CN113402319A - Slow-release fertilizer for rape and preparation method thereof - Google Patents
Slow-release fertilizer for rape and preparation method thereof Download PDFInfo
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- CN113402319A CN113402319A CN202110610548.8A CN202110610548A CN113402319A CN 113402319 A CN113402319 A CN 113402319A CN 202110610548 A CN202110610548 A CN 202110610548A CN 113402319 A CN113402319 A CN 113402319A
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- fertilizer
- rape
- sulfate
- slow release
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- 239000003337 fertilizer Substances 0.000 title claims abstract description 83
- 238000002360 preparation method Methods 0.000 title abstract description 6
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 claims abstract description 26
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 claims abstract description 26
- 108010020346 Polyglutamic Acid Proteins 0.000 claims abstract description 23
- 229920002643 polyglutamic acid Polymers 0.000 claims abstract description 23
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 20
- 229910052700 potassium Inorganic materials 0.000 claims abstract description 19
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims abstract description 17
- 229940090496 Urease inhibitor Drugs 0.000 claims abstract description 17
- 239000011591 potassium Substances 0.000 claims abstract description 17
- 239000002601 urease inhibitor Substances 0.000 claims abstract description 17
- 239000007952 growth promoter Substances 0.000 claims abstract description 14
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims abstract description 13
- LFVGISIMTYGQHF-UHFFFAOYSA-N ammonium dihydrogen phosphate Chemical compound [NH4+].OP(O)([O-])=O LFVGISIMTYGQHF-UHFFFAOYSA-N 0.000 claims abstract description 13
- 229910000387 ammonium dihydrogen phosphate Inorganic materials 0.000 claims abstract description 13
- APUPEJJSWDHEBO-UHFFFAOYSA-P ammonium molybdate Chemical compound [NH4+].[NH4+].[O-][Mo]([O-])(=O)=O APUPEJJSWDHEBO-UHFFFAOYSA-P 0.000 claims abstract description 13
- 239000011609 ammonium molybdate Substances 0.000 claims abstract description 13
- 235000018660 ammonium molybdate Nutrition 0.000 claims abstract description 13
- 229940010552 ammonium molybdate Drugs 0.000 claims abstract description 13
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000004327 boric acid Substances 0.000 claims abstract description 13
- 239000004202 carbamide Substances 0.000 claims abstract description 13
- 239000011790 ferrous sulphate Substances 0.000 claims abstract description 13
- 235000003891 ferrous sulphate Nutrition 0.000 claims abstract description 13
- BAUYGSIQEAFULO-UHFFFAOYSA-L iron(2+) sulfate (anhydrous) Chemical compound [Fe+2].[O-]S([O-])(=O)=O BAUYGSIQEAFULO-UHFFFAOYSA-L 0.000 claims abstract description 13
- 229910000359 iron(II) sulfate Inorganic materials 0.000 claims abstract description 13
- 229910052943 magnesium sulfate Inorganic materials 0.000 claims abstract description 13
- 235000019341 magnesium sulphate Nutrition 0.000 claims abstract description 13
- 235000019837 monoammonium phosphate Nutrition 0.000 claims abstract description 13
- 239000006012 monoammonium phosphate Substances 0.000 claims abstract description 13
- 239000001103 potassium chloride Substances 0.000 claims abstract description 13
- 235000011164 potassium chloride Nutrition 0.000 claims abstract description 13
- OTYBMLCTZGSZBG-UHFFFAOYSA-L potassium sulfate Chemical compound [K+].[K+].[O-]S([O-])(=O)=O OTYBMLCTZGSZBG-UHFFFAOYSA-L 0.000 claims abstract description 13
- 229910052939 potassium sulfate Inorganic materials 0.000 claims abstract description 13
- 235000011151 potassium sulphates Nutrition 0.000 claims abstract description 13
- NWONKYPBYAMBJT-UHFFFAOYSA-L zinc sulfate Chemical compound [Zn+2].[O-]S([O-])(=O)=O NWONKYPBYAMBJT-UHFFFAOYSA-L 0.000 claims abstract description 13
- 229960001763 zinc sulfate Drugs 0.000 claims abstract description 13
- 229910000368 zinc sulfate Inorganic materials 0.000 claims abstract description 13
- PUKLDDOGISCFCP-JSQCKWNTSA-N 21-Deoxycortisone Chemical compound C1CC2=CC(=O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@@](C(=O)C)(O)[C@@]1(C)CC2=O PUKLDDOGISCFCP-JSQCKWNTSA-N 0.000 claims abstract description 7
- FCYKAQOGGFGCMD-UHFFFAOYSA-N Fulvic acid Natural products O1C2=CC(O)=C(O)C(C(O)=O)=C2C(=O)C2=C1CC(C)(O)OC2 FCYKAQOGGFGCMD-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000000945 filler Substances 0.000 claims abstract description 7
- 239000002509 fulvic acid Substances 0.000 claims abstract description 7
- 229940095100 fulvic acid Drugs 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 5
- 238000003756 stirring Methods 0.000 claims description 37
- QJZYHAIUNVAGQP-UHFFFAOYSA-N 3-nitrobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid Chemical compound C1C2C=CC1C(C(=O)O)C2(C(O)=O)[N+]([O-])=O QJZYHAIUNVAGQP-UHFFFAOYSA-N 0.000 claims description 19
- 239000004021 humic acid Substances 0.000 claims description 19
- 239000000463 material Substances 0.000 claims description 19
- 238000010438 heat treatment Methods 0.000 claims description 14
- 239000000843 powder Substances 0.000 claims description 14
- 239000008187 granular material Substances 0.000 claims description 13
- 238000002156 mixing Methods 0.000 claims description 12
- 239000002002 slurry Substances 0.000 claims description 11
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical group [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 8
- 238000000034 method Methods 0.000 claims description 8
- 229910052757 nitrogen Inorganic materials 0.000 claims description 8
- 229910052698 phosphorus Inorganic materials 0.000 claims description 7
- 238000012216 screening Methods 0.000 claims description 5
- 238000007873 sieving Methods 0.000 claims description 5
- 229910000019 calcium carbonate Inorganic materials 0.000 claims description 4
- 239000000284 extract Substances 0.000 claims description 4
- 239000011777 magnesium Substances 0.000 claims description 4
- 229910052749 magnesium Inorganic materials 0.000 claims description 4
- 239000002207 metabolite Substances 0.000 claims description 4
- 230000000813 microbial effect Effects 0.000 claims description 4
- 239000002245 particle Substances 0.000 claims description 3
- 229920001282 polysaccharide Polymers 0.000 claims description 3
- 239000005017 polysaccharide Substances 0.000 claims description 3
- 230000001737 promoting effect Effects 0.000 claims description 3
- 229910052717 sulfur Inorganic materials 0.000 claims description 3
- 108010016626 Dipeptides Proteins 0.000 claims description 2
- 239000004480 active ingredient Substances 0.000 claims description 2
- 150000001413 amino acids Chemical class 0.000 claims description 2
- 229960002645 boric acid Drugs 0.000 claims description 2
- 235000010338 boric acid Nutrition 0.000 claims description 2
- 150000001720 carbohydrates Chemical class 0.000 claims description 2
- 229910052799 carbon Inorganic materials 0.000 claims description 2
- 229910052801 chlorine Inorganic materials 0.000 claims description 2
- 239000011248 coating agent Substances 0.000 claims description 2
- 238000000576 coating method Methods 0.000 claims description 2
- 238000001816 cooling Methods 0.000 claims description 2
- 125000004122 cyclic group Chemical group 0.000 claims description 2
- 229960001781 ferrous sulfate Drugs 0.000 claims description 2
- 229910052739 hydrogen Inorganic materials 0.000 claims description 2
- 229960003390 magnesium sulfate Drugs 0.000 claims description 2
- 229910052760 oxygen Inorganic materials 0.000 claims description 2
- 239000002718 pyrimidine nucleoside Substances 0.000 claims description 2
- 229910052708 sodium Inorganic materials 0.000 claims description 2
- 238000005303 weighing Methods 0.000 claims description 2
- 150000004676 glycans Chemical class 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 12
- 238000011161 development Methods 0.000 abstract description 5
- 235000015816 nutrient absorption Nutrition 0.000 abstract description 4
- 238000003973 irrigation Methods 0.000 abstract description 2
- 230000002262 irrigation Effects 0.000 abstract description 2
- 238000006243 chemical reaction Methods 0.000 description 16
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 12
- 239000002689 soil Substances 0.000 description 12
- 230000000052 comparative effect Effects 0.000 description 9
- 239000011573 trace mineral Substances 0.000 description 8
- 235000013619 trace mineral Nutrition 0.000 description 8
- 238000002474 experimental method Methods 0.000 description 7
- 235000015097 nutrients Nutrition 0.000 description 7
- 150000001875 compounds Chemical class 0.000 description 6
- 241000196324 Embryophyta Species 0.000 description 5
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 5
- 239000011574 phosphorus Substances 0.000 description 5
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 4
- 239000011575 calcium Substances 0.000 description 4
- 229910052791 calcium Inorganic materials 0.000 description 4
- 230000004720 fertilization Effects 0.000 description 4
- 238000011282 treatment Methods 0.000 description 4
- 108010046334 Urease Proteins 0.000 description 3
- 238000010521 absorption reaction Methods 0.000 description 3
- 229940047608 chelated magnesium Drugs 0.000 description 3
- -1 magnesium iron zinc molybdenum boron salt Chemical compound 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 239000003921 oil Substances 0.000 description 3
- 238000004806 packaging method and process Methods 0.000 description 3
- 238000004064 recycling Methods 0.000 description 3
- 150000003839 salts Chemical class 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 2
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 2
- 240000002791 Brassica napus Species 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 2
- 208000027418 Wounds and injury Diseases 0.000 description 2
- 239000013543 active substance Substances 0.000 description 2
- 239000000783 alginic acid Substances 0.000 description 2
- 235000010443 alginic acid Nutrition 0.000 description 2
- 229920000615 alginic acid Polymers 0.000 description 2
- 229960001126 alginic acid Drugs 0.000 description 2
- 150000004781 alginic acids Chemical class 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 229910052796 boron Inorganic materials 0.000 description 2
- 230000006378 damage Effects 0.000 description 2
- 238000013461 design Methods 0.000 description 2
- 239000008157 edible vegetable oil Substances 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000002650 habitual effect Effects 0.000 description 2
- 208000014674 injury Diseases 0.000 description 2
- 150000002596 lactones Chemical class 0.000 description 2
- 239000000618 nitrogen fertilizer Substances 0.000 description 2
- 150000004804 polysaccharides Chemical class 0.000 description 2
- 208000024891 symptom Diseases 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- FPIPGXGPPPQFEQ-UHFFFAOYSA-N 13-cis retinol Natural products OCC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-UHFFFAOYSA-N 0.000 description 1
- 241000219198 Brassica Species 0.000 description 1
- 235000011293 Brassica napus Nutrition 0.000 description 1
- 235000004977 Brassica sinapistrum Nutrition 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
- 102000018997 Growth Hormone Human genes 0.000 description 1
- 108010051696 Growth Hormone Proteins 0.000 description 1
- 241000238631 Hexapoda Species 0.000 description 1
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 1
- 231100000674 Phytotoxicity Toxicity 0.000 description 1
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- FPIPGXGPPPQFEQ-BOOMUCAASA-N Vitamin A Natural products OC/C=C(/C)\C=C\C=C(\C)/C=C/C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-BOOMUCAASA-N 0.000 description 1
- 229930003316 Vitamin D Natural products 0.000 description 1
- QYSXJUFSXHHAJI-XFEUOLMDSA-N Vitamin D3 Natural products C1(/[C@@H]2CC[C@@H]([C@]2(CCC1)C)[C@H](C)CCCC(C)C)=C/C=C1\C[C@@H](O)CCC1=C QYSXJUFSXHHAJI-XFEUOLMDSA-N 0.000 description 1
- 229930003427 Vitamin E Natural products 0.000 description 1
- 241000607479 Yersinia pestis Species 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- PNNCWTXUWKENPE-UHFFFAOYSA-N [N].NC(N)=O Chemical compound [N].NC(N)=O PNNCWTXUWKENPE-UHFFFAOYSA-N 0.000 description 1
- FPIPGXGPPPQFEQ-OVSJKPMPSA-N all-trans-retinol Chemical compound OC\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-OVSJKPMPSA-N 0.000 description 1
- 150000001408 amides Chemical class 0.000 description 1
- XKMRRTOUMJRJIA-UHFFFAOYSA-N ammonia nh3 Chemical compound N.N XKMRRTOUMJRJIA-UHFFFAOYSA-N 0.000 description 1
- 238000003556 assay Methods 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 239000013522 chelant Substances 0.000 description 1
- 238000012258 culturing Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 235000005911 diet Nutrition 0.000 description 1
- 230000000378 dietary effect Effects 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 210000005069 ears Anatomy 0.000 description 1
- 238000004134 energy conservation Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000000855 fermentation Methods 0.000 description 1
- 230000004151 fermentation Effects 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 description 1
- 238000005469 granulation Methods 0.000 description 1
- 230000003179 granulation Effects 0.000 description 1
- 239000000122 growth hormone Substances 0.000 description 1
- 238000003306 harvesting Methods 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 229910017053 inorganic salt Inorganic materials 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 239000002609 medium Substances 0.000 description 1
- 235000010755 mineral Nutrition 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 239000002686 phosphate fertilizer Substances 0.000 description 1
- 230000010152 pollination Effects 0.000 description 1
- 229940072033 potash Drugs 0.000 description 1
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 1
- 235000015320 potassium carbonate Nutrition 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000010193 shuanglong Substances 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 238000002560 therapeutic procedure Methods 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 235000019155 vitamin A Nutrition 0.000 description 1
- 239000011719 vitamin A Substances 0.000 description 1
- 235000019166 vitamin D Nutrition 0.000 description 1
- 239000011710 vitamin D Substances 0.000 description 1
- 150000003710 vitamin D derivatives Chemical class 0.000 description 1
- 235000019165 vitamin E Nutrition 0.000 description 1
- 229940046009 vitamin E Drugs 0.000 description 1
- 239000011709 vitamin E Substances 0.000 description 1
- 229940045997 vitamin a Drugs 0.000 description 1
- 229940046008 vitamin d Drugs 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/40—Mixtures of one or more fertilisers with additives not having a specially fertilising activity for affecting fertiliser dosage or release rate; for affecting solubility
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/90—Mixtures of one or more fertilisers with additives not having a specially fertilising activity for affecting the nitrification of ammonium compounds or urea in the soil
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Pest Control & Pesticides (AREA)
- Soil Sciences (AREA)
- Fertilizers (AREA)
Abstract
The invention provides a slow release fertilizer for rape and a preparation method thereof, wherein the fertilizer comprises the following raw materials of 370-400 parts of urea, 130-160 parts of monoammonium phosphate, 20-40 parts of potassium chloride, 240-270 parts of potassium sulfate, 20-30 parts of magnesium sulfate, 6-8 parts of zinc sulfate, 2-6 parts of ferrous sulfate, 0.5-1 part of ammonium molybdate, 15-25 parts of boric acid, 8-10 parts of polyglutamic acid, 6-10 parts of potassium fulvic acid, 0.01-0.02 part of intelligent agent, 0.01-0.02 part of growth promoter, 100-125 parts of filler and 1-3 parts of urease inhibitor. The special fertilizer formula designed according to the normal growth, development and cultivation characteristics of the rape, irrigation habits and nutrient absorption rules provides a researched combined formula aiming at the characteristics and fertilizer preference characteristics of the rape, and can be used as a base fertilizer or an additional fertilizer to improve the yield and stress resistance of the rape; the slow release fertilizer also has the slow release effect, can promote the nutrient absorption of the rape, and improves the utilization rate of effective components in the fertilizer, thereby reducing the using amount of the fertilizer.
Description
Technical Field
The invention relates to the field of fertilizers; more particularly relates to a slow release fertilizer for rape and a preparation method thereof.
Background
1-year-old herbaceous plants of brassica brassicaceae, which are important oil crops in China, play a key role in ensuring the safety of edible oil in China. The rape is rich in various vitamins such as vitamin A, vitamin D and vitamin E, has high nutritive value and comprehensive dietary therapy value, is not only good edible oil, but also has wide industrial application. The development of rape production has important significance for improving the life of people and increasing the income of the masses. With the continuous improvement of the yield per unit of rape, a large amount of nutrients must be taken away from the soil, the application of nitrogen, phosphorus and potassium fertilizers is often considered in the actual production, the current situation that trace elements in the soil are deficient is increasingly aggravated by neglecting the application of medium trace element fertilizers, and the medium trace elements are very likely to become new limiting factors of the yield of the rape.
Rape is sensitive to the reaction of phosphorus, potassium and boron. When the content of the available phosphorus in the soil is less than 5mg/kg, the phosphorus deficiency symptom is obvious, and meanwhile, the content of the available boron in the soil is required to be higher than 0.5mg/kg and is 5 times higher than other crops. According to the research, each 100kg of rapeseed produced needs to absorb 8.8-11.3 kg of N and P2O53.0～3.9kg、K28.5-10.1 kg of O, the fertilizer ratio is about 3: 1: 3, and other trace elements are needed, according to the theory of short plates of the wooden barrel, if other nutrients are lacked, the plant cannot grow normally, is thin and small, has irregular ears, is low in pollination rate, and seriously affects the yield.
Firstly, adopting simple substance nitrogen fertilizer, phosphate fertilizer and potash fertilizer to artificially prepare and apply rape according to the required amount; and secondly, granulating the compound fertilizer by adopting a steam rotary drum physical granulation method. The two modes have the defects of low fertilizer efficiency utilization rate, energy conservation and environmental protection.
Disclosure of Invention
The invention provides a slow release fertilizer for rape and a preparation method thereof, and the slow release fertilizer has the characteristics of complete nutrients, uniform release and no seedling burning.
The technical scheme of the invention is that the slow release fertilizer for rape comprises the following raw materials in parts by weight: 370-400 parts of urea, 130-160 parts of monoammonium phosphate, 20-40 parts of potassium chloride, 240-270 parts of potassium sulfate, 20-30 parts of magnesium sulfate, 6-8 parts of zinc sulfate, 2-6 parts of ferrous sulfate, 0.5-1 part of ammonium molybdate, 15-25 parts of boric acid, 8-10 parts of polyglutamic acid, 6-10 parts of brown yellow humic acid, 0.01-0.02 part of intelligent agent, 0.01-0.02 part of growth promoter, 100-125 parts of filler and 1-3 parts of urease inhibitor.
In the preferable scheme, the fertilizer comprises 385 parts of urea, 146 parts of monoammonium phosphate, 30 parts of potassium chloride, 255 parts of potassium sulfate, 25 parts of magnesium sulfate, 7 parts of zinc sulfate, 4 parts of ferrous sulfate, 1 part of ammonium molybdate, 20 parts of boric acid, 10 parts of polyglutamic acid, 10 parts of brown yellow humic acid, 0.01 part of intelligent agent, 0.015 part of growth promoter, 105 parts of filler and 2 parts of urease inhibitor.
Further, the filler is calcium carbonate.
Further, the humic acid content of the brown fulvic acid is more than 60 wt%, and the fulvic acid content is more than 20wt% in terms of dry basis.
Furthermore, the growth hormone contains 5% of microbial metabolites, 90% of polysaccharide and the balance organic matters.
Furthermore, the intelligent agent is a plant endophyte extract, and active ingredients of the intelligent agent comprise cyclic dipeptides, pyrimidine nucleosides, amino acids and saccharides; wherein C, H, O, N, P, S element accounts for more than 94% of the total extract, Na, K, Cl and Mg account for more than 5%, and the rest is microelement. The intelligent activity is 10 times of that of sphacelainide lactone, 10000 times of that of fulvic acid and 100000 times of that of humic acid and alginic acid.
The invention also relates to a method for preparing the slow release fertilizer for rape, which comprises the following steps:
s1, weighing the raw materials according to the proportion, and then uniformly mixing urea and a urease inhibitor;
s2, heating, stirring and uniformly mixing the material obtained in the step S1 with potassium sulfate, potassium chloride and monoammonium phosphate to form slurry in a molten state;
s3, heating, stirring and uniformly mixing magnesium sulfate, zinc sulfate, ferrous sulfate, ammonium molybdate, boric acid and polyglutamic acid;
s4, enabling the material obtained in the step S2 to flow into the material S3, adding the brown yellow humic acid potassium and the intelligent growth promoting agent, heating and mixing uniformly; throwing and granulating the formed slurry from high altitude, and then screening; and finally, obtaining a fertilizer with the particle diameter of 2-4 mm, and cooling, coating and anti-caking to obtain the slow release fertilizer for the rape.
Furthermore, the heating temperature in S2 is 115-118 ℃, the stirring speed is 130-150 r/min, and the stirring time is 3-5 min.
Further, the heating temperature in S3 is 50-70 ℃, the stirring speed is 30-50 r/min, and the stirring time is 30-35 min.
Further, in the case of the sifting in S4, a powder material of 2 mm or less and particles of 4 mm or more are sifted out, and the sifted material is returned to the step S2, and is mixed with the material obtained in S1.
The invention has the following beneficial effects:
1. the medium trace elements in the fertilizer are added in the form of inorganic salt, and are not added in the form of chelating salt, so that the cost can be saved; by adding polyglutamic acid, the polyglutamic acid can form chelate salt with medium and trace elements, so that sulfate, oxalate, carbonate and the like in fertilizer and soil are effectively prevented from being combined with the medium and trace elements such as magnesium, zinc, iron and the like, low-solubility salts and precipitation are avoided, the slow-release effect is achieved, the absorption effect of crops is improved, the utilization is more sufficient, the development of root systems is promoted, and the resistance is enhanced.
2. The N source in the invention is amide nitrogen which is easy to be absorbed by crops, but the slow release effect is poor, and the urease inhibitor is added into the fertilizer, so that the slow release effect is good.
3. The intelligent smart fertilizer synergist can improve the drought resistance and cold resistance of crops, relieve the symptoms of plant diseases and insect pests, phytotoxicity, fertilizer injury and freezing injury of the crops, and is beneficial to the safe overwintering of rapes.
4. The potassium fulvate and the growth promoter are rich in micromolecular active substances, can effectively promote the growth and development of plants and improve the yield of rape.
5. The invention designs a special fertilizer formula according to the normal growth, development and cultivation characteristics of rape, irrigation habit and nutrient absorption rule, provides a researched combined formula aiming at the characteristics and fertilizer preference characteristics of rape, wherein the formula contains three major elements of nitrogen, phosphorus and potassium, medium elements of sulfur, magnesium and the like, humic acid organic matter and polyglutamic acid chelated trace elements. Thereby having the characteristics of complete nutrients, uniform release and no seedling burning. The fertilizer can be used as a rape fertilizer, can be used as a base fertilizer or an additional fertilizer, improves the yield and the stress resistance of rape, simplifies the fertilization times and improves the yield; the slow release effect can promote the nutrient absorption of the rape, and the utilization rate of effective components in the fertilizer is improved, so that the using amount of the fertilizer is reduced; the quality of crops is improved, the method is green and environment-friendly, the oil yield is high, the quality is good, and the commodity performance is obviously improved.
Drawings
FIG. 1 is a graph of the effect of different treatments on soil urease activity in assay one.
FIG. 2 shows NH of soil by different treatments in experiment I4 +-influence graph of N content.
Detailed Description
Embodiments of the present invention will be described in detail below with reference to examples, but those skilled in the art will appreciate that the following examples are only illustrative of the present invention and should not be construed as limiting the scope of the present invention.
Example 1:
a slow release fertilizer for rape is prepared from 370 kg of urea, 155 kg of monoammonium phosphate, 25kg of potassium chloride, 265 kg of potassium sulfate, 27 kg of magnesium sulfate, 8 kg of zinc sulfate, 2kg of ferrous sulfate, 1kg of ammonium molybdate, 23 kg of boric acid, 8 kg of polyglutamic acid, 6kg of brown yellow potassium humate, 0.01kg of intelligent agent, 0.01kg of growth promoter, 108 kg of calcium carbonate powder and 2kg of urease inhibitor.
The brown yellow humic acid potassium is preferably produced by Xinjiang Shuanglong humic acid Limited company, and is a product which is processed by natural mineral humic acid and contains both brown black humic acid with large molecular weight and yellow humic acid with small molecular weight.
The polyglutamic acid is produced by Nanjing Xuan Kai Biotechnology Limited and is an ecological fertilizer auxiliary agent prepared by microbial fermentation, the utilization rate of the added synergistic fertilizer can be improved from 30-35% to 40-50%, and the average utilization rate of the fertilizer is improved by 8%.
The urease inhibitor is specifically NBPT.
The growth promoter contains microbial metabolite 5%, polysaccharide 90%, and other organic substances 5%. Preferred is a bio-stimulant of Wuhan Borun science and technology, Inc.
The intelligent agent is produced by Shandong Bobo biotechnology (Wuhan) Limited company, is a metabolite mixture of endophytes, has activity 10 times of cloud moss lactone, 10000 times of fulvic acid and 100000 times of humic acid and alginic acid.
The specific production process of the slow release fertilizer comprises the following steps: uniformly mixing 2kg of urease inhibitor and 370 kg of urea, conveying the mixture into a reaction kettle A through a conveyor belt, mixing and heating the mixture with 265 kg of potassium sulfate, 25kg of potassium chloride, 155 kg of monoammonium phosphate and system return materials, stirring at the speed of 130 revolutions per minute and the temperature of 115-118 ℃, and stirring for 3 minutes; 8 kg of polyglutamic acid, 27 kg of magnesium sulfate, 8 kg of zinc sulfate, 23 kg of boric acid, 2kg of ferrous sulfate and 1kg of ammonium molybdate which are conveyed in a metering way are stirred and chelated in a reaction kettle B at the stirring temperature of 50-70 ℃, the stirring speed of 30 r/min and the stirring time of 30 min to form stable polyglutamic acid chelated magnesium iron zinc molybdenum boron salt; feeding the material in the reaction kettle A into a reaction kettle B, adding 6kg of brown yellow potassium humate, 0.01kg of intelligent agent, 0.01kg of growth promoter and 108 kg of calcium carbonate powder according to parts by mass, heating and stirring at the stirring speed of 200 revolutions per minute at the stirring temperature of 100-110 ℃ for 1 minute; the chelating slurry is scattered from the high altitude, the surface tension reason is changed into a spherical shape when the chelating slurry is scattered, the chelating slurry exchanges heat with the air in the tower cylinder body to form granules, fine powder below 2 mm and large granules above 4 mm are removed through sieving and screening, the fine powder and the large granules are returned to the reaction kettle A for recycling, and finally uniform granular fertilizer with the granule diameter of 2-4 mm is obtained, and then the uniform granular fertilizer is cooled, coated, anti-caking and packaged in a packaging system to obtain the product of the invention.
Example 2:
a slow release fertilizer for rape is prepared from 395 kg of urea, 130 kg of monoammonium phosphate, 40 kg of potassium chloride, 247 kg of potassium sulfate, 21 kg of magnesium sulfate, 6kg of zinc sulfate, 6kg of ferrous sulfate, 1kg of ammonium molybdate, 15kg of boric acid, 7kg of polyglutamic acid, 7kg of brown yellow potassium humate, 0.02 kg of intelligent agent, 0.01kg of growth promoter, 123 kg of calcium powder and 2kg of urease inhibitor.
The specific production process comprises the following steps: 2 kilograms of urease inhibitor and 395 kilograms of urea are uniformly mixed, and are conveyed into a reaction kettle A through a conveyor belt to be mixed, heated and stirred with 247 kilograms of potassium sulfate, 40 kilograms of potassium chloride, 130 kilograms of monoammonium phosphate and system return materials at the stirring speed of 130 revolutions per minute and the temperature of 115-118 ℃ for 3 minutes; stirring and chelating 7kg of polyglutamic acid, 21 kg of magnesium sulfate, 6kg of zinc sulfate, 15kg of boric acid, 6kg of ferrous sulfate and 1kg of ammonium molybdate in a reaction kettle B at the stirring temperature of 50-70 ℃, the stirring speed of 30 r/min and the stirring time of 30 min to form stable polyglutamic acid chelated magnesium iron zinc molybdenum boron salt; feeding the material in the reaction kettle A into a reaction kettle B, adding 7kg of brown yellow potassium humate, 0.02 kg of intelligent agent, 0.01kg of growth promoter and 123 kg of calcium powder according to parts by mass, heating and stirring at the stirring speed of 200 revolutions per minute at the stirring temperature of 100-110 ℃, and stirring for 1 minute; the chelating slurry is scattered from the high altitude, the surface tension reason is changed into a spherical shape during scattering, the chelating slurry exchanges heat with the air in the tower cylinder body to form granules, fine powder below 2 mm and large granules above 4 mm are removed through sieving and screening, the fine powder and the large granules are returned to the reaction kettle A for recycling, and finally uniform granular fertilizer with the granule diameter of 2-4 mm is obtained, and then the uniform granular fertilizer is cooled, coated, anti-caking and packaged in a packaging system to obtain the product.
Example 3:
a slow release fertilizer for rape is prepared from 385Kg of urea, 146Kg of monoammonium phosphate, 30Kg of potassium chloride, 255Kg of potassium sulfate, 25Kg of magnesium sulfate, 7Kg of zinc sulfate, 4Kg of ferrous sulfate, 1Kg of ammonium molybdate, 20Kg of boric acid, 10Kg of polyglutamic acid, 10Kg of brown yellow potassium humate, 0.01Kg of intelligent agent, 0.015Kg of growth promoter, 105Kg of calcium powder and 2Kg of urease inhibitor.
The specific production process comprises the following steps: 2 kilograms of urease inhibitor and 385 kilograms of urea are uniformly mixed, and are conveyed into a reaction kettle A through a conveyor belt to be mixed, heated and stirred with 255 kilograms of potassium sulfate, 30 kilograms of potassium chloride, 146 kilograms of monoammonium phosphate and system return materials at the stirring speed of 130 revolutions per minute and the temperature of 115-118 ℃ for 3 minutes; 10kg of polyglutamic acid, 25kg of magnesium sulfate, 7kg of zinc sulfate, 20kg of boric acid, 4kg of ferrous sulfate and 1kg of ammonium molybdate which are conveyed in a metering way are stirred and chelated in a reaction kettle B at the stirring temperature of 50-70 ℃, the stirring speed of 30 r/min and the stirring time of 30 min to form stable polyglutamic acid chelated magnesium iron zinc molybdenum boron salt; feeding the material in the reaction kettle A into a reaction kettle B, adding 10Kg of brown yellow potassium humate, 0.01Kg of intelligent agent, 0.015Kg of growth promoter and 105Kg of calcium powder according to the mass Kg, heating and stirring at the stirring speed of 200 revolutions per minute and the stirring temperature of 100-110 ℃, and stirring for 1 minute; the chelating slurry is scattered from the high altitude, the surface tension reason is changed into a spherical shape during scattering, the chelating slurry exchanges heat with the air in the tower cylinder body to form granules, fine powder below 2 mm and large granules above 4 mm are removed through sieving and screening, the fine powder and the large granules are returned to the reaction kettle A for recycling, and finally uniform granular fertilizer with the granule diameter of 2-4 mm is obtained, and then the uniform granular fertilizer is cooled, coated, anti-caking and packaged in a packaging system to obtain the product.
The invention optimizes the formula of the common rape fertilizer, and has good product quality and high fertilizer efficiency.
Comparative example 1: on the basis of example 3, no urease inhibitor was added.
Comparative example 2: on the basis of example 3, potassium fulvate was not added.
Comparative example 3: on the basis of example 3, no polyglutamic acid was added.
Comparative example 4: on the basis of example 3, no intelligent agent and no growth-promoting agent were added.
Comparative example 5: on the basis of example 3, no urease inhibitor, potassium fulvate, polyglutamic acid, smart hearing and growth promoting elements were added.
Test No.)
Performing equal nitrogen amount experiments on the compound fertilizers prepared in the examples 1-3 and the comparative example 1 and common fertilizers, culturing by adopting a pot experiment, wherein the pure nitrogen amount in the air-dried soil of the pot experiment is 0.50g/kg, fully mixing the weighed fertilizers and the soil, and observing the urease activity and the ammonium nitrogen content in the soil; a total of 5 treatments were set: and comparing the nitrogen content of the compound fertilizer prepared in the examples 1-3 and the comparative example 1 by taking local habitual fertilization as a control. As shown in fig. 1 and 2 in particular at 1.
As can be seen from the graphs 1 and 2, the rape special fertilizer provided by the invention can inhibit the activity of soil urease in a certain period of time, reduce the hydrolysis release rate of a urea nitrogen fertilizer in soil, effectively prolong the fertilizer efficiency and provide stable fertilizer efficiency for the whole growth period of rape growth.
Test No. two
The compound fertilizers prepared in the examples 1 to 3 and the comparative examples 1 to 5 are compared with common fertilizers in fertilization experiments, the variety of the tested rape is hua-you-za 668, the tested fertilizer is the special fertilizer for rape containing humic acid and the conventional compound fertilizer (equal-nutrient compound fertilizer) of the invention, the experiment method is the fertilization comparison of the equal-area field, the experiment adopts a random block design, and 9 treatments are arranged in a place in the north of a lake: yield was measured at harvest time, compared to an equivalent application of examples 1 to 3 and comparative examples 1 to 5, using 50 kg/acre of local habitual fertilisation (15-15-15). (experimental comparison data in table 1):
TABLE 1
As can be seen from the table 1, the rape special fertilizer provided by the invention has rich nutrient substances, can promote the growth of rape, and also contains active substances such as polyglutamic acid, humic acid and the like, so that the rape special fertilizer can meet the absorption of the rape to various nutrients, improve the yield and the quality of the rape, promote the absorption of the rape to the nutrients, and improve the utilization rate of effective components in the fertilizer, thereby reducing the using amount of the fertilizer, improving the crop quality, protecting the environment, improving the oil yield of the rape, ensuring high quality and obviously improving the commodity performance of the rape.
In conclusion, the humic acid-containing fertilizer special for rape provided by the embodiment of the invention has rich nutrition and is not easy to cake, and can greatly improve the yield of rape and the quality of rapeseeds; the preparation method of the humic acid-containing rape special fertilizer provided by the embodiment of the invention is simple in technology, convenient to operate and suitable for large-scale production.
Claims (10)
1. The slow release fertilizer for the rape is characterized by comprising the following raw materials in parts by weight:
370-400 parts of urea, 130-160 parts of monoammonium phosphate, 20-40 parts of potassium chloride, 240-270 parts of potassium sulfate, 20-30 parts of magnesium sulfate, 6-8 parts of zinc sulfate, 2-6 parts of ferrous sulfate, 0.5-1 part of ammonium molybdate, 15-25 parts of boric acid, 8-10 parts of polyglutamic acid, 6-10 parts of brown yellow humic acid, 0.01-0.02 part of intelligent agent, 0.01-0.02 part of growth promoter, 100-125 parts of filler and 1-3 parts of urease inhibitor.
2. The slow release fertilizer for rape as claimed in claim 1, wherein: the fertilizer comprises 385 parts of urea, 146 parts of monoammonium phosphate, 30 parts of potassium chloride, 255 parts of potassium sulfate, 25 parts of magnesium sulfate, 7 parts of zinc sulfate, 4 parts of ferrous sulfate, 1 part of ammonium molybdate, 20 parts of boric acid, 10 parts of polyglutamic acid, 10 parts of potassium fulvic, 0.01 part of intelligent agent, 0.015 part of growth promoter, 105 parts of filler and 2 parts of urease inhibitor.
3. The slow release fertilizer for rape as claimed in claim 1 or 2, wherein: the filler is calcium carbonate.
4. The slow release fertilizer for rape as claimed in claim 1 or 2, wherein: the humic acid content of the brown fulvic acid is more than 60 wt%, and the fulvic acid content is more than 20wt% in terms of dry basis.
5. The slow release fertilizer for rape as claimed in claim 1 or 2, wherein: the growth promoter contains 5% of microbial metabolite, 90% of polysaccharide and the balance organic matters.
6. The slow release fertilizer for rape as claimed in claim 1 or 2, wherein: the intelligent agent is a plant endophyte extract, and active ingredients of the intelligent agent comprise cyclic dipeptides, pyrimidine nucleosides, amino acids and saccharides; wherein C, H, O, N, P, S element accounts for more than 94% of the total extract, Na, K, Cl and Mg account for more than 5%, and the rest is microelement.
7. The method for preparing the slow release fertilizer for the rape as claimed in any one of claims 1 to 6 is characterized by comprising the following specific steps of:
s1, weighing the raw materials according to the proportion, and then uniformly mixing urea and a urease inhibitor;
s2, heating, stirring and uniformly mixing the material obtained in the step S1 with potassium sulfate, potassium chloride and monoammonium phosphate to form slurry in a molten state;
s3, heating, stirring and uniformly mixing magnesium sulfate, zinc sulfate, ferrous sulfate, ammonium molybdate, boric acid and polyglutamic acid;
s4, enabling the material obtained in the step S2 to flow into the material S3, adding the brown yellow humic acid potassium and the intelligent growth promoting agent, heating and mixing uniformly; throwing and granulating the formed slurry from high altitude, and then screening; and finally, obtaining a fertilizer with the particle diameter of 2-4 mm, and cooling, coating and anti-caking to obtain the slow release fertilizer for the rape.
8. The method of claim 7, wherein: in the S2, the heating temperature is 115-118 ℃, the stirring speed is 130-150 r/min, and the stirring time is 3-5 min.
9. The method of claim 7, wherein: in the S3, the heating temperature is 50-70 ℃, the stirring speed is 30-50 r/min, and the stirring time is 30-35 min.
10. The method of claim 7, wherein: and (4) during the sieving in the S4, sieving out powder materials below 2 mm and granules above 4 mm, returning the sieved materials to the S2 step, and adding and mixing the sieved materials with the materials obtained in the S1.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN116640024A (en) * | 2023-06-14 | 2023-08-25 | 新洋丰农业科技股份有限公司 | Special fertilizer for rape in middle and downstream regions of Yangtze river and preparation method thereof |
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| CN105777352A (en) * | 2014-08-27 | 2016-07-20 | 杨献美 | Method for producing special-purpose formulated fertilizer for oilseed rape by tower-type melting granulation |
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| CN103804092A (en) * | 2014-02-24 | 2014-05-21 | 华强化工集团股份有限公司 | Special fertilizer for sugarcane and preparation method of fertilizer |
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