CN113559039A - Deep skin-cleaning amino acid facial cleanser containing natural bamboo charcoal powder - Google Patents
Deep skin-cleaning amino acid facial cleanser containing natural bamboo charcoal powder Download PDFInfo
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- CN113559039A CN113559039A CN202110820176.1A CN202110820176A CN113559039A CN 113559039 A CN113559039 A CN 113559039A CN 202110820176 A CN202110820176 A CN 202110820176A CN 113559039 A CN113559039 A CN 113559039A
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61K8/645—Proteins of vegetable origin; Derivatives or degradation products thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/738—Cyclodextrins
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9728—Fungi, e.g. yeasts
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/41—Particular ingredients further characterized by their size
- A61K2800/413—Nanosized, i.e. having sizes below 100 nm
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/56—Compounds, absorbed onto or entrapped into a solid carrier, e.g. encapsulated perfumes, inclusion compounds, sustained release forms
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/596—Mixtures of surface active compounds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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Abstract
The invention discloses deep skin-cleaning amino acid facial cleanser containing natural bamboo charcoal powder and a preparation method thereof. The facial cleanser comprises skin-cleaning active substances composed of mild natural surfactant of potassium oat protein hydrolyzed by cocoyl fatty acid, amino acid surfactant and acidic soap, and citric acid for keeping pH of the facial cleanser weakly acidic and improving skin affinity, and solves irritation problem caused by high pH of soap-based facial cleanser. The adopted carbon powder is nano active bamboo carbon powder, has large specific surface area, high chemical stability, developed pore structure and unique surface activity, is an excellent adsorbent, can adsorb and remove dirt in deep layers of skin, removes blackheads of the skin and balances grease secretion. The yeast/grape fermentation product extract and various plant extracts have effects of scavenging free radicals, resisting inflammation, killing bacteria, keeping moisture, and promoting blood circulation.
Description
Technical Field
The invention belongs to the field of cosmetics, and particularly relates to deep skin-cleaning amino acid facial cleanser containing natural bamboo charcoal powder and a preparation method thereof.
Background
The amino acid facial cleanser is a mild amino acid surfactant with weak acidity, the pH value is close to that of human skin, and the amino acid is a basic substance forming protein, so that the amino acid facial cleanser is mild and skin-friendly, is suitable for people with acne skin, and can be used for sensitive skin.
Most of the prior amino acid facial cleansers have the effects of softness and no irritation by directly adding an amino acid organic component into the facial cleanser, however, the cleaning effect of the facial cleanser is poor, although the cleansing is mild, the cleansing cleanser only can clean stains on the epidermis of the face, but cannot clean deeper pores of the face, and the aim of ensuring the mildness and no irritation of the facial cleanser and having higher cleaning effect of the facial cleanser cannot be achieved. The invention relates to a facial cleanser developed for meeting the requirement of people on deep skin cleaning.
Disclosure of Invention
The invention aims to overcome the defects of the existing facial cleanser and provides deep skin-cleaning amino acid facial cleanser containing natural bamboo charcoal powder and a preparation method thereof.
To achieve the above object, the present invention adopts the following technical solution
A deep skin cleaning amino acid facial cleanser containing natural bamboo charcoal powder comprises glycerol, sodium cocoyl glycinate, disodium 2-sulfo-laurate, cocoyl hydrolyzed oat protein potassium, disodium cocoyl glutamate, trehalose, acrylic acid (ester) copolymer, charcoal powder, yeast/grape fermentation product extract, cyclodextrin, peach resin extract, cactus stem extract, radix Inulae Giraldii Nitsche leaf extract, hydroxypropyl methylcellulose, sodium cocoate, coconut oil acid, sodium chloride, citric acid, p-hydroxyacetophenone, caprylyl glycol, essence, butanediol, and deionized water.
The deep skin-cleaning amino acid facial cleanser containing natural bamboo charcoal powder comprises the components in parts by mass
Preferably, the deep skin-cleaning amino acid facial cleanser containing natural bamboo charcoal powder comprises the following components in parts by mass:
preferably, the deep skin-cleaning amino acid facial cleanser containing natural bamboo charcoal powder comprises the following components in parts by mass:
in order to prepare the facial cleanser, the invention adopts the following preparation method:
adding glycerin, sodium cocoyl glycinate, disodium 2-sulfo-laurate, potassium cocoyl hydrolyzed oat protein, disodium cocoyl glutamate, trehalose, yeast/grape fermentation product extract, sodium cocoyl oleate, coconut oil acid, sodium chloride, citric acid, butanediol and part of deionized water into an emulsifying pot, heating, stirring and dissolving until no particles exist completely, preserving heat for 30 minutes, sterilizing and defoaming;
dispersing the acrylic acid (ester) copolymer by using part of water, adding the dispersed acrylic acid (ester) copolymer into an emulsifying pot, fully and uniformly stirring until no particles exist, defoaming and cooling;
thirdly, cooling to 45 ℃, adding the rest components in sequence, and fully and uniformly stirring;
cooling to 35-38 ℃, sampling, inspecting, and discharging after the product is qualified.
Compared with the prior art, the invention has the following advantages and effects:
(1) the skin-cleaning active substance is composed of mild natural surfactant potassium oat protein hydrolyzed by cocoyl, amino acid surfactant and acid soap, and the pH value of the facial cleanser is kept to be weakly acidic by citric acid, so that the skin-friendly property is good, and the problem of irritation caused by high pH value of soap base facial cleanser is solved.
(2) The adopted carbon powder is nano active bamboo carbon powder, has large specific surface area, high chemical stability, developed pore structure and unique surface activity, is an excellent adsorbent, can adsorb and remove dirt in deep layers of skin, removes blackheads of the skin and balances grease secretion. The nano bamboo charcoal contains rich oxygen-containing functional groups such as-OH, -COOH and the like, and is the main active site of the nano bamboo charcoal, and the active sites enable the surface of the nano bamboo charcoal to have weak properties such as hydrophilicity, oxidability, acidity and the like. The plant extract usually contains functional groups with strong polarity such as-NH, -CO-, -OH and the like, and can be adsorbed by active sites in the nano bamboo charcoal. Therefore, the active factors in the system can be held and slowly released into the skin, and the aim of helping the skin to absorb the effective substances is fulfilled.
(3) The yeast/grape fermentation product extract, peach resin extract, opuntia ficus-indica stem extract and folium ibrii palustris extract have the effects of resisting free radicals, resisting inflammation, sterilizing, keeping moisture, promoting blood circulation and the like.
Detailed Description
The present invention will be described in further detail with reference to examples, but the embodiments of the present invention are not limited thereto.
The test methods in the following examples, in which specific experimental conditions are not specified, are generally performed according to conventional experimental conditions or according to the experimental conditions recommended by the manufacturer.
Examples 1-3 deep skin cleansing amino acid facial cleanser containing natural bamboo charcoal powder
The formulations of the deep skin cleansing amino acid facial cleansers containing natural bamboo charcoal powder of examples 1 to 3 are shown in table 1, and the amounts are in mass fractions.
TABLE 1
The preparation method comprises the following steps:
adding glycerin, sodium cocoyl glycinate, disodium 2-sulfo-laurate, potassium cocoyl hydrolyzed oat protein, disodium cocoyl glutamate, trehalose, yeast/grape fermentation product extract, sodium cocoyl oleate, coconut oil acid, sodium chloride, citric acid, butanediol and part of deionized water into an emulsifying pot, heating, stirring and dissolving until no particles exist completely, preserving heat for 30 minutes, sterilizing and defoaming;
dispersing the acrylic acid (ester) copolymer by using part of water, adding the dispersed acrylic acid (ester) copolymer into an emulsifying pot, fully and uniformly stirring until no particles exist, defoaming and cooling;
thirdly, cooling to 45 ℃, adding the rest components in sequence, and fully and uniformly stirring;
cooling to 35-38 ℃, sampling, inspecting, and discharging after the product is qualified.
Comparative example 1 cleansing milk containing no charcoal powder
The procedure was as in example 1 except that no carbon powder was contained.
Comparative example 2 citric acid-free face cleanser
The procedure was as in example 1 except that citric acid was not contained.
Comparative example 2 facial cleanser without extract
The same as example 1 except that the extract of the fermentation product of yeast/grape, the extract of peach resin, the extract of stem of opuntia ficus indica, and the extract of leaf of burley leaf were not contained
Experimental example 1 evaluation experiment of oil control efficiency
1. Principle of experiment
The skin was tested for oil content using the oil tester SebumeterSM 815. Based on the principle of a photometer, a special extinction adhesive tape with the thickness of 0.1mm can be changed into a semitransparent adhesive tape after absorbing grease on human skin, the light transmission quantity of the semitransparent adhesive tape can be changed, the more grease is absorbed, the greater the light transmission quantity is, and the content of the grease on the skin can be measured.
2. The test instrument:
SebumetersM815 (Courage + Khazaha, Germany)
3. Test sample
The face washes prepared in examples 1-3.
4. Test method
30 oily scalp subjects. The subjects were rested for 30 minutes in a laboratory at a temperature of 22 + -3 deg.C and a relative humidity of 50 + -5%, skin oil content of the left and right forehead, respectively, was measured with an oil tester SebumererSM 815, data recorded as D0, samples were distributed to each subject, bathing once a day for 28 days, and skin oil content was measured back to the constant temperature laboratory on days 14 and 28, respectively, data recorded as D14 and D28. Respectively calculating the oil content change rate of D14 and D28 according to the following formula:
the rate of change in fat content { (fat content after use sample-fat content before use sample)/fat content before use sample } × 100%
5. The experimental results are as follows:
the results are shown in Table 3.
TABLE 3
| Test sample | D14 change in fat (%) | D28 change in fat (%) |
| Example 1 | -19.2％ | -26.4％ |
| Comparative example 1 | -5.4％ | -7.5％ |
The result shows that the facial cleanser provided by the invention has a good oil control effect. And the comparison proportion effect is good, which shows that the bamboo charcoal is helpful for controlling oil of skin.
Experimental example 2 irritation test
The creams of examples 1 to 3 and the cream of comparative example 2 were tested for irritation according to the "analysis of the results of the multiple skin irritation tests for different types of cosmetic products" described in 2016, 10, 30, 5, toxicological journal.
The results show that the facial cleansers of examples 1-3 appeared non-irritating, while the facial cleanser of comparative example 2 appeared moderately irritating, indicating that citric acid keeps the product weakly acidic to reduce irritation.
Experimental example 3 evaluation of moisturizing Effect
1. Sample preparation and instrumentation
The face cleansers prepared in examples 1 to 3 were prepared separately and the following experiment was performed.
The experimental apparatus was a skin moisture Corneometer test probe manufactured by Courage + Khazaka, Germany (CK, Germany).
2. Principle of experiment
The higher the skin moisture, the higher the skin moisture content and the lower the TEWL value for skin moisture loss.
3. Skin moisture content testing method
The water content test in the experiment adopts
Farad-capacitive method.
100 dry skin people are selected, wherein the age is 20-45 years, and the age is half of that of men and women. Before the test, the subjects were asked to wash their facial skin and sit still for 30min in a constant temperature and humidity room at a temperature of 22. + -. 1 ℃ and a humidity of 50. + -. 5% 2 hours after washing, and kept in a relaxed state.
The facial skin of the volunteers was selected for skin moisture content test and moisture loss (TEWL) test, and the average of 3 values was taken as the moisture content data (D0). After the test is finished, the volunteers need to use the facial cleanser according to the requirements, the facial cleanser is used for 28 days continuously every day, and the 14 th (D14) and 28 th (D28) days of the test are required to be revisited.
4. Test results
The results of the moisture content change rate test are shown in table 4.
TABLE 4
| Group of | D14 moisture content | D28 moisture content |
| Example 1 | 23.9±2.1 | 30.3±2.5 |
| Comparative example 1 | 18.6±2.5 | 22.4±2.7 |
The result shows that the facial cleanser provided by the invention has a good moisturizing effect and a good comparison ratio, and the natural extract is beneficial to moisturizing the skin.
Experimental example 4 evaluation of Using effects
The product of example 1 was randomly distributed to 300 test subjects, 5 bottles were distributed, and the test subjects returned home for use, and after 1 month of use, the test subjects filled in and fed back a use report.
The statistical result shows that more than 96% of testers think that the facial cleanser is mild and non-irritant, has good effects of controlling oil, moisturizing, shrinking pores and removing blackheads, and particularly has clean, smooth, plump and fine skin, good elasticity and fresh and comfortable feel after being used.
The embodiments of the present invention have been described in detail, but the embodiments are merely examples, and the present invention is not limited to the embodiments described above. Any equivalent modifications and substitutions to those skilled in the art are also within the scope of the present invention. Accordingly, equivalent changes and modifications made without departing from the spirit and scope of the present invention should be covered by the present invention.
Claims (5)
1. A deep skin-cleaning amino acid facial cleanser containing natural bamboo charcoal powder is characterized by comprising glycerin, sodium cocoyl glycinate, disodium 2-sulfo-laurate, potassium cocoyl hydrolyzed oat protein, disodium cocoyl glutamate, trehalose, acrylic acid (ester) copolymer, charcoal powder, yeast/grape fermentation product extract, cyclodextrin, peach resin extract, opuntia ficus indica stem extract, radix orostachydis cumini leaf extract, hydroxypropyl methyl cellulose, sodium cocoate, coconut oil acid, sodium chloride, citric acid, p-hydroxyacetophenone, caprylyl glycol, essence, butanediol and deionized water.
2. The deep skin-cleaning amino acid facial cleanser containing natural bamboo charcoal powder as claimed in claim 1, wherein the mass fraction of each component is as follows:
3. the deep skin-cleaning amino acid facial cleanser containing natural bamboo charcoal powder as claimed in claim 1, wherein the mass fraction of each component is as follows:
4. the deep skin-cleaning amino acid facial cleanser containing natural bamboo charcoal powder as claimed in claim 1, wherein the mass fraction of each component is as follows:
5. the method for preparing the deep skin-cleaning amino acid facial cleanser containing natural bamboo charcoal powder as claimed in claim 1, comprising the steps of,
adding glycerin, sodium cocoyl glycinate, disodium 2-sulfo-laurate, potassium cocoyl hydrolyzed oat protein, disodium cocoyl glutamate, trehalose, yeast/grape fermentation product extract, sodium cocoyl oleate, coconut oil acid, sodium chloride, citric acid, butanediol and part of deionized water into an emulsifying pot, heating, stirring and dissolving until no particles exist completely, preserving heat for 30 minutes, sterilizing and defoaming;
dispersing the acrylic acid (ester) copolymer by using part of water, adding the dispersed acrylic acid (ester) copolymer into an emulsifying pot, fully and uniformly stirring until no particles exist, defoaming and cooling;
thirdly, cooling to 45 ℃, adding the rest components in sequence, and fully and uniformly stirring;
cooling to 35-38 ℃, sampling, inspecting, and discharging after the product is qualified.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110820176.1A CN113559039A (en) | 2021-07-20 | 2021-07-20 | Deep skin-cleaning amino acid facial cleanser containing natural bamboo charcoal powder |
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| CN202110820176.1A CN113559039A (en) | 2021-07-20 | 2021-07-20 | Deep skin-cleaning amino acid facial cleanser containing natural bamboo charcoal powder |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114903834A (en) * | 2022-06-30 | 2022-08-16 | 羽楠(广州)化妆品有限公司 | Cold-storable mild double-tube facial cleanser and preparation method thereof |
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2021
- 2021-07-20 CN CN202110820176.1A patent/CN113559039A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114903834A (en) * | 2022-06-30 | 2022-08-16 | 羽楠(广州)化妆品有限公司 | Cold-storable mild double-tube facial cleanser and preparation method thereof |
| CN114903834B (en) * | 2022-06-30 | 2024-05-14 | 羽楠(广州)化妆品有限公司 | Cold-storable mild double-tube facial cleanser and preparation method thereof |
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