CN113304082A

CN113304082A - Waxy fluffy hair care foam aerosol and preparation method thereof

Info

Publication number: CN113304082A
Application number: CN202110657012.1A
Authority: CN
Inventors: 张展适; 张建研; 余洁仪; 贺青; 杨君莲
Original assignee: Zhongshan Oson Fine Chemical Industry Co ltd
Current assignee: Zhongshan Oson Fine Chemical Industry Co ltd
Priority date: 2021-06-11
Filing date: 2021-06-11
Publication date: 2021-08-27

Abstract

The invention provides a waxy fluffy hair care foam aerosol and a preparation method thereof, which comprises a film forming agent, grease, an emulsifier, a thickening agent, a humectant, a foaming agent, a softening agent, a preservative, triethanolamine, phenoxyethanol, a POLYGONUM MULTIFLORUM (POLYGONUM MULTIFLORUM) root extract, kaolin, essence, deionized water and a propellant. The hair conditioner is prepared by compounding wax raw materials, grease, an emulsifier and effective nutritional components, wherein a mixed propellant is used as an aerosol for spraying, the aerosol is sprayed to be in a foam shape, the hair conditioner has a natural setting effect, can endow hair with natural luster, refreshing, non-sticky and non-white scurf, a film formed on the hair has certain elasticity, different hairstyles can be repeatedly molded, the hair conditioner has better curling holding capacity, is natural, lasting and attractive in setting, has secondary setting capacity, has the functions of nourishing, protecting and conditioning the hair, and has the functions of moistening, nourishing and protecting the hair.

Description

Waxy fluffy hair care foam aerosol and preparation method thereof

Technical Field

The invention relates to the field of aerosols of daily chemical hair cosmetics, in particular to a waxy fluffy hair care foam aerosol and a preparation method thereof.

Background

With the increasing economic living standard, people pursue more natural beauty and also put forward natural, healthy and beautiful requirements on hairdressing products. The hair styling product is a cosmetic mainly aiming at beautifying the hair style, and is used for keeping the hair with a certain beautiful appearance, making the hair be dull but not greasy, making the hair easy to decorate and style, and having a certain conditioning and nursing effect and smooth hand feeling. Mousse, hair gel, gel water and the like are hair styling products with wide application, the formula of the product generally takes high molecular polymers such as polyvinylpyrrolidone (rubber powder K30, K90 and the like) and acrylic resin (rubber paste) as film forming materials, and the principle is that the polymer forms a firm high molecular film on the surface of hair to achieve the purpose of keeping the hair style. The following problems are present when using acrylate copolymers: firstly, the film-forming material has over-strong viscosity, is easy to cause hair adhesion, is hard and unnatural, and is only suitable for one-time shaping; secondly, the hair is dull and lusterless after the hair brush is used, and the hand feeling is rough; the polymer is easy to be white and opaque after forming a film on hair, and powder falls off after being combed, so that the attractiveness and the product experience feeling are seriously influenced; and fourthly, during cleaning, part of the polymer is poor in water solubility and is not easy to clean, and the resin is accumulated on the hair to cause the hair to be too heavy, so that the hair is not beneficial to healthy growth. Poor compatibility with hydrocarbon propellants.

Disclosure of Invention

In order to overcome the defects of the prior art, the invention provides a waxy fluffy hair care foam aerosol and a preparation method thereof.

A waxy puffing and shaping hair care foam aerosol comprises film forming agent, oil, emulsifier, thickener, humectant, foaming agent, emollient, antiseptic, triethanolamine, phenoxyethanol, radix Polygoni Multiflori (POLYGONUM MULTIFLORUM) root extract, kaolin, essence, deionized water and propellant.

In a further improvement, the extract of black sesame (SESAMUM INDICUM) is also included.

In a further improvement, the extract of the root of Glycyrrhiza GLABRA (Glycyrrhiza Glabra) is also included.

In a further improvement, the film forming agent comprises one or more of microcrystalline wax, white beeswax, myristic acid and cetyl alcohol.

In a further development, the propellant comprises propane, butane and nitrogen.

In a further improvement, the grease comprises one or more of hydrogenated polyisobutene, cyclopentadimethylsiloxane, cyclotetradimethylsiloxane and isodecyl neopentanoate.

In a further refinement, the emulsifier comprises one or more combinations of ceteareth-25, PEG-40 hydrogenated castor oil, hydrogenated palmitoleic acid, sorbitan stearate, polysorbate-60, and p-hydroxyacetophenone.

In a further development, the foaming agent comprises lauramidopropyl betaine; the softening agent is hydrogenated vegetable oil and ethylhexyl glycerin; the preservative is one or more of climbazole and chlorphenesin; the humectant comprises one or more of propylene glycol, polyquaternium-10, tocopherol (vitamin E) and butanediol; the thickening agent comprises one or more of guar hydroxypropyl trimethyl ammonium chloride, sodium chloride and stearyl alcohol stearate.

In a further improvement, the waxy fluffy shaping hair care foam aerosol comprises the following components in percentage by mass: 1.1 to 4.5 percent of propane, 2.5 to 5.5 percent of butane, 0.35 to 0.88 percent of nitrogen, 0 to 0.8 percent of microcrystalline wax, 0.4 to 0.9 percent of hydrogenated vegetable oil, 0 to 1.0 percent of white beeswax, 0.05 to 1.5 percent of hydrogenated palmitoleic acid, 0.05 to 1.3 percent of stearyl stearate, 0.8 to 3.5 percent of myristic acid, 0.8 to 1.5 percent of cetyl alcohol, 0.6 to 1.6 percent of hydrogenated polyisobutene, 0.2 to 0.9 percent of cyclopenta dimethyl siloxane, 0 to 0.5 percent of cyclotetra dimethyl siloxane, 0.8 to 1.2 percent of isodecyl neopentanoate, 0.2 to 3.5 percent of ceteareth-250.8, 0.2 to 0.6 percent of PEG-40 hydrogenated castor oil, 0.03 to 0.10 percent of guar hydroxypropyl trimethyl ammonium chloride, 0 to 0.05 percent of sodium chloride, 2.8 to 8 percent of propylene glycol, 0.2 to 0.6 percent of triethanolamine, 0.05 to 0.05 percent of polyquaternium, 0.0.1 to 0.1.1 percent of vitamin E, and 0.01 to 3.1 percent of lauryl betaine, 0.03-0.6% of phenoxyethanol, 0-1.2% of ethylhexyl glycerol, 0-0.0001% of black sesame (sesamom INDICUM) extract, 0.02-0.05% of POLYGONUM MULTIFLORUM (Polygonum MULTIFLORUM) root extract, 0-0.03% of GLYCYRRHIZA GLABRA (Glycyrrhiza GLABRA) root extract, 0.02-0.05% of climbazole, 0.22-0.55% of kaolin, 0.1-0.5% of essence, 0.1-0.8% of sorbitan stearate, 600.1-0.8% of polysorbate, 0-0.5% of p-hydroxyacetophenone, 0-0.5% of chlorphenesin, 0-0.5% of butanediol and 52.2-85.5% of deionized water.

A preparation method of waxy fluffy hair care foam aerosol comprises the following steps:

s1, mixing and heating the water phase raw materials in a water phase pot to 65-90 ℃ to completely dissolve the water phase raw materials to obtain a first dissolved substance;

s2, mixing and heating the grease and the wax raw materials in an oil phase pot to 65-90 ℃ to completely dissolve the grease and the wax raw materials to obtain a solute II;

s3, pumping the first dissolved matter and the second dissolved matter into an emulsifying pot, homogenizing at the rotating speed of 1500-3000 REV/min, stopping homogenizing after 5-10min of homogenization, stirring at the rotating speed of 15-30 REV/min, adding a thickening agent, a humectant, a foaming agent, a softening agent, a preservative, triethanolamine, phenoxyethanol, a POLYGONUM MULTIFLORUM (POLYGONUM MULTIFLORUM) root extract, kaolin and essence when stirring and cooling to 45 ℃, and uniformly stirring to obtain a mixture;

and S4, standing the mixture for 48 hours, filling the mixture into an aerosol can, and filling a propellant to obtain the waxy fluffy hair care foam shaping aerosol.

The principle and the beneficial effects of the invention are as follows:

the invention breaks through the material habit of the traditional formula, adopts the wax materials such as microcrystalline wax, white beeswax, myristic acid, cetyl alcohol and the like to form a film forming substance, does not contain polyvinylpyrrolidone and acrylic resin raw materials, can endow hair with natural luster, and has natural setting effect, refreshing, no stickiness and no white scurf; the wax material has good toughness and strong plasticity, and the formed film has certain elasticity, and different hairstyles can be repeatedly molded without re-spraying after being dried and solidified, so that the defect that the traditional hairdressing product can only be used for shaping once is overcome, and the consumers can conveniently and quickly finish the decorative hair;

the formula of the invention does not contain a setting high molecular polymer film-forming agent at all, but plays a setting role and is suitable for slightly curved hair.

According to the formula, hydrogenated polyisobutene, cyclopentadidimethyl siloxane, cyclotetradimethyl siloxane and isodecyl neopentanoate are adopted to form the grease component, so that the product has the effects of nourishing, protecting and conditioning hair, the problems of withered and yellow hair, brittleness, easy breakage and the like are solved, and the healthy growth of the hair is facilitated;

according to the formula, the functional nutritional components with the hair nourishing and moistening effects are formed by tocopherol (vitamin E), black sesame extract, polygonum multiflorum extract and glycyrrhiza glabra extract, so that the hair nourishing and moistening functions are achieved;

the formula of the invention adopts the mixed gas of propane, butane and nitrogen as the gas propellant, the spraying effect of the content is good, and the nitrogen is particularly doped as the protective gas to avoid the oxidative deterioration of the raw materials.

The product of the invention has good water solubility, is easy to be cleaned by shampoo, has no residue, can keep transparency in a wider temperature range, has good stability, and can not generate coagulum when standing or storing.

The invention is compounded by wax raw materials, grease, emulsifier and functional nutritional components for nourishing and moistening hair, the mixed propellant is used as aerosol, can be used for hair shaping by a spraying mode and is sprayed to be in a foam shape,

the hair styling gel has natural styling effect, can endow hair with natural luster, refreshing, no stickiness, no white scurf, has certain elasticity of a film formed on the hair, can repeatedly shape different hairstyles, has better curl retention capacity, is natural, lasting and attractive in styling, has secondary styling capacity, has nourishing, protecting and conditioning effects on the hair, and has functions of moistening, nourishing and caring the hair.

The present application will be described in further detail with reference to examples.

Detailed Description

Example one

The waxy fluffy hair-care foam aerosol comprises the following components in percentage by mass:

3.5% of propane, 4.5% of butane, 0.38% of nitrogen, 0.3% of microcrystalline wax, 0.4% of hydrogenated vegetable oil, 0.9% of white beeswax, 1.2% of hydrogenated palmitoleic acid, 1.2% of stearyl stearate, 1.2% of myristic acid, 1.1% of cetyl alcohol, 1.6% of hydrogenated polyisobutene, 0.5% of cyclopentadimethylsiloxane, 0.4% of cyclotetramethyldisiloxane, 1.1% of isodecyl neopentanoate, 1.8% of ceteareth-251.5%, 0.55% of PEG-40 hydrogenated castor oil, 0.10% of guar hydroxypropyltrimonium chloride, 0.02% of sodium chloride, 3.5% of propylene glycol, 0.35% of triethanolamine, 100.12% of polyquaternium, 0.01% of tocopherol (vitamin E), 2.3% of lauramidopropylphenoxybetaine, 0.15% of ethanol, 0.37% of ethylhexylglycerin, 0.0001% of black sesame (SESAMUM INUM) extract, 0.0001% of Polygonum (POLYPHOSPHORULOM) root extract, 0.04% of Glycyrrhiza GLABRA (GLZA GLABRA) extract, 0.03% of climbazole, 0.28% of kaolin, 0.10% of essence, 0.2% of sorbitan stearate, polysorbate-600.25%, 0.15% of p-hydroxyacetophenone, 0.3% of chlorphenesin, 0.15% of butanediol and the balance of deionized water.

s1, mixing and heating the water phase raw materials in a water phase pot to 65 ℃ to completely dissolve the water phase raw materials to obtain a first dissolved substance;

s2, mixing and heating the grease and the wax raw materials in an oil phase pot to 65 ℃ to completely dissolve the grease and the wax raw materials to obtain a solute II;

s3, pumping the first dissolved matter and the second dissolved matter into an emulsifying pot, homogenizing at the speed of 1500REV/min, stopping homogenizing after 5min of homogenizing, stirring at the speed of 15REV/min, adding a thickening agent, a humectant, a foaming agent, a softening agent, a preservative, triethanolamine, phenoxyethanol, a POLYGONUM MULTIFLORUM (Polygonum MULTIFLORUM) root extract, kaolin and essence when stirring and cooling to 45 ℃, and uniformly stirring to obtain a mixture;

Example two

3.5% of propane, 5.5% of butane, 0.4% of nitrogen, 0.5% of microcrystalline wax, 0.5% of hydrogenated vegetable oil, 1.0% of white beeswax, 1.4% of hydrogenated palmitoleic acid, 1.3% of stearyl stearate, 1.2% of myristic acid, 1.1% of cetyl alcohol, 1.5% of hydrogenated polyisobutene, 0.6% of cyclopentadimethylsiloxane, 0.4% of cyclotetramethyldisiloxane, 1.0% of isodecyl neopentanoate, 1.0% of ceteareth-251.5%, 0.55% of PEG-40 hydrogenated castor oil, 0.05% of guar hydroxypropyltrimonium chloride, 0.02% of sodium chloride, 4.5% of propylene glycol, 0.25% of triethanolamine, 0. 100.15% of polyquaternium, 0.01% of tocopherol (vitamin E), 2.3% of lauramidopropyl betaine, 0.15% of phenoxyethanol, 0.37% of ethylhexylglycerin, 0.0001% of black sesame (SEUM INUM) extract, 0.05% of PolyPOM MULUM root extract, 0.05% of Glycyrrhiza GLABRA (Glycyrrhiza GLABRA) extract (Glycyrrhiza GLABRA fruit root extract, 0.03% of climbazole, 0.3% of kaolin, 0.20% of essence, 0.5% of sorbitan stearate, 600.6% of polysorbate, 0.3% of p-hydroxyacetophenone, 0.3% of butanediol and the balance of deionized water.

s1, mixing and heating the water phase raw materials in a water phase pot to 75 ℃ to completely dissolve the water phase raw materials to obtain a first dissolved substance;

s2, mixing and heating the grease and the wax raw materials in an oil phase pot to 75 ℃ to completely dissolve the grease and the wax raw materials to obtain a solute II;

s3, pumping the first dissolved matter and the second dissolved matter into an emulsifying pot, homogenizing at the rotation speed of 2300REV/min, stopping homogenizing after 7.5min of homogenizing, stirring at the rotation speed of 23REV/min, adding a thickening agent, a humectant, a foaming agent, a softening agent, a preservative, triethanolamine, phenoxyethanol, a POLYGONUM MULTIFLORUM (Polygonum MULTIFLORUM) root extract, kaolin and essence when stirring and cooling to 45 ℃, and uniformly stirring to obtain a mixture;

EXAMPLE III

propane 2.5%, butane 5.5%, nitrogen 0.5%, microcrystalline wax 0.3%, hydrogenated vegetable oil 0.5%, white beeswax 0.8%, hydrogenated palmitoleic acid 1.3%, stearyl stearate 1.0%, myristic acid 2.2%, cetyl alcohol 1.0%, hydrogenated polyisobutene 1.5%, cyclopentadimethylsiloxane 0.5%, cyclotetramethyldisiloxane 0.5%, isodecyl neopentanoate 1.0%, ceteareth-252.8%, PEG-40 hydrogenated castor oil 0.6%, guar hydroxypropyltrimonium chloride 0.30%, sodium chloride 0.02%, propylene glycol 5.5%, triethanolamine 0.45%, polyquaternium-100.15%, tocopherol (vitamin E) 0.01%, lauramidopropylphenoxybetaine 2.5%, cetoxyethanol 0.15%, ethylhexylglycerin 0.35%, black sesame (sesamonum) extract 0.0001%, Polygonum MULTIFLORUM (Polygonum MULTIFLORUM) root extract 0.05%, Glycyrrhiza glabra 0.02%, Glycyrrhiza glabra (Glycyrrhiza glabra) extract 0.02%, (Glycyrrhiza glabra) root extract 0.05%, Glycyrrhiza glabra (Glycyrrhiza glabra 0.02%), 0.03% of climbazole, 0.5% of kaolin, 0.20% of essence, 0.8% of sorbitan stearate, polysorbate-600.75%, 0.45% of p-hydroxyacetophenone, 0.5% of chlorphenesin, 0.45% of butanediol and the balance of deionized water.

s1, mixing and heating the water phase raw materials in a water phase pot to 90 ℃ to completely dissolve the water phase raw materials to obtain a first dissolved substance;

s2, mixing and heating the grease and the wax raw materials in an oil phase pot to 90 ℃ to completely dissolve the grease and the wax raw materials to obtain a solute II;

s3, pumping the first dissolved matter and the second dissolved matter into an emulsifying pot, homogenizing at a rotating speed of 3000REV/min, stopping homogenizing after homogenizing for 10min, stirring at a rotating speed of 30REV/min, adding a thickening agent, a humectant, a foaming agent, a softening agent, a preservative, triethanolamine, phenoxyethanol, a POLYGONUM MULTIFLORUM (Polygonum MULTIFLORUM) root extract, kaolin and essence when stirring and cooling to 45 ℃, and uniformly stirring to obtain a mixture;

The above preferred embodiments should be considered as examples of the embodiments of the present application, and technical deductions, substitutions, improvements and the like similar to, similar to or based on the embodiments of the present application should be considered as the protection scope of the present patent.

Claims

1. A waxy puffing and shaping hair care foam aerosol is characterized by comprising a film forming agent, grease, an emulsifier, a thickening agent, a humectant, a foaming agent, a softening agent, a preservative, triethanolamine, phenoxyethanol, a POLYGONUM MULTIFLORUM (Polygonum MULTIFLORUM) root extract, kaolin, essence, deionized water and a propellant.

2. The waxy, fluffy styling hair care foam aerosol of claim 1, further comprising black sesame (SESAMUM INDICUM) extract.

3. The waxy puff styling hair care foam aerosol formulation according to claim 1, further comprising GLYCYRRHIZA GLABRA (GLYCYRRHIZA GLABRA) root extract.

4. The waxy, puff, hair care foam aerosol formulation according to claim 1, wherein said film forming agent comprises one or more of microcrystalline wax, beeswax, myristic acid and cetyl alcohol.

5. The waxy, puff hair care foam aerosol of claim 1, wherein said propellant comprises propane, butane and nitrogen.

6. The waxy puff styling hair care foam aerosol of claim 1, wherein the oil comprises one or more of hydrogenated polyisobutylene, cyclopentadimethylsiloxane, cyclotetradimethicone, and isodecyl pivalate in combination.

7. The waxy, fluffy styling hair care foam aerosol formulation according to claim 1, wherein the emulsifier comprises one or more of ceteareth-25, PEG-40 hydrogenated castor oil, hydrogenated palmitoleic acid, sorbitan stearate, polysorbate-60, and p-hydroxyacetophenone.

8. The waxy, puff hair care foam aerosol formulation according to claim 1, wherein said foaming agent comprises lauramidopropyl betaine; the softening agent is hydrogenated vegetable oil and ethylhexyl glycerin; the preservative is one or more of climbazole and chlorphenesin; the humectant comprises one or more of propylene glycol, polyquaternium-10, tocopherol (vitamin E) and butanediol; the thickening agent comprises one or more of guar hydroxypropyl trimethyl ammonium chloride, sodium chloride and stearyl alcohol stearate.

9. The waxy, fluffy styling hair care foam aerosol according to claims 1 to 8, characterized by comprising the following components by mass percent: 1.1 to 4.5 percent of propane, 2.5 to 5.5 percent of butane, 0.35 to 0.88 percent of nitrogen, 0 to 0.8 percent of microcrystalline wax, 0.4 to 0.9 percent of hydrogenated vegetable oil, 0 to 1.0 percent of white beeswax, 0.05 to 1.5 percent of hydrogenated palmitoleic acid, 0.05 to 1.3 percent of stearyl stearate, 0.8 to 3.5 percent of myristic acid, 0.8 to 1.5 percent of cetyl alcohol, 0.6 to 1.6 percent of hydrogenated polyisobutene, 0.2 to 0.9 percent of cyclopenta dimethyl siloxane, 0 to 0.5 percent of cyclotetra dimethyl siloxane, 0.8 to 1.2 percent of isodecyl neopentanoate, 0.2 to 3.5 percent of ceteareth-250.8, 0.2 to 0.6 percent of PEG-40 hydrogenated castor oil, 0.03 to 0.10 percent of guar hydroxypropyl trimethyl ammonium chloride, 0 to 0.05 percent of sodium chloride, 2.8 to 8 percent of propylene glycol, 0.2 to 0.6 percent of triethanolamine, 0.05 to 0.05 percent of polyquaternium, 0.0.1 to 0.1.1 percent of vitamin E, and 0.01 to 3.1 percent of lauryl betaine, 0.03-0.6% of phenoxyethanol, 0-1.2% of ethylhexyl glycerol, 0-0.0001% of black sesame (sesamom INDICUM) extract, 0.02-0.05% of POLYGONUM MULTIFLORUM (Polygonum MULTIFLORUM) root extract, 0-0.03% of GLYCYRRHIZA GLABRA (Glycyrrhiza GLABRA) root extract, 0.02-0.05% of climbazole, 0.22-0.55% of kaolin, 0.1-0.5% of essence, 0.1-0.8% of sorbitan stearate, 600.1-0.8% of polysorbate, 0-0.5% of p-hydroxyacetophenone, 0-0.5% of chlorphenesin, 0-0.5% of butanediol and 52.2-85.5% of deionized water.

10. A preparation method of waxy fluffy hair care foam aerosol is characterized by comprising the following steps: