CN113321488B - Purple gold and silver milli-architectural cup - Google Patents
Purple gold and silver milli-architectural cup Download PDFInfo
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- CN113321488B CN113321488B CN202110718628.5A CN202110718628A CN113321488B CN 113321488 B CN113321488 B CN 113321488B CN 202110718628 A CN202110718628 A CN 202110718628A CN 113321488 B CN113321488 B CN 113321488B
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- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 title abstract description 22
- 229910052737 gold Inorganic materials 0.000 title abstract description 22
- 239000010931 gold Substances 0.000 title abstract description 22
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 title abstract description 17
- 229910052709 silver Inorganic materials 0.000 title abstract description 17
- 239000004332 silver Substances 0.000 title abstract description 17
- 238000002360 preparation method Methods 0.000 claims abstract description 17
- 239000002283 diesel fuel Substances 0.000 claims description 69
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 25
- 241000196324 Embryophyta Species 0.000 claims description 23
- 238000002156 mixing Methods 0.000 claims description 20
- 230000032683 aging Effects 0.000 claims description 19
- 238000007873 sieving Methods 0.000 claims description 19
- 239000002002 slurry Substances 0.000 claims description 16
- 238000000034 method Methods 0.000 claims description 15
- 235000008331 Pinus X rigitaeda Nutrition 0.000 claims description 13
- 235000011613 Pinus brutia Nutrition 0.000 claims description 13
- 241000018646 Pinus brutia Species 0.000 claims description 13
- 239000002689 soil Substances 0.000 claims description 13
- 239000005995 Aluminium silicate Substances 0.000 claims description 12
- 235000007164 Oryza sativa Nutrition 0.000 claims description 12
- 244000302661 Phyllostachys pubescens Species 0.000 claims description 12
- 235000003570 Phyllostachys pubescens Nutrition 0.000 claims description 12
- 235000012211 aluminium silicate Nutrition 0.000 claims description 12
- DLHONNLASJQAHX-UHFFFAOYSA-N aluminum;potassium;oxygen(2-);silicon(4+) Chemical compound [O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[Al+3].[Si+4].[Si+4].[Si+4].[K+] DLHONNLASJQAHX-UHFFFAOYSA-N 0.000 claims description 12
- 238000010304 firing Methods 0.000 claims description 12
- 238000000227 grinding Methods 0.000 claims description 12
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims description 12
- 235000009566 rice Nutrition 0.000 claims description 12
- 239000002023 wood Substances 0.000 claims description 12
- 239000010903 husk Substances 0.000 claims description 11
- 229910001710 laterite Inorganic materials 0.000 claims description 11
- 239000011504 laterite Substances 0.000 claims description 11
- 241000205585 Aquilegia canadensis Species 0.000 claims description 10
- 235000015895 biscuits Nutrition 0.000 claims description 10
- 238000001914 filtration Methods 0.000 claims description 10
- 238000010438 heat treatment Methods 0.000 claims description 10
- 230000001376 precipitating effect Effects 0.000 claims description 10
- 238000005406 washing Methods 0.000 claims description 10
- 238000007670 refining Methods 0.000 claims description 6
- 238000009966 trimming Methods 0.000 claims description 6
- 240000007594 Oryza sativa Species 0.000 claims 3
- 239000013078 crystal Substances 0.000 abstract description 4
- 239000010977 jade Substances 0.000 abstract description 2
- 239000002956 ash Substances 0.000 description 24
- 230000000052 comparative effect Effects 0.000 description 16
- 241000209094 Oryza Species 0.000 description 9
- 238000010276 construction Methods 0.000 description 9
- 230000000694 effects Effects 0.000 description 7
- AJBZENLMTKDAEK-UHFFFAOYSA-N 3a,5a,5b,8,8,11a-hexamethyl-1-prop-1-en-2-yl-1,2,3,4,5,6,7,7a,9,10,11,11b,12,13,13a,13b-hexadecahydrocyclopenta[a]chrysene-4,9-diol Chemical compound CC12CCC(O)C(C)(C)C1CCC(C1(C)CC3O)(C)C2CCC1C1C3(C)CCC1C(=C)C AJBZENLMTKDAEK-UHFFFAOYSA-N 0.000 description 6
- 235000003880 Calendula Nutrition 0.000 description 6
- 240000001432 Calendula officinalis Species 0.000 description 6
- 238000011156 evaluation Methods 0.000 description 6
- 239000000203 mixture Substances 0.000 description 5
- PQTCMBYFWMFIGM-UHFFFAOYSA-N gold silver Chemical compound [Ag].[Au] PQTCMBYFWMFIGM-UHFFFAOYSA-N 0.000 description 4
- 229910052573 porcelain Inorganic materials 0.000 description 4
- 244000269722 Thea sinensis Species 0.000 description 2
- 239000003086 colorant Substances 0.000 description 2
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 description 1
- 235000002918 Fraxinus excelsior Nutrition 0.000 description 1
- 244000017020 Ipomoea batatas Species 0.000 description 1
- 235000002678 Ipomoea batatas Nutrition 0.000 description 1
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 238000011534 incubation Methods 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/32—Burning methods
- C04B33/34—Burning methods combined with glazing
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
- C04B2235/6562—Heating rate
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
- C04B2235/6565—Cooling rate
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
- C04B2235/6567—Treatment time
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/66—Specific sintering techniques, e.g. centrifugal sintering
- C04B2235/661—Multi-step sintering
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/60—Production of ceramic materials or ceramic elements, e.g. substitution of clay or shale by alternative raw materials, e.g. ashes
Abstract
The invention relates to a purple gold and silver milli-build cup. Specifically, the invention provides a preparation process of a purple gold and silver milli-scale cup, which comprises the following steps: glazing the green body, and roasting the glazed green body to obtain the purple Jin Yinhao cup. The glaze of the purple Jin Yinhao building cup disclosed by the invention is densely distributed with silver hairlines, is moist and smooth, has good definition and uniformity, is beautiful and jade in quality and strong in layering sense, belongs to top-level hairlines, has graceful and crystal purple gold stripes among silver hairlines, is like broken gold spreading, is rich in color and strong in relief sense, and has attractive appearance, artistic and collection values, and the glaze is sparkled with golden light, beautiful and primitive in the sun.
Description
Technical Field
The invention relates to the technical field of porcelain, in particular to a purple Jin Yinhao cup.
Background
The build cup is a bright pearl on ceramic history, the build cup is ancient and simple in modeling, the glaze color changes into a phantom, is gorgeous and colorful, and the build cup has excellent artistic level and is famous in the world, and compared with other porcelain, the build cup has unique beauty and is still fashionable over thousands of years.
However, the construction cup is very difficult to fire, the formulation, firing atmosphere and temperature are difficult to select, defects such as cracking and deformation of a blank, foaming of a glaze surface and plaque are often generated, and the fired construction cup is often dull and dull in color, fuzzy in filigree and poor in texture, so that firing failure is caused. As appreciation and art levels continue to increase, there is an increasing demand for porcelain having a beautiful appearance and a collectable value. How to fire a build cup with an attractive appearance to improve the art and collection value of the build cup becomes a hot spot of research in the porcelain industry today.
Thus, there is a need in the art to develop a build cup that has a beautiful appearance, artistic and collectible value.
Disclosure of Invention
The invention aims to provide a purple gold and silver milli-scale cup with attractive appearance, art and collection value.
In order to achieve the above purpose, the present invention adopts the following technical scheme:
the first aspect of the invention provides a preparation process of a purple gold and silver milli-scale cup, which comprises the following steps:
(1) Mixing and crushing 7-9 parts by weight of kaolin and 1.5-2.5 parts by weight of laterite, adding water for washing, sieving with a 80-120 mesh sieve, precipitating, press-filtering, mud refining, ageing, pulling and trimming, and then performing biscuit firing for 4-6 hours at 820-860 ℃ and taking out to obtain a blank;
(2) Mixing 2.5-3.5 parts by weight of moso bamboo, 0.5-1.5 parts by weight of pine wood and 1.5-2.5 parts by weight of rice husk, burning, and collecting ash to obtain plant ash;
(3) Grinding 7-8 parts by weight of glaze ore, 0.5-1.5 parts by weight of potassium feldspar, 0.1-0.4 part by weight of red soil, 0.3-0.7 part by weight of plant ash prepared in the step (2) and 6-8 parts by weight of water, sieving with a 80-120 mesh sieve, and aging for 3-5 days to obtain glaze slurry;
(4) Applying the glaze slurry prepared in the step (3) to the blank prepared in the step (1), and airing to obtain a glazed blank with glazing thickness of 0.4-0.6 mm;
(5) Roasting the glazed blank obtained in the step (4) in an electric kiln, wherein the roasting step is as follows:
(5.1) raising the furnace temperature from normal temperature to 1320-1360 ℃ at the speed of 240-280 ℃/h, preserving heat for 7-9min at 1320-1360 ℃, then adding diesel oil into the electric kiln, adding the diesel oil every 4-6min for 3 times, adding 580-620g diesel oil into each cubic meter of electric kiln space, and preserving heat for 4-6min at 1320-1360 ℃ after the diesel oil is added;
(5.2) reducing the temperature of the furnace from 1320-1360 ℃ to 1030-1070 ℃ at the speed of 200-240 ℃/h, then adding diesel oil into the electric kiln, adding once every 9-11min for 2 times, adding 280-320g of diesel oil into each cubic meter of electric kiln space, heating the furnace from 1030-1070 ℃ to 1320-1360 ℃ at the speed of 310-350 ℃/h after the diesel oil is added, and keeping the temperature at 1320-1360 ℃ for 9-11min;
(5.3) reducing the temperature of the furnace from 1320-1360 ℃ to 380-420 ℃ at the speed of 130-170 ℃/h, stopping the furnace, opening the furnace door, and reducing the temperature of the furnace to normal temperature to obtain the purple Jin Yinhao cup.
In a preferred embodiment of the invention, the process comprises the steps of:
(1) Mixing and crushing 7.5-8.5 parts by weight of kaolin and 1.8-2.2 parts by weight of laterite, adding water for washing, sieving with a 100-mesh sieve, precipitating, press-filtering, mud refining, ageing, pulling a blank, trimming the blank, and then performing biscuit firing at 830-850 ℃ for 4.5-5.5 hours, and taking out to obtain a blank;
(2) Mixing 2.8-3.2 parts by weight of moso bamboo, 0.8-1.2 parts by weight of pine wood and 1.8-2.2 parts by weight of rice husk, burning, and collecting ash to obtain plant ash;
(3) Putting 7.2-7.8 parts by weight of glaze ore, 0.8-1.2 parts by weight of potassium feldspar, 0.1-0.3 part by weight of red soil, 0.4-0.6 part by weight of plant ash prepared in the step (2) and 6.8-7.2 parts by weight of water into a ball mill, grinding, sieving with a 100-mesh sieve, and ageing for 3.8-4.2 days to obtain glaze slip;
(4) Applying the glaze slurry prepared in the step (3) to the blank prepared in the step (1), and airing to obtain a glazed blank with glazing thickness of 0.4-0.6 mm;
(5) Roasting the glazed blank obtained in the step (4) in an electric kiln, wherein the roasting step is as follows:
(5.1) raising the furnace temperature from normal temperature to 1330-1350 ℃ at the speed of 250-270 ℃/h, preserving heat for 7-9min at 1330-1350 ℃, then adding the firewood into the electric kiln, adding the firewood once every 4.8-5.2min for 3 times, adding 580-620g of firewood into each cubic meter of electric kiln space, and preserving heat for 4.8-5.2min at 1330-1350 ℃ after the firewood is added;
(5.2) reducing the temperature of the furnace from 1330-1350 ℃ to 1040-1060 ℃ at the speed of 210-230 ℃/h, then adding diesel oil into the electric kiln, adding the diesel oil every 9-11min for 2 times, adding 290-310g of diesel oil into each cubic meter of electric kiln space, heating the furnace from 1040-1060 ℃ to 1330-1350 ℃ at the speed of 320-340 ℃/h after the diesel oil is added, and keeping the temperature at 1330-1350 ℃ for 9-11min;
(5.3) reducing the temperature of the furnace from 1330-1350 ℃ to 390-410 ℃ at the speed of 140-160 ℃/h, stopping the furnace, opening the furnace door, and reducing the temperature of the furnace to normal temperature to obtain the purple Jin Yinhao cup.
In a preferred embodiment of the invention, the process comprises the steps of:
(1) Mixing 8 parts by weight of kaolin and 2 parts by weight of laterite, crushing, adding water for washing, sieving with a 100-mesh sieve, precipitating, press-filtering, pugging, ageing, pulling a blank, repairing the blank, and performing biscuit firing at 840 ℃ for 5 hours, and taking out to obtain a blank;
(2) Mixing 3 parts by weight of moso bamboo, 1 part by weight of pine wood and 2 parts by weight of rice husk, burning, and collecting ash to obtain plant ash;
(3) Grinding 7.5 parts by weight of glaze ore, 1 part by weight of potassium feldspar, 0.2 part by weight of red soil, 0.5 part by weight of plant ash prepared in the step (2) and 7 parts by weight of water, sieving with a 100-mesh sieve, and aging for 4 days to obtain glaze slurry;
(4) Applying the glaze slurry prepared in the step (3) to the blank prepared in the step (1), and airing to obtain a glazed blank with glazing thickness of 0.5 mm;
(5) Roasting the glazed blank obtained in the step (4) in an electric kiln, wherein the roasting step is as follows:
(5.1) raising the furnace temperature from normal temperature to 1340 ℃ at a speed of 260 ℃/h, preserving heat at 1340 ℃ for 8min, then adding diesel oil into the electric kiln, adding the diesel oil every 5min for 3 times, adding 600g of diesel oil into each cubic meter of electric kiln space each time, and preserving heat at 1340 ℃ for 5min continuously after the diesel oil is added;
(5.2) reducing the temperature of the furnace from 1340 ℃ to 1050 ℃ at a speed of 220 ℃/h, then adding diesel oil into the electric kiln, adding the diesel oil every 10min for 2 times, adding 300g of diesel oil into the space of the electric kiln per cubic meter each time, and after the diesel oil is added, heating the furnace from 1050 ℃ to 1340 ℃ at a speed of 330 ℃/h, and continuously preserving the temperature at 1340 ℃ for 10min;
(5.3) reducing the temperature of the furnace from 1340 ℃ to 400 ℃ at a speed of 150 ℃/h, stopping the furnace, opening the furnace door, and reducing the temperature of the furnace to normal temperature to obtain the purple Jin Yinhao cup.
In a preferred embodiment of the present invention, in the step (2), the moso bamboo is sun-dried moso bamboo.
In a preferred embodiment of the present invention, in the step (2), the pine wood is sun-dried pine wood.
In a preferred embodiment of the present invention, in the step (2), the rice husk is dried rice husk.
In a preferred embodiment of the present invention, in the step (3), the grinding is performed in a ball mill.
In a preferred embodiment of the present invention, in the step (3), glaze ore, potassium feldspar, laterite, plant ash and water are put into a ball mill to be ground.
In a preferred embodiment of the present invention, in the step (5.3), the furnace is shut down, and the furnace door is opened to cool down naturally.
In a preferred embodiment of the present invention, the room temperature is 18-22 ℃, preferably 20 ℃.
In a preferred embodiment of the present invention, the kaolin is derived from water geen in the Jianyang region of southern Pingzhi, fujian.
In a preferred embodiment of the invention, the red soil is from a water town in the Jianyang region of the southern Pingzhi of Fujian.
In a preferred embodiment of the present invention, the glaze ore is from southern Lin Cun, jianyang district, pingzhi, fujian.
In a preferred embodiment of the invention, the purple honeysuckle tea cup is shown in figure 1 of the specification.
In a second aspect, the invention provides a purple honeysuckle jersey, which is prepared by the process according to the first aspect of the invention.
In a preferred embodiment of the invention, the purple honeysuckle tea cup is shown in figure 1 of the specification.
Within the scope of the invention, the above-described individual features of the invention may be combined with one another in order to form new or preferred embodiments.
Drawings
FIG. 1 shows a UV Jin Yinhao cup prepared in example 1 of the present invention.
Detailed Description
The invention discloses a purple honeysuckle milli-Jian cup and a preparation process thereof, wherein the process comprises the following steps: glazing the green body, and roasting the glazed green body to obtain the purple Jin Yinhao cup. The glaze of the purple Jin Yinhao building cup disclosed by the invention is densely distributed with silver hairlines, is moist and smooth, has good definition and uniformity, is beautiful and jade in quality and strong in layering sense, belongs to top-level hairlines, has graceful and crystal purple gold stripes among silver hairlines, is like broken gold spreading, is rich in color and strong in relief sense, and has attractive appearance, artistic and collection values, and the glaze is sparkled with golden light, beautiful and primitive in the sun.
Terminology
As used herein, the terms "comprising," "including," and "containing" are used interchangeably, and include not only open-ended definitions, but also semi-closed, and closed-ended definitions. In other words, the term includes "consisting of … …", "consisting essentially of … …".
In the invention, the firewood is pine root rich in rosin and can be burnt vigorously.
As used herein, the term "parts by weight" may be any fixed weight in milligrams, grams, or kilograms (e.g., 1mg, 1g, or 1kg, etc.). For example, a combination of 1 part by weight of component a and 9 parts by weight of component b may be a combination of 1 gram of component a+9 gram of component b, or 10 grams of component a+90 gram of component b, or the like. In the combination, the percentage content of a certain component= (the parts by weight of the component/the sum of the parts by weight of all components) ×100%, and therefore, in the composition composed of 1 part by weight of component a and 9 parts by weight of component b, the content of component a is 10%, and the content of component b is 90%.
Purple honeysuckle Haojian cup and preparation process thereof
The invention provides a preparation process of a purple gold and silver milli-scale cup with attractive appearance and collection value.
Typically, the violet Jin Yinhao set forth in the present invention is shown in fig. 1.
In a preferred embodiment of the invention, a preparation process of the purple gold silver milli-scale calendula is provided, and the process comprises the following steps:
(1) Mixing and crushing 7-9 parts by weight of kaolin and 1.5-2.5 parts by weight of laterite, adding water for washing, sieving with a 80-120 mesh sieve, precipitating, press-filtering, mud refining, ageing, pulling and trimming, and then performing biscuit firing for 4-6 hours at 820-860 ℃ and taking out to obtain a blank;
(2) Mixing 2.5-3.5 parts by weight of moso bamboo, 0.5-1.5 parts by weight of pine wood and 1.5-2.5 parts by weight of rice husk, burning, and collecting ash to obtain plant ash;
(3) Grinding 7-8 parts by weight of glaze ore, 0.5-1.5 parts by weight of potassium feldspar, 0.1-0.4 part by weight of red soil, 0.3-0.7 part by weight of plant ash prepared in the step (2) and 6-8 parts by weight of water, sieving with a 80-120 mesh sieve, and aging for 3-5 days to obtain glaze slurry;
(4) Applying the glaze slurry prepared in the step (3) to the blank prepared in the step (1), and airing to obtain a glazed blank with glazing thickness of 0.4-0.6 mm;
(5) Roasting the glazed blank obtained in the step (4) in an electric kiln, wherein the roasting step is as follows:
(5.1) raising the furnace temperature from normal temperature to 1320-1360 ℃ at the speed of 240-280 ℃/h, preserving heat for 7-9min at 1320-1360 ℃, then adding diesel oil into the electric kiln, adding the diesel oil every 4-6min for 3 times, adding 580-620g diesel oil into each cubic meter of electric kiln space, and preserving heat for 4-6min at 1320-1360 ℃ after the diesel oil is added;
(5.2) reducing the temperature of the furnace from 1320-1360 ℃ to 1030-1070 ℃ at the speed of 200-240 ℃/h, then adding diesel oil into the electric kiln, adding once every 9-11min for 2 times, adding 280-320g of diesel oil into each cubic meter of electric kiln space, heating the furnace from 1030-1070 ℃ to 1320-1360 ℃ at the speed of 310-350 ℃/h after the diesel oil is added, and keeping the temperature at 1320-1360 ℃ for 9-11min;
(5.3) reducing the temperature of the furnace from 1320-1360 ℃ to 380-420 ℃ at the speed of 130-170 ℃/h, stopping the furnace, opening the furnace door, and reducing the temperature of the furnace to normal temperature to obtain the purple Jin Yinhao cup.
In a preferred embodiment of the invention, a preparation process of the purple gold silver milli-scale calendula is provided, and the process comprises the following steps:
(1) Mixing and crushing 7.5-8.5 parts by weight of kaolin and 1.8-2.2 parts by weight of laterite, adding water for washing, sieving with a 100-mesh sieve, precipitating, press-filtering, mud refining, ageing, pulling a blank, trimming the blank, and then performing biscuit firing at 830-850 ℃ for 4.5-5.5 hours, and taking out to obtain a blank;
(2) Mixing 2.8-3.2 parts by weight of moso bamboo, 0.8-1.2 parts by weight of pine wood and 1.8-2.2 parts by weight of rice husk, burning, and collecting ash to obtain plant ash;
(3) Putting 7.2-7.8 parts by weight of glaze ore, 0.8-1.2 parts by weight of potassium feldspar, 0.1-0.3 part by weight of red soil, 0.4-0.6 part by weight of plant ash prepared in the step (2) and 6.8-7.2 parts by weight of water into a ball mill, grinding, sieving with a 100-mesh sieve, and ageing for 3.8-4.2 days to obtain glaze slip;
(4) Applying the glaze slurry prepared in the step (3) to the blank prepared in the step (1), and airing to obtain a glazed blank with glazing thickness of 0.4-0.6 mm;
(5) Roasting the glazed blank obtained in the step (4) in an electric kiln, wherein the roasting step is as follows:
(5.1) raising the furnace temperature from normal temperature to 1330-1350 ℃ at the speed of 250-270 ℃/h, preserving heat for 7-9min at 1330-1350 ℃, then adding the firewood into the electric kiln, adding the firewood once every 4.8-5.2min for 3 times, adding 580-620g of firewood into each cubic meter of electric kiln space, and preserving heat for 4.8-5.2min at 1330-1350 ℃ after the firewood is added;
(5.2) reducing the temperature of the furnace from 1330-1350 ℃ to 1040-1060 ℃ at the speed of 210-230 ℃/h, then adding diesel oil into the electric kiln, adding the diesel oil every 9-11min for 2 times, adding 290-310g of diesel oil into each cubic meter of electric kiln space, heating the furnace from 1040-1060 ℃ to 1330-1350 ℃ at the speed of 320-340 ℃/h after the diesel oil is added, and keeping the temperature at 1330-1350 ℃ for 9-11min;
(5.3) reducing the temperature of the furnace from 1330-1350 ℃ to 390-410 ℃ at the speed of 140-160 ℃/h, stopping the furnace, opening the furnace door, and reducing the temperature of the furnace to normal temperature to obtain the purple Jin Yinhao cup.
Typically, the preparation process of the purple Jin Yinhao cup provided by the invention comprises the following steps:
(1) Mixing 8 parts by weight of kaolin and 2 parts by weight of laterite, crushing, adding water for washing, sieving with a 100-mesh sieve, precipitating, press-filtering, pugging, ageing, pulling a blank, repairing the blank, and performing biscuit firing at 840 ℃ for 5 hours, and taking out to obtain a blank;
(2) Mixing 3 parts by weight of moso bamboo, 1 part by weight of pine wood and 2 parts by weight of rice husk, burning, and collecting ash to obtain plant ash;
(3) Grinding 7.5 parts by weight of glaze ore, 1 part by weight of potassium feldspar, 0.2 part by weight of red soil, 0.5 part by weight of plant ash prepared in the step (2) and 7 parts by weight of water, sieving with a 100-mesh sieve, and aging for 4 days to obtain glaze slurry;
(4) Applying the glaze slurry prepared in the step (3) to the blank prepared in the step (1), and airing to obtain a glazed blank with glazing thickness of 0.5 mm;
(5) Roasting the glazed blank obtained in the step (4) in an electric kiln, wherein the roasting step is as follows:
(5.1) raising the furnace temperature from normal temperature to 1340 ℃ at a speed of 260 ℃/h, preserving heat at 1340 ℃ for 8min, then adding diesel oil into the electric kiln, adding the diesel oil every 5min for 3 times, adding 600g of diesel oil into each cubic meter of electric kiln space each time, and preserving heat at 1340 ℃ for 5min continuously after the diesel oil is added;
(5.2) reducing the temperature of the furnace from 1340 ℃ to 1050 ℃ at a speed of 220 ℃/h, then adding diesel oil into the electric kiln, adding the diesel oil every 10min for 2 times, adding 300g of diesel oil into the space of the electric kiln per cubic meter each time, and after the diesel oil is added, heating the furnace from 1050 ℃ to 1340 ℃ at a speed of 330 ℃/h, and continuously preserving the temperature at 1340 ℃ for 10min;
(5.3) reducing the temperature of the furnace from 1340 ℃ to 400 ℃ at a speed of 150 ℃/h, stopping the furnace, opening the furnace door, and reducing the temperature of the furnace to normal temperature to obtain the purple Jin Yinhao cup.
In a preferred embodiment of the invention, the preparation process of the purple honeysuckle Haojian cup is prepared by the method described in the specific embodiment 1 of the invention.
In a preferred embodiment of the invention, the purple sweet potato majors are shown in the figure 1 of the specification.
The excellent effects of the present invention include:
the invention develops a preparation process of a purple gold and silver milli-construction cup, and the glaze surface of the purple Jin Yinhao milli-construction cup prepared by the process is densely covered with silver milli-patterns, is moist, has good, clear and uniform, beautiful and strong in layering sense, belongs to top-grade milli-patterns, has graceful and crystal purple gold stripes among silver milli-patterns, is like broken gold spreading, is rich in color and strong in relief sense, and has a sparkling, beautiful and primitive feel and strong third dimension in sunlight, so that the purple gold and silver milli-construction cup prepared by the process has graceful milli-patterns and colors, and has graceful appearance, art and collection value.
The invention will be further illustrated with reference to specific examples. It should be understood that the following specific examples give detailed embodiments and specific operation procedures on the premise of the present technical solution, but the scope of the present invention is not limited to the examples.
Examples and comparative examples
The red soil comes from the Fujian southern Pingzhi Jianyang area Shui Ji town;
kaolin comes from the Jianyang region Shui Ji town in the southern Pingshi of Fujian province;
glaze ore is from southern Lin Cun, jianyang region in southern Pingzhi, fujian province.
Example 1 purple Jin Yinhao Jianzhi
The embodiment 1 provides a preparation process of purple honeysuckle Haojian cup, which comprises the following steps:
(1) Mixing 8 parts by weight of kaolin and 2 parts by weight of laterite, crushing, adding water for washing, sieving with a 100-mesh sieve, precipitating, press-filtering, pugging, ageing, pulling a blank, repairing the blank, and performing biscuit firing at 840 ℃ for 5 hours, and taking out to obtain a blank.
(2) Mixing and burning 3 parts by weight of dried phyllostachys pubescens, 1 part by weight of dried pine wood and 2 parts by weight of dried rice hulls, and collecting ashes to obtain plant ash.
(3) 7.5 parts by weight of glaze ore, 1 part by weight of potassium feldspar, 0.2 part by weight of red soil, 0.5 part by weight of plant ash prepared in the step (2) and 7 parts by weight of water are put into a ball mill for grinding, and the mixture is sieved by a 100-mesh sieve and aged for 4 days to obtain glaze slip.
(4) And (3) applying the glaze slurry prepared in the step (3) to the green body prepared in the step (1), and airing to obtain a glazed green body with glazing thickness of 0.5 mm.
(5) Roasting the glazed blank obtained in the step (4) in an electric kiln, wherein the roasting step is as follows:
(5.1) raising the furnace temperature from normal temperature (20 ℃) to 1340 ℃ at a speed of 260 ℃/h, preserving heat at 1340 ℃ for 8min, then adding diesel oil into the electric kiln, adding the diesel oil every 5min for 3 times, adding 600g of diesel oil into each cubic meter of electric kiln space each time, and preserving heat at 1340 ℃ for 5min after the diesel oil is added;
(5.2) reducing the temperature of the furnace from 1340 ℃ to 1050 ℃ at a speed of 220 ℃/h, then adding diesel oil into the electric kiln, adding the diesel oil every 10min for 2 times, adding 300g of diesel oil into the space of the electric kiln per cubic meter each time, and after the diesel oil is added, heating the furnace from 1050 ℃ to 1340 ℃ at a speed of 330 ℃/h, and continuously preserving the temperature at 1340 ℃ for 10min;
(5.3) the furnace temperature is reduced from 1340 ℃ to 400 ℃ at a speed of 150 ℃/h, the furnace is stopped, the furnace door is opened, and the furnace temperature is naturally reduced to normal temperature (20 ℃), so that the UV Jin Yinhao building cup is obtained.
Effect evaluation:
the construction cup prepared in example 1 is a purple Jin Yinhao construction cup shown in fig. 1, and as can be seen from fig. 1, the glaze of the purple gold silver construction cup is densely covered with silver hairlines, is moist, has good definition and uniformity, is beautiful and strong in layering, belongs to top-grade hairlines, has graceful and crystal purple gold speckle between silver hairlines, is like broken gold sprinkle, is rich in color and strong in relief sense, and is sparkled, beautiful and primitive in nature and strong in third dimension, so that the purple gold silver construction cup prepared in example 1 has graceful hairlines and colors, and has graceful appearance, art and collection value.
Comparative example 1
This comparative example 1 is similar to the preparation process of example 1, except that: in the step (3): 7.5 parts by weight of glaze ore, 1 part by weight of potassium feldspar, 0.5 part by weight of plant ash prepared in the step (2) and 7 parts by weight of water are put into a ball mill to be ground, and the mixture is screened by a 100-mesh sieve and aged for 4 days to obtain glaze slip.
Effect evaluation:
the glaze surface filigree of the calendula prepared in the comparative example 1 is blurred, basically has no purple gold speckle and has poor texture.
Comparative example 2
This comparative example 2 is similar to the preparation process of example 1, except that: in the step (3): 7.5 parts by weight of glaze ore, 0.2 part by weight of red soil, 0.5 part by weight of plant ash prepared in the step (2) and 7 parts by weight of water are put into a ball mill for grinding, and the mixture is screened by a 100-mesh sieve and aged for 4 days to obtain glaze slip.
Effect evaluation:
the calendula glaze prepared in comparative example 2 had blurred and intricate filaments, dark purple gold stripes, air holes and poor stereoscopic impression.
Comparative example 3
This comparative example 3 is similar to the preparation process of example 1, except that: in the step (5): the roasting step is as follows:
(5.1) raising the furnace temperature from normal temperature (20 ℃) to 1340 ℃ at a speed of 260 ℃/h, preserving heat at 1340 ℃ for 8min, then adding diesel oil into the electric kiln, adding the diesel oil every 5min for 3 times, adding 600g of diesel oil into each cubic meter of electric kiln space each time, and preserving heat at 1340 ℃ for 5min after the diesel oil is added;
(5.2) the furnace temperature is reduced from 1340 ℃ to 400 ℃ at a speed of 150 ℃/h, the furnace is stopped, the furnace door is opened, and the furnace temperature is naturally reduced to normal temperature (20 ℃), so that the cup is obtained.
Effect evaluation:
the glaze surface filigree of the calendula prepared in the comparative example 3 is fuzzy, has no purple gold speckle and fails to burn.
Comparative example 4
This comparative example 4 is similar to the preparation process of example 1, except that: in step (5.2): the roasting step is as follows:
(5.2) the furnace temperature is reduced from 1340 ℃ to 1180 ℃ at the speed of 220 ℃/h, then the firewood is put into the electric kiln, the firewood is put into the electric kiln every 10min for 2 times, 300g of firewood is put into the electric kiln every cubic meter of space, after the firewood is put into the electric kiln, the furnace temperature is increased from 1180 ℃ to 1340 ℃ at the speed of 330 ℃/h, and the electric kiln is kept at the temperature of 1340 ℃ for 10min.
Effect evaluation:
the glaze of the calendula prepared in comparative example 4 has bubbles, blurred and irregular filigree, dark purple gold stripes, and poor texture and third dimension.
Comparative example 5
This comparative example 5 is similar to the preparation process of example 1, except that: in step (5.2): the roasting step is as follows:
(5.2) the furnace temperature was lowered from 1340℃to 1050℃at 220℃per hour, then the furnace temperature was raised from 1050℃to 1340℃at 330℃per hour, and the incubation was continued at 1340℃for 10min.
Effect evaluation:
the glaze of the architectural cup prepared in the comparative example 5 has bubbles, blurred filigree, dark purple gold stripes and poor layering,
while the invention has been described in terms of one embodiment, it should be noted that modifications could be made without departing from the principles of the invention, which would be apparent to those skilled in the art, would also be considered to be within the scope of the invention.
Claims (4)
1. The preparation process of the purple honeysuckle milli-Jian cup is characterized by comprising the following steps of:
(1) Mixing and crushing 7-9 parts by weight of kaolin and 1.5-2.5 parts by weight of laterite, adding water for washing, sieving with a 80-120 mesh sieve, precipitating, press-filtering, mud refining, ageing, pulling and trimming, and then performing biscuit firing for 4-6 hours at 820-860 ℃ and taking out to obtain a blank;
(2) Mixing 2.5-3.5 parts by weight of moso bamboo, 0.5-1.5 parts by weight of pine wood and 1.5-2.5 parts by weight of rice husk, burning, and collecting ash to obtain plant ash;
(3) Grinding 7-8 parts by weight of glaze ore, 0.5-1.5 parts by weight of potassium feldspar, 0.1-0.4 part by weight of red soil, 0.3-0.7 part by weight of plant ash prepared in the step (2) and 6-8 parts by weight of water, sieving with a 80-120 mesh sieve, and aging for 3-5 days to obtain glaze slurry;
(4) Applying the glaze slurry prepared in the step (3) to the blank prepared in the step (1), and airing to obtain a glazed blank with glazing thickness of 0.4-0.6 mm;
(5) Roasting the glazed blank obtained in the step (4) in an electric kiln, wherein the roasting step is as follows:
(5.1) raising the furnace temperature from normal temperature to 1320-1360 ℃ at the speed of 240-280 ℃/h, preserving heat for 7-9min at 1320-1360 ℃, then adding diesel oil into the electric kiln, adding the diesel oil every 4-6min for 3 times, adding 580-620g diesel oil into each cubic meter of electric kiln space, and preserving heat for 4-6min at 1320-1360 ℃ after the diesel oil is added;
(5.2) reducing the temperature of the furnace from 1320-1360 ℃ to 1030-1070 ℃ at the speed of 200-240 ℃/h, then adding diesel oil into the electric kiln, adding once every 9-11min for 2 times, adding 280-320g of diesel oil into each cubic meter of electric kiln space, heating the furnace from 1030-1070 ℃ to 1320-1360 ℃ at the speed of 310-350 ℃/h after the diesel oil is added, and keeping the temperature at 1320-1360 ℃ for 9-11min;
(5.3) reducing the temperature of the furnace from 1320-1360 ℃ to 380-420 ℃ at the speed of 130-170 ℃/h, stopping the furnace, opening the furnace door, and reducing the temperature of the furnace to normal temperature to obtain the purple Jin Yinhao cup.
2. The process of claim 1, wherein the process comprises the steps of:
(1) Mixing and crushing 7.5-8.5 parts by weight of kaolin and 1.8-2.2 parts by weight of laterite, adding water for washing, sieving with a 100-mesh sieve, precipitating, press-filtering, mud refining, ageing, pulling a blank, trimming the blank, and then performing biscuit firing at 830-850 ℃ for 4.5-5.5 hours, and taking out to obtain a blank;
(2) Mixing 2.8-3.2 parts by weight of moso bamboo, 0.8-1.2 parts by weight of pine wood and 1.8-2.2 parts by weight of rice husk, burning, and collecting ash to obtain plant ash;
(3) Putting 7.2-7.8 parts by weight of glaze ore, 0.8-1.2 parts by weight of potassium feldspar, 0.1-0.3 part by weight of red soil, 0.4-0.6 part by weight of plant ash prepared in the step (2) and 6.8-7.2 parts by weight of water into a ball mill, grinding, sieving with a 100-mesh sieve, and ageing for 3.8-4.2 days to obtain glaze slip;
(4) Applying the glaze slurry prepared in the step (3) to the blank prepared in the step (1), and airing to obtain a glazed blank with glazing thickness of 0.4-0.6 mm;
(5) Roasting the glazed blank obtained in the step (4) in an electric kiln, wherein the roasting step is as follows:
(5.1) raising the furnace temperature from normal temperature to 1330-1350 ℃ at the speed of 250-270 ℃/h, preserving heat for 7-9min at 1330-1350 ℃, then adding the firewood into the electric kiln, adding the firewood once every 4.8-5.2min for 3 times, adding 580-620g of firewood into each cubic meter of electric kiln space, and preserving heat for 4.8-5.2min at 1330-1350 ℃ after the firewood is added;
(5.2) reducing the temperature of the furnace from 1330-1350 ℃ to 1040-1060 ℃ at the speed of 210-230 ℃/h, then adding diesel oil into the electric kiln, adding the diesel oil every 9-11min for 2 times, adding 290-310g of diesel oil into each cubic meter of electric kiln space, heating the furnace from 1040-1060 ℃ to 1330-1350 ℃ at the speed of 320-340 ℃/h after the diesel oil is added, and keeping the temperature at 1330-1350 ℃ for 9-11min;
(5.3) reducing the temperature of the furnace from 1330-1350 ℃ to 390-410 ℃ at the speed of 140-160 ℃/h, stopping the furnace, opening the furnace door, and reducing the temperature of the furnace to normal temperature to obtain the purple Jin Yinhao cup.
3. The process of claim 1, wherein the process comprises the steps of:
(1) Mixing 8 parts by weight of kaolin and 2 parts by weight of laterite, crushing, adding water for washing, sieving with a 100-mesh sieve, precipitating, press-filtering, pugging, ageing, pulling a blank, repairing the blank, and performing biscuit firing at 840 ℃ for 5 hours, and taking out to obtain a blank;
(2) Mixing 3 parts by weight of moso bamboo, 1 part by weight of pine wood and 2 parts by weight of rice husk, burning, and collecting ash to obtain plant ash;
(3) Grinding 7.5 parts by weight of glaze ore, 1 part by weight of potassium feldspar, 0.2 part by weight of red soil, 0.5 part by weight of plant ash prepared in the step (2) and 7 parts by weight of water, sieving with a 100-mesh sieve, and aging for 4 days to obtain glaze slurry;
(4) Applying the glaze slurry prepared in the step (3) to the blank prepared in the step (1), and airing to obtain a glazed blank with glazing thickness of 0.5 mm;
(5) Roasting the glazed blank obtained in the step (4) in an electric kiln, wherein the roasting step is as follows:
(5.1) raising the furnace temperature from normal temperature to 1340 ℃ at a speed of 260 ℃/h, preserving heat at 1340 ℃ for 8min, then adding diesel oil into the electric kiln, adding the diesel oil every 5min for 3 times, adding 600g of diesel oil into each cubic meter of electric kiln space each time, and preserving heat at 1340 ℃ for 5min continuously after the diesel oil is added;
(5.2) reducing the temperature of the furnace from 1340 ℃ to 1050 ℃ at a speed of 220 ℃/h, then adding diesel oil into the electric kiln, adding the diesel oil every 10min for 2 times, adding 300g of diesel oil into the space of the electric kiln per cubic meter each time, and after the diesel oil is added, heating the furnace from 1050 ℃ to 1340 ℃ at a speed of 330 ℃/h, and continuously preserving the temperature at 1340 ℃ for 10min;
(5.3) reducing the temperature of the furnace from 1340 ℃ to 400 ℃ at a speed of 150 ℃/h, stopping the furnace, opening the furnace door, and reducing the temperature of the furnace to normal temperature to obtain the purple Jin Yinhao cup.
4. The purple honeysuckle jersey cup is characterized in that the purple honeysuckle jersey cup is prepared by the process according to claim 1.
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