CN113384914A - Natural products ultrasonic circulation extraction equipment - Google Patents

Natural products ultrasonic circulation extraction equipment Download PDF

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Publication number
CN113384914A
CN113384914A CN202110522509.2A CN202110522509A CN113384914A CN 113384914 A CN113384914 A CN 113384914A CN 202110522509 A CN202110522509 A CN 202110522509A CN 113384914 A CN113384914 A CN 113384914A
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shell
natural product
extraction equipment
pipe
circulation extraction
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CN202110522509.2A
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CN113384914B (en
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简婷婷
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Wuxi Jianyuxi Biological Technology Co ltd
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Wuxi Jianyuxi Biological Technology Co ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D11/00Solvent extraction
    • B01D11/02Solvent extraction of solids
    • B01D11/0261Solvent extraction of solids comprising vibrating mechanisms, e.g. mechanical, acoustical
    • B01D11/0265Applying ultrasound
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D36/00Filter circuits or combinations of filters with other separating devices
    • B01D36/003Filters in combination with devices for the removal of liquids
    • B01D36/008Means to filter or treat the separated liquid
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/08Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J19/10Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing sonic or ultrasonic vibrations
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C18/00Disintegrating by knives or other cutting or tearing members which chop material into fragments
    • B02C18/06Disintegrating by knives or other cutting or tearing members which chop material into fragments with rotating knives
    • B02C18/08Disintegrating by knives or other cutting or tearing members which chop material into fragments with rotating knives within vertical containers
    • B02C18/12Disintegrating by knives or other cutting or tearing members which chop material into fragments with rotating knives within vertical containers with drive arranged below container
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C18/00Disintegrating by knives or other cutting or tearing members which chop material into fragments
    • B02C18/06Disintegrating by knives or other cutting or tearing members which chop material into fragments with rotating knives
    • B02C18/16Details
    • B02C18/18Knives; Mountings thereof

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Food Science & Technology (AREA)
  • Physics & Mathematics (AREA)
  • Acoustics & Sound (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Mechanical Engineering (AREA)
  • Extraction Or Liquid Replacement (AREA)

Abstract

The invention discloses ultrasonic circulation extraction equipment for natural products, which comprises a supporting assembly and a supporting frame, wherein the supporting assembly comprises a supporting frame, a placing hole is formed in the supporting frame, and a supporting shell is arranged at the placing hole; the stirring assembly comprises a shell and a top cover, wherein a stirring cavity is arranged in the shell, the top cover is arranged at an open top of the shell, a feeding pipe is arranged at the center of the top cover, and a water inlet pipe is arranged close to the side edge; a discharge pipe is arranged at the bottom of the shell close to the side face, a motor shaft penetrates through the center of the bottom of the shell and is arranged in the stirring cavity, and a driving motor is arranged at the end part of the motor shaft; a first crushing piece is arranged at the other end of the motor shaft, a second crushing piece is arranged on the top cover, and the first crushing piece is matched with the second crushing piece; an ultrasonic generating piece is arranged in the supporting shell; the plant raw materials are thoroughly crushed by the cooperation of the first crushing piece and the second crushing piece, dissolved and extracted, and the emulsion is prepared by ultrasonic emulsification.

Description

Natural products ultrasonic circulation extraction equipment
Technical Field
The invention relates to the technical field of extraction equipment, in particular to natural product ultrasonic circulation extraction equipment.
Background
The frequency of sound waves that human ears can hear is 20-20000 Hz, and when the vibration frequency of sound waves is more than 20000Hz, human ears cannot hear. Ultrasound is known for its lower frequency limit approximately equal to the upper human hearing limit. Therefore, we refer to sound waves with frequencies above 20000 hertz as "ultrasound". Ultrasonic waves are mechanical waves, and mechanical vibrations and waves are the physical basis for the action of ultrasonic waves.
Ultrasonic emulsification realizes ' water-in-oil ' emulsification, ' oil-in-water ' emulsification, ' water-in-oil ' emulsification, ' mixing homogenization of a dispersed phase and a ' continuous ' phase by using ' cavitation effect ' of ultrasonic waves, and is a modern sonochemical means for replacing traditional emulsification processes such as a propeller, a colloid mill and a homogenizer.
The production of medicines usually needs to extract components from natural products, and the process needs to crush, stir, dissolve, emulsify and the like medicinal materials, and the ultrasonic wave can realize the emulsification effect by the cavitation effect and has high emulsification quality, so that a crushing and emulsification extraction device is designed.
Disclosure of Invention
This section is for the purpose of summarizing some aspects of embodiments of the invention and to briefly introduce some preferred embodiments, and in this section as well as in the abstract and the title of the invention of this application some simplifications or omissions may be made to avoid obscuring the purpose of this section, the abstract and the title of the invention, and such simplifications or omissions are not intended to limit the scope of the invention.
The present invention has been made keeping in mind the above problems occurring in the prior art and/or the problems occurring in the prior art.
Therefore, the technical problems to be solved by the invention are the problems of poor crushing effect and poor emulsifying effect in the prior art.
In order to solve the technical problems, the invention provides the following technical scheme: an ultrasonic circulation extraction device for natural products comprises,
the supporting assembly comprises a supporting frame, wherein a placing hole is formed in the supporting frame, and a supporting shell is arranged at the placing hole;
the stirring assembly comprises a shell and a top cover, wherein a stirring cavity is arranged in the shell, the top cover is arranged at an open top of the shell, a feeding pipe is arranged at the center of the top cover, and a water inlet pipe is arranged close to the side edge;
a discharge pipe is arranged at the bottom of the shell close to the side face, a motor shaft penetrates through the center of the bottom of the shell and is arranged in the stirring cavity, and a driving motor is arranged at the end part of the motor shaft;
a first crushing piece is arranged at the other end of the motor shaft, a second crushing piece is arranged on the top cover, and the first crushing piece is matched with the second crushing piece;
an ultrasonic generating piece is arranged in the supporting shell.
As a preferable scheme of the natural product ultrasonic circulation extraction equipment, the natural product ultrasonic circulation extraction equipment comprises the following steps: the first crushing piece comprises a first end plate and a ring cylinder, the first end plate is arranged at the end part of the motor shaft, and the ring cylinder is sleeved on the periphery of the motor shaft by taking the first end plate as a support; a first cavity is formed between the annular cylinder and the motor shaft.
As a preferable scheme of the natural product ultrasonic circulation extraction equipment, the natural product ultrasonic circulation extraction equipment comprises the following steps: the second crushing piece comprises a material receiving pipe, a second end plate and a filter pipe, and the material receiving pipe is arranged on the top cover and is in butt joint with the material inlet pipe; the second end plate is arranged at the end part of the material receiving pipe, a through hole is formed in the second end plate, the filter pipe is arranged at the through hole, and a second cavity is formed between the material receiving pipe and the filter pipe;
the filter tube is embedded in the first chamber.
As a preferable scheme of the natural product ultrasonic circulation extraction equipment, the natural product ultrasonic circulation extraction equipment comprises the following steps: and the filter tube is provided with filter holes.
As a preferable scheme of the natural product ultrasonic circulation extraction equipment, the natural product ultrasonic circulation extraction equipment comprises the following steps: the filter tube is provided with a crushing piece.
As a preferable scheme of the natural product ultrasonic circulation extraction equipment, the natural product ultrasonic circulation extraction equipment comprises the following steps: the ring section of thick bamboo lateral wall is provided with the long notch along axial direction, long notch both ends are provided with outer scraper blade and interior scraper blade respectively, outer scraper blade draws together towards the ring section of thick bamboo outside, interior scraper blade orientation first cavity inboard is received.
As a preferable scheme of the natural product ultrasonic circulation extraction equipment, the natural product ultrasonic circulation extraction equipment comprises the following steps: the ring cylinder is arranged in the second chamber, the end part of the outer scraper is close to the inner surface of the material receiving pipe, and the end part of the inner scraper is close to the outer surface of the filter pipe.
As a preferable scheme of the natural product ultrasonic circulation extraction equipment, the natural product ultrasonic circulation extraction equipment comprises the following steps: the end of the crushing piece is close to the inner side wall of the ring cylinder.
As a preferable scheme of the natural product ultrasonic circulation extraction equipment, the natural product ultrasonic circulation extraction equipment comprises the following steps: still be provided with the stirring piece on the motor shaft, the stirring piece is provided with in the stirring chamber.
As a preferable scheme of the natural product ultrasonic circulation extraction equipment, the natural product ultrasonic circulation extraction equipment comprises the following steps: and a fine filter screen is arranged in the discharge pipe.
The invention has the beneficial effects that: the plant raw materials are thoroughly crushed by the cooperation of the first crushing piece and the second crushing piece, dissolved and extracted, and the natural product emulsion is prepared by ultrasonic emulsification.
Drawings
In order to more clearly illustrate the technical solutions of the embodiments of the present invention, the drawings needed to be used in the description of the embodiments will be briefly introduced below, and it is obvious that the drawings in the following description are only some embodiments of the present invention, and it is obvious for those skilled in the art to obtain other drawings based on these drawings without inventive exercise. Wherein:
fig. 1 is a schematic view of the overall structure of an ultrasonic circulation extraction apparatus for natural products according to an embodiment of the present invention;
FIG. 2 is a schematic cross-sectional view of the overall structure of an ultrasonic circulation extraction apparatus for natural products according to an embodiment of the present invention;
FIG. 3 is a schematic structural diagram of a first crushing member in the natural product ultrasonic circulation extraction equipment according to an embodiment of the invention;
FIG. 4 is a schematic structural diagram of a second crushing member in the natural product ultrasonic circulation extraction apparatus according to an embodiment of the present invention;
fig. 5 is a schematic view of an assembly structure of a first crushing member and a second crushing member in the natural product ultrasonic circulation extraction apparatus according to an embodiment of the present invention.
Detailed Description
In order to make the aforementioned objects, features and advantages of the present invention comprehensible, embodiments accompanied with figures are described in detail below.
In the following description, numerous specific details are set forth in order to provide a thorough understanding of the present invention, but the present invention may be practiced in other ways than those specifically described and will be readily apparent to those of ordinary skill in the art without departing from the spirit of the present invention, and therefore the present invention is not limited to the specific embodiments disclosed below.
Next, the present invention will be described in detail with reference to the drawings, wherein the cross-sectional views illustrating the structure of the device are not enlarged partially according to the general scale for convenience of illustration when describing the embodiments of the present invention, and the drawings are only examples, which should not limit the scope of the present invention. In addition, the three-dimensional dimensions of length, width and depth should be included in the actual fabrication.
Further, reference herein to "one embodiment" or "an embodiment" means that a particular feature, structure, or characteristic described in connection with the embodiment is included in at least one implementation of the invention. The appearances of the phrase "in one embodiment" in various places in the specification are not necessarily all referring to the same embodiment, nor are separate or alternative embodiments mutually exclusive of other embodiments.
Example 1
Referring to fig. 1 to 5, the present embodiment provides a natural product ultrasonic circulation extraction apparatus, including,
the supporting assembly 100 comprises a supporting frame 101, wherein a placing hole 102 is formed in the supporting frame 101, and a supporting shell 103 is arranged at the placing hole 102;
the stirring assembly 200 comprises a shell 201 and a top cover 202, wherein a stirring cavity 203 is arranged in the shell 201, the top cover 202 is arranged at an opening at the top of the shell 201, a feeding pipe 204 is arranged at the center of the top cover 202, and a water inlet pipe 205 is arranged close to the side edge;
a discharge pipe 206 is arranged at the bottom of the shell 201 close to the side, a motor shaft 207 penetrates through the center of the bottom of the shell 201 and is arranged in the stirring cavity 203, and a driving motor 208 is arranged at the end part of the motor shaft 207;
the other end of the motor shaft 207 is provided with a first crushing piece 301, the top cover 202 is provided with a second crushing piece 302, and the first crushing piece 301 is matched with the second crushing piece 302;
the holder case 103 is provided with an ultrasonic generating member 104.
The invention adopts ultrasonic extraction technology to extract medicinal components, wherein ultrasonic refers to electromagnetic wave with the frequency of about 20 kHz-50 MHz, and the ultrasonic is a mechanical wave which needs an energy carrier-medium to be transmitted. The ultrasonic waves have positive and negative pressure alternating cycles in the transmission process, and extrude medium molecules in the positive phase, so that the original density of the medium is increased; in the negative phase, the medium molecules are sparse and discrete, and the medium density is reduced.
That is, the ultrasonic wave does not polarize molecules in the sample, but generates acoustic cavitation between the solvent and the sample, resulting in the formation, growth and explosive compression of bubbles in the solution, thereby dispersing the solid sample, increasing the contact area between the sample and the extraction solvent, and increasing the mass transfer rate of the target from the solid phase to the liquid phase.
In industrial application, ultrasonic wave is used for cleaning, drying, sterilizing, atomizing, nondestructive testing and the like, and the ultrasonic wave is a mature and widely applied technology. The principle of ultrasonic extraction the superiority of ultrasonic extraction of Chinese medicinal materials is based on the special physical properties of ultrasonic. The solid-liquid extraction separation is realized mainly by reducing the acting force between the target extract and a sample matrix through the quick mechanical vibration wave generated by the piezoelectric transducer.
When ultrasonic waves with the acoustic wave frequency higher than 20KHz are propagated in a continuous medium (such as water), the medium particles (including particles of important effective components of medicinal materials) are caused to move on a propagated wave front according to the Huygens fluctuation principle, so that the medium particles move by huge acceleration and kinetic energy. The acceleration of the mass point can be calculated to be more than two thousand times of the gravity acceleration.
The medium particles act on the particles of the effective components of the medicinal materials to obtain great acceleration and kinetic energy, which can quickly escape from the medicinal material matrix and dissociate in water.
Ultrasonic wave is transmitted in a liquid medium to generate a special 'cavitation effect', the 'cavitation effect' continuously generates countless micro-air holes with the internal pressure reaching thousands of atmospheric pressures and continuously 'explodes' to generate microcosmic strong shock waves to act on the traditional Chinese medicinal materials, so that medicinal material components are bombarded to escape, a medicinal material matrix is continuously corroded, and medicinal components which do not belong to a plant structure are continuously separated. Accelerate the extraction of the effective components of the plants.
The ultrasonic vibration homogenization (sonification) makes the action on each point in the sample medium consistent, so that the whole sample is extracted more uniformly. In conclusion, the effective substances in the traditional Chinese medicinal materials can be used as medium particles to obtain self huge acceleration and kinetic energy under the action of an ultrasonic field, and strong external impact is obtained through the cavitation effect, so that the effective substances can be efficiently and fully separated.
The ultrasonic extraction is suitable for extracting effective components of Chinese medicinal materials, and is a new method and process for preparing Chinese medicinal materials by thoroughly changing the conventional water decoction and alcohol precipitation extraction method. Compared with the water boiling and alcohol precipitation process, the ultrasonic extraction has the following outstanding characteristics (taking the ultrasonic extraction of the honeysuckle extract as an example):
(1) high temperatures are not required. The ultrasonic wave is used for strengthening extraction at the water temperature of 40-50 ℃, the water boiling is not carried out at high temperature, and certain medicinal components with the characteristics of heat instability, easy hydrolysis or oxidation in the traditional Chinese medicinal materials are not damaged. The ultrasonic wave can break the wall of plant cell and improve the curative effect of Chinese medicine. (2) The normal pressure extraction has good safety, simple and easy operation and convenient maintenance.
(2) The extraction efficiency is high. The best extraction rate can be obtained after the ultrasonic wave enhanced extraction is carried out for 20-40 minutes, and the extraction time is only one third or less of that of a water boiling and alcohol precipitation method. The extraction is sufficient, and the extraction amount is more than twice of that of the traditional method. According to statistics, the working efficiency of the ultrasonic wave at 65-70 ℃ is very high. The effective components of the Chinese herbal medicine plants are basically not damaged within 65 ℃.
After ultrasonic wave is added (under the condition of 65 ℃), the effective components of honeysuckle are extracted for about 40 minutes. The cooking time of the cooking method is usually two to three hours, which is more than 3 times of the ultrasonic extraction time. Extracting for 3 times per pot, and extracting more than 90% of effective components.
(3) Has broad spectrum. The applicability is wide, and various components of most plant raw materials can be prepared into natural products through ultrasonic extraction.
(4) The energy consumption is reduced. Because the ultrasonic extraction does not need heating or the heating temperature is low, the extraction time is short, and the energy consumption is greatly reduced.
(5) The processing capacity of the raw materials of the medicinal materials is large and is improved by times or several times, the impurities are few, and the effective components are easy to separate and purify.
(6) The extraction process has low cost and remarkable comprehensive economic benefit.
It should be noted that the ultrasonic wave generating component (104) mainly includes a sound wave emitting component, which is disposed in the supporting shell (103), and also includes some auxiliary components, which are disposed on the supporting frame (101), including but not limited to a transducer, a power supply/sound wave control box, a horn, etc., to support the sound wave emitting component to work, and the composition and principle thereof are prior art, and thus are not described again.
The top cover 202 is detachably fixed at the opening of the shell 201, and the fixing mode can be threaded fixing.
Specifically, the first crushing member 301 includes a first end plate 301a and a ring barrel 301b, the first end plate 301a is disposed at the end of the motor shaft 207, and the ring barrel 301b is sleeved on the periphery of the motor shaft 207 by using the first end plate 301a as a support; a first chamber 301c is formed between the collar 301b and the motor shaft 207.
Further, the second crushing member 302 includes a receiving tube 302a, a second end plate 302b and a filtering tube 302c, the receiving tube 302a is disposed on the top cover 202 and is abutted with the feeding tube 204; the second end plate 302b is arranged at the end of the receiving pipe 302a, the second end plate 302b is provided with a through hole 302d, the filter pipe 302c is arranged at the through hole 302d, and a second chamber 302e is formed between the receiving pipe 302a and the filter pipe 302 c; the filter tube 302c is embedded in the first chamber 301 c.
It should be noted that the through-hole 302d communicates with the stirring chamber 203.
The filter tube 302c is provided with filter holes 302 f; the filter tube 302c is provided with a crushing member 302 g.
It should be noted that the shredder 302g may be a tapered needle punch disposed on the outside wall of the filter tube 302c, with the end near the inside surface of the collar 301 b.
The side wall of the ring barrel 301b is provided with a long notch 301d along the axial direction, two ends of the long notch 301d are respectively provided with an outer scraper 301e and an inner scraper 301f, the outer scraper 301e extends towards the outer side of the ring barrel 301b, and the inner scraper 301f extends towards the inner side of the first cavity 301 c.
It should be noted that the inner scraper 301f is provided with a concave pit or a groove for the crushed pieces 302g to pass through, so as to block most of the medicinal materials.
The ring barrel 301b is arranged in the second chamber 302e, the end part of the outer scraper 301e is close to the inner surface of the material receiving pipe 302a, and the end part of the inner scraper 301f is close to the outer surface of the filter pipe 302 c.
The end of the crushing member 302g approaches the inner side wall of the ring barrel 301 b; the motor shaft 207 is also provided with a stirring member 207a, and the stirring member 207a is disposed in the stirring chamber 203.
It should be noted that the stirring member 207a may be a stirring rod or a stirring paddle. A fine screen 206a is provided in the discharge pipe 206.
In this embodiment, during the extraction process, the plant material is fed from the feed pipe 204, water is injected into the stirring chamber 203 from the feed pipe 205, and the driving motor 208 and the ultrasonic generating member 104 are turned on.
The medicinal materials are fed into the receiving tube 302a from the feeding tube 204, and fall into the second chamber 302e, specifically between the receiving tube 302a and the ring barrel 301b, because the first end plate 301a is located in the middle of the receiving tube 302a, the medicinal materials fall into the second chamber 302e, the outer scraper 301e rotates counterclockwise in the direction shown in fig. 5, the plant materials in the second chamber 302e are scraped at one side of the outer scraper 301e, enter the area between the ring barrel 301b and the filter tube 302c from the long notch 301d, and are cut and ground when contacting with the stirring piece 207a, the crushed particles reaching the proper size can enter the filter tube 302c from the filter hole 302f and fall into the stirring cavity 203 through the through hole 302d, and enter the ring barrel 301b along the line if the size is not reached, and all the way is crushed until the inner scraper 301f is contacted with the inner scraper 301f to be blocked by the inner scraper 301f, further crushed by the stirring member 207a and passed through the filter holes 302f of the filter tube 302c into the interior of the filter tube 302c by the scraping action of the inner scraper 301 f.
Outer scraper blade 301e is used for receiving and scrapes, and interior scraper blade 301f is used for intercepting and scrapes and makes suitable size can pass through filtration pore 302f, changes the structure and can make plant raw materials cut and grind and target in place, meets water the back and emulsify under the combined action of ultrasonic wave and stirring piece, and the refilter is discharged when discharging pipe 206.
The stirring member 207a can stir and emulsify the ingredients dissolved in water and also can accelerate the dissolution of the ingredients, and the ultrasonic generator 104 also has an emulsifying function, and the fine filter 206a is used for filtering the residues in the stirring chamber 203.
It is important to note that the construction and arrangement of the present application as shown in the various exemplary embodiments is illustrative only. Although only a few embodiments have been described in detail in this disclosure, those skilled in the art who review this disclosure will readily appreciate that many modifications are possible (e.g., variations in sizes, dimensions, structures, shapes and proportions of the various elements, values of parameters (e.g., temperatures, pressures, etc.), mounting arrangements, use of materials, colors, orientations, etc.) without materially departing from the novel teachings and advantages of the subject matter recited in this application. For example, elements shown as integrally formed may be constructed of multiple parts or elements, the position of elements may be reversed or otherwise varied, and the nature or number of discrete elements or positions may be altered or varied. Accordingly, all such modifications are intended to be included within the scope of this invention. The order or sequence of any process or method steps may be varied or re-sequenced according to alternative embodiments. In the claims, any means-plus-function clause is intended to cover the structures described herein as performing the recited function and not only structural equivalents but also equivalent structures. Other substitutions, modifications, changes and omissions may be made in the design, operating conditions and arrangement of the exemplary embodiments without departing from the scope of the present inventions. Therefore, the present invention is not limited to a particular embodiment, but extends to various modifications that nevertheless fall within the scope of the appended claims.
Moreover, in an effort to provide a concise description of the exemplary embodiments, all features of an actual implementation may not be described (i.e., those unrelated to the presently contemplated best mode of carrying out the invention, or those unrelated to enabling the invention).
It should be appreciated that in the development of any such actual implementation, as in any engineering or design project, numerous implementation-specific decisions may be made. Such a development effort might be complex and time consuming, but would nevertheless be a routine undertaking of design, fabrication, and manufacture for those of ordinary skill having the benefit of this disclosure, without undue experimentation.
It should be noted that the above-mentioned embodiments are only for illustrating the technical solutions of the present invention and not for limiting, and although the present invention has been described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that modifications or equivalent substitutions may be made on the technical solutions of the present invention without departing from the spirit and scope of the technical solutions of the present invention, which should be covered by the claims of the present invention.

Claims (10)

1. A natural product ultrasonic circulation extraction equipment which characterized in that: comprises the steps of (a) preparing a mixture of a plurality of raw materials,
the supporting assembly (100) comprises a supporting frame (101), a placing hole (102) is formed in the supporting frame (101), and a supporting shell (103) is arranged at the placing hole (102);
the stirring assembly (200) comprises a shell (201) and a top cover (202), wherein a stirring cavity (203) is arranged in the shell (201), the top cover (202) is arranged at an opening at the top of the shell (201), a feeding pipe (204) is arranged at the center of the top cover (202), and a water inlet pipe (205) is arranged close to the side edge;
a discharge pipe (206) is arranged at the bottom of the shell (201) close to the side surface, a motor shaft (207) penetrates through the center of the bottom of the shell (201) and is arranged in the stirring cavity (203), and a driving motor (208) is arranged at the end part of the motor shaft (207);
a first crushing piece (301) is arranged at the other end of the motor shaft (207), a second crushing piece (302) is arranged on the top cover (202), and the first crushing piece (301) is matched with the second crushing piece (302);
an ultrasonic generating piece (104) is arranged in the supporting shell (103).
2. The natural product ultrasonic circulation extraction equipment according to claim 1, characterized in that: the first crushing piece (301) comprises a first end plate (301a) and a ring cylinder (301b), the first end plate (301a) is arranged at the end part of the motor shaft (207), and the ring cylinder (301b) is sleeved on the periphery of the motor shaft (207) by taking the first end plate (301a) as a support; a first chamber (301c) is formed between the ring barrel (301b) and the motor shaft (207).
3. The natural product ultrasonic circulation extraction equipment according to claim 1 or 2, characterized in that: the second crushing piece (302) comprises a material receiving pipe (302a), a second end plate (302b) and a filter pipe (302c), and the material receiving pipe (302a) is arranged on the top cover (202) and is butted with the material feeding pipe (204); the second end plate (302b) is arranged at the end part of the material receiving pipe (302a), a through hole (302d) is formed in the second end plate (302b), the filter pipe (302c) is arranged at the through hole (302d), and a second chamber (302e) is formed between the material receiving pipe (302a) and the filter pipe (302 c);
the filter tube (302c) is embedded in the first chamber (301 c).
4. The natural product ultrasonic circulation extraction equipment of claim 3, characterized in that: the filter tube (302c) is provided with filter holes (302 f).
5. The natural product ultrasonic circulation extraction equipment of claim 4, characterized in that: the filter tube (302c) is provided with a crushing piece (302 g).
6. The natural product ultrasonic circulation extraction equipment of claim 5, characterized in that: the ring section of thick bamboo (301b) lateral wall is provided with long notch (301d) along axial direction, long notch (301d) both ends are provided with outer scraper blade (301e) and interior scraper blade (301f) respectively, outer scraper blade (301e) draw together towards the ring section of thick bamboo (301b) outside, interior scraper blade (301f) orientation first cavity (301c) inboard is received.
7. The natural product ultrasonic circulation extraction equipment according to any one of claims 4 to 6, characterized in that: the ring barrel (301b) is arranged in a second chamber (302e), the end part of the outer scraper (301e) is close to the inner surface of the material receiving pipe (302a), and the end part of the inner scraper (301f) is close to the outer surface of the filter pipe (302 c).
8. The natural product ultrasonic circulation extraction equipment of claim 7, characterized in that: the end of the crushing piece (302g) is close to the inner side wall of the ring cylinder (301 b).
9. The natural product ultrasonic circulation extraction equipment of claim 8, characterized in that: the motor shaft (207) is also provided with a stirring piece (207a), and the stirring piece (207a) is arranged in the stirring cavity (203).
10. The natural product ultrasonic circulation extraction apparatus according to claim 8 or 9, characterized in that: a fine filter screen (206a) is arranged in the discharge pipe (206).
CN202110522509.2A 2021-05-13 2021-05-13 Natural products ultrasonic circulation extraction equipment Active CN113384914B (en)

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CN113384914A true CN113384914A (en) 2021-09-14
CN113384914B CN113384914B (en) 2022-09-30

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DE2844950A1 (en) * 1978-10-16 1980-04-24 Buckau Wolf Maschf R Diffusion tower for extn. of sugar beet shreds - with central and concentric hollow shafts for transport blades contra-rotating at different speeds
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RU2039753C1 (en) * 1993-05-27 1995-07-20 Научно-производственное объединение по крахмалопродуктам Device for comminuting raw material containing starch
CN101274157A (en) * 2006-12-31 2008-10-01 中国科学院过程工程研究所 Cross current intrinsic cycle ultrasonic and microwave leaching reactor and leaching method thereof
JP2015205245A (en) * 2014-04-21 2015-11-19 三菱日立パワーシステムズ株式会社 Classifier and vertical pulverization classifier comprising the same
CN205730451U (en) * 2016-06-28 2016-11-30 重庆三峡云海药业股份有限公司 Chinese crude drug constituents extraction unit
CN108355756A (en) * 2018-02-10 2018-08-03 安徽唯诗杨信息科技有限公司 A kind of multistage automatic cycle grinding device of fining and its course of work
CN208448700U (en) * 2018-07-05 2019-02-01 楚雄医药高等专科学校 A kind of separate type natural drug extractor

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2844950A1 (en) * 1978-10-16 1980-04-24 Buckau Wolf Maschf R Diffusion tower for extn. of sugar beet shreds - with central and concentric hollow shafts for transport blades contra-rotating at different speeds
KR930019264A (en) * 1992-03-02 1993-10-18 정인식 Ultrasonic Extraction Method and Apparatus
RU2039753C1 (en) * 1993-05-27 1995-07-20 Научно-производственное объединение по крахмалопродуктам Device for comminuting raw material containing starch
CN101274157A (en) * 2006-12-31 2008-10-01 中国科学院过程工程研究所 Cross current intrinsic cycle ultrasonic and microwave leaching reactor and leaching method thereof
JP2015205245A (en) * 2014-04-21 2015-11-19 三菱日立パワーシステムズ株式会社 Classifier and vertical pulverization classifier comprising the same
CN205730451U (en) * 2016-06-28 2016-11-30 重庆三峡云海药业股份有限公司 Chinese crude drug constituents extraction unit
CN108355756A (en) * 2018-02-10 2018-08-03 安徽唯诗杨信息科技有限公司 A kind of multistage automatic cycle grinding device of fining and its course of work
CN208448700U (en) * 2018-07-05 2019-02-01 楚雄医药高等专科学校 A kind of separate type natural drug extractor

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