CN113481463A - Heat treatment process of piston - Google Patents

Heat treatment process of piston Download PDF

Info

Publication number
CN113481463A
CN113481463A CN202110101976.8A CN202110101976A CN113481463A CN 113481463 A CN113481463 A CN 113481463A CN 202110101976 A CN202110101976 A CN 202110101976A CN 113481463 A CN113481463 A CN 113481463A
Authority
CN
China
Prior art keywords
workpiece
cooling
heat treatment
temperature
annealing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202110101976.8A
Other languages
Chinese (zh)
Inventor
谢艳云
邱佳
刘少娟
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Changsha Chaojin'gang Machinery Manufacturing Co ltd
Original Assignee
Changsha Chaojin'gang Machinery Manufacturing Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Changsha Chaojin'gang Machinery Manufacturing Co ltd filed Critical Changsha Chaojin'gang Machinery Manufacturing Co ltd
Priority to CN202110101976.8A priority Critical patent/CN113481463A/en
Publication of CN113481463A publication Critical patent/CN113481463A/en
Pending legal-status Critical Current

Links

Images

Classifications

    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C8/00Solid state diffusion of only non-metal elements into metallic material surfaces; Chemical surface treatment of metallic material by reaction of the surface with a reactive gas, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C8/06Solid state diffusion of only non-metal elements into metallic material surfaces; Chemical surface treatment of metallic material by reaction of the surface with a reactive gas, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using gases
    • C23C8/08Solid state diffusion of only non-metal elements into metallic material surfaces; Chemical surface treatment of metallic material by reaction of the surface with a reactive gas, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using gases only one element being applied
    • C23C8/20Carburising
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C21D1/18Hardening; Quenching with or without subsequent tempering
    • C21D1/19Hardening; Quenching with or without subsequent tempering by interrupted quenching
    • C21D1/20Isothermal quenching, e.g. bainitic hardening
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C21D1/26Methods of annealing
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C21D1/26Methods of annealing
    • C21D1/28Normalising
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C21D1/78Combined heat-treatments not provided for above
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D9/00Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
    • C21D9/0068Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor for particular articles not mentioned below
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C8/00Solid state diffusion of only non-metal elements into metallic material surfaces; Chemical surface treatment of metallic material by reaction of the surface with a reactive gas, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C8/40Solid state diffusion of only non-metal elements into metallic material surfaces; Chemical surface treatment of metallic material by reaction of the surface with a reactive gas, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using liquids, e.g. salt baths, liquid suspensions
    • C23C8/42Solid state diffusion of only non-metal elements into metallic material surfaces; Chemical surface treatment of metallic material by reaction of the surface with a reactive gas, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using liquids, e.g. salt baths, liquid suspensions only one element being applied
    • C23C8/44Carburising
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C8/00Solid state diffusion of only non-metal elements into metallic material surfaces; Chemical surface treatment of metallic material by reaction of the surface with a reactive gas, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C8/60Solid state diffusion of only non-metal elements into metallic material surfaces; Chemical surface treatment of metallic material by reaction of the surface with a reactive gas, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using solids, e.g. powders, pastes
    • C23C8/62Solid state diffusion of only non-metal elements into metallic material surfaces; Chemical surface treatment of metallic material by reaction of the surface with a reactive gas, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using solids, e.g. powders, pastes only one element being applied
    • C23C8/64Carburising
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C8/00Solid state diffusion of only non-metal elements into metallic material surfaces; Chemical surface treatment of metallic material by reaction of the surface with a reactive gas, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C8/80After-treatment

Abstract

The invention provides a heat treatment process of a piston, which relates to the technical field of heat treatment of pistons, and comprises the following steps: s1, carburizing, namely firstly putting the workpiece into an active carburizing medium, then heating the workpiece to a single-phase austenite region with the temperature of 850-950 ℃, and after heat preservation is carried out for 5 to 11 hours, enabling active carbon atoms decomposed from the carburizing medium to permeate into the surface layer of the workpiece; s2, primary annealing, then putting the workpiece into a heat treatment furnace to be heated to a eutectoid temperature for annealing, carrying out heat preservation operation after annealing is finished, carrying out cooling operation after heat preservation is finished, and discharging from the furnace for air cooling after cooling is finished; s3, secondary annealing, heating the workpiece to eutectoid temperature for secondary annealing, preserving heat for 2-4h, cooling to 500-600 ℃, reheating to 745 ℃, and cooling to 580 ℃, wherein the surface layer high carbon is generated on the surface of the workpiece, so that the structural strength of the workpiece is enhanced, and meanwhile, the stability in the production process is good, the energy consumption is low, and the practical use is facilitated.

Description

Heat treatment process of piston
Technical Field
The invention relates to the technical field of piston heat treatment, in particular to a heat treatment process of a piston.
Background
The heat treatment is a metal hot working process which is characterized in that a metal material is placed in a certain medium for heating, heat preservation and cooling, and the performance of the metal material is controlled by changing the metallographic structure on the surface or in the material. The heat treatment process comprises three processes of heating, heat preservation and cooling, and sometimes only comprises two processes of heating and cooling. These processes are connected with each other without interruption. Heating is one of the important steps of heat treatment. The heating methods for metal heat treatment are many, and charcoal and coal were used as heat sources for the first time, and liquid and gaseous fuels were used. The application of electricity makes the heating easy to control and has no environmental pollution. The heat source may be used for direct heating or may be used for indirect heating of the floating particles by means of molten salts or metals.
The existing piston heat treatment process has the problem that the hardness of a processed piston is low in the practical application process, the piston is easy to crack in the practical application process, the abrasion resistance of the piston is poor, and scratches are easy to leave on the surface of the piston in the long-term use process.
Disclosure of Invention
The invention aims to solve the defects in the prior art and provides a heat treatment process of a piston.
In order to achieve the purpose, the invention adopts the following technical scheme: a heat treatment process for a piston, the heat treatment process for a piston comprising the steps of:
s1, carburizing, namely firstly putting the workpiece into an active carburizing medium, then heating the workpiece to a single-phase austenite region with the temperature of 850-950 ℃, and after heat preservation is carried out for 5 to 11 hours, enabling active carbon atoms decomposed from the carburizing medium to permeate into the surface layer of the workpiece;
s2, primary annealing, then putting the workpiece into a heat treatment furnace to be heated to a eutectoid temperature for annealing, carrying out heat preservation operation after annealing is finished, carrying out cooling operation after heat preservation is finished, and discharging from the furnace for air cooling after cooling is finished;
s3, secondary annealing, heating the workpiece to a eutectoid temperature for secondary annealing, preserving heat for 2-4h, cooling to 500-600 ℃, reheating to 745 ℃, and cooling to 580 ℃;
s4, normalizing, heating the workpiece to 900-;
s5, isothermal quenching, namely heating the workpiece to 855-;
s6, tempering, namely tempering the workpiece, and cooling to room temperature to obtain the workpiece with the pearlite content of more than 60%;
and S7, freezing, cooling the workpiece to 50 ℃ below zero, keeping for 3-4 h, cooling the workpiece to room temperature in air, and taking out the workpiece.
Further, in S1, after the activated carbon atoms penetrate into the surface layer of the workpiece, a surface layer high carbon may be generated on the surface of the workpiece.
Further, in S2, the eutectoid temperature is 720-920 ℃, the heat preservation time is 2.1-2.5h, and the temperature reduction temperature is 420-660 ℃.
Further, in S2, the tapping air cooling period is 1 h.
Further, in S5, the molten salt is a mixture of KNO3, NaNO2 and NaNO3, and the mass ratio of KNO3, NaNO2 and NaNO3 is 53: 40: 7.
further, in S6, the tempering temperature is 510-590 ℃, and the holding time is 2-3 h.
Further, in S6, after the workpiece is cooled to room temperature, the workpiece is left standing for 2 hours.
Further, in S7, the air cooling time is 5h, and the workpiece is taken out by vertically clamping the workpiece by the clamping hand.
Compared with the prior art, the surface layer high carbon is generated on the surface of the workpiece, so that the structural strength of the workpiece is enhanced, the surface layer high carbon can effectively prevent the workpiece from being scratched, the service life of the workpiece is prolonged to a certain extent, and meanwhile, the surface layer high carbon film has the characteristic of high production efficiency in practical application, has good stability in the production process and low energy consumption, accords with the environmental protection concept, has less pollution, is beneficial to environmental protection, and simultaneously produces a product with stable quality, and is beneficial to practical use.
Additional features and advantages of the invention will be set forth in the description which follows, and in part will be obvious from the description, or may be learned by practice of the invention. The objectives and other advantages of the invention will be realized and attained by the structure particularly pointed out in the written description and claims hereof as well as the appended drawings.
The technical solution of the present invention is further described in detail by the accompanying drawings and embodiments.
Drawings
In order to more clearly illustrate the embodiments or technical solutions of the present invention, the drawings used in the description of the embodiments or the prior art will be briefly introduced below, it is obvious that the drawings in the following description are only some embodiments of the present invention, and for those skilled in the art, other drawings can be obtained according to the drawings without creative efforts
Fig. 1 is a diagram illustrating a heat treatment process for a piston according to the present invention.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
In a first embodiment, referring to fig. 1, the heat treatment process of the piston includes the following steps:
s1, carburizing, namely firstly putting the workpiece into an active carburizing medium, then heating the workpiece to a single-phase austenite region at 850 ℃, and after heat preservation is carried out for 5 hours, enabling active carbon atoms decomposed from the carburizing medium to permeate into the surface layer of the workpiece;
s2, primary annealing, then putting the workpiece into a heat treatment furnace to be heated to a eutectoid temperature for annealing, carrying out heat preservation operation after annealing is finished, carrying out cooling operation after heat preservation is finished, and discharging from the furnace for air cooling after cooling is finished;
s3, secondary annealing, heating the workpiece to a eutectoid temperature for secondary annealing, preserving heat for 2 hours, cooling to 500 ℃, reheating to 745 ℃, and cooling to 580 ℃;
s4, normalizing, heating the workpiece to 925 ℃, preserving heat for 2h, and then carrying out air cooling after batch charging;
s5, isothermal quenching, namely heating the workpiece to 855 ℃, and then putting the workpiece into 250 ℃ molten salt for heat preservation for 1.2 h;
s6, tempering, namely tempering the workpiece, and cooling to room temperature to obtain the workpiece with the pearlite content of more than 60%;
and S7, freezing, cooling the workpiece to 50 ℃ below zero, keeping the temperature for 3 hours, and taking the workpiece out after the workpiece is cooled to room temperature by air.
Preferably, in S1, after the activated carbon atoms penetrate into the surface layer of the workpiece, a surface layer high carbon may be generated on the surface of the workpiece.
Preferably, in S2, the eutectoid temperature is 720 ℃, the heat preservation time is 2.1h, and the temperature for temperature reduction is 420 ℃.
Preferably, in S2, the tapping air cooling period is 1 h.
Preferably, in S5, the molten salt is a mixture of KNO3, NaNO2 and NaNO3, and the mass ratio among KNO3, NaNO2 and NaNO3 is 53: 40: 7.
preferably, in S6, the tempering temperature is 510 ℃ and the holding time is 2 h.
Preferably, in S6, after the workpiece is cooled to room temperature, the workpiece is left standing for 2 hours.
Preferably, in S7, the air cooling time is 5h, and the workpiece is taken out vertically by a gripper.
In a second embodiment, referring to fig. 1, the heat treatment process of the piston includes the following steps:
s1, carburizing, namely putting the workpiece into an active carburizing medium, heating to a single-phase austenite region at 860 ℃, and keeping the temperature for 7 hours to ensure that active carbon atoms decomposed from the carburizing medium permeate into the surface layer of the workpiece;
s2, primary annealing, then putting the workpiece into a heat treatment furnace to be heated to a eutectoid temperature for annealing, carrying out heat preservation operation after annealing is finished, carrying out cooling operation after heat preservation is finished, and discharging from the furnace for air cooling after cooling is finished;
s3, secondary annealing, heating the workpiece to a eutectoid temperature for secondary annealing, preserving heat for 3 hours, cooling to 510 ℃, reheating to 745 ℃, and cooling to 580 ℃;
s4, normalizing, heating the workpiece to 905 ℃, preserving heat for 2.5 hours, and then carrying out air cooling after batch charging;
s5, isothermal quenching, heating the workpiece to 857 ℃, and then putting the workpiece into 305 ℃ molten salt for heat preservation for 1.4 h;
s6, tempering, namely tempering the workpiece, and cooling to room temperature to obtain the workpiece with the pearlite content of more than 60%;
and S7, freezing, cooling the workpiece to 50 ℃ below zero, keeping the temperature for 3.2 hours, and taking the workpiece out after the workpiece is cooled to room temperature by air.
Preferably, in S1, after the activated carbon atoms penetrate into the surface layer of the workpiece, a surface layer high carbon may be generated on the surface of the workpiece.
Preferably, in S2, the eutectoid temperature is 735 ℃, the heat preservation time is 2.2h, and the temperature for temperature reduction is 460 ℃.
Preferably, in S2, the tapping air cooling period is 1 h.
Preferably, in S5, the molten salt is a mixture of KNO3, NaNO2 and NaNO3, and the mass ratio among KNO3, NaNO2 and NaNO3 is 53: 40: 7.
preferably, in S6, the tempering temperature is 520 ℃, and the holding time is 2.2 h.
Preferably, in S6, after the workpiece is cooled to room temperature, the workpiece is left standing for 2 hours.
Preferably, in S7, the air cooling time is 5h, and the workpiece is taken out vertically by a gripper.
In a third embodiment, referring to fig. 1, the heat treatment process of the piston includes the following steps:
s1, carburizing, namely putting the workpiece into an active carburizing medium, heating to a single-phase austenite region at 870 ℃, and after heat preservation for 7 hours, enabling active carbon atoms decomposed from the carburizing medium to permeate into the surface layer of the workpiece;
s2, primary annealing, then putting the workpiece into a heat treatment furnace to be heated to a eutectoid temperature for annealing, carrying out heat preservation operation after annealing is finished, carrying out cooling operation after heat preservation is finished, and discharging from the furnace for air cooling after cooling is finished;
s3, secondary annealing, heating the workpiece to a eutectoid temperature for secondary annealing, preserving heat for 2.8 hours, cooling to 509 ℃, reheating to 745 ℃, and cooling to 580 ℃;
s4, normalizing, heating the workpiece to 933 ℃, preserving heat for 2.8h, and then performing air cooling after batch furnace charging;
s5, isothermal quenching, namely heating the workpiece to 858 ℃, and then putting the workpiece into 260 ℃ molten salt for heat preservation for 2 hours;
s6, tempering, namely tempering the workpiece, and cooling to room temperature to obtain the workpiece with the pearlite content of more than 60%;
and S7, freezing, cooling the workpiece to 50 ℃ below zero, keeping for 4 hours, and taking out the workpiece after the workpiece is cooled to room temperature by air.
Preferably, in S1, after the activated carbon atoms penetrate into the surface layer of the workpiece, a surface layer high carbon may be generated on the surface of the workpiece.
Preferably, in S2, the eutectoid temperature is 790 ℃, the heat preservation time is 2.3 hours, and the temperature for temperature reduction is 550 ℃.
Preferably, in S2, the tapping air cooling period is 1 h.
Preferably, in S5, the molten salt is a mixture of KNO3, NaNO2 and NaNO3, and the mass ratio among KNO3, NaNO2 and NaNO3 is 53: 40: 7.
preferably, in S6, the tempering temperature is 540 ℃ and the holding time is 3 h.
Preferably, in S6, after the workpiece is cooled to room temperature, the workpiece is left standing for 2 hours.
Preferably, in S7, the air cooling time is 5h, and the workpiece is taken out vertically by a gripper.
In a fourth embodiment, referring to fig. 1, the heat treatment process of the piston includes the following steps:
s1, carburizing, namely firstly putting the workpiece into an active carburizing medium, then heating the workpiece to a single-phase austenite region at 950 ℃, and after heat preservation is carried out for 11 hours, enabling active carbon atoms decomposed from the carburizing medium to permeate into the surface layer of the workpiece;
s2, primary annealing, then putting the workpiece into a heat treatment furnace to be heated to a eutectoid temperature for annealing, carrying out heat preservation operation after annealing is finished, carrying out cooling operation after heat preservation is finished, and discharging from the furnace for air cooling after cooling is finished;
s3, secondary annealing, heating the workpiece to a eutectoid temperature for secondary annealing, preserving heat for 4 hours, cooling to 600 ℃, reheating to 745 ℃, and cooling to 580 ℃;
s4, normalizing, heating the workpiece to 940 ℃, preserving heat for 3 hours, and then carrying out air cooling after batch charging;
s5, isothermal quenching, namely heating the workpiece to 865 ℃, and then putting the workpiece into 310 ℃ molten salt for heat preservation for 2.5 hours;
s6, tempering, namely tempering the workpiece, and cooling to room temperature to obtain the workpiece with the pearlite content of more than 60%;
and S7, freezing, cooling the workpiece to 50 ℃ below zero, keeping for 4 hours, and taking out the workpiece after the workpiece is cooled to room temperature by air.
Preferably, in S1, after the activated carbon atoms penetrate into the surface layer of the workpiece, a surface layer high carbon may be generated on the surface of the workpiece.
Preferably, in S2, the eutectoid temperature is 920 ℃, the heat preservation time is 2.5 hours, and the temperature for temperature reduction is 660 ℃.
Preferably, in S2, the tapping air cooling period is 1 h.
Preferably, in S5, the molten salt is a mixture of KNO3, NaNO2 and NaNO3, and the mass ratio among KNO3, NaNO2 and NaNO3 is 53: 40: 7.
preferably, in S6, the tempering temperature is 590 ℃, and the holding time is 3 h.
Preferably, in S6, after the workpiece is cooled to room temperature, the workpiece is left standing for 2 hours.
Preferably, in S7, the air cooling time is 5h, and the workpiece is taken out vertically by a gripper.
The workpieces prepared in the first to fourth examples were subjected to the following performance tests:
and (3) testing hardness performance: the hardness test is carried out on an HRS-150 Rockwell hardness tester, and the test loading force is 150kgThe test force retention time was 8 seconds.
And (3) testing tensile property: processing the material into a tensile sample according to GBT228.1-2010 metal material tensile test, wherein the tensile speed in the test is 2mm/min, the extensometer is Y25/5-N type, and the precision grade is 0.5.
And (3) impact performance test: the samples were prepared by wire cutting into standard impact specimens, and the dimensional deviation of the specimens should be strictly controlled in terms of shape, size and surface roughness according to GB/T229-1994.
The results are shown in Table 1.
Table 1 performance test data
Test specimen HRC Tensile strength (MPa) Yield strength (MPa) Impact work (J)
Example one 48.8 989 596 156
Example two 47.6 976 582 146
EXAMPLE III 45.8 968 559 145
Example four 46.1 912 586 155
As can be seen from the data in table 1, the first to fourth examples all have good performance, and the first example is the most preferable example, which has the highest hardness of 48.8HRC and the highest strength.
It will be apparent to those skilled in the art that various changes and modifications may be made in the present invention without departing from the spirit and scope of the invention. Thus, if such modifications and variations of the present invention fall within the scope of the claims of the present invention and their equivalents, the present invention is also intended to include such modifications and variations.

Claims (8)

1. The heat treatment process of the piston is characterized by comprising the following steps of:
s1, carburizing, namely firstly putting the workpiece into an active carburizing medium, then heating the workpiece to a single-phase austenite region with the temperature of 850-950 ℃, and after heat preservation is carried out for 5 to 11 hours, enabling active carbon atoms decomposed from the carburizing medium to permeate into the surface layer of the workpiece;
s2, primary annealing, then putting the workpiece into a heat treatment furnace to be heated to a eutectoid temperature for annealing, carrying out heat preservation operation after annealing is finished, carrying out cooling operation after heat preservation is finished, and discharging from the furnace for air cooling after cooling is finished;
s3, secondary annealing, heating the workpiece to a eutectoid temperature for secondary annealing, preserving heat for 2-4h, cooling to 500-600 ℃, reheating to 745 ℃, and cooling to 580 ℃;
s4, normalizing, heating the workpiece to 900-;
s5, isothermal quenching, namely heating the workpiece to 855-;
s6, tempering, namely tempering the workpiece, and cooling to room temperature to obtain the workpiece with the pearlite content of more than 60%;
and S7, freezing, cooling the workpiece to 50 ℃ below zero, keeping for 3-4 h, cooling the workpiece to room temperature in air, and taking out the workpiece.
2. A heat treatment process for a piston according to claim 1, wherein: in S1, after the activated carbon atoms penetrate into the surface layer of the workpiece, a surface layer high carbon may be generated on the surface of the workpiece.
3. A heat treatment process for a piston according to claim 1, wherein: in S2, the eutectoid temperature is 720-920 ℃, the heat preservation time is 2.1-2.5h, and the temperature reduction temperature is 420-660 ℃.
4. A heat treatment process for a piston according to claim 1, wherein: in S2, the tapping air cooling period is 1 h.
5. A heat treatment process for a piston according to claim 1, wherein: in S5, the molten salt is a mixture of KNO3, NaNO2 and NaNO3, and the mass ratio among KNO3, NaNO2 and NaNO3 is 53: 40: 7.
6. a heat treatment process for a piston according to claim 1, wherein: in S6, the tempering temperature is 510-590 ℃, and the holding time is 2-3 h.
7. A heat treatment process for a piston according to claim 1, wherein: in S6, after the workpiece is cooled to room temperature, the workpiece is left standing for 2 hours.
8. A heat treatment process for a piston according to claim 1, wherein: in S7, the air cooling time is 5h, and the workpiece is taken out vertically by the gripper.
CN202110101976.8A 2021-01-26 2021-01-26 Heat treatment process of piston Pending CN113481463A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202110101976.8A CN113481463A (en) 2021-01-26 2021-01-26 Heat treatment process of piston

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202110101976.8A CN113481463A (en) 2021-01-26 2021-01-26 Heat treatment process of piston

Publications (1)

Publication Number Publication Date
CN113481463A true CN113481463A (en) 2021-10-08

Family

ID=77933315

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202110101976.8A Pending CN113481463A (en) 2021-01-26 2021-01-26 Heat treatment process of piston

Country Status (1)

Country Link
CN (1) CN113481463A (en)

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102424976A (en) * 2011-11-28 2012-04-25 湖南志辉矿山机械有限公司 Heat treatment process of down-the-hole hammer piston
CN102776471A (en) * 2012-07-10 2012-11-14 镇江中船设备有限公司 Carburizing quenching technology for low-carbon alloy steel parts
CN108070703A (en) * 2016-11-18 2018-05-25 贵州宏博轴承有限公司 A kind of bearing heat treatment process
CN108950467A (en) * 2018-08-15 2018-12-07 上海精科粉末冶金科技有限公司 A kind of dedicated carburizing and quenching furnace technology of MIM iron-base part
KR101959985B1 (en) * 2018-11-16 2019-03-20 석재현 Method of heat treatment of metal parts
CN110157868A (en) * 2019-06-28 2019-08-23 含山县兴达球墨铸铁厂 A kind of heat treatment process of spheroidal graphite cast-iron Piston Casting

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102424976A (en) * 2011-11-28 2012-04-25 湖南志辉矿山机械有限公司 Heat treatment process of down-the-hole hammer piston
CN102776471A (en) * 2012-07-10 2012-11-14 镇江中船设备有限公司 Carburizing quenching technology for low-carbon alloy steel parts
CN108070703A (en) * 2016-11-18 2018-05-25 贵州宏博轴承有限公司 A kind of bearing heat treatment process
CN108950467A (en) * 2018-08-15 2018-12-07 上海精科粉末冶金科技有限公司 A kind of dedicated carburizing and quenching furnace technology of MIM iron-base part
KR101959985B1 (en) * 2018-11-16 2019-03-20 석재현 Method of heat treatment of metal parts
CN110157868A (en) * 2019-06-28 2019-08-23 含山县兴达球墨铸铁厂 A kind of heat treatment process of spheroidal graphite cast-iron Piston Casting

Similar Documents

Publication Publication Date Title
CN108517461B (en) High-performance martensitic stainless steel flange and manufacturing method thereof
CN103454123A (en) Preparation method for high-hardness standard Brinell hardness block
CN101648334A (en) Manufacturing technique of austenitic stainless steel cold-rolled plate with good surface performance
CN105369015A (en) 42 CrMo shaft part quenching and heat-treatment technology
CN109778109B (en) Method for solving problem of unqualified carbonitriding quality
CN104232859B (en) A kind of GCr15SiMn Heat Treatment Of Steel method
CN109371212B (en) Large-deformation-enhanced rapid ion nitriding method
CN114433648A (en) Cold-drawing processing method of high-carbon chromium bearing steel guide rail blank
CN113481463A (en) Heat treatment process of piston
US2679466A (en) Surface decarburization of carboncontaining alloys
CN111074046A (en) Environment-friendly water-soluble quenching liquid and preparation method thereof
CN114369702A (en) Quenching method of Cr12 roller
CN112609124A (en) 1Cr17Ni2 stainless steel screw and heat treatment process thereof
CN111455143A (en) Heat treatment method for low-temperature 9Ni steel two-phase region quenching
CN110918864A (en) Forging method of cross shaft forging
CN114589456B (en) Production process of high-nitrogen stainless steel ball
CN114959215B (en) 7-series aluminum alloy hot extrusion die steel and heat treatment method thereof
CN109136494A (en) Quenching oil is used in a kind of production of leaf spring
CN113523165B (en) Hydrogen sulfide resistant stainless steel forging for oil exploitation operation and preparation method thereof
CN113088639B (en) Bearing steel pipe inspection quality control method for cold rolling and expanding bearing
CN115287584B (en) Carburizing and quenching method for medium alloy carburizing steel
CN114603079B (en) Carbide refining method for flat-bottom bearing ring
CN114990292B (en) Heat treatment method for hot work die steel
Tashkoziyeva MATERIALS FOR CEMENTING THE SURFACES OF DETAILS AND THEIR STANDARDIZATION
CN115385723A (en) Method for improving mechanical property of Sialon ceramic product

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20211008