-current positive polarity high voltage of 30kV is applied between a collecting high potential pole 8 and a collecting low potential pole 7 of the static collecting unit, and the fibers are collected by the low potential pole.
S04, the collected dispersed fibers can be recycled by applying a positive dc voltage of 5kV between the high potential pole and the low potential pole.
Example 3
As shown in fig. 2, compared to example 1, the present embodiment is without the charging unit and the cyclone 9. The pressure storage container 1 adopts a piston compressor, the pressure release shutdown device 2 adopts an electromagnetic valve, and the pressure release port 3 adopts a mesh.
The method for collecting and dispersing fibers by using the device for collecting and dispersing fibers of the embodiment comprises the following steps:
and S01, accumulating gas pressure of 800kPa in the pressure storage container 1, releasing pressure to the 6mm nylon fiber cluster in the fiber cluster container 4 through the pressure release stopping device 2 and the pressure release port 3 within 8S, and realizing deagglomeration and dispersion of the fiber cluster through high-pressure air flow impact.
S02, the disaggregated and dispersed fibers enter a static collecting unit, pulse positive polarity high voltage of 60kV is applied between a collecting high potential pole 8 and a collecting low potential pole 7 of the static collecting unit, and the fibers are collected by the low potential pole.
S03, the collected dispersed fibers can be reused by applying a pulse negative voltage of 15kV between the high potential pole and the low potential pole.
Example 4
As shown in fig. 3, in the present embodiment, compared to embodiment 1, the charging unit and the static electricity collecting unit are provided in the same module and share one high-voltage power supply. The pressure storage container 1 adopts a centrifugal compressor, the pressure release stopping device 2 adopts a pressure limiting valve, and the pressure release port 3 is circular.
The method for collecting and dispersing fibers by using the device for collecting and dispersing fibers of the embodiment comprises the following steps:
s01, accumulating 300kPa gas pressure in the pressure storage container 1, releasing pressure to the 15mm glass fiber cluster in the fiber cluster container 4 through the pressure release stopping device 2 and the pressure release port 3 within 4S, and realizing deagglomeration and dispersion of the fiber cluster through high-pressure air impact;
s02, the fibers which are dispersed by de-agglomeration enter the same module consisting of the charging unit and the static collecting unit, the charging high-voltage electrode and the collecting high-potential electrode share the same power supply, 20kV positive polarity direct current high-voltage electricity is applied between the charging high-voltage electrode 5 and the charging low-potential electrode 6 and between the collecting high-potential electrode 8 and the collecting low-potential electrode 7, and the fibers are collected by the collecting low-potential electrode 7.
S03, the collected dispersed fibers can be reused by applying a pulse positive polarity voltage of 6kV between the high potential pole and the low potential pole.
As shown in fig. 4, which is a diagram of the dispersion and collection effect of the present invention, it can be seen that the dispersion state of the carbon fibers can be maintained by using the apparatus and method of the present invention, which is beneficial to subsequent reuse.
The embodiments described above are intended to illustrate the technical solutions and advantages of the present invention, and it should be understood that the above-mentioned embodiments are only specific embodiments of the present invention, and are not intended to limit the present invention, and any modifications, additions and equivalents made within the scope of the principles of the present invention should be included in the scope of the present invention.

Claims (10)

1. A fiber dispersion and collection device based on airflow impact and static electricity is characterized by comprising an impact dispersion unit and a static electricity collection unit which are connected in sequence;
the impact dispersion unit comprises a pressure storage container, a pressure release device and a fiber cluster container which are sequentially connected;
the static electricity collecting unit comprises a collecting high-potential pole, a collecting low-potential pole and a corresponding first high-voltage power supply.
2. The gas impingement and static electricity based fiber dispersion collection device of claim 1, wherein said pressure storage vessel comprises one or a combination of, but not limited to, positive displacement compressor, piston compressor, rotary compressor, centrifugal compressor, screw compressor, gas cylinder.
3. The airflow impingement and static electricity based fiber dispersion collection apparatus of claim 1 wherein said pressure relief means comprises a pressure relief shut-off means and a pressure relief port;
the pressure release stopping device is used for starting and stopping pressure release in unit time, and the pressure release port is used for forming high-pressure impact airflow; the ratio of the storage pressure of the pressure storage container to the area of the pressure release opening is not less than 8 x 106kPa/m2
4. The airflow impingement and static electricity based fiber dispersion collection device of claim 1, wherein a cyclone is connected to the tail of said static electricity collection unit.
5. The airflow impact and static electricity based fiber dispersion collection device according to claim 1, wherein a charging unit is further arranged between the impact dispersion unit and the static electricity collection unit, and the charging unit comprises a charging high-voltage electrode, a charging low-potential electrode and a corresponding second high-voltage power supply.
6. The airflow impingement and static electricity based fiber dispersion collection apparatus of claim 5 wherein said charging unit and said static electricity collection unit are disposed in the same module.
7. A fiber dispersion and collection method based on air flow impact and static electricity, which is characterized in that the fiber dispersion and collection device of any claim 1 to 4 is adopted, and the method comprises the following steps:
(1) accumulating gas pressure in the pressure storage container, releasing pressure to the fiber clusters through a pressure release device in unit time, and realizing deagglomeration and dispersion of the fiber clusters through high-pressure airflow impact;
(2) the fibers after the de-agglomeration and dispersion enter a static collecting unit along with airflow, high voltage is applied to the static collecting unit, and the surfaces of the fibers are collected by a low-potential electrode after being charged.
8. The fiber dispersion collection method based on air flow impingement and static electricity according to claim 7, wherein in step (1), the pressure accumulated in the pressure storage vessel ranges from 100 to 800 kPa; the unit time range of pressure release is 0.1 ms-10 s.
9. The fiber dispersion collection method based on air flow impact and static electricity according to claim 7, wherein in the step (2), a high voltage including but not limited to one or a combination of direct current, alternating current and pulse is applied to the static electricity collection unit, the polarity of the high voltage can be one of positive polarity or negative polarity, and the difference between the high voltage and zero potential is 1-80 kV.
10. A fiber dispersion collection method based on air flow impact and static electricity, characterized in that the fiber dispersion collection device of claim 5 or 6 is used, comprising:
(1) accumulating gas pressure in the pressure storage container, releasing pressure to the fiber clusters through a pressure release device in unit time, and realizing deagglomeration and dispersion of the fiber clusters through high-pressure airflow impact;
(2) the fibers after the de-agglomeration and dispersion enter a charge unit along with airflow, positive direct-current high-voltage electricity is applied between a charge high-voltage electrode and a charge low-potential electrode, and the fibers are charged on the charge unit;
(3) the fiber passing through the charging unit enters the electrostatic collecting unit, high voltage is applied between the collecting high-potential electrode and the collecting low-potential electrode, and the fiber surface is charged and then collected by the collecting low-potential electrode.
CN202110755726.6A 2021-07-05 2021-07-05 Fiber dispersing and collecting device and method based on airflow impact and static electricity Active CN113564753B (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114159990A (en) * 2021-12-03 2022-03-11 河海大学 Device and method for dispersing carbon fibers in material
CN115367548A (en) * 2022-07-27 2022-11-22 浙江大学 Large-scale fine carbon fiber dispersing, collecting and secondary conveying device and method
CN115367548B (en) * 2022-07-27 2024-06-11 浙江大学 Large-scale micro carbon fiber dispersion collection and secondary conveying device and method

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Publication number Priority date Publication date Assignee Title
WO2000024517A1 (en) * 1998-10-28 2000-05-04 Koichi Fujibayasi Powder dispersion-treating method and device therefor and powder treating device
US20050205801A1 (en) * 2004-03-17 2005-09-22 Epion Corporation Method and apparatus for improved beam stability in high current gas-cluster ion beam processing system
CN101491784A (en) * 2009-01-19 2009-07-29 西北工业大学 Superfine preparation method and device using jet static electricity
CN107297182A (en) * 2015-09-10 2017-10-27 青岛科技大学 A kind of CNT dispersing apparatus with electrostatic precipitator
CN112342643A (en) * 2020-11-27 2021-02-09 湖南东映碳材料科技有限公司 High-thermal-conductivity carbon fiber powder and preparation method thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2000024517A1 (en) * 1998-10-28 2000-05-04 Koichi Fujibayasi Powder dispersion-treating method and device therefor and powder treating device
US20050205801A1 (en) * 2004-03-17 2005-09-22 Epion Corporation Method and apparatus for improved beam stability in high current gas-cluster ion beam processing system
CN101491784A (en) * 2009-01-19 2009-07-29 西北工业大学 Superfine preparation method and device using jet static electricity
CN107297182A (en) * 2015-09-10 2017-10-27 青岛科技大学 A kind of CNT dispersing apparatus with electrostatic precipitator
CN112342643A (en) * 2020-11-27 2021-02-09 湖南东映碳材料科技有限公司 High-thermal-conductivity carbon fiber powder and preparation method thereof

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114159990A (en) * 2021-12-03 2022-03-11 河海大学 Device and method for dispersing carbon fibers in material
CN115367548A (en) * 2022-07-27 2022-11-22 浙江大学 Large-scale fine carbon fiber dispersing, collecting and secondary conveying device and method
CN115367548B (en) * 2022-07-27 2024-06-11 浙江大学 Large-scale micro carbon fiber dispersion collection and secondary conveying device and method

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