CN113527967A - Preparation method of fragrant color paste blasting bead capable of forming film after drying - Google Patents
Preparation method of fragrant color paste blasting bead capable of forming film after drying Download PDFInfo
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- CN113527967A CN113527967A CN202110833905.7A CN202110833905A CN113527967A CN 113527967 A CN113527967 A CN 113527967A CN 202110833905 A CN202110833905 A CN 202110833905A CN 113527967 A CN113527967 A CN 113527967A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
- C09D133/04—Homopolymers or copolymers of esters
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D105/00—Coating compositions based on polysaccharides or on their derivatives, not provided for in groups C09D101/00 or C09D103/00
- C09D105/04—Alginic acid; Derivatives thereof
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/06—Artists' paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/36—Pearl essence, e.g. coatings containing platelet-like pigments for pearl lustre
Abstract
The invention provides a preparation method of a fragrant color paste bead capable of forming a film after drying, and relates to the technical field of bead blasting production. The color paste bead blasting preparation method comprises an internal phase slurry and an external phase slurry, wherein the internal phase slurry comprises the following raw materials: thickening agent, calcium salt, acrylate polymer, humectant, preservative, acid-base regulator, color paste, essence, pearlescent glitter powder and purified water, wherein the external phase slurry comprises the following raw materials: purified water, sodium alginate, carrageenan, chitosan and preservative. Through essence, mill base, acrylic ester polymer and pearly-lustre glittering powder, be convenient for keep fragrant, increase the amusement interest, internal phase material body can form the color film after using the writing brush drawing dry after the explosion thick liquid, has guaranteed the aesthetic property after the drawing, can not only enrich the form of mill base product, satisfies consumer's interest and recreational, can also improve the storage form of waterborne mill base simultaneously, is worth widelys popularization.
Description
Technical Field
The invention relates to the technical field of bead blasting production, in particular to a preparation method of a fragrant color paste bead blasting material capable of forming a film after being dried.
Background
The blasting beads are also called as fragrant pills, brittle capsules and beads, the blasting beads have large and small sizes, the diameter is more than 2.6mm, the blasting beads can be broken by extrusion, the blasting beads have a burst feeling when being broken, the color paste blasting beads wrap color paste in a film, when the painting is needed, the outer film is broken by extrusion, and the wrapped color paste is broken to meet the painting requirement.
The existing color paste for painting is poor in interestingness when in use, and cannot form a color film after the color paste is dried thoroughly, so that the attractiveness after painting is poor, and the stability and the moisture retention performance of a color paste product during transportation are poor.
Disclosure of Invention
Technical problem to be solved
Aiming at the defects of the prior art, the invention provides a preparation method of an exploded bead of fragrant color paste capable of forming a film after being dried, and solves the problems of poor interest of the existing color paste in use and poor attractiveness after painting.
(II) technical scheme
In order to achieve the purpose, the invention is realized by the following technical scheme: a preparation method of an explosion bead of fragrant color paste capable of forming a film after being dried comprises 5.0-8.0% of thickening agent, 5.0-8.0% of calcium salt, 5.0-8.0% of acrylate polymer, 5.0-8.0% of humectant, 2.0-4.0% of preservative, 5.0-8.0% of acid-base regulator, 10-20% of color paste, 8.0-10.0% of essence, 10.0-15.0% of pearlescent shimmering powder and 45.0-95.0% of purified water;
the raw materials of the external phase slurry comprise: 90.0 to 99.0 percent of purified water, 5.0 to 10.0 percent of sodium alginate, 2.0 to 3.0 percent of carrageenan, 2.0 to 3.0 percent of chitosan and 1.0 to 3.0 percent of preservative.
Preferably, the preparation method of the internal phase slurry comprises the following steps:
s1, heating and stirring
Placing 3/4 purified water into a stirring tank, heating the purified water to 60-65 ℃, stirring the purified water in the stirring tank at a rotating speed of 50-100 r/min, uniformly dropwise adding a thickening agent xanthan gum into the stirring tank while stirring, uniformly dispersing the thickening agent xanthan gum in the purified water until no particles exist, and keeping the temperature of the stirring tank at constant temperature for 30-35 min after dropwise adding;
s2, cooling and dissolving
Putting the residual purified water and the calcium salt into a dissolving bucket, stirring the dissolving bucket at a rotating speed of 50-100 r/min until the calcium salt is completely dissolved, then slowly dripping the calcium salt solution into the stirring tank, stirring the stirring tank at a rotating speed of 50-80 r/min, and simultaneously cooling the stirring tank to 35-40 ℃;
s3, initial stirring
After the solution in the stirring tank is cooled to 35-40 ℃, sequentially and uniformly dripping the acrylate polymer and the humectant into the stirring tank, stirring the stirring tank at the rotating speed of 200-300 r/min until the solution is uniformly stirred, then putting essence into a solubilizer and dripping a solubilizer into the solubilizer, slowly dripping the solution into the stirring tank after dripping is finished, stirring the stirring tank at the rotating speed of 150-200 r/min, and continuously stirring for 10-15 min until the solution is uniformly stirred;
s4, final preparation
And (3) slowly and uniformly dropwise adding the preservative, the acid-base regulator, the color paste and the pearlescent glitter powder into the stirring tank in sequence, stirring the stirring tank at the rotating speed of 300-400 r/min for 5-10 min until the stirring is uniform, taking out the mixed liquid in the stirring tank, standing and cooling the mixed liquid to room temperature for later use, thus preparing the internal phase slurry.
Preferably, the preparation method of the external phase slurry comprises the following steps:
s1, heating and stirring
Putting purified water into a stirring tank, heating the water to 85-90 ℃, sequentially and uniformly dropwise adding sodium alginate, carrageenan and chitosan into the stirring tank, stirring the sodium alginate, the carrageenan and the chitosan in the stirring tank at a rotating speed of 250-350 r/min, keeping the temperature for 30-40 min after continuously stirring for 5-8 min, fully swelling a material body in the stirring tank, and continuously stirring at a rotating speed of 50-100 r/min until no particulate matter exists;
s2. Final preparation
And (3) putting the stirring tank into a cooling machine, cooling the material body in the stirring tank to below 35 ℃, then adding the preservative into the stirring tank, continuously stirring at the rotating speed of 100-150 r/min for 5-10 min until the preservative is uniformly stirred, and then taking out the material body in the stirring tank and cooling to room temperature for later use to obtain the external phase slurry.
Preferably, the preparation method of the color paste blasting bead comprises the following steps: and respectively adding the prepared inner phase slurry and outer phase slurry into bead blasting production equipment, dripping the inner phase slurry into the outer phase slurry by using the bead blasting production equipment according to an equipment operation method, staying the dripped inner phase slurry in the outer phase slurry for 2-7 min, fishing out the bead blasting in the outer phase slurry by using a filter screen, and cleaning by using clear water to obtain the color paste bead blasting.
Preferably, the thickener is made of xanthan gum, the humectant is propylene glycol or glycerin, and the preservative is phenoxyethanol.
(III) advantageous effects
The invention provides a preparation method of an aroma color paste bead capable of forming a film after drying. The method has the following beneficial effects:
the invention is convenient to preserve fragrance and increase entertainment interest through the essence, the color paste, the acrylate polymer and the pearlescent glittering powder, the color paste, the essence, the glittering powder and the like can be wrapped in the external phase paste by the wrapping technology of the color paste after the paste explosion, so that a color film can be formed after the internal phase body is used for drawing with a writing brush and dried, the attractiveness after the drawing is ensured, the color paste wrapping technology can wrap the color paste, the essence, the glittering powder and the like in the external phase paste, thereby protecting the storage property of the aqueous color paste for a longer time, effectively and uniformly dispersing fragrant substances, reducing the volatilization loss of the fragrance and effectively releasing the fragrance, simultaneously, the usability of the traditional external color paste can be changed by wrapping the glittering powder in the color paste, the bead explosion color paste adopts a reverse phase film forming method, the color paste, the essence, the glittering powder and the like are wrapped in the external phase paste, the color paste can be exploded out from the film formed by the external phase paste by slightly extruding with hands, the interestingness of the paste explosion is created, or the bead is filled in a container with a cover and the container, and the bead is shaken up and down, let the mill base rupture of membranes of parcel and go out, the mill base that the slurry explosion and go out can be painted with the writing brush, scribbles the look on paper, can form the color film after dry, can also prepare the bead explosion mill base of the different particle diameters of size simultaneously and be used for satisfying different paintings and scribble the look and color the user demand, can not only enrich the form of mill base product, satisfy consumer's interest and recreational, can also improve the storage form of waterborne mill base simultaneously, the moisture retention of transportation stability and product is worth wideling popularize.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The first embodiment is as follows:
the embodiment of the invention provides a preparation method of an exploded bead of a fragrant color paste capable of forming a film after being dried, which comprises an internal phase paste and an external phase paste, wherein the internal phase paste comprises the following raw materials: 5.0 percent of thickening agent, 5.0 percent of calcium salt, 5.0 percent of acrylate polymer, 5.0 percent of humectant, 2.0 percent of preservative, 5.0 percent of acid-base regulator, 10 percent of color paste, 8.0 percent of essence, 10.0 percent of pearlescent shimmering powder and 45.0 percent of purified water;
the raw materials of the external phase slurry comprise: 90.0% of purified water, 5.0% of sodium alginate, 2.0% of carrageenan, 2.0% of chitosan and 1.0% of preservative.
The preparation method of the inner phase slurry comprises the following steps:
s1, heating and stirring
3/4, putting purified water into a stirring tank, heating the purified water to 65 ℃, stirring the purified water in the stirring tank at a rotating speed of 100r/min, uniformly dropwise adding a thickening agent xanthan gum into the stirring tank while stirring, uniformly dispersing the thickening agent xanthan gum in the purified water until no particles exist, and keeping the constant temperature in the stirring tank for 35min after dropwise adding;
s2, cooling and dissolving
Putting the residual purified water and the calcium salt into a dissolving bucket, stirring the dissolving bucket at the rotating speed of 100r/min until the calcium salt is completely dissolved, then slowly dripping the calcium salt solution into the stirring tank, stirring the stirring tank at the rotating speed of 80r/min, and simultaneously cooling the stirring tank to 40 ℃;
s3, initial stirring
After the solution in the stirring tank is cooled to 40 ℃, sequentially and uniformly dripping the acrylate polymer and the humectant into the stirring tank, stirring the stirring tank at the rotating speed of 300r/min until the solution is uniformly stirred, then putting essence into a dissolution enhancer, dripping a solubilizer into the dissolution enhancer, slowly dripping the solution into the stirring tank after dripping is finished, stirring the stirring tank at the rotating speed of 200r/min, and continuously stirring for 15min until the solution is uniformly stirred;
s4, final preparation
And (3) slowly and uniformly dropwise adding the preservative, the acid-base regulator, the color paste and the pearlescent glitter powder into the stirring tank in sequence, stirring the stirring tank at the rotating speed of 400r/min for 10min till the stirring is uniform, taking out the mixed liquid in the stirring tank, standing and cooling the mixed liquid to room temperature for later use, thus preparing the inner phase slurry.
The preparation method of the external phase slurry comprises the following steps:
s1, heating and stirring
Putting purified water into a stirring tank, heating the water to 90 ℃, sequentially and uniformly dropwise adding sodium alginate, carrageenan and chitosan into the stirring tank, stirring the stirring tank at the rotating speed of 350r/min, keeping the temperature for 40min at constant temperature after continuously stirring for 8min, fully swelling a material body in the stirring tank, and continuously stirring at the rotating speed of 100r/min until no particulate matter exists;
s2. Final preparation
And (3) putting the stirring tank into a cooling machine, cooling the material body in the stirring tank to below 35 ℃, then adding the preservative into the stirring tank, continuously stirring at the rotating speed of 150r/min for 10min until the preservative is uniformly stirred, and then taking out the material body in the stirring tank and cooling to room temperature for later use to obtain the external phase slurry.
The preparation method of the color paste bead comprises the following steps: the prepared inner phase slurry and outer phase slurry are respectively added into bead blasting production equipment, the inner phase slurry is dripped into the outer phase slurry by the bead blasting production equipment according to an equipment operation method, the dripped inner phase slurry stays in the outer phase slurry for 7min, then the bead blasting in the outer phase slurry is fished out by using a filter screen, and the bead blasting of the color paste can be prepared by cleaning with clear water, the color paste bead blasting is convenient to preserve fragrance and increases entertainment interest through essence, color paste, acrylate polymer and pearlescent flashing powder, the inner phase can be used for painting by using a writing brush after the bead blasting, a color film can be formed after the inner phase is dried, the attractiveness after painting is ensured, the color paste wrapping technology can wrap the color paste, the essence, the flashing powder and the like in the outer phase slurry, so that the storage property of the aqueous color paste for a long time is protected, the fragrant substances are effectively and uniformly dispersed, the volatilization loss of the fragrance is reduced, the fragrance is effectively released, and the usability of the traditional appearance can be changed by wrapping the flashing powder in the color paste, the bead blasting color paste adopts a reverse film forming method, color paste, essence, flash powder and the like are wrapped in the external phase paste and are slightly extruded by hands, the color paste can be blasted out from a film formed by the external phase paste to create the interest of the blasting paste, or the blasting beads are filled in a container with a cover, the blasting beads are shaken up and down by shaking, the wrapped color paste breaks the film and is discharged, the color paste discharged by the blasting paste can be painted on paper by using a writing brush, a color film can be formed after the color film is dried, meanwhile, the bead blasting color paste with different particle sizes can be prepared for meeting the use requirements of different painting colors and coloring, the forms of color paste products can be enriched, the interest and entertainment of consumers are met, and meanwhile, the storage form of the water-based color paste, the transportation stability and the moisture retention of the product can be improved.
The thickening agent is made of xanthan gum, the humectant is propylene glycol or glycerin, and the preservative is phenoxyethanol.
Example two:
the embodiment of the invention provides a preparation method of an exploded bead of a fragrant color paste capable of forming a film after being dried, which comprises an internal phase paste and an external phase paste, wherein the internal phase paste comprises the following raw materials: 8.0 percent of thickening agent, 8.0 percent of calcium salt, 8.0 percent of acrylate polymer, 8.0 percent of humectant, 4.0 percent of preservative, 8.0 percent of acid-base regulator, 20 percent of color paste, 10.0 percent of essence, 15.0 percent of pearlescent shimmering powder and 95.0 percent of purified water;
the raw materials of the external phase slurry comprise: 99.0% of purified water, 10.0% of sodium alginate, 3.0% of carrageenan, 3.0% of chitosan and 3.0% of preservative.
The preparation method of the inner phase slurry comprises the following steps:
s1, heating and stirring
3/4, putting purified water into a stirring tank, heating the purified water to 60 ℃, stirring the purified water in the stirring tank at a rotating speed of 50r/min, uniformly dropwise adding a thickening agent xanthan gum into the stirring tank while stirring, uniformly dispersing the thickening agent xanthan gum in the purified water until no particles exist, and keeping the temperature of the stirring tank at constant temperature for 30min after dropwise adding;
s2, cooling and dissolving
Putting the residual purified water and the calcium salt into a dissolving bucket, stirring the dissolving bucket at the rotating speed of 50r/min until the calcium salt is completely dissolved, slowly dripping the calcium salt solution into the stirring tank, stirring the stirring tank at the rotating speed of 50r/min, and simultaneously cooling the stirring tank to 35 ℃;
s3, initial stirring
After the solution in the stirring tank is cooled to 35 ℃, sequentially and uniformly dripping the acrylate polymer and the humectant into the stirring tank, stirring the stirring tank at the rotating speed of 200r/min until the solution is uniformly stirred, then putting essence into a dissolution enhancer, dripping a solubilizer into the dissolution enhancer, slowly dripping the solution into the stirring tank after dripping is finished, stirring the stirring tank at the rotating speed of 150r/min, and continuously stirring for 10min until the solution is uniformly stirred;
s4, final preparation
And (3) sequentially and uniformly dropwise adding the preservative, the acid-base regulator, the color paste and the pearlescent glitter powder into the stirring tank, stirring the stirring tank at the rotating speed of 300r/min for 5min till the stirring is uniform, taking out the mixed liquid in the stirring tank, standing and cooling the mixed liquid to room temperature for later use, thus preparing the inner phase slurry.
The preparation method of the external phase slurry comprises the following steps:
s1, heating and stirring
Putting purified water into a stirring tank, heating the water to 85 ℃, sequentially and uniformly dropwise adding sodium alginate, carrageenan and chitosan into the stirring tank, stirring the stirring tank at a rotating speed of 250r/min, keeping the temperature for 30min at a constant temperature after continuously stirring for 5min, fully swelling a material body in the stirring tank, and continuously stirring the material body at a rotating speed of 50r/min until no particulate matter exists;
s2. Final preparation
And (3) putting the stirring tank into a cooling machine, cooling the material body in the stirring tank to below 35 ℃, then adding the preservative into the stirring tank, continuously stirring at the rotating speed of 100r/min for 5min until the preservative is uniformly stirred, and then taking out the material body in the stirring tank and cooling to room temperature for later use to obtain the external phase slurry.
The preparation method of the color paste bead comprises the following steps: the prepared inner phase slurry and outer phase slurry are respectively added into bead blasting production equipment, the inner phase slurry is dripped into the outer phase slurry by the bead blasting production equipment according to an equipment operation method, the dripped inner phase slurry stays in the outer phase slurry for 2min, then the bead blasting in the outer phase slurry is fished out by using a filter screen, and the bead blasting of the color paste can be prepared by cleaning with clear water, the color paste bead blasting is convenient to preserve fragrance and increases entertainment interest through essence, color paste, acrylate polymer and pearlescent flashing powder, the inner phase can be used for painting by using a writing brush after the bead blasting, a color film can be formed after the inner phase is dried, the attractiveness after painting is ensured, the color paste wrapping technology can wrap the color paste, the essence, the flashing powder and the like in the outer phase slurry, so that the storage property of the aqueous color paste for a long time is protected, the fragrant substances are effectively and uniformly dispersed, the volatilization loss of the fragrance is reduced, the fragrance is effectively released, and the usability of the traditional appearance can be changed by wrapping the flashing powder in the color paste, the bead blasting color paste adopts a reverse film forming method, color paste, essence, flash powder and the like are wrapped in the external phase paste and are slightly extruded by hands, the color paste can be blasted out from a film formed by the external phase paste to create the interest of the blasting paste, or the blasting beads are filled in a container with a cover, the blasting beads are shaken up and down by shaking, the wrapped color paste breaks the film and is discharged, the color paste discharged by the blasting paste can be painted on paper by using a writing brush, a color film can be formed after the color film is dried, meanwhile, the bead blasting color paste with different particle sizes can be prepared for meeting the use requirements of different painting colors and coloring, the forms of color paste products can be enriched, the interest and entertainment of consumers are met, and meanwhile, the storage form of the water-based color paste, the transportation stability and the moisture retention of the product can be improved.
The thickening agent is made of xanthan gum, the humectant is propylene glycol or glycerin, and the preservative is phenoxyethanol.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (5)
1. The fragrant color paste blasting bead capable of forming a film after being dried comprises an internal phase slurry and an external phase slurry, and is characterized in that: the raw materials of the inner phase slurry include: 5.0 to 8.0 percent of thickening agent, 5.0 to 8.0 percent of calcium salt, 5.0 to 8.0 percent of acrylate polymer, 5.0 to 8.0 percent of humectant, 2.0 to 4.0 percent of preservative, 5.0 to 8.0 percent of acid-base regulator, 10 to 20 percent of color paste, 8.0 to 10.0 percent of essence, 10.0 to 15.0 percent of pearl flashing powder and 45.0 to 95.0 percent of purified water;
the raw materials of the external phase slurry comprise: 90.0 to 99.0 percent of purified water, 5.0 to 10.0 percent of sodium alginate, 2.0 to 3.0 percent of carrageenan, 2.0 to 3.0 percent of chitosan and 1.0 to 3.0 percent of preservative.
2. The method for preparing the explosion bead of the fragrant color paste capable of forming a film after being dried according to claim 1, which is characterized in that: the preparation method of the inner phase slurry comprises the following steps:
s1, heating and stirring
Placing 3/4 purified water into a stirring tank, heating the purified water to 60-65 ℃, stirring the purified water in the stirring tank at a rotating speed of 50-100 r/min, uniformly dropwise adding a thickening agent xanthan gum into the stirring tank while stirring, uniformly dispersing the thickening agent xanthan gum in the purified water until no particles exist, and keeping the temperature of the stirring tank at constant temperature for 30-35 min after dropwise adding;
s2, cooling and dissolving
Putting the residual purified water and the calcium salt into a dissolving bucket, stirring the dissolving bucket at a rotating speed of 50-100 r/min until the calcium salt is completely dissolved, then slowly dripping the calcium salt solution into the stirring tank, stirring the stirring tank at a rotating speed of 50-80 r/min, and simultaneously cooling the stirring tank to 35-40 ℃;
s3, initial stirring
After the solution in the stirring tank is cooled to 35-40 ℃, sequentially and uniformly dripping the acrylate polymer and the humectant into the stirring tank, stirring the stirring tank at the rotating speed of 200-300 r/min until the solution is uniformly stirred, then putting essence into a solubilizer and dripping a solubilizer into the solubilizer, slowly dripping the solution into the stirring tank after dripping is finished, stirring the stirring tank at the rotating speed of 150-200 r/min, and continuously stirring for 10-15 min until the solution is uniformly stirred;
s4, final preparation
And (3) slowly and uniformly dropwise adding the preservative, the acid-base regulator, the color paste and the pearlescent glitter powder into the stirring tank in sequence, stirring the stirring tank at the rotating speed of 300-400 r/min for 5-10 min until the stirring is uniform, taking out the mixed liquid in the stirring tank, standing and cooling the mixed liquid to room temperature for later use, thus preparing the internal phase slurry.
3. The method for preparing the explosion bead of the fragrant color paste capable of forming a film after being dried according to claim 1, which is characterized in that: the preparation method of the external phase slurry comprises the following steps:
s1, heating and stirring
Putting purified water into a stirring tank, heating the water to 85-90 ℃, sequentially and uniformly dropwise adding sodium alginate, carrageenan and chitosan into the stirring tank, stirring the sodium alginate, the carrageenan and the chitosan in the stirring tank at a rotating speed of 250-350 r/min, keeping the temperature for 30-40 min after continuously stirring for 5-8 min, fully swelling a material body in the stirring tank, and continuously stirring at a rotating speed of 50-100 r/min until no particulate matter exists;
s2. Final preparation
And (3) putting the stirring tank into a cooling machine, cooling the material body in the stirring tank to below 35 ℃, then adding the preservative into the stirring tank, continuously stirring at the rotating speed of 100-150 r/min for 5-10 min until the preservative is uniformly stirred, and then taking out the material body in the stirring tank and cooling to room temperature for later use to obtain the external phase slurry.
4. The method for preparing the explosion bead of the fragrant color paste capable of forming a film after being dried according to claim 1, which is characterized in that: the preparation method of the color paste bead comprises the following steps: and respectively adding the prepared inner phase slurry and outer phase slurry into bead blasting production equipment, dripping the inner phase slurry into the outer phase slurry by using the bead blasting production equipment according to an equipment operation method, staying the dripped inner phase slurry in the outer phase slurry for 2-7 min, fishing out the bead blasting in the outer phase slurry by using a filter screen, and cleaning by using clear water to obtain the color paste bead blasting.
5. The popping bead of the fragrant color paste capable of forming a film after being dried according to claim 1, which is characterized in that: the thickening agent is made of xanthan gum, the humectant is propylene glycol or glycerin, and the preservative is phenoxyethanol.
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| CN106666822A (en) * | 2016-11-29 | 2017-05-17 | 将军烟草集团有限公司 | Cigarette blast bead and preparation method thereof |
| CN111171724A (en) * | 2018-11-09 | 2020-05-19 | 万喜人家(北京)健康科技有限公司 | Preparation method and preparation equipment of shell powder art coating capable of removing formaldehyde |
| CN111436651A (en) * | 2019-01-16 | 2020-07-24 | 深圳波顿香料有限公司 | Blasting bead for cigarette and preparation method thereof |
| CN109907367A (en) * | 2019-03-01 | 2019-06-21 | 江西中烟工业有限责任公司 | A kind of quick-fried pearl of cigarette gel and preparation method thereof |
| CN110537729A (en) * | 2019-09-20 | 2019-12-06 | 安徽坤大生物工程技术有限公司 | Instant cigarette blasting bead |
| CN113046198A (en) * | 2021-03-17 | 2021-06-29 | 东莞波顿香料有限公司 | Preparation method and application of microcapsule blasting beads |
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