CN113265316A - Processing method of Zhibai rehmannia health wine - Google Patents

Processing method of Zhibai rehmannia health wine Download PDF

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CN113265316A
CN113265316A CN202110540151.6A CN202110540151A CN113265316A CN 113265316 A CN113265316 A CN 113265316A CN 202110540151 A CN202110540151 A CN 202110540151A CN 113265316 A CN113265316 A CN 113265316A
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wine
mixture
prepared
boiling
traditional chinese
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张志年
张靖悦
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Xuzhou Lvzhiye Biological Foodstuff Co Ltd
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Xuzhou Lvzhiye Biological Foodstuff Co Ltd
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    • C12GWINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
    • C12G3/00Preparation of other alcoholic beverages
    • C12G3/04Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs
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    • A61K36/40Cornaceae (Dogwood family)
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    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/65Paeoniaceae (Peony family), e.g. Chinese peony
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    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/80Scrophulariaceae (Figwort family)
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    • A61K36/884Alismataceae (Water-plantain family)
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    • A61K36/894Dioscoreaceae (Yam family)
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    • A61K36/896Liliaceae (Lily family), e.g. daylily, plantain lily, Hyacinth or narcissus
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Abstract

The invention relates to a processing method of an Anemarrhena, phellodendron and rehmannia health wine, which is characterized in that eight traditional Chinese medicine raw materials of prepared rehmannia root, cornus officinalis (prepared), Chinese yam, tree peony bark, tuckahoe, rhizoma alismatis, rhizoma anemarrhenae and phellodendron are used according to the weight ratio of the raw materials: fructus Corni (prepared): chinese yam: moutan bark: tuckahoe, poria cocos: rhizoma alismatis: rhizoma anemarrhenae: phellodendron = 8-16: 4-8: 4-8: 3-6: 3-6: 3-6: 2-4: 2-4, preparing a traditional Chinese medicine extracting solution according to the proportion of the traditional Chinese medicine extracting solution: the weight ratio of the wine is 50: the wine is prepared by using 500-1000 parts of base wine, wherein the base wine is white wine, grape wine, yellow wine, beer or fruit wine, and the prepared wine is prepared by processing the traditional Chinese medicine extract and different base wines by using the method disclosed by the invention, so that the selection requirements of health care and health of mass consumers can be met according to different preferences of people on drinking.

Description

Processing method of Zhibai rehmannia health wine
Technical Field
The invention belongs to the technical field of wine processing and production, relates to the field of mixed wine processing, and particularly relates to a processing method of a Zhibai Dihuang health wine.
Background
The history of Zhibai Dihuang Wan is from Song, Qian second (child's drug evidence directly know) Ji Xie Dihuang Wan Jia Wei, and the prescription is from national Chinese patent medicine prescription Collection (Tianjin, Beijing prescription). Recorded in Anemarrhena, and rehmannia pill, first edition of the pharmacopoeia of the people's republic of China, 2010, the composition is composed of radix rehmanniae Preparata, Cornus officinalis Linne (prepared), rhizoma Dioscoreae, cortex moutan, Poria, Alismatis rhizoma, rhizoma anemarrhenae, and cortex Phellodendri. The prescription is a long-standing famous Chinese medicinal preparation and has the effects of nourishing yin and reducing pathogenic fire. The traditional Chinese medicine is mainly used for treating fire excess from yin deficiency, tidal fever and night sweat, dry mouth and sore throat, tinnitus and spermatorrhea, and scanty and brownish urine clinically. The compatibility of the medicines of the formula has obvious curative effect, and is carried by the past generation and modern Chinese medicine book. With the progress of the traditional Chinese medicine technology and the deepening of pharmacological research, the theoretical research related to the efficacy of the Zhibai Dihuang Wan is deepened continuously, and a more beneficial theoretical basis is provided for the clinical application of the medicine. The clinical application of Zhibai Dihuang Wan is reported in the literature as follows: 1. fever due to yin deficiency, or consumption of yin fluid due to long-term fever, or misuse of warm-dry herbs, etc., can lead to yin essence deficiency, yin deficiency leading to yang excess, water failure causing fire, afternoon tidal fever, bone steaming, fatigue heat, night fever, feverish sensation in the palms and soles, and dysphoria. 2. Night sweat is caused by overwork, blood loss and essence loss, or yin consumption due to pathogenic heat, so that yin essence deficiency, deficient fire is generated internally, yin fluid is disturbed and can not be hidden and discharged, and the symptoms of sweating in sleep, spontaneous stopping after waking, dysphoria with smothery sensation in the chest or tidal fever, red cheeks, thirst and dry throat are caused. 3. Chronic pharyngitis caused by yin deficiency or heat damaging body fluid, flaring up of deficient fire, and smoking and burning throat, and has symptoms of dry and uncomfortable throat, burning, dull pain, itching throat and dry cough, foreign body sensation, soreness and weakness in waist and knee joints, and dysphoria with feverish sensation in five hearts; chronic pharyngitis is seen in the above syndromes. 4. Tinnitus is caused by deficiency of vital essence in the kidney of old people, or loss of sexual intercourse, kidney yin deficiency, and malnutrition of the ear orifices, and has symptoms of tinnitus, vertigo, soreness and weakness in the lower back and knee joints; those with nerve deafness who see the above syndromes. 5. Spermatorrhea is caused by excessive sexual intercourse, indulgence in sexual desire, or parapsoria and disturbance of the sexual intercourse, and has the symptoms of spermatorrhea, dizziness, tinnitus, soreness and weakness in the lower back and knee joints and listlessness; sexual dysfunction with the above syndrome. In addition, it can be used for treating oral ulcer, climacteric syndrome, intermenstrual hemorrhage, chronic prostatitis, and simple breast early development of girl. The pharmacological research of the product has the effects of reducing blood sugar, regulating neuroendocrine, enhancing immunity and the like. 1. The blood sugar reducing product can reduce the blood sugar of mice with hyperglycemia caused by normal and alloxan and reduce the water intake of the mice. 2. The product can resist Leptin induced precocious puberty of young female mouse; can improve the levels of adrenocorticotropic hormone (ACTH), adrenocorticotropic hormone (CRH) and adrenal gland index (CRH) in rat plasma with renal yin deficiency, and restore the morphology of adrenal tissue and normal secretion function of cells. 3. The product can improve the level of IL-2, IL-6, TgG in the serum of young rats with renal yin deficiency and spleen index caused by adrenocortical hormone; relieve the alteration of spleen tissue structure caused by hydrocortisone, and antagonize the immunosuppressive effect of hydrocortisone. Adverse reactions reported in Zhibai Dihuang Wan (national pharmacopoeia Committee, pharmacopoeia of people's republic of China. clinical requirement of Chinese medicinal prescription preparation book, 2010 edition, 557) are not retrieved at present.
With the improvement of social progress and living standard, nutrition and health are the development trend of social happy life, the major health industry becomes an important topic of social attention, health and life prolonging are more important for people, and the formula combination of the long-standing Zhibai Dihuang pill is researched and developed for health food, in particular for developing a wine product which is popular with people, so that the health care requirement of people can be helped, and the development theme of diet for keeping and improving health is met. Through retrieval, reports and patent applications related to the Zhibai Dihuang health wine are not retrieved at present.
Disclosure of Invention
The invention aims to provide a processing method of Zhibai Dihuang health wine, which develops an ancient and modern still-used traditional Chinese medicine Zhibai Dihuang pill formula into a health wine by the scheme of the invention, expands a new formulation and application range, and enables the Zhibai Dihuang pill formula to be a unique new health wine which is popular among the popular consumer groups in taste, style and flavor, so as to improve the health care effect, meet the health requirements of people, further enrich the variety of wine and flourish the wine culture in the market.
In order to realize the invention, the following technical scheme is adopted:
the invention relates to a processing method of an Anemarrhena, phellodendron and rehmannia health wine, which is characterized in that eight traditional Chinese medicine raw materials of prepared rehmannia root, cornus officinalis (prepared), Chinese yam, tree peony bark, tuckahoe, rhizoma alismatis, rhizoma anemarrhenae and phellodendron are used according to the weight ratio of the raw materials: fructus Corni (prepared): chinese yam: moutan bark: tuckahoe, poria cocos: rhizoma alismatis: rhizoma anemarrhenae: phellodendron = 8-16: 4-8: 4-8: 3-6: 3-6: 3-6: 2-4: 2-4, preparing a traditional Chinese medicine extracting solution according to the proportion of the traditional Chinese medicine extracting solution: the weight ratio of the wine is 50: the preparation method comprises the following specific steps of preparing the raw materials in a ratio of 500-1000:
firstly, weighing qualified processed clean medicinal materials, grinding the Chinese yam, the tree peony bark, the poria cocos, the rhizoma alismatis, the rhizoma anemarrhenae and the golden cypress into coarse powder, then smashing the coarse powder together with the prepared rehmannia root and the dogwood pulp, placing the smashed mixture into an oven, drying the mixture at 75-85 ℃, taking out the dried mixture, cooling the dried mixture, and crushing the cooled mixture into 65-75-mesh powder to obtain mixed Chinese medicinal powder;
placing the traditional Chinese medicine mixed powder obtained in the step (I) into a sandwich reaction pot, adding edible alcohol with concentration content of 40-45% V/V, which is 5 times of the weight of the traditional Chinese medicine raw materials, uniformly mixing and sealing, introducing steam through a sandwich layer, heating, stirring and leaching for 12-18 hours at the temperature of 45-50 ℃, distilling under reduced pressure at-0.055 MPa to-0.085 MPa and the distillation temperature of 65-85 ℃, and collecting 45 kg of distillate for later use;
pouring out residual liquid and material residues distilled in the step (II), squeezing to obtain juice and material residues, and storing the juice and the material residues in another juice extractor; material slag is reserved;
adding purified water which is 5 times of the weight of the raw materials into the material residues in the step (three), heating to 100 ℃, stirring, boiling and extracting for 2 times, boiling and extracting for 3 hours each time, and combining the boiling and extracting solutions;
step five, combining the squeezed juice obtained in the step three and the decoction obtained in the step four, performing centrifugal separation at a centrifugal rotation speed of 12000-16000 rpm, and collecting supernatant;
filtering the supernatant obtained in the step (five) to obtain filtrate;
step seven, concentrating the filtrate obtained in the step six to 5 kg of clear paste at the temperature of between 50 and 75 ℃ and under the pressure of between-0.06 and-0.1 MPa;
adding the 5 kg of the fluid extracts obtained in the step (seven) into 45 kg of the distillate obtained in the step (two), and completely and uniformly metering to 50 kg of the distillate to obtain Chinese herbal medicine extracting solution;
step (nine), the traditional Chinese medicine extracting solution obtained in the step (eight) is prepared according to the following traditional Chinese medicine extracting solution: wine = 50: mixing at a mass ratio of 500-1000, and stirring and mixing uniformly;
placing the wine liquid obtained in the step (nine) at a temperature of between 2 ℃ below zero and 2 ℃, aging for 30 days, and then carrying out fine filtration and subpackage at a temperature of between 2 ℃ below zero and 2 ℃ to obtain a product; the wine is white spirit, wine, yellow wine, beer or fruit wine.
The prepared fructus corni in the invention is prepared according to the traditional well-known processing method of traditional Chinese medicinal materials. For example, fructus Corni is prepared by mixing with yellow wine, placing in a suitable container, sealing, heating in water, steaming until the wine is completely absorbed, taking out, and drying. Every 100 kg of cornus officinalis is treated with 20 kg of yellow rice wine (Dinganyiwei et al, Chinese traditional medicine, elephant Press, 1 st edition of 12 months 2004, page 214).
The following is a further optimization or selection of the above technical solution:
a wrapping type presser is selected for pressing in the step (III); the centrifugal separation in the step (five) is preferably performed by using a horizontal screw centrifuge.
And (5) filtering the mixture by using kieselguhr.
The preferable concentration condition in the step (VII) is 55-70 ℃, and-0.075 MPa-0.095 MPa; and (f) concentrating by using a vacuum rotary evaporator, a tubular evaporation concentrator or a plate evaporation concentrator.
And (5) filtering the fine filter in the step (ten) by using a membrane with the pore diameter of less than 0.20 mu m.
The fine filtration in the step (ten) can also adopt a rotary vacuum filter for filtration.
The above-mentioned equipments of the present invention are all equipments conventional in the art.
The invention is further preferred:
the invention relates to a processing method of Zhibai Dihuang health wine, which adopts an optimized scheme that prepared rehmannia root: fructus Corni (prepared): chinese yam: moutan bark: tuckahoe, poria cocos: rhizoma alismatis: rhizoma anemarrhenae: phellodendron = 16: 8: 8: 6: 6: 6: 4: 4, preparing the traditional Chinese medicine extracting solution according to the mass ratio: the wine is 50: the adhesive is prepared by mixing the components in a ratio of 500-1000, and comprises the following specific steps:
firstly, weighing qualified processed clean medicinal materials, grinding the Chinese yam, the tree peony bark, the poria cocos, the rhizoma alismatis, the rhizoma anemarrhenae and the golden cypress into coarse powder, then smashing the coarse powder together with the prepared rehmannia root and the dogwood pulp, placing the smashed mixture into an oven, drying the mixture at 75-85 ℃, taking out the dried mixture, cooling the dried mixture, and crushing the cooled mixture into 65-75-mesh powder to obtain mixed Chinese medicinal powder;
placing the traditional Chinese medicine mixed powder obtained in the step (I) into a sandwich reaction pot, adding edible alcohol with concentration content of 40-45% V/V, which is 5 times of the weight of the traditional Chinese medicine raw materials, uniformly mixing and sealing, introducing steam through a sandwich layer, heating, stirring and leaching for 12-18 hours at the temperature of 45-50 ℃, distilling under reduced pressure at-0.055 MPa to-0.085 MPa and the distillation temperature of 65-85 ℃, and collecting 45 kg of distillate for later use;
pouring out residual liquid and material residues distilled in the step (II), squeezing to obtain juice and material residues, and storing the juice and the material residues in another juice extractor; material slag is reserved;
adding purified water which is 5 times of the weight of the raw materials into the material residues in the step (three), heating to 100 ℃, stirring, boiling and extracting for 2 times, boiling and extracting for 3 hours each time, and combining the boiling and extracting solutions;
step five, combining the squeezed juice obtained in the step three and the decoction obtained in the step four, performing centrifugal separation at a centrifugal rotation speed of 12000-16000 rpm, and collecting supernatant;
filtering the supernatant obtained in the step (five) to obtain filtrate;
step seven, concentrating the filtrate obtained in the step six to 5 kg of clear paste at the temperature of between 50 and 75 ℃ and under the pressure of between-0.06 and-0.1 MPa;
adding the 5 kg of the fluid extracts obtained in the step (seven) into 45 kg of the distillate obtained in the step (two), and completely and uniformly metering to 50 kg of the distillate to obtain Chinese herbal medicine extracting solution;
step (nine), the traditional Chinese medicine extracting solution obtained in the step (eight) is prepared according to the following traditional Chinese medicine extracting solution: wine = 50: mixing at a mass ratio of 500-1000, and stirring and mixing uniformly;
and (ten) placing the wine liquid obtained in the step (nine) at the temperature of between 2 ℃ below zero and 2 ℃, aging for 30 days, and then carrying out fine filtration and subpackage at the temperature of between 2 ℃ below zero and 2 ℃ to obtain the product.
The present invention further preferably consists in:
the invention relates to a processing method of Zhibai Dihuang health wine, which further optimizes the scheme that the Zhibai Dihuang health wine is prepared from the following raw materials: fructus Corni (prepared): chinese yam: moutan bark: tuckahoe, poria cocos: rhizoma alismatis: rhizoma anemarrhenae: phellodendron = 12: 6: 6: 4.5: 4.5: 4.5: 3: 3, preparing the traditional Chinese medicine extracting solution according to the mass ratio: the wine is 50: the adhesive is prepared by mixing the components in a ratio of 500-1000, and comprises the following specific steps:
firstly, weighing qualified processed clean medicinal materials, grinding the Chinese yam, the tree peony bark, the poria cocos, the rhizoma alismatis, the rhizoma anemarrhenae and the golden cypress into coarse powder, then smashing the coarse powder together with the prepared rehmannia root and the dogwood pulp, placing the smashed mixture into an oven, drying the mixture at 75-85 ℃, taking out the dried mixture, cooling the dried mixture, and crushing the cooled mixture into 65-75-mesh powder to obtain mixed Chinese medicinal powder;
placing the traditional Chinese medicine mixed powder obtained in the step (I) into a sandwich reaction pot, adding edible alcohol with concentration content of 40-45% V/V, which is 5 times of the weight of the traditional Chinese medicine raw materials, uniformly mixing and sealing, introducing steam through a sandwich layer, heating, stirring and leaching for 12-18 hours at the temperature of 45-50 ℃, distilling under reduced pressure at-0.055 MPa to-0.085 MPa and the distillation temperature of 65-85 ℃, and collecting 45 kg of distillate for later use;
pouring out residual liquid and material residues distilled in the step (II), squeezing to obtain juice and material residues, and storing the juice and the material residues in another juice extractor; material slag is reserved;
adding purified water which is 5 times of the weight of the raw materials into the material residues in the step (three), heating to 100 ℃, stirring, boiling and extracting for 2 times, boiling and extracting for 3 hours each time, and combining the boiling and extracting solutions;
step five, combining the squeezed juice obtained in the step three and the decoction obtained in the step four, performing centrifugal separation at a centrifugal rotation speed of 12000-16000 rpm, and collecting supernatant;
filtering the supernatant obtained in the step (five) to obtain filtrate;
step seven, concentrating the filtrate obtained in the step six to 5 kg of clear paste at the temperature of between 50 and 75 ℃ and under the pressure of between-0.06 and-0.1 MPa;
adding the 5 kg of the fluid extracts obtained in the step (seven) into 45 kg of the distillate obtained in the step (two), and completely and uniformly metering to 50 kg of the distillate to obtain Chinese herbal medicine extracting solution;
step (nine), the traditional Chinese medicine extracting solution obtained in the step (eight) is prepared according to the following traditional Chinese medicine extracting solution: wine = 50: mixing at a mass ratio of 500-1000, and stirring and mixing uniformly;
and (ten) placing the wine liquid obtained in the step (nine) at the temperature of between 2 ℃ below zero and 2 ℃, aging for 30 days, and then carrying out fine filtration and subpackage at the temperature of between 2 ℃ below zero and 2 ℃ to obtain the product.
The present invention further preferably consists in:
the invention relates to a processing method of Zhibai Dihuang health wine, which further optimizes the scheme that the Zhibai Dihuang health wine is prepared from the following raw materials: fructus Corni (prepared): chinese yam: moutan bark: tuckahoe, poria cocos: rhizoma alismatis: rhizoma anemarrhenae: phellodendron = 8: 4: 4: 3: 3: 3: 2: 2, preparing the traditional Chinese medicine extracting solution according to the mass ratio: the wine is 50: the adhesive is prepared by mixing the components in a ratio of 500-1000, and comprises the following specific steps:
firstly, weighing qualified processed clean medicinal materials, grinding the Chinese yam, the tree peony bark, the poria cocos, the rhizoma alismatis, the rhizoma anemarrhenae and the golden cypress into coarse powder, then smashing the coarse powder together with the prepared rehmannia root and the dogwood pulp, placing the smashed mixture into an oven, drying the mixture at 75-85 ℃, taking out the dried mixture, cooling the dried mixture, and crushing the cooled mixture into 65-75-mesh powder to obtain mixed Chinese medicinal powder;
placing the traditional Chinese medicine mixed powder obtained in the step (I) into a sandwich reaction pot, adding edible alcohol with concentration content of 40-45% V/V, which is 5 times of the weight of the traditional Chinese medicine raw materials, uniformly mixing and sealing, introducing steam through a sandwich layer, heating, stirring and leaching for 12-18 hours at the temperature of 45-50 ℃, distilling under reduced pressure at-0.055 MPa to-0.085 MPa and the distillation temperature of 65-85 ℃, and collecting 45 kg of distillate for later use;
pouring out residual liquid and material residues distilled in the step (II), squeezing to obtain juice and material residues, and storing the juice and the material residues in another juice extractor; material slag is reserved;
adding purified water which is 5 times of the weight of the raw materials into the material residues in the step (three), heating to 100 ℃, stirring, boiling and extracting for 2 times, boiling and extracting for 3 hours each time, and combining the boiling and extracting solutions;
step five, combining the squeezed juice obtained in the step three and the decoction obtained in the step four, performing centrifugal separation at a centrifugal rotation speed of 12000-16000 rpm, and collecting supernatant;
filtering the supernatant obtained in the step (five) to obtain filtrate;
step seven, concentrating the filtrate obtained in the step six to 5 kg of clear paste at the temperature of between 50 and 75 ℃ and under the pressure of between-0.06 and-0.1 MPa;
adding the 5 kg of the fluid extracts obtained in the step (seven) into 45 kg of the distillate obtained in the step (two), and completely and uniformly metering to 50 kg of the distillate to obtain Chinese herbal medicine extracting solution;
step (nine), the traditional Chinese medicine extracting solution obtained in the step (eight) is prepared according to the following traditional Chinese medicine extracting solution: wine = 50: mixing at a mass ratio of 500-1000, and stirring and mixing uniformly;
and (ten) placing the wine liquid obtained in the step (nine) at the temperature of between 2 ℃ below zero and 2 ℃, aging for 30 days, and then carrying out fine filtration and subpackage at the temperature of between 2 ℃ below zero and 2 ℃ to obtain the product.
As a traditional Chinese medicine preparation, Zhibai Dihuang Wan has the functions of nourishing yin and reducing fire, and is widely used for treating diseases such as fire excess from yin deficiency, tidal fever, night sweat, dry mouth, pharyngalgia, tinnitus, spermatorrhea, scanty and brownish urine and the like in clinic. The prescription is prepared from eight traditional Chinese medicines of prepared rehmannia root, dogwood fruit (prepared), Chinese yam, tuckahoe, rhizoma alismatis, tree peony bark, rhizoma anemarrhenae and phellodendron, wherein the prepared rehmannia root is used as a monarch drug for nourishing yin and tonifying kidney, and replenishing vital essence and marrow. The pulp of dogwood fruit and the yam can tonify kidney, secure essence, tonify qi and nourish yin, and help the prepared rehmannia root to nourish kidney yin; rhizoma anemarrhenae is sweet, cold and moist in nature, can clear deficiency heat and nourish kidney yin; the golden cypress is bitter and cold, purges deficient fire, strengthens the true yin, is matched with the prepared rehmannia root to nourish yin and reduce fire, and all the medicines are used as ministerial medicines. Poria has effects in invigorating spleen and eliminating dampness; alisma orientale induces diuresis to clear heat; cortex moutan has the effects of clearing heat and cooling blood, and the three medicines are used together as adjuvant medicines for reinforcing middle energizer and reducing diarrhea, but reinforcing without greasiness. The medicines are combined to play the role of nourishing yin and reducing fire (national pharmacopoeia committee, pharmacopoeia of people's republic of China, clinical medicine need know Chinese medicine prescription preparation volume, 2010 edition, 557 page).
The invention has the following advantages:
1. the raw materials of the invention are selected from traditional Chinese medicine formula components which are derived from traditional Chinese medicine finished formula Zhibai Dihuang pills, prepared fructus Corni, rhizoma dioscoreae, cortex moutan, Poria cocos, rhizoma alismatis, rhizoma anemarrhenae and cortex phellodendri and have the effects of nourishing yin and reducing pathogenic fire, and the Zhibai Dihuang health care wine product is prepared by extracting and blending the traditional Chinese medicine formula components with the existing wine, thereby not only exploiting the application of the ancient finished formula in wine products and leading people to obtain beneficial health care effects while drinking wine, but also enriching wine culture; 2. white spirit, grape wine, yellow wine, beer or other fruit wines such as cherry wine, hawthorn wine, apple wine, medlar wine, strawberry wine, raspberry wine, pomegranate wine and the like of the Zhibai Dihuang wine prepared by the method are base wines, so that the product not only reflects the original style and flavor of the base wine, but also is added with a traditional Chinese medicine extracting solution with a health-care effect, and people can drink different wines according to own preference and benefit from the beneficial health-care effect of the traditional Chinese medicine raw materials; 3. the method comprises the steps of crushing the traditional Chinese medicine materials, stirring and extracting the crushed traditional Chinese medicine materials by low-alcohol edible ethanol at the low temperature of 45-50 ℃, then distilling the crushed traditional Chinese medicine materials under reduced pressure at the temperature of 65-85 ℃, collecting distillate, and adopting the low temperature conditions in the steps of crushing, extracting and distilling, so that the loss of organic matters and volatile substances of the traditional Chinese medicine materials can be avoided or reduced, and a good effect is achieved on ensuring the effective application of the raw materials of the traditional Chinese medicine materials; 4. the process comprises the steps of leaching the medicinal materials by using dilute alcohol, distilling to obtain alcohol and water-soluble organic components, primarily extracting fragrant substances in the volatile traditional Chinese medicinal materials along with distillate, boiling and extracting decoction dregs by using water, further and more fully extracting the water-soluble components of the medicinal materials, and performing high-speed centrifugal separation treatment, diatomite filtration, concentration and other technologies on an extracting solution, so that the yield of extract substances is improved, the clarity is better, and the aged product is filtered by using a membrane filter or a rotary vacuum filter, so that the quality of the product is ensured; 5. the processing method of the Zhibai Dihuang health wine provided by the invention is simple in process, easy to control, short in production period, low in cost, capable of realizing industrial production, and suitable for popularization and drinking of the public. The product has clear and transparent appearance, no layering and sedimentation phenomena, no change in appearance and no generation of floccules after being stored for 24 months at room temperature after sample retention, and can better ensure the product quality; 6. the base wine adopted by the invention is white wine, yellow wine, beer or other fruit wine (such as cherry wine, hawthorn wine, strawberry wine, medlar wine, raspberry wine, apple wine, pomegranate wine, waxberry wine and the like), and the compound wine prepared by the invention through the traditional Chinese medicine extract and different base wines can meet the selection requirements of health care and healthy wine of mass consumers aiming at different preferences of people for drinking; 7. the invention adopts the low-temperature freezing and aging process at the temperature of 2 ℃ below zero to 2 ℃ to better fuse the traditional Chinese medicine extracting solution and the base wine, so that the finished product keeps the style and the flavor characteristics of the original base wine and has no bad peculiar smell, and people can benefit from the beneficial health care effect of the traditional Chinese medicine raw materials while drinking different wines.
Detailed Description
The following embodiments are further described in conjunction with the examples, and although the present invention is disclosed as the preferred embodiments, it should not be construed as the limitation of the present invention, and the following preferred embodiments should be considered as the protection scope of the present invention by the improvement and decoration of the technical principle of the present invention without departing from the technical principle of the present invention.
Example 1
Firstly, weighing 16 kg of processed and qualified clean medicinal materials of prepared rehmannia root, 8 kg of cornus officinalis (prepared), 8 kg of Chinese yam, 6 kg of moutan bark, 6 kg of poria cocos, 6 kg of rhizoma alismatis, 4 kg of rhizoma anemarrhenae and 4 kg of phellodendron, grinding six materials of Chinese yam, moutan bark, poria cocos, rhizoma alismatis, rhizoma anemarrhenae and phellodendron into coarse powder, mixing the coarse powder with the prepared rehmannia root and the cornus officinalis, smashing the mixture together, placing the mixture in an oven, fully drying the mixture at 75 ℃, taking out the mixture, cooling the mixture, crushing the mixture, and sieving the powder by a 75-mesh sieve to obtain Chinese medicinal mixed powder;
secondly, placing the mixed powder of the traditional Chinese medicines obtained in the first step into a reaction pot with an interlayer, adding 290 kg of edible alcohol with the concentration of 45% V/V, uniformly mixing, sealing, introducing steam through the interlayer for heating, keeping the temperature of the feed liquid at 45 ℃, stirring and leaching for 18 hours, then carrying out reduced pressure distillation under the conditions of-0.055 MPa and the distillation temperature of 85 ℃, and collecting 45 kg of distillate for later use;
(III) pouring out the residual liquid and the material residues after the distillation in the step (II), squeezing by using a wrapping type squeezing machine to respectively obtain juice and the material residues, storing the juice in another container, and reserving the material residues for later use;
adding 290 kg of purified water into the material residue in the third step, heating to 100 ℃, stirring, boiling and extracting for 3 hours, filtering and taking the boiling extract, adding 290 kg of purified water into the filter residue, stirring, boiling and extracting for 3 hours under the condition of heating to 100 ℃, filtering and taking the boiling extract, and combining the boiling extracts for 2 times;
(V) combining the juice obtained in the step (III) and the decoction obtained in the step (IV), performing centrifugal separation by using a horizontal spiral centrifuge at the centrifugal rotation speed of 14000rpm, and collecting supernatant;
sixthly, adding 2.9 kilograms of diatomite into the supernatant obtained in the fifth step, fully stirring and uniformly mixing, and filtering by using a diatomite filter to obtain filtrate;
seventhly, concentrating the filtrate obtained in the sixth step into 5 kg of clear paste by using a vacuum rotary evaporator under the conditions of 60 ℃ and-0.085 MPa;
(eighthly), adding 5 kg of clear paste obtained in the seventh step into 45 kg of distillate obtained in the second step, and fully and uniformly containing 50 kg of traditional Chinese medicine extracting solution;
mixing 50 kg of the Chinese medicine extracting solution obtained in the step (eight) with 1000 kg of white spirit, and uniformly stirring;
and (ten) aging the wine liquid obtained in the step (nine) at-2 ℃ for 30 days, filtering by using an organic membrane tubular ultrafiltration device with the membrane aperture of 0.18 mu m at-2 ℃, and subpackaging to obtain the Zhibai Dihuang health care wine product.
Example 2
Firstly, weighing 16 kg of processed and qualified clean medicinal materials of prepared rehmannia root, 8 kg of cornus officinalis (prepared), 8 kg of Chinese yam, 6 kg of moutan bark, 6 kg of poria cocos, 6 kg of rhizoma alismatis, 4 kg of rhizoma anemarrhenae and 4 kg of phellodendron, grinding six materials of Chinese yam, moutan bark, poria cocos, rhizoma alismatis, rhizoma anemarrhenae and phellodendron into coarse powder, mixing the coarse powder with the prepared rehmannia root and the cornus officinalis, smashing the mixture together, placing the mixture in an oven, fully drying the mixture at 75 ℃, taking out the mixture, cooling the mixture, crushing the mixture, and sieving the powder by a 75-mesh sieve to obtain Chinese medicinal mixed powder;
placing the mixed powder of the traditional Chinese medicines obtained in the step (one) in a reaction pot with an interlayer, adding 290 kg of edible alcohol with the concentration of 45% V/V, uniformly mixing, sealing, introducing steam through the interlayer for heating, keeping the temperature of the feed liquid at 45 ℃, stirring and leaching for 18 hours, then carrying out reduced pressure distillation under the conditions of-0.055 MPa and the distillation temperature of 85 ℃, and collecting 45 kg of distillate for later use;
(III) pouring out the residual liquid and the material residues after the distillation in the step (II), and squeezing by using a wrapping type squeezer to respectively obtain juice and the material residues, wherein the juice is stored in another device, and the material residues are reserved;
adding 290 kg of purified water into the material residue in the third step, heating to 100 ℃, stirring, boiling and extracting for 3 hours, filtering and taking the boiling extract, adding 290 kg of purified water into the filter residue, stirring, boiling and extracting for 3 hours under the condition of heating to 100 ℃, filtering and taking the boiling extract, and combining the boiling extracts for 2 times;
(V) combining the juice obtained in the step (III) and the decoction obtained in the step (IV), performing centrifugal separation by using a horizontal spiral centrifuge, and collecting supernate at the centrifugal rotation speed of 15000 rpm;
sixthly, adding 2.9 kilograms of diatomite into the supernatant obtained in the fifth step, fully stirring and uniformly mixing, and filtering by using a diatomite filter to obtain filtrate;
seventhly, concentrating the filtrate obtained in the sixth step into 5 kg of clear paste by using a vacuum rotary evaporator under the conditions of 60 ℃ and-0.085 MPa;
(eighthly), adding 5 kg of clear paste obtained in the seventh step into 45 kg of distillate obtained in the second step, and fully and uniformly containing 50 kg of traditional Chinese medicine extracting solution;
mixing 50 kg of the Chinese medicine extracting solution obtained in the step (eight) with 500 kg of white spirit, and uniformly stirring;
and (ten) aging the wine liquid obtained in the step (nine) at-2 ℃ for 30 days, filtering by using an organic membrane tubular ultrafiltration device with the membrane aperture of 0.18 mu m at-2 ℃, and subpackaging to obtain the Zhibai Dihuang health care wine product.
Example 3
Firstly, weighing 16 kg of processed and qualified clean medicinal materials of prepared rehmannia root, 8 kg of cornus officinalis (prepared), 8 kg of Chinese yam, 6 kg of moutan bark, 6 kg of poria cocos, 6 kg of rhizoma alismatis, 4 kg of rhizoma anemarrhenae and 4 kg of phellodendron, grinding six materials of Chinese yam, moutan bark, poria cocos, rhizoma alismatis, rhizoma anemarrhenae and phellodendron into coarse powder, mixing the coarse powder with the prepared rehmannia root and the cornus officinalis, smashing the mixture together, placing the mixture in an oven, fully drying the mixture at 75 ℃, taking out the mixture, cooling the mixture, crushing the mixture, and sieving the powder by a 75-mesh sieve to obtain Chinese medicinal mixed powder;
placing the mixed powder of the traditional Chinese medicines obtained in the step (one) in a reaction pot with an interlayer, adding 290 kg of edible alcohol with the concentration of 45% V/V, uniformly mixing, sealing, introducing steam through the interlayer for heating, keeping the temperature of the feed liquid at 45 ℃, stirring and leaching for 18 hours, then carrying out reduced pressure distillation under the conditions of-0.055 MPa and the distillation temperature of 85 ℃, and collecting 45 kg of distillate for later use;
(III) pouring out the residual liquid and the material residues after the distillation in the step (II), and squeezing by using a wrapping type squeezer to respectively obtain juice and the material residues, wherein the juice is stored in another device, and the material residues are reserved;
adding 290 kg of purified water into the material residue in the third step, heating to 100 ℃, stirring, boiling and extracting for 3 hours, filtering and taking the boiling extract, adding 290 kg of purified water into the filter residue, stirring, boiling and extracting for 3 hours under the condition of heating to 100 ℃, filtering and taking the boiling extract, and combining the boiling extracts for 2 times;
(V) combining the juice obtained in the step (III) and the decoction obtained in the step (IV), performing centrifugal separation by using a horizontal spiral centrifuge, and collecting supernate at the centrifugal rotation speed of 16000 rpm;
sixthly, adding 2.9 kilograms of diatomite into the supernatant obtained in the fifth step, fully stirring and uniformly mixing, and filtering by using a diatomite filter to obtain filtrate;
seventhly, concentrating the filtrate obtained in the sixth step into 5 kg of clear paste by using a vacuum rotary evaporator under the conditions of 60 ℃ and 0.083 MPa;
(eighthly), adding 5 kg of clear paste obtained in the seventh step into 45 kg of distillate obtained in the second step, and fully and uniformly containing 50 kg of traditional Chinese medicine extracting solution;
mixing 50 kg of the Chinese medicine extracting solution obtained in the step (eight) with 950 kg of white spirit, and uniformly stirring;
and (ten) aging the wine liquid obtained in the step (nine) at the temperature of-2 ℃ for 30 days, filtering by using a rotary vacuum filter at the temperature of-2 ℃, and subpackaging to obtain the Zhibai Dihuang health care wine product.
Example 4
Firstly, weighing 16 kg of processed and qualified clean medicinal materials of prepared rehmannia root, 8 kg of cornus officinalis (prepared), 8 kg of Chinese yam, 6 kg of moutan bark, 6 kg of poria cocos, 6 kg of rhizoma alismatis, 4 kg of rhizoma anemarrhenae and 4 kg of phellodendron, grinding six materials of Chinese yam, moutan bark, poria cocos, rhizoma alismatis, rhizoma anemarrhenae and phellodendron into coarse powder, mixing the coarse powder with the prepared rehmannia root and the cornus officinalis, smashing the mixture together, placing the mixture in an oven, fully drying the mixture at 75 ℃, taking out the mixture, cooling the mixture, crushing the mixture, and sieving the powder by a 75-mesh sieve to obtain Chinese medicinal mixed powder;
placing the mixed powder of the traditional Chinese medicines obtained in the step (one) in a reaction pot with an interlayer, adding 290 kg of edible alcohol with the concentration of 45% V/V, uniformly mixing, sealing, introducing steam through the interlayer for heating, keeping the temperature of the feed liquid at 45 ℃, stirring and leaching for 18 hours, then carrying out reduced pressure distillation under the conditions of-0.055 MPa and the distillation temperature of 85 ℃, and collecting 45 kg of distillate for later use;
(III) pouring out the residual liquid and the material residues after the distillation in the step (II), and squeezing by using a wrapping type squeezer to respectively obtain juice and the material residues, wherein the juice is stored in another device, and the material residues are reserved;
adding 290 kg of purified water into the material residue in the third step, heating to 100 ℃, stirring, boiling and extracting for 3 hours, filtering and taking the boiling extract, adding 290 kg of purified water into the filter residue, stirring, boiling and extracting for 3 hours under the condition of heating to 100 ℃, filtering and taking the boiling extract, and combining the boiling extracts for 2 times;
(V) combining the juice obtained in the step (III) and the decoction obtained in the step (IV), performing centrifugal separation by using a horizontal spiral centrifuge, and collecting supernate at the centrifugal rotation speed of 16000 rpm;
sixthly, adding 2.9 kilograms of diatomite into the supernatant obtained in the fifth step, fully stirring and uniformly mixing, and filtering by using a diatomite filter to obtain filtrate;
seventhly, concentrating the filtrate obtained in the sixth step into 5 kg of clear paste by using a vacuum rotary evaporator under the conditions of 60 ℃ and 0.083 MPa;
(eighthly), adding 5 kg of clear paste obtained in the seventh step into 45 kg of distillate obtained in the second step, and fully and uniformly containing 50 kg of traditional Chinese medicine extracting solution;
mixing 50 kg of the Chinese medicine extracting solution obtained in the step (eight) with 650 kg of white spirit, and uniformly stirring;
and (ten) aging the wine liquid obtained in the step (nine) at the temperature of-2 ℃ for 30 days, filtering by using a rotary vacuum filter at the temperature of-2 ℃, and subpackaging to obtain the Zhibai Dihuang health care wine product.
Example 5
Firstly, weighing 16 kg of processed and qualified clean medicinal materials of prepared rehmannia root, 8 kg of cornus officinalis (prepared), 8 kg of Chinese yam, 6 kg of moutan bark, 6 kg of poria cocos, 6 kg of rhizoma alismatis, 4 kg of rhizoma anemarrhenae and 4 kg of phellodendron, grinding six materials of Chinese yam, moutan bark, poria cocos, rhizoma alismatis, rhizoma anemarrhenae and phellodendron into coarse powder, mixing the coarse powder with the prepared rehmannia root and the cornus officinalis, smashing the mixture together, placing the mixture in an oven, fully drying the mixture at 75 ℃, taking out the mixture, cooling the mixture, crushing the mixture, and sieving the powder by a 75-mesh sieve to obtain Chinese medicinal mixed powder;
placing the mixed powder of the traditional Chinese medicines obtained in the step (one) in a reaction pot with an interlayer, adding 290 kg of edible alcohol with the concentration of 45% V/V, uniformly mixing, sealing, introducing steam through the interlayer for heating, keeping the temperature of the feed liquid at 45 ℃, stirring and leaching for 18 hours, then carrying out reduced pressure distillation under the conditions of-0.055 MPa and the distillation temperature of 85 ℃, and collecting 45 kg of distillate for later use;
(III) pouring out the residual liquid and the material residues after the distillation in the step (II), and squeezing by using a wrapping type squeezer to respectively obtain juice and the material residues, wherein the juice is stored in another device, and the material residues are reserved;
adding 290 kg of purified water into the material residue in the third step, heating to 100 ℃, stirring, boiling and extracting for 3 hours, filtering and taking the boiling extract, adding 290 kg of purified water into the filter residue, stirring, boiling and extracting for 3 hours under the condition of heating to 100 ℃, filtering and taking the boiling extract, and combining the boiling extracts for 2 times;
(V) combining the juice obtained in the step (III) and the decoction obtained in the step (IV), performing centrifugal separation by using a horizontal spiral centrifuge, and collecting supernate at the centrifugal rotation speed of 16000 rpm;
sixthly, adding 2.9 kilograms of diatomite into the supernatant obtained in the fifth step, fully stirring and uniformly mixing, and filtering by using a diatomite filter to obtain filtrate;
seventhly, concentrating the filtrate obtained in the sixth step into 5 kg of clear paste by using a vacuum rotary evaporator under the conditions of 60 ℃ and 0.083 MPa;
(eighthly), adding 5 kg of clear paste obtained in the seventh step into 45 kg of distillate obtained in the second step, and fully and uniformly containing 50 kg of traditional Chinese medicine extracting solution;
mixing 50 kg of the Chinese medicine extracting solution obtained in the step (eight) with 750 kg of white spirit, and uniformly stirring;
and (ten) aging the wine liquid obtained in the step (nine) at the temperature of-2 ℃ for 30 days, filtering by using a rotary vacuum filter at the temperature of-2 ℃, and subpackaging to obtain the Zhibai Dihuang health care wine product.
Example 6
Firstly, weighing 16 kg of processed and qualified clean medicinal materials of prepared rehmannia root, 8 kg of cornus officinalis (prepared), 8 kg of Chinese yam, 6 kg of moutan bark, 6 kg of poria cocos, 6 kg of rhizoma alismatis, 4 kg of rhizoma anemarrhenae and 4 kg of phellodendron, grinding six materials of Chinese yam, moutan bark, poria cocos, rhizoma alismatis, rhizoma anemarrhenae and phellodendron into coarse powder, mixing the coarse powder with the prepared rehmannia root and the cornus officinalis, smashing the mixture together, placing the mixture in an oven, fully drying the mixture at 75 ℃, taking out the mixture, cooling the mixture, crushing the mixture, and sieving the powder by a 75-mesh sieve to obtain Chinese medicinal mixed powder;
placing the mixed powder of the traditional Chinese medicines obtained in the step (one) in a reaction pot with an interlayer, adding 290 kg of edible alcohol with the concentration of 45% V/V, uniformly mixing, sealing, introducing steam through the interlayer for heating, keeping the temperature of the feed liquid at 45 ℃, stirring and leaching for 18 hours, then carrying out reduced pressure distillation under the conditions of-0.055 MPa and the distillation temperature of 85 ℃, and collecting 45 kg of distillate for later use;
(III) pouring out the residual liquid and the material residues after the distillation in the step (II), and squeezing by using a wrapping type squeezer to respectively obtain juice and the material residues, wherein the juice is stored in another device, and the material residues are reserved;
adding 290 kg of purified water into the material residue in the third step, heating to 100 ℃, stirring, boiling and extracting for 3 hours, filtering and taking the boiling extract, adding 290 kg of purified water into the filter residue, stirring, boiling and extracting for 3 hours under the condition of heating to 100 ℃, filtering and taking the boiling extract, and combining the boiling extracts for 2 times;
(V) combining the juice obtained in the step (III) and the decoction obtained in the step (IV), performing centrifugal separation by using a horizontal spiral centrifuge, and collecting supernate at the centrifugal rotation speed of 16000 rpm;
sixthly, adding 2.9 kilograms of diatomite into the supernatant obtained in the fifth step, fully stirring and uniformly mixing, and filtering by using a diatomite filter to obtain filtrate;
seventhly, concentrating the filtrate obtained in the sixth step into 5 kg of clear paste by using a vacuum rotary evaporator under the conditions of 60 ℃ and 0.083 MPa;
(eighthly), adding 5 kg of clear paste obtained in the seventh step into 45 kg of distillate obtained in the second step, and fully and uniformly containing 50 kg of traditional Chinese medicine extracting solution;
mixing 50 kg of the Chinese medicine extracting solution obtained in the step (eight) with 850 kg of white spirit, and uniformly stirring;
and (ten) aging the wine liquid obtained in the step (nine) at the temperature of-2 ℃ for 30 days, filtering by using a rotary vacuum filter at the temperature of-2 ℃, and subpackaging to obtain the Zhibai Dihuang health care wine product.
Example 7
Firstly, weighing 12 kg of processed and qualified clean medicinal materials of prepared rehmannia root, 6 kg of cornus officinalis (prepared), 6 kg of Chinese yam, 4.5 kg of moutan bark, 4.5 kg of poria cocos, 4.5 kg of rhizoma alismatis, 3 kg of rhizoma anemarrhenae and 3 kg of phellodendron, grinding the six medicines of Chinese yam, moutan bark, poria cocos, rhizoma alismatis, rhizoma anemarrhenae and phellodendron into coarse powder, mixing the coarse powder with the prepared rehmannia root and the cornus officinalis, smashing the mixture together, placing the mixture in an oven, fully drying the mixture at the temperature of 80 ℃, taking out the mixture, cooling the mixture, crushing the mixture, and sieving the crushed mixture through a 70-mesh sieve to obtain Chinese medicinal mixed powder;
secondly, placing the mixed powder of the traditional Chinese medicines obtained in the first step into a reaction pot with a sandwich layer, adding 217.5 kg of edible alcohol with the concentration of 42% V/V, uniformly mixing, sealing, introducing steam into the reaction pot with the sandwich layer for heating, keeping the temperature of the feed liquid at 43 ℃, stirring and leaching for 16 hours, then carrying out reduced pressure distillation at the distillation temperature of-0.073 MPa at 70 ℃, and collecting 45 kg of distillate for later use;
(III) pouring out the residual liquid and the material residues after the distillation in the step (II), and squeezing by using a wrapping type squeezer to respectively obtain juice and the material residues, wherein the juice is stored in another device, and the material residues are reserved;
adding 217.5 kg of purified water into the residue in the step (III), heating to 100 ℃, stirring, boiling and extracting for 3 hours, filtering to obtain a boiling extract, adding 217.5 kg of purified water into the residue, stirring and boiling and extracting for 3 hours at 100 ℃, filtering to obtain a boiling extract, and combining the boiling extracts for 2 times;
(V) combining the juice obtained in the step (III) and the decoction obtained in the step (IV), performing centrifugal separation by using a horizontal spiral centrifuge, wherein the centrifugal rotation speed is 13000rpm, and collecting supernate;
sixthly, adding 2.18 kg of diatomite into the supernatant obtained in the fifth step, fully stirring and uniformly mixing, and filtering by using a diatomite filter to obtain filtrate;
seventhly, concentrating the filtrate obtained in the sixth step into 5 kg of clear paste by using a tubular evaporation concentrator at the temperature of 55 ℃ and the pressure of-0.095 MPa;
(eighthly), adding 5 kg of clear paste obtained in the seventh step into 45 kg of distillate obtained in the second step, and fully and uniformly containing 50 kg of traditional Chinese medicine extracting solution;
mixing 50 kg of the Chinese medicine extracting solution obtained in the step (eight) with 1000 kg of white spirit, and uniformly stirring;
and (ten) aging the wine liquid obtained in the step (nine) at-2 ℃ for 30 days, filtering by using an organic membrane tubular ultrafiltration device with the membrane aperture of 0.16 mu m at-2 ℃, and subpackaging to obtain the Zhibai Dihuang health care wine product.
Example 8
Firstly, weighing 12 kg of processed and qualified clean medicinal materials of prepared rehmannia root, 6 kg of cornus officinalis (prepared), 6 kg of Chinese yam, 4.5 kg of moutan bark, 4.5 kg of poria cocos, 4.5 kg of rhizoma alismatis, 3 kg of rhizoma anemarrhenae and 3 kg of phellodendron, grinding the six medicines of Chinese yam, moutan bark, poria cocos, rhizoma alismatis, rhizoma anemarrhenae and phellodendron into coarse powder, mixing the coarse powder with the prepared rehmannia root and the cornus officinalis, smashing the mixture together, placing the mixture in an oven, fully drying the mixture at the temperature of 80 ℃, taking out the mixture, cooling the mixture, crushing the mixture, and sieving the crushed mixture through a 70-mesh sieve to obtain Chinese medicinal mixed powder;
placing the mixed powder of the traditional Chinese medicines obtained in the step (one) in a reaction pot with an interlayer, adding 217.5 kg of edible alcohol with the concentration of 42% V/V, uniformly mixing, sealing, introducing steam through the interlayer for heating, keeping the temperature of the feed liquid at 43 ℃, stirring and leaching for 16 hours, then carrying out reduced pressure distillation under the conditions of-0.073 MPa and the distillation temperature of 70 ℃, and collecting 45 kg of distillate for later use;
(III) pouring out the residual liquid and the material residues after the distillation in the step (II), and squeezing by using a wrapping type squeezer to respectively obtain juice and the material residues, wherein the juice is stored in another device, and the material residues are reserved;
adding 217.5 kg of purified water into the residue in the step (III), heating to 100 ℃, stirring, boiling and extracting for 3 hours, filtering to obtain a boiling extract, adding 217.5 kg of purified water into the residue, stirring and boiling and extracting for 3 hours at 100 ℃, filtering to obtain a boiling extract, and combining the boiling extracts for 2 times;
(V) combining the juice obtained in the step (III) and the decoction obtained in the step (IV), performing centrifugal separation by using a horizontal spiral centrifuge, wherein the centrifugal rotation speed is 13000rpm, and collecting supernate;
sixthly, adding 2.18 kg of diatomite into the supernatant obtained in the fifth step, fully stirring and uniformly mixing, and filtering by using a diatomite filter to obtain filtrate;
seventhly, concentrating the filtrate obtained in the sixth step into 5 kg of clear paste by using a tubular evaporation concentrator at the temperature of 55 ℃ and the pressure of-0.095 MPa;
(eighthly), adding 5 kg of clear paste obtained in the seventh step into 45 kg of distillate obtained in the second step, and fully and uniformly containing 50 kg of traditional Chinese medicine extracting solution;
mixing 50 kg of the traditional Chinese medicine extracting solution obtained in the step (eight) with 550 kg of white spirit, and uniformly stirring;
and (ten) aging the wine liquid obtained in the step (nine) at-2 ℃ for 30 days, filtering by using an organic membrane tubular ultrafiltration device with the membrane aperture of 0.16 mu m at-2 ℃, and subpackaging to obtain the Zhibai Dihuang health care wine product.
Example 9
Firstly, weighing 12 kg of processed and qualified clean medicinal materials of prepared rehmannia root, 6 kg of cornus officinalis (prepared), 6 kg of Chinese yam, 4.5 kg of moutan bark, 4.5 kg of poria cocos, 4.5 kg of rhizoma alismatis, 3 kg of rhizoma anemarrhenae and 3 kg of phellodendron, grinding the six medicines of Chinese yam, moutan bark, poria cocos, rhizoma alismatis, rhizoma anemarrhenae and phellodendron into coarse powder, mixing the coarse powder with the prepared rehmannia root and the cornus officinalis, smashing the mixture together, placing the mixture in an oven, fully drying the mixture at the temperature of 80 ℃, taking out the mixture, cooling the mixture, crushing the mixture, and sieving the crushed mixture through a 70-mesh sieve to obtain Chinese medicinal mixed powder;
placing the mixed powder of the traditional Chinese medicines obtained in the step (one) in a reaction pot with an interlayer, adding 217.5 kg of edible alcohol with the concentration of 42% V/V, uniformly mixing, sealing, introducing steam through the interlayer for heating, keeping the temperature of the feed liquid at 43 ℃, stirring and leaching for 16 hours, then carrying out reduced pressure distillation under the conditions of-0.073 MPa and the distillation temperature of 70 ℃, and collecting 45 kg of distillate for later use;
(III) pouring out the residual liquid and the material residues after the distillation in the step (II), and squeezing by using a wrapping type squeezer to respectively obtain juice and the material residues, wherein the juice is stored in another device, and the material residues are reserved;
adding 217.5 kg of purified water into the residue in the step (III), heating to 100 ℃, stirring, boiling and extracting for 3 hours, filtering to obtain a boiling extract, adding 217.5 kg of purified water into the residue, stirring and boiling and extracting for 3 hours at 100 ℃, filtering to obtain a boiling extract, and combining the boiling extracts for 2 times;
(V) combining the juice obtained in the step (III) and the decoction obtained in the step (IV), performing centrifugal separation by using a horizontal spiral centrifuge at the centrifugal rotation speed of 14000rpm, and collecting supernatant;
sixthly, adding 2.18 kg of diatomite into the supernatant obtained in the fifth step, fully stirring and uniformly mixing, and filtering by using a diatomite filter to obtain filtrate;
seventhly, concentrating the filtrate obtained in the sixth step into 5 kg of clear paste by using a tubular evaporation concentrator at the temperature of 55 ℃ and the pressure of-0.095 MPa;
(eighthly), adding 5 kg of clear paste obtained in the seventh step into 45 kg of distillate obtained in the second step, and fully and uniformly containing 50 kg of traditional Chinese medicine extracting solution;
mixing 50 kg of the Chinese medicine extracting solution obtained in the step (eight) with 950 kg of white spirit, and uniformly stirring;
and (ten) aging the wine liquid obtained in the step (nine) at-2 ℃ for 30 days, filtering by using an organic membrane tubular ultrafiltration device with the membrane aperture of 0.16 mu m at-2 ℃, and subpackaging to obtain the Zhibai Dihuang health care wine product.
Example 10
Firstly, weighing 12 kg of processed and qualified clean medicinal materials of prepared rehmannia root, 6 kg of cornus officinalis (prepared), 6 kg of Chinese yam, 4.5 kg of moutan bark, 4.5 kg of poria cocos, 4.5 kg of rhizoma alismatis, 3 kg of rhizoma anemarrhenae and 3 kg of phellodendron, grinding the six medicines of Chinese yam, moutan bark, poria cocos, rhizoma alismatis, rhizoma anemarrhenae and phellodendron into coarse powder, mixing the coarse powder with the prepared rehmannia root and the cornus officinalis, smashing the mixture together, placing the mixture in an oven, fully drying the mixture at the temperature of 80 ℃, taking out the mixture, cooling the mixture, crushing the mixture, and sieving the crushed mixture through a 70-mesh sieve to obtain Chinese medicinal mixed powder;
placing the mixed powder of the traditional Chinese medicines obtained in the step (one) in a reaction pot with an interlayer, adding 217.5 kg of edible alcohol with the concentration of 42% V/V, uniformly mixing, sealing, introducing steam through the interlayer for heating, keeping the temperature of the feed liquid at 43 ℃, stirring and leaching for 16 hours, then carrying out reduced pressure distillation under the conditions of-0.073 MPa and the distillation temperature of 70 ℃, and collecting 45 kg of distillate for later use;
(III) pouring out the residual liquid and the material residues after the distillation in the step (II), and squeezing by using a wrapping type squeezer to respectively obtain juice and the material residues, wherein the juice is stored in another device, and the material residues are reserved;
adding 217.5 kg of purified water into the residue in the step (III), heating to 100 ℃, stirring, boiling and extracting for 3 hours, filtering to obtain a boiling extract, adding 217.5 kg of purified water into the residue, stirring and boiling and extracting for 3 hours at 100 ℃, filtering to obtain a boiling extract, and combining the boiling extracts for 2 times;
(V) combining the juice obtained in the step (III) and the decoction obtained in the step (IV), performing centrifugal separation by using a horizontal spiral centrifuge at the centrifugal rotation speed of 12000rpm, and collecting supernate;
sixthly, adding 2.18 kg of diatomite into the supernatant obtained in the fifth step, fully stirring and uniformly mixing, and filtering by using a diatomite filter to obtain filtrate;
seventhly, concentrating the filtrate obtained in the sixth step into 5 kg of clear paste by using a tubular evaporation concentrator at the temperature of 55 ℃ and the pressure of-0.095 MPa;
(eighthly), adding 5 kg of clear paste obtained in the seventh step into 45 kg of distillate obtained in the second step, and fully and uniformly containing 50 kg of traditional Chinese medicine extracting solution;
mixing 50 kg of the Chinese medicine extracting solution obtained in the step (eight) with 850 kg of white spirit, and uniformly stirring;
and (ten) aging the wine liquid obtained in the step (nine) at-2 ℃ for 30 days, filtering by using an organic membrane tubular ultrafiltration device with the membrane aperture of 0.16 mu m at-2 ℃, and subpackaging to obtain the Zhibai Dihuang health care wine product.
Example 11
Firstly, weighing 12 kg of processed and qualified clean medicinal materials of prepared rehmannia root, 6 kg of cornus officinalis (prepared), 6 kg of Chinese yam, 4.5 kg of moutan bark, 4.5 kg of poria cocos, 4.5 kg of rhizoma alismatis, 3 kg of rhizoma anemarrhenae and 3 kg of phellodendron, grinding the six medicines of Chinese yam, moutan bark, poria cocos, rhizoma alismatis, rhizoma anemarrhenae and phellodendron into coarse powder, mixing the coarse powder with the prepared rehmannia root and the cornus officinalis, smashing the mixture together, placing the mixture in an oven, fully drying the mixture at the temperature of 80 ℃, taking out the mixture, cooling the mixture, crushing the mixture, and sieving the crushed mixture through a 70-mesh sieve to obtain Chinese medicinal mixed powder;
placing the mixed powder of the traditional Chinese medicines obtained in the step (one) in a reaction pot with an interlayer, adding 217.5 kg of edible alcohol with the concentration of 42% V/V, uniformly mixing, sealing, introducing steam through the interlayer for heating, keeping the temperature of the feed liquid at 43 ℃, stirring and leaching for 16 hours, then carrying out reduced pressure distillation under the conditions of-0.073 MPa and the distillation temperature of 70 ℃, and collecting 45 kg of distillate for later use;
(III) pouring out the residual liquid and the material residues after the distillation in the step (II), and squeezing by using a wrapping type squeezer to respectively obtain juice and the material residues, wherein the juice is stored in another device, and the material residues are reserved;
adding 217.5 kg of purified water into the residue in the step (III), heating to 100 ℃, stirring, boiling and extracting for 3 hours, filtering to obtain a boiling extract, adding 217.5 kg of purified water into the residue, stirring and boiling and extracting for 3 hours at 100 ℃, filtering to obtain a boiling extract, and combining the boiling extracts for 2 times;
(V) combining the juice obtained in the step (III) and the decoction obtained in the step (IV), performing centrifugal separation by using a horizontal spiral centrifuge, wherein the centrifugal rotation speed is 13000rpm, and collecting supernate;
sixthly, adding 2.18 kg of diatomite into the supernatant obtained in the fifth step, fully stirring and uniformly mixing, and filtering by using a diatomite filter to obtain filtrate;
seventhly, concentrating the filtrate obtained in the sixth step into 5 kg of clear paste by using a tubular evaporation concentrator at the temperature of 55 ℃ and the pressure of-0.095 MPa;
(eighthly), adding 5 kg of clear paste obtained in the seventh step into 45 kg of distillate obtained in the second step, and fully and uniformly containing 50 kg of traditional Chinese medicine extracting solution;
mixing 50 kg of the Chinese medicine extracting solution obtained in the step (eight) with 750 kg of white spirit, and uniformly stirring;
and (ten) aging the wine liquid obtained in the step (nine) at-2 ℃ for 30 days, filtering by using an organic membrane tubular ultrafiltration device with the membrane aperture of 0.16 mu m at-2 ℃, and subpackaging to obtain the Zhibai Dihuang health care wine product.
Example 12
Firstly, weighing 8 kg of processed and qualified clean medicinal materials of prepared rehmannia root, 4 kg of cornus officinalis (prepared), 4 kg of Chinese yam, 3 kg of tree peony bark, 3 kg of poria cocos, 3 kg of rhizoma alismatis, 2 kg of rhizoma anemarrhenae and 2 kg of golden cypress, grinding six materials of Chinese yam, tree peony bark, poria cocos, rhizoma alismatis, rhizoma anemarrhenae and golden cypress into coarse powder, mixing the coarse powder with the prepared rehmannia root and the cornus officinalis, smashing the mixture together, placing the mixture in an oven, fully drying the mixture at 75 ℃, taking the mixture out, cooling the mixture, crushing the mixture, and sieving the powder by a 75-mesh sieve to obtain Chinese medicinal mixed powder;
secondly, putting the mixed powder of the traditional Chinese medicines obtained in the first step into a sandwich reaction pot, adding 145 kg of edible alcohol with the concentration of 40% V/V, uniformly mixing, sealing, introducing steam through a sandwich layer for heating, keeping the temperature of the feed liquid at 50 ℃, stirring and leaching for 12 hours, then carrying out reduced pressure distillation under the conditions of-0.085 MPa and the distillation temperature of 85 ℃, and collecting 45 kg of distillate for later use;
(III) pouring out the residual liquid and the material residues after the distillation in the step (II), and squeezing by using a wrapping type squeezer to respectively obtain juice and the material residues, wherein the juice is stored in another device, and the material residues are reserved;
adding 145 kg of purified water into the material residue in the third step, heating to 100 ℃, stirring, boiling and extracting for 3 hours, filtering to obtain a boiling extract, adding 145 kg of purified water into the filter residue, stirring, boiling and extracting for 3 hours under the condition of heating to 100 ℃, filtering to obtain a boiling extract, and combining the boiling extracts for 2 times;
(V) combining the juice obtained in the step (III) and the decoction obtained in the step (IV), performing centrifugal separation by using a horizontal spiral centrifuge, wherein the centrifugal rotation speed is 11000rpm, and collecting supernatant;
sixthly, adding 1.45 kg of diatomite into the supernatant obtained in the fifth step, fully stirring and uniformly mixing, and filtering by using a diatomite filter to obtain filtrate;
seventhly, concentrating the filtrate obtained in the sixth step into 5 kg of clear paste by using a plate-type evaporation concentrator at the temperature of 70 ℃ and the pressure of-0.075 MPa;
(eighthly), adding 5 kg of clear paste obtained in the seventh step into 45 kg of distillate obtained in the second step, and fully and uniformly containing 50 kg of traditional Chinese medicine extracting solution;
mixing 50 kg of the Chinese medicine extracting solution obtained in the step (eight) with 1000 kg of white spirit, and uniformly stirring;
and (ten) aging the wine liquid obtained in the step (nine) at-1 ℃ for 30 days, filtering by using an organic membrane tubular ultrafiltration device with the membrane aperture of 0.16 mu m at-1 ℃, and subpackaging to obtain the Zhibai Dihuang health care wine product.
Example 13
Firstly, weighing 8 kg of processed and qualified clean medicinal materials of prepared rehmannia root, 4 kg of cornus officinalis (prepared), 4 kg of Chinese yam, 3 kg of tree peony bark, 3 kg of poria cocos, 3 kg of rhizoma alismatis, 2 kg of rhizoma anemarrhenae and 2 kg of golden cypress, grinding six materials of Chinese yam, tree peony bark, poria cocos, rhizoma alismatis, rhizoma anemarrhenae and golden cypress into coarse powder, mixing the coarse powder with the prepared rehmannia root and the cornus officinalis, smashing the mixture together, placing the mixture in an oven, fully drying the mixture at 75 ℃, taking the mixture out, cooling the mixture, crushing the mixture, and sieving the powder by a 75-mesh sieve to obtain Chinese medicinal mixed powder;
secondly, putting the mixed powder of the traditional Chinese medicines obtained in the first step into a sandwich reaction pot, adding 145 kg of edible alcohol with the concentration of 40% V/V, uniformly mixing, sealing, introducing steam through a sandwich layer for heating, keeping the temperature of the feed liquid at 50 ℃, stirring and leaching for 12 hours, then carrying out reduced pressure distillation under the conditions of-0.085 MPa and the distillation temperature of 85 ℃, and collecting 45 kg of distillate for later use;
(III) pouring out the residual liquid and the material residues after the distillation in the step (II), and squeezing by using a wrapping type squeezer to respectively obtain juice and the material residues, wherein the juice is stored in another device, and the material residues are reserved;
adding 145 kg of purified water into the material residue in the third step, heating to 100 ℃, stirring, boiling and extracting for 3 hours, filtering to obtain a boiling extract, adding 145 kg of purified water into the filter residue, stirring, boiling and extracting for 3 hours under the condition of heating to 100 ℃, filtering to obtain a boiling extract, and combining the boiling extracts for 2 times;
(V) combining the juice obtained in the step (III) and the decoction obtained in the step (IV), performing centrifugal separation by using a horizontal spiral centrifuge, wherein the centrifugal rotation speed is 11000rpm, and collecting supernatant;
sixthly, adding 1.45 kg of diatomite into the supernatant obtained in the fifth step, fully stirring and uniformly mixing, and filtering by using a diatomite filter to obtain filtrate;
seventhly, concentrating the filtrate obtained in the sixth step into 5 kg of clear paste by using a plate-type evaporation concentrator at the temperature of 70 ℃ and the pressure of-0.075 MPa;
(eighthly), adding 5 kg of clear paste obtained in the seventh step into 45 kg of distillate obtained in the second step, and fully and uniformly containing 50 kg of traditional Chinese medicine extracting solution;
mixing 50 kg of the Chinese medicine extracting solution obtained in the step (eight) with 950 kg of white spirit, and uniformly stirring;
and (ten) aging the wine liquid obtained in the step (nine) at-1 ℃ for 30 days, filtering by using an organic membrane tubular ultrafiltration device with the membrane aperture of 0.16 mu m at-1 ℃, and subpackaging to obtain the Zhibai Dihuang health care wine product.
Example 14
Firstly, weighing 8 kg of processed and qualified clean medicinal materials of prepared rehmannia root, 4 kg of cornus officinalis (prepared), 4 kg of Chinese yam, 3 kg of tree peony bark, 3 kg of poria cocos, 3 kg of rhizoma alismatis, 2 kg of rhizoma anemarrhenae and 2 kg of golden cypress, grinding six materials of Chinese yam, tree peony bark, poria cocos, rhizoma alismatis, rhizoma anemarrhenae and golden cypress into coarse powder, mixing the coarse powder with the prepared rehmannia root and the cornus officinalis, smashing the mixture together, placing the mixture in an oven, fully drying the mixture at 75 ℃, taking the mixture out, cooling the mixture, crushing the mixture, and sieving the powder by a 75-mesh sieve to obtain Chinese medicinal mixed powder;
secondly, putting the mixed powder of the traditional Chinese medicines obtained in the first step into a sandwich reaction pot, adding 145 kg of edible alcohol with the concentration of 40% V/V, uniformly mixing, sealing, introducing steam through a sandwich layer for heating, keeping the temperature of the feed liquid at 50 ℃, stirring and leaching for 12 hours, then carrying out reduced pressure distillation under the conditions of-0.085 MPa and the distillation temperature of 85 ℃, and collecting 45 kg of distillate for later use;
(III) pouring out the residual liquid and the material residues after the distillation in the step (II), and squeezing by using a wrapping type squeezer to respectively obtain juice and the material residues, wherein the juice is stored in another device, and the material residues are reserved;
adding 145 kg of purified water into the material residue in the third step, heating to 100 ℃, stirring, boiling and extracting for 3 hours, filtering to obtain a boiling extract, adding 145 kg of purified water into the filter residue, stirring, boiling and extracting for 3 hours under the condition of heating to 100 ℃, filtering to obtain a boiling extract, and combining the boiling extracts for 2 times;
(V) combining the juice obtained in the step (III) and the decoction obtained in the step (IV), separating by using a horizontal spiral centrifuge, centrifuging at the rotating speed of 12000rpm, and collecting supernatant;
sixthly, adding 1.45 kg of diatomite into the supernatant obtained in the fifth step, fully stirring and uniformly mixing, and filtering by using a diatomite filter to obtain filtrate;
seventhly, concentrating the filtrate obtained in the sixth step into 5 kg of clear paste by using a plate-type evaporation concentrator at the temperature of 70 ℃ and the pressure of-0.075 MPa;
(eighthly), adding 5 kg of clear paste obtained in the seventh step into 45 kg of distillate obtained in the second step, and fully and uniformly containing 50 kg of traditional Chinese medicine extracting solution;
mixing 50 kg of the Chinese medicine extracting solution obtained in the step (eight) with 500 kg of white spirit, and uniformly stirring;
and (ten) aging the wine liquid obtained in the step (nine) at-1 ℃ for 30 days, filtering by using an organic membrane tubular ultrafiltration device with the membrane aperture of 0.16 mu m at-1 ℃, and subpackaging to obtain the Zhibai Dihuang health care wine product.
Example 15
Firstly, weighing 8 kg of processed and qualified clean medicinal materials of prepared rehmannia root, 4 kg of cornus officinalis (prepared), 4 kg of Chinese yam, 3 kg of tree peony bark, 3 kg of poria cocos, 3 kg of rhizoma alismatis, 2 kg of rhizoma anemarrhenae and 2 kg of golden cypress, grinding six materials of Chinese yam, tree peony bark, poria cocos, rhizoma alismatis, rhizoma anemarrhenae and golden cypress into coarse powder, mixing the coarse powder with the prepared rehmannia root and the cornus officinalis, smashing the mixture together, placing the mixture in an oven, fully drying the mixture at 75 ℃, taking the mixture out, cooling the mixture, crushing the mixture, and sieving the powder by a 75-mesh sieve to obtain Chinese medicinal mixed powder;
secondly, putting the mixed powder of the traditional Chinese medicines obtained in the first step into a sandwich reaction pot, adding 145 kg of edible alcohol with the concentration of 40% V/V, uniformly mixing, sealing, introducing steam through a sandwich layer for heating, keeping the temperature of the feed liquid at 50 ℃, stirring and leaching for 12 hours, then carrying out reduced pressure distillation under the conditions of-0.085 MPa and the distillation temperature of 85 ℃, and collecting 45 kg of distillate for later use;
(III) pouring out the residual liquid and the material residues after the distillation in the step (II), and squeezing by using a wrapping type squeezer to respectively obtain juice and the material residues, wherein the juice is stored in another device, and the material residues are reserved;
adding 145 kg of purified water into the material residue in the third step, heating to 100 ℃, stirring, boiling and extracting for 3 hours, filtering to obtain a boiling extract, adding 145 kg of purified water into the filter residue, stirring, boiling and extracting for 3 hours under the condition of heating to 100 ℃, filtering to obtain a boiling extract, and combining the boiling extracts for 2 times;
(V) combining the juice obtained in the step (III) and the decoction obtained in the step (IV), performing centrifugal separation by using a horizontal spiral centrifuge at the centrifugal rotation speed of 12000rpm, and collecting supernate;
sixthly, adding 1.45 kg of diatomite into the supernatant obtained in the fifth step, fully stirring and uniformly mixing, and filtering by using a diatomite filter to obtain filtrate;
seventhly, concentrating the filtrate obtained in the sixth step into 5 kg of clear paste by using a plate-type evaporation concentrator at the temperature of 70 ℃ and the pressure of-0.075 MPa;
(eighthly), adding 5 kg of clear paste obtained in the seventh step into 45 kg of distillate obtained in the second step, and fully and uniformly containing 50 kg of traditional Chinese medicine extracting solution;
mixing 50 kg of the Chinese medicine extracting solution obtained in the step (eight) with 850 kg of white spirit, and uniformly stirring;
and (ten) aging the wine liquid obtained in the step (nine) at-1 ℃ for 30 days, filtering by using an organic membrane tubular ultrafiltration device with the membrane aperture of 0.16 mu m at-1 ℃, and subpackaging to obtain the Zhibai Dihuang health care wine product.
Example 16
Firstly, weighing 12 kg of processed and qualified clean medicinal materials of prepared rehmannia root, 6 kg of cornus officinalis (prepared), 6 kg of Chinese yam, 4.5 kg of moutan bark, 4.5 kg of poria cocos, 4.5 kg of rhizoma alismatis, 3 kg of rhizoma anemarrhenae and 3 kg of phellodendron, grinding the six medicines of Chinese yam, moutan bark, poria cocos, rhizoma alismatis, rhizoma anemarrhenae and phellodendron into coarse powder, mixing the coarse powder with the prepared rehmannia root and the cornus officinalis, smashing the mixture together, placing the mixture in an oven, fully drying the mixture at the temperature of 80 ℃, taking out the mixture, cooling the mixture, crushing the mixture, and sieving the crushed mixture through a 70-mesh sieve to obtain Chinese medicinal mixed powder;
placing the mixed powder of the traditional Chinese medicines obtained in the step (one) in a reaction pot with an interlayer, adding 217.5 kg of edible alcohol with the concentration of 42% V/V, uniformly mixing, sealing, introducing steam through the interlayer for heating, keeping the temperature of the feed liquid at 43 ℃, stirring and leaching for 16 hours, then carrying out reduced pressure distillation under the conditions of-0.073 MPa and the distillation temperature of 70 ℃, and collecting 45 kg of distillate for later use;
(III) pouring out the residual liquid and the material residues after the distillation in the step (II), and squeezing by using a wrapping type squeezer to respectively obtain juice and the material residues, wherein the juice is stored in another device, and the material residues are reserved;
adding 217.5 kg of purified water into the residue in the step (III), heating to 100 ℃, stirring, boiling and extracting for 3 hours, filtering to obtain a boiling extract, adding 217.5 kg of purified water into the residue, stirring and boiling and extracting for 3 hours at 100 ℃, filtering to obtain a boiling extract, and combining the boiling extracts for 2 times;
(V) combining the juice obtained in the step (III) and the decoction obtained in the step (IV), performing centrifugal separation by using a horizontal spiral centrifuge at the centrifugal rotation speed of 14000rpm, and collecting supernatant;
sixthly, adding 2.18 kg of diatomite into the supernatant obtained in the fifth step, fully stirring and uniformly mixing, and filtering by using a diatomite filter to obtain filtrate;
seventhly, concentrating the filtrate obtained in the sixth step into 5 kg of clear paste by using a tubular evaporation concentrator at the temperature of 55 ℃ and the pressure of-0.095 MPa;
(eighthly), adding 5 kg of clear paste obtained in the seventh step into 45 kg of distillate obtained in the second step, and fully and uniformly containing 50 kg of traditional Chinese medicine extracting solution;
mixing 50 kg of the traditional Chinese medicine extracting solution obtained in the step (eight) with 1000 kg of wine, and uniformly stirring;
and (ten) aging the wine liquid obtained in the step (nine) at 2 ℃ for 30 days, filtering by using an organic membrane tubular ultrafiltration device with the membrane aperture of 0.16 mu m at 2 ℃, and subpackaging to obtain the Zhibai Dihuang wine product.
Example 17
Firstly, weighing 12 kg of processed and qualified clean medicinal materials of prepared rehmannia root, 6 kg of cornus officinalis (prepared), 6 kg of Chinese yam, 4.5 kg of moutan bark, 4.5 kg of poria cocos, 4.5 kg of rhizoma alismatis, 3 kg of rhizoma anemarrhenae and 3 kg of phellodendron, grinding the six medicines of Chinese yam, moutan bark, poria cocos, rhizoma alismatis, rhizoma anemarrhenae and phellodendron into coarse powder, mixing the coarse powder with the prepared rehmannia root and the cornus officinalis, smashing the mixture together, placing the mixture in an oven, fully drying the mixture at the temperature of 80 ℃, taking out the mixture, cooling the mixture, crushing the mixture, and sieving the crushed mixture through a 70-mesh sieve to obtain Chinese medicinal mixed powder;
placing the mixed powder of the traditional Chinese medicines obtained in the step (one) in a reaction pot with an interlayer, adding 217.5 kg of edible alcohol with the concentration of 42% V/V, uniformly mixing, sealing, introducing steam through the interlayer for heating, keeping the temperature of the feed liquid at 43 ℃, stirring and leaching for 16 hours, then carrying out reduced pressure distillation under the conditions of-0.073 MPa and the distillation temperature of 70 ℃, and collecting 45 kg of distillate for later use;
(III) pouring out the residual liquid and the material residues after the distillation in the step (II), and squeezing by using a wrapping type squeezer to respectively obtain juice and the material residues, wherein the juice is stored in another device, and the material residues are reserved;
adding 217.5 kg of purified water into the residue in the step (III), heating to 100 ℃, stirring, boiling and extracting for 3 hours, filtering to obtain a boiling extract, adding 217.5 kg of purified water into the residue, stirring and boiling and extracting for 3 hours at 100 ℃, filtering to obtain a boiling extract, and combining the boiling extracts for 2 times;
(V) combining the juice obtained in the step (III) and the decoction obtained in the step (IV), performing centrifugal separation by using a horizontal spiral centrifuge, and collecting supernate at the centrifugal rotation speed of 15000 rpm;
sixthly, adding 2.18 kg of diatomite into the supernatant obtained in the fifth step, fully stirring and uniformly mixing, and filtering by using a diatomite filter to obtain filtrate;
seventhly, concentrating the filtrate obtained in the sixth step into 5 kg of clear paste by using a vacuum rotary evaporator under the conditions of 55 ℃ and-0.095 MPa;
(eighthly), adding 5 kg of clear paste obtained in the seventh step into 45 kg of distillate obtained in the second step, and fully and uniformly containing 50 kg of traditional Chinese medicine extracting solution;
mixing 50 kg of the traditional Chinese medicine extracting solution obtained in the step (eight) with 500 kg of wine, and uniformly stirring;
and (ten) aging the wine liquid obtained in the step (nine) at 2 ℃ for 30 days, filtering by using an organic membrane tubular ultrafiltration device with the membrane aperture of 0.16 mu m at 2 ℃, and subpackaging to obtain the Zhibai Dihuang wine product.
Example 18
Firstly, weighing 12 kg of processed and qualified clean medicinal materials of prepared rehmannia root, 6 kg of cornus officinalis (prepared), 6 kg of Chinese yam, 4.5 kg of moutan bark, 4.5 kg of poria cocos, 4.5 kg of rhizoma alismatis, 3 kg of rhizoma anemarrhenae and 3 kg of phellodendron, grinding the six medicines of Chinese yam, moutan bark, poria cocos, rhizoma alismatis, rhizoma anemarrhenae and phellodendron into coarse powder, mixing the coarse powder with the prepared rehmannia root and the cornus officinalis, smashing the mixture together, placing the mixture in an oven, fully drying the mixture at the temperature of 80 ℃, taking out the mixture, cooling the mixture, crushing the mixture, and sieving the crushed mixture through a 70-mesh sieve to obtain Chinese medicinal mixed powder;
placing the mixed powder of the traditional Chinese medicines obtained in the step (one) in a reaction pot with an interlayer, adding 217.5 kg of edible alcohol with the concentration of 42% V/V, uniformly mixing, sealing, introducing steam through the interlayer for heating, keeping the temperature of the feed liquid at 43 ℃, stirring and leaching for 16 hours, then carrying out reduced pressure distillation under the conditions of-0.073 MPa and the distillation temperature of 70 ℃, and collecting 45 kg of distillate for later use;
(III) pouring out the residual liquid and the material residues after the distillation in the step (II), and squeezing by using a wrapping type squeezer to respectively obtain juice and the material residues, wherein the juice is stored in another device, and the material residues are reserved;
adding 217.5 kg of purified water into the residue in the step (III), heating to 100 ℃, stirring, boiling and extracting for 3 hours, filtering to obtain a boiling extract, adding 217.5 kg of purified water into the residue, stirring and boiling and extracting for 3 hours at 100 ℃, filtering to obtain a boiling extract, and combining the boiling extracts for 2 times;
(V) combining the juice obtained in the step (III) and the decoction obtained in the step (IV), performing centrifugal separation by using a horizontal spiral centrifuge at the centrifugal rotation speed of 14000rpm, and collecting supernatant;
sixthly, adding 2.18 kg of diatomite into the supernatant obtained in the fifth step, fully stirring and uniformly mixing, and filtering by using a diatomite filter to obtain filtrate;
seventhly, concentrating the filtrate obtained in the sixth step into 5 kg of clear paste by using a tubular evaporation concentrator at the temperature of 55 ℃ and the pressure of-0.095 MPa;
(eighthly), adding 5 kg of clear paste obtained in the seventh step into 45 kg of distillate obtained in the second step, and fully and uniformly containing 50 kg of traditional Chinese medicine extracting solution;
mixing 50 kg of the traditional Chinese medicine extracting solution obtained in the step (eight) with 750 kg of wine, and uniformly stirring;
and (ten) aging the wine liquid obtained in the step (nine) at 2 ℃ for 30 days, filtering by using an organic membrane tubular ultrafiltration device with the membrane aperture of 0.16 mu m at 2 ℃, and subpackaging to obtain the Zhibai Dihuang wine product.
Example 19
Firstly, weighing 12 kg of processed and qualified clean medicinal materials of prepared rehmannia root, 6 kg of cornus officinalis (prepared), 6 kg of Chinese yam, 4.5 kg of moutan bark, 4.5 kg of poria cocos, 4.5 kg of rhizoma alismatis, 3 kg of rhizoma anemarrhenae and 3 kg of phellodendron, grinding the six medicines of Chinese yam, moutan bark, poria cocos, rhizoma alismatis, rhizoma anemarrhenae and phellodendron into coarse powder, mixing the coarse powder with the prepared rehmannia root and the cornus officinalis, smashing the mixture together, placing the mixture in an oven, fully drying the mixture at the temperature of 80 ℃, taking out the mixture, cooling the mixture, crushing the mixture, and sieving the crushed mixture through a 70-mesh sieve to obtain Chinese medicinal mixed powder;
placing the mixed powder of the traditional Chinese medicines obtained in the step (one) in a reaction pot with an interlayer, adding 217.5 kg of edible alcohol with the concentration of 42% V/V, uniformly mixing, sealing, introducing steam through the interlayer for heating, keeping the temperature of the feed liquid at 43 ℃, stirring and leaching for 16 hours, then carrying out reduced pressure distillation under the conditions of-0.073 MPa and the distillation temperature of 70 ℃, and collecting 45 kg of distillate for later use;
(III) pouring out the residual liquid and the material residues after the distillation in the step (II), and squeezing by using a wrapping type squeezer to respectively obtain juice and the material residues, wherein the juice is stored in another device, and the material residues are reserved;
adding 217.5 kg of purified water into the residue in the step (III), heating to 100 ℃, stirring, boiling and extracting for 3 hours, filtering to obtain a boiling extract, adding 217.5 kg of purified water into the residue, stirring and boiling and extracting for 3 hours at 100 ℃, filtering to obtain a boiling extract, and combining the boiling extracts for 2 times;
(V) combining the juice obtained in the step (III) and the decoction obtained in the step (IV), performing centrifugal separation by using a horizontal spiral centrifuge, wherein the centrifugal rotation speed is 13000rpm, and collecting supernate;
sixthly, adding 2.18 kg of diatomite into the supernatant obtained in the fifth step, fully stirring and uniformly mixing, and filtering by using a diatomite filter to obtain filtrate;
seventhly, concentrating the filtrate obtained in the sixth step into 5 kg of clear paste by using a vacuum rotary evaporator under the conditions of 55 ℃ and-0.095 MPa;
(eighthly), adding 5 kg of clear paste obtained in the seventh step into 45 kg of distillate obtained in the second step, and fully and uniformly containing 50 kg of traditional Chinese medicine extracting solution;
mixing 50 kg of the traditional Chinese medicine extracting solution obtained in the step (eight) with 500 kg of wine, and uniformly stirring;
and (ten) aging the wine liquid obtained in the step (nine) at 2 ℃ for 30 days, filtering by using an organic membrane tubular ultrafiltration device with the membrane aperture of 0.16 mu m at 2 ℃, and subpackaging to obtain the Zhibai Dihuang wine product.
Example 20
Firstly, weighing 12 kg of processed and qualified clean medicinal materials of prepared rehmannia root, 6 kg of cornus officinalis (prepared), 6 kg of Chinese yam, 4.5 kg of moutan bark, 4.5 kg of poria cocos, 4.5 kg of rhizoma alismatis, 3 kg of rhizoma anemarrhenae and 3 kg of phellodendron, grinding the six medicines of Chinese yam, moutan bark, poria cocos, rhizoma alismatis, rhizoma anemarrhenae and phellodendron into coarse powder, mixing the coarse powder with the prepared rehmannia root and the cornus officinalis, smashing the mixture together, placing the mixture in an oven, fully drying the mixture at the temperature of 80 ℃, taking out the mixture, cooling the mixture, crushing the mixture, and sieving the crushed mixture through a 70-mesh sieve to obtain Chinese medicinal mixed powder;
placing the mixed powder of the traditional Chinese medicines obtained in the step (one) in a reaction pot with an interlayer, adding 217.5 kg of edible alcohol with the concentration of 42% V/V, uniformly mixing, sealing, introducing steam through the interlayer for heating, keeping the temperature of the feed liquid at 43 ℃, stirring and leaching for 16 hours, then carrying out reduced pressure distillation under the conditions of-0.073 MPa and the distillation temperature of 70 ℃, and collecting 45 kg of distillate for later use;
(III) pouring out the residual liquid and the material residues after the distillation in the step (II), and squeezing by using a wrapping type squeezer to respectively obtain juice and the material residues, wherein the juice is stored in another device, and the material residues are reserved;
adding 217.5 kg of purified water into the residue in the step (III), heating to 100 ℃, stirring, boiling and extracting for 3 hours, filtering to obtain a boiling extract, adding 217.5 kg of purified water into the residue, stirring and boiling and extracting for 3 hours at 100 ℃, filtering to obtain a boiling extract, and combining the boiling extracts for 2 times;
(V) combining the juice obtained in the step (III) and the decoction obtained in the step (IV), performing centrifugal separation by using a horizontal spiral centrifuge at the centrifugal rotation speed of 14000rpm, and collecting supernatant;
sixthly, adding 2.18 kg of diatomite into the supernatant obtained in the fifth step, fully stirring and uniformly mixing, and filtering by using a diatomite filter to obtain filtrate;
seventhly, concentrating the filtrate obtained in the sixth step into 5 kg of clear paste by using a tubular evaporation concentrator at the temperature of 55 ℃ and the pressure of-0.095 MPa;
(eighthly), adding 5 kg of clear paste obtained in the seventh step into 45 kg of distillate obtained in the second step, and fully and uniformly containing 50 kg of traditional Chinese medicine extracting solution;
mixing 50 kg of the traditional Chinese medicine extracting solution obtained in the step (VIII) with 500 kg of yellow wine, and uniformly stirring;
and (ten) aging the wine liquid obtained in the step (nine) at 2 ℃ for 30 days, filtering by using an organic membrane tubular ultrafiltration device with the membrane aperture of 0.16 mu m at 2 ℃, and subpackaging to obtain the Zhibai Dihuang yellow wine product.
Example 21
Firstly, weighing 12 kg of processed and qualified clean medicinal materials of prepared rehmannia root, 6 kg of cornus officinalis (prepared), 6 kg of Chinese yam, 4.5 kg of moutan bark, 4.5 kg of poria cocos, 4.5 kg of rhizoma alismatis, 3 kg of rhizoma anemarrhenae and 3 kg of phellodendron, grinding the six medicines of Chinese yam, moutan bark, poria cocos, rhizoma alismatis, rhizoma anemarrhenae and phellodendron into coarse powder, mixing the coarse powder with the prepared rehmannia root and the cornus officinalis, smashing the mixture together, placing the mixture in an oven, fully drying the mixture at the temperature of 80 ℃, taking out the mixture, cooling the mixture, crushing the mixture, and sieving the crushed mixture through a 70-mesh sieve to obtain Chinese medicinal mixed powder;
placing the mixed powder of the traditional Chinese medicines obtained in the step (one) in a reaction pot with an interlayer, adding 217.5 kg of edible alcohol with the concentration of 42% V/V, uniformly mixing, sealing, introducing steam through the interlayer for heating, keeping the temperature of the feed liquid at 43 ℃, stirring and leaching for 16 hours, then carrying out reduced pressure distillation under the conditions of-0.073 MPa and the distillation temperature of 70 ℃, and collecting 45 kg of distillate for later use;
(III) pouring out the residual liquid and the material residues after the distillation in the step (II), and squeezing by using a wrapping type squeezer to respectively obtain juice and the material residues, wherein the juice is stored in another device, and the material residues are reserved;
adding 217.5 kg of purified water into the residue in the step (III), heating to 100 ℃, stirring, boiling and extracting for 3 hours, filtering to obtain a boiling extract, adding 217.5 kg of purified water into the residue, stirring and boiling and extracting for 3 hours at 100 ℃, filtering to obtain a boiling extract, and combining the boiling extracts for 2 times;
(V) combining the juice obtained in the step (III) and the decoction obtained in the step (IV), performing centrifugal separation by using a horizontal spiral centrifuge, and collecting supernate at the centrifugal rotation speed of 15000 rpm;
sixthly, adding 2.18 kg of diatomite into the supernatant obtained in the fifth step, fully stirring and uniformly mixing, and filtering by using a diatomite filter to obtain filtrate;
seventhly, concentrating the filtrate obtained in the sixth step into 5 kg of clear paste by using a tubular evaporation concentrator at the temperature of 55 ℃ and the pressure of-0.095 MPa;
(eighthly), adding 5 kg of clear paste obtained in the seventh step into 45 kg of distillate obtained in the second step, and fully and uniformly containing 50 kg of traditional Chinese medicine extracting solution;
mixing 50 kg of the traditional Chinese medicine extract obtained in the step (VIII) with 1000 kg of yellow wine, and uniformly stirring;
and (ten) aging the wine liquid obtained in the step (nine) at 2 ℃ for 30 days, filtering by using an organic membrane tubular ultrafiltration device with the membrane aperture of 0.16 mu m at 2 ℃, and subpackaging to obtain the Zhibai Dihuang yellow wine product.
Example 22
Firstly, weighing 12 kg of processed and qualified clean medicinal materials of prepared rehmannia root, 6 kg of cornus officinalis (prepared), 6 kg of Chinese yam, 4.5 kg of moutan bark, 4.5 kg of poria cocos, 4.5 kg of rhizoma alismatis, 3 kg of rhizoma anemarrhenae and 3 kg of phellodendron, grinding the six medicines of Chinese yam, moutan bark, poria cocos, rhizoma alismatis, rhizoma anemarrhenae and phellodendron into coarse powder, mixing the coarse powder with the prepared rehmannia root and the cornus officinalis, smashing the mixture together, placing the mixture in an oven, fully drying the mixture at the temperature of 80 ℃, taking out the mixture, cooling the mixture, crushing the mixture, and sieving the crushed mixture through a 70-mesh sieve to obtain Chinese medicinal mixed powder;
placing the mixed powder of the traditional Chinese medicines obtained in the step (one) in a reaction pot with an interlayer, adding 217.5 kg of edible alcohol with the concentration of 42% V/V, uniformly mixing, sealing, introducing steam through the interlayer for heating, keeping the temperature of the feed liquid at 43 ℃, stirring and leaching for 16 hours, then carrying out reduced pressure distillation under the conditions of-0.073 MPa and the distillation temperature of 70 ℃, and collecting 45 kg of distillate for later use;
(III) pouring out the residual liquid and the material residues after the distillation in the step (II), and squeezing by using a wrapping type squeezer to respectively obtain juice and the material residues, wherein the juice is stored in another device, and the material residues are reserved;
adding 217.5 kg of purified water into the residue in the step (III), heating to 100 ℃, stirring, boiling and extracting for 3 hours, filtering to obtain a boiling extract, adding 217.5 kg of purified water into the residue, stirring and boiling and extracting for 3 hours at 100 ℃, filtering to obtain a boiling extract, and combining the boiling extracts for 2 times;
(V) combining the juice obtained in the step (III) and the decoction obtained in the step (IV), performing centrifugal separation by using a horizontal spiral centrifuge at the centrifugal rotation speed of 14000rpm, and collecting supernatant;
sixthly, adding 2.18 kg of diatomite into the supernatant obtained in the fifth step, fully stirring and uniformly mixing, and filtering by using a diatomite filter to obtain filtrate;
seventhly, concentrating the filtrate obtained in the sixth step into 5 kg of clear paste by using a plate-type evaporation concentrator at the temperature of 55 ℃ and the pressure of-0.095 MPa;
(eighthly), adding 5 kg of clear paste obtained in the seventh step into 45 kg of distillate obtained in the second step, and fully and uniformly containing 50 kg of traditional Chinese medicine extracting solution;
mixing 50 kg of the traditional Chinese medicine extracting solution obtained in the step (VIII) with 550 kg of yellow wine, and uniformly stirring;
and (ten) aging the wine liquid obtained in the step (nine) at 2 ℃ for 30 days, filtering by using an organic membrane tubular ultrafiltration device with the membrane aperture of 0.16 mu m at 2 ℃, and subpackaging to obtain the Zhibai Dihuang yellow wine product.
Example 23
Firstly, weighing 8 kg of processed and qualified clean medicinal materials of prepared rehmannia root, 4 kg of cornus officinalis (prepared), 4 kg of Chinese yam, 3 kg of tree peony bark, 3 kg of poria cocos, 3 kg of rhizoma alismatis, 2 kg of rhizoma anemarrhenae and 2 kg of golden cypress, grinding six materials of Chinese yam, tree peony bark, poria cocos, rhizoma alismatis, rhizoma anemarrhenae and golden cypress into coarse powder, mixing the coarse powder with the prepared rehmannia root and the cornus officinalis, smashing the mixture together, placing the mixture in an oven, fully drying the mixture at 75 ℃, taking the mixture out, cooling the mixture, crushing the mixture, and sieving the powder by a 75-mesh sieve to obtain Chinese medicinal mixed powder;
secondly, putting the mixed powder of the traditional Chinese medicines obtained in the first step into a sandwich reaction pot, adding 145 kg of edible alcohol with the concentration of 40% V/V, uniformly mixing, sealing, introducing steam through a sandwich layer for heating, keeping the temperature of the feed liquid at 50 ℃, stirring and leaching for 12 hours, then carrying out reduced pressure distillation under the conditions of-0.085 MPa and the distillation temperature of 85 ℃, and collecting 45 kg of distillate for later use;
(III) pouring out the residual liquid and the material residues after the distillation in the step (II), and squeezing by using a wrapping type squeezer to respectively obtain juice and the material residues, wherein the juice is stored in another device, and the material residues are reserved;
adding 145 kg of purified water into the material residue in the third step, heating to 100 ℃, stirring, boiling and extracting for 3 hours, filtering to obtain a boiling extract, adding 145 kg of purified water into the filter residue, stirring, boiling and extracting for 3 hours under the condition of heating to 100 ℃, filtering to obtain a boiling extract, and combining the boiling extracts for 2 times;
(V) combining the juice obtained in the step (III) and the decoction obtained in the step (IV), performing centrifugal separation by using a horizontal spiral centrifuge, wherein the centrifugal rotation speed is 13000rpm, and collecting supernate;
sixthly, adding 1.45 kg of diatomite into the supernatant obtained in the fifth step, fully stirring and uniformly mixing, and filtering by using a diatomite filter to obtain filtrate;
seventhly, concentrating the filtrate obtained in the sixth step into 5 kg of clear paste by using a vacuum rotary evaporator under the conditions of 70 ℃ and-0.075 MPa;
(eighthly), adding 5 kg of clear paste obtained in the seventh step into 45 kg of distillate obtained in the second step, and fully and uniformly containing 50 kg of traditional Chinese medicine extracting solution;
mixing 50 kg of the traditional Chinese medicine extracting solution obtained in the step (eight) with 1000 kg of wine, and uniformly stirring;
and (ten) aging the wine liquid obtained in the step (nine) at 2 ℃ for 30 days, filtering by using an organic membrane tubular ultrafiltration device with the membrane aperture of 0.16 mu m at 2 ℃, and subpackaging to obtain the Zhibai Dihuang wine product.
Example 24
Firstly, weighing 8 kg of processed and qualified clean medicinal materials of prepared rehmannia root, 4 kg of cornus officinalis (prepared), 4 kg of Chinese yam, 3 kg of tree peony bark, 3 kg of poria cocos, 3 kg of rhizoma alismatis, 2 kg of rhizoma anemarrhenae and 2 kg of golden cypress, grinding six materials of Chinese yam, tree peony bark, poria cocos, rhizoma alismatis, rhizoma anemarrhenae and golden cypress into coarse powder, mixing the coarse powder with the prepared rehmannia root and the cornus officinalis, smashing the mixture together, placing the mixture in an oven, fully drying the mixture at 75 ℃, taking the mixture out, cooling the mixture, crushing the mixture, and sieving the powder by a 75-mesh sieve to obtain Chinese medicinal mixed powder;
secondly, putting the mixed powder of the traditional Chinese medicines obtained in the first step into a sandwich reaction pot, adding 145 kg of edible alcohol with the concentration of 40% V/V, uniformly mixing, sealing, introducing steam through a sandwich layer for heating, keeping the temperature of the feed liquid at 50 ℃, stirring and leaching for 12 hours, then carrying out reduced pressure distillation under the conditions of-0.085 MPa and the distillation temperature of 85 ℃, and collecting 45 kg of distillate for later use;
(III) pouring out the residual liquid and the material residues after the distillation in the step (II), and squeezing by using a wrapping type squeezer to respectively obtain juice and the material residues, wherein the juice is stored in another device, and the material residues are reserved;
adding 145 kg of purified water into the material residue in the third step, heating to 100 ℃, stirring, boiling and extracting for 3 hours, filtering to obtain a boiling extract, adding 145 kg of purified water into the filter residue, stirring, boiling and extracting for 3 hours under the condition of heating to 100 ℃, filtering to obtain a boiling extract, and combining the boiling extracts for 2 times;
(V) combining the juice obtained in the step (III) and the decoction obtained in the step (IV), performing centrifugal separation by using a horizontal spiral centrifuge at the centrifugal rotation speed of 12000rpm, and collecting supernate;
sixthly, adding 1.45 kg of diatomite into the supernatant obtained in the fifth step, fully stirring and uniformly mixing, and filtering by using a diatomite filter to obtain filtrate;
seventhly, concentrating the filtrate obtained in the sixth step into 5 kg of clear paste by using a vacuum rotary evaporator under the conditions of 70 ℃ and-0.075 MPa;
(eighthly), adding 5 kg of clear paste obtained in the seventh step into 45 kg of distillate obtained in the second step, and fully and uniformly containing 50 kg of traditional Chinese medicine extracting solution;
mixing 50 kg of the traditional Chinese medicine extracting solution obtained in the step (eight) with 500 kg of wine, and uniformly stirring;
and (ten) aging the wine liquid obtained in the step (nine) at 2 ℃ for 30 days, filtering by using an organic membrane tubular ultrafiltration device with the membrane aperture of 0.16 mu m at 2 ℃, and subpackaging to obtain the Zhibai Dihuang wine product.
Example 25
Firstly, weighing 8 kg of processed and qualified clean medicinal materials of prepared rehmannia root, 4 kg of cornus officinalis (prepared), 4 kg of Chinese yam, 3 kg of tree peony bark, 3 kg of poria cocos, 3 kg of rhizoma alismatis, 2 kg of rhizoma anemarrhenae and 2 kg of golden cypress, grinding six materials of Chinese yam, tree peony bark, poria cocos, rhizoma alismatis, rhizoma anemarrhenae and golden cypress into coarse powder, mixing the coarse powder with the prepared rehmannia root and the cornus officinalis, smashing the mixture together, placing the mixture in an oven, fully drying the mixture at 75 ℃, taking the mixture out, cooling the mixture, crushing the mixture, and sieving the powder by a 75-mesh sieve to obtain Chinese medicinal mixed powder;
secondly, putting the mixed powder of the traditional Chinese medicines obtained in the first step into a sandwich reaction pot, adding 145 kg of edible alcohol with the concentration of 40% V/V, uniformly mixing, sealing, introducing steam through a sandwich layer for heating, keeping the temperature of the feed liquid at 50 ℃, stirring and leaching for 12 hours, then carrying out reduced pressure distillation under the conditions of-0.085 MPa and the distillation temperature of 85 ℃, and collecting 45 kg of distillate for later use;
(III) pouring out the residual liquid and the material residues after the distillation in the step (II), and squeezing by using a wrapping type squeezer to respectively obtain juice and the material residues, wherein the juice is stored in another device, and the material residues are reserved;
adding 145 kg of purified water into the material residue in the third step, heating to 100 ℃, stirring, boiling and extracting for 3 hours, filtering to obtain a boiling extract, adding 145 kg of purified water into the filter residue, stirring, boiling and extracting for 3 hours under the condition of heating to 100 ℃, filtering to obtain a boiling extract, and combining the boiling extracts for 2 times;
(V) combining the juice obtained in the step (III) and the decoction obtained in the step (IV), performing centrifugal separation by using a horizontal spiral centrifuge at the centrifugal rotation speed of 12000rpm, and collecting supernate;
sixthly, adding 1.45 kg of diatomite into the supernatant obtained in the fifth step, fully stirring and uniformly mixing, and filtering by using a diatomite filter to obtain filtrate;
seventhly, concentrating the filtrate obtained in the sixth step into 5 kg of clear paste by using a vacuum rotary evaporator under the conditions of 70 ℃ and-0.075 MPa;
(eighthly), adding 5 kg of clear paste obtained in the seventh step into 45 kg of distillate obtained in the second step, and fully and uniformly containing 50 kg of traditional Chinese medicine extracting solution;
mixing 50 kg of the traditional Chinese medicine extracting solution obtained in the step (eight) with 550 kg of wine, and uniformly stirring;
and (ten) aging the wine liquid obtained in the step (nine) at 2 ℃ for 30 days, filtering by using an organic membrane tubular ultrafiltration device with the membrane aperture of 0.16 mu m at 2 ℃, and subpackaging to obtain the Zhibai Dihuang wine product.
Example 26
Firstly, weighing 8 kg of processed and qualified clean medicinal materials of prepared rehmannia root, 4 kg of cornus officinalis (prepared), 4 kg of Chinese yam, 3 kg of tree peony bark, 3 kg of poria cocos, 3 kg of rhizoma alismatis, 2 kg of rhizoma anemarrhenae and 2 kg of golden cypress, grinding six materials of Chinese yam, tree peony bark, poria cocos, rhizoma alismatis, rhizoma anemarrhenae and golden cypress into coarse powder, mixing the coarse powder with the prepared rehmannia root and the cornus officinalis, smashing the mixture together, placing the mixture in an oven, fully drying the mixture at 75 ℃, taking the mixture out, cooling the mixture, crushing the mixture, and sieving the powder by a 75-mesh sieve to obtain Chinese medicinal mixed powder;
secondly, putting the mixed powder of the traditional Chinese medicines obtained in the first step into a sandwich reaction pot, adding 145 kg of edible alcohol with the concentration of 40% V/V, uniformly mixing, sealing, introducing steam through a sandwich layer for heating, keeping the temperature of the feed liquid at 50 ℃, stirring and leaching for 12 hours, then carrying out reduced pressure distillation under the conditions of-0.085 MPa and the distillation temperature of 85 ℃, and collecting 45 kg of distillate for later use;
(III) pouring out the residual liquid and the material residues after the distillation in the step (II), and squeezing by using a wrapping type squeezer to respectively obtain juice and the material residues, wherein the juice is stored in another device, and the material residues are reserved;
adding 145 kg of purified water into the material residue in the third step, heating to 100 ℃, stirring, boiling and extracting for 3 hours, filtering to obtain a boiling extract, adding 145 kg of purified water into the filter residue, stirring, boiling and extracting for 3 hours under the condition of heating to 100 ℃, filtering to obtain a boiling extract, and combining the boiling extracts for 2 times;
(V) combining the juice obtained in the step (III) and the decoction obtained in the step (IV), performing centrifugal separation by using a horizontal spiral centrifuge, and collecting supernate at the centrifugal rotation speed of 15000 rpm;
sixthly, adding 1.45 kg of diatomite into the supernatant obtained in the fifth step, fully stirring and uniformly mixing, and filtering by using a diatomite filter to obtain filtrate;
seventhly, concentrating the filtrate obtained in the sixth step into 5 kg of clear paste by using a tubular evaporation concentrator under the conditions of 70 ℃ and-0.075 MPa;
(eighthly), adding 5 kg of clear paste obtained in the seventh step into 45 kg of distillate obtained in the second step, and fully and uniformly containing 50 kg of traditional Chinese medicine extracting solution;
mixing 50 kg of the traditional Chinese medicine extracting solution obtained in the step (eight) with 850 kg of wine, and uniformly stirring;
and (ten) aging the wine liquid obtained in the step (nine) at 1 ℃ for 30 days, filtering by using an organic membrane tubular ultrafiltration device with the membrane aperture of 0.18 mu m at 1 ℃, and subpackaging to obtain the Zhibai Dihuang wine product.
Example 27
Firstly, weighing 8 kg of processed and qualified clean medicinal materials of prepared rehmannia root, 4 kg of cornus officinalis (prepared), 4 kg of Chinese yam, 3 kg of tree peony bark, 3 kg of poria cocos, 3 kg of rhizoma alismatis, 2 kg of rhizoma anemarrhenae and 2 kg of golden cypress, grinding six materials of Chinese yam, tree peony bark, poria cocos, rhizoma alismatis, rhizoma anemarrhenae and golden cypress into coarse powder, mixing the coarse powder with the prepared rehmannia root and the cornus officinalis, smashing the mixture together, placing the mixture in an oven, fully drying the mixture at 75 ℃, taking the mixture out, cooling the mixture, crushing the mixture, and sieving the powder by a 75-mesh sieve to obtain Chinese medicinal mixed powder;
secondly, putting the mixed powder of the traditional Chinese medicines obtained in the first step into a sandwich reaction pot, adding 145 kg of edible alcohol with the concentration of 40% V/V, uniformly mixing, sealing, introducing steam through a sandwich layer for heating, keeping the temperature of the feed liquid at 50 ℃, stirring and leaching for 12 hours, then carrying out reduced pressure distillation under the conditions of-0.085 MPa and the distillation temperature of 85 ℃, and collecting 45 kg of distillate for later use;
(III) pouring out the residual liquid and the material residues after the distillation in the step (II), and squeezing by using a wrapping type squeezer to respectively obtain juice and the material residues, wherein the juice is stored in another device, and the material residues are reserved;
adding 145 kg of purified water into the material residue in the third step, heating to 100 ℃, stirring, boiling and extracting for 3 hours, filtering to obtain a boiling extract, adding 145 kg of purified water into the filter residue, stirring, boiling and extracting for 3 hours under the condition of heating to 100 ℃, filtering to obtain a boiling extract, and combining the boiling extracts for 2 times;
(V) combining the juice obtained in the step (III) and the decoction obtained in the step (IV), performing centrifugal separation by using a horizontal spiral centrifuge at the centrifugal rotation speed of 14000rpm, and collecting supernatant;
sixthly, adding 1.45 kg of diatomite into the supernatant obtained in the fifth step, fully stirring and uniformly mixing, and filtering by using a diatomite filter to obtain filtrate;
seventhly, concentrating the filtrate obtained in the sixth step into 5 kg of clear paste by using a plate-type evaporation concentrator at the temperature of 70 ℃ and the pressure of-0.075 MPa;
(eighthly), adding 5 kg of clear paste obtained in the seventh step into 45 kg of distillate obtained in the second step, and fully and uniformly containing 50 kg of traditional Chinese medicine extracting solution;
mixing 50 kg of the traditional Chinese medicine extracting solution obtained in the step (eight) with 750 kg of wine, and uniformly stirring;
and (ten) aging the wine liquid obtained in the step (nine) at 1 ℃ for 30 days, filtering by using an organic membrane tubular ultrafiltration device with the membrane aperture of 0.18 mu m at 1 ℃, and subpackaging to obtain the Zhibai Dihuang wine product.
Example 28
Firstly, weighing 8 kg of processed and qualified clean medicinal materials of prepared rehmannia root, 4 kg of cornus officinalis (prepared), 4 kg of Chinese yam, 3 kg of tree peony bark, 3 kg of poria cocos, 3 kg of rhizoma alismatis, 2 kg of rhizoma anemarrhenae and 2 kg of golden cypress, grinding six materials of Chinese yam, tree peony bark, poria cocos, rhizoma alismatis, rhizoma anemarrhenae and golden cypress into coarse powder, mixing the coarse powder with the prepared rehmannia root and the cornus officinalis, smashing the mixture together, placing the mixture in an oven, fully drying the mixture at 75 ℃, taking the mixture out, cooling the mixture, crushing the mixture, and sieving the powder by a 75-mesh sieve to obtain Chinese medicinal mixed powder;
secondly, putting the mixed powder of the traditional Chinese medicines obtained in the first step into a sandwich reaction pot, adding 145 kg of edible alcohol with the concentration of 40% V/V, uniformly mixing, sealing, introducing steam through a sandwich layer for heating, keeping the temperature of the feed liquid at 50 ℃, stirring and leaching for 12 hours, then carrying out reduced pressure distillation under the conditions of-0.085 MPa and the distillation temperature of 85 ℃, and collecting 45 kg of distillate for later use;
(III) pouring out the residual liquid and the material residues after the distillation in the step (II), and squeezing by using a wrapping type squeezer to respectively obtain juice and the material residues, wherein the juice is stored in another device, and the material residues are reserved;
adding 145 kg of purified water into the material residue in the third step, heating to 100 ℃, stirring, boiling and extracting for 3 hours, filtering to obtain a boiling extract, adding 145 kg of purified water into the filter residue, stirring, boiling and extracting for 3 hours under the condition of heating to 100 ℃, filtering to obtain a boiling extract, and combining the boiling extracts for 2 times;
(V) combining the juice obtained in the step (III) and the decoction obtained in the step (IV), performing centrifugal separation by using a horizontal spiral centrifuge, and collecting supernate at the centrifugal rotation speed of 15000 rpm;
sixthly, adding 1.45 kg of diatomite into the supernatant obtained in the fifth step, fully stirring and uniformly mixing, and filtering by using a diatomite filter to obtain filtrate;
seventhly, concentrating the filtrate obtained in the sixth step into 5 kg of clear paste by using a vacuum rotary evaporator under the conditions of 70 ℃ and-0.075 MPa;
(eighthly), adding 5 kg of clear paste obtained in the seventh step into 45 kg of distillate obtained in the second step, and fully and uniformly containing 50 kg of traditional Chinese medicine extracting solution;
mixing 50 kg of the traditional Chinese medicine extracting solution obtained in the step (eight) with 950 kg of yellow wine, and uniformly stirring;
and (ten) aging the wine liquid obtained in the step (nine) at 1 ℃ for 30 days, filtering by using an organic membrane tubular ultrafiltration device with the membrane aperture of 0.18 mu m at 1 ℃, and subpackaging to obtain the Zhibai Dihuang yellow wine product.
Example 29
Firstly, weighing 8 kg of processed and qualified clean medicinal materials of prepared rehmannia root, 4 kg of cornus officinalis (prepared), 4 kg of Chinese yam, 3 kg of tree peony bark, 3 kg of poria cocos, 3 kg of rhizoma alismatis, 2 kg of rhizoma anemarrhenae and 2 kg of golden cypress, grinding six materials of Chinese yam, tree peony bark, poria cocos, rhizoma alismatis, rhizoma anemarrhenae and golden cypress into coarse powder, mixing the coarse powder with the prepared rehmannia root and the cornus officinalis, smashing the mixture together, placing the mixture in an oven, fully drying the mixture at 75 ℃, taking the mixture out, cooling the mixture, crushing the mixture, and sieving the powder by a 75-mesh sieve to obtain Chinese medicinal mixed powder;
secondly, putting the mixed powder of the traditional Chinese medicines obtained in the first step into a sandwich reaction pot, adding 145 kg of edible alcohol with the concentration of 40% V/V, uniformly mixing, sealing, introducing steam through a sandwich layer for heating, keeping the temperature of the feed liquid at 50 ℃, stirring and leaching for 12 hours, then carrying out reduced pressure distillation under the conditions of-0.085 MPa and the distillation temperature of 85 ℃, and collecting 45 kg of distillate for later use;
(III) pouring out the residual liquid and the material residues after the distillation in the step (II), and squeezing by using a wrapping type squeezer to respectively obtain juice and the material residues, wherein the juice is stored in another device, and the material residues are reserved;
adding 145 kg of purified water into the material residue in the third step, heating to 100 ℃, stirring, boiling and extracting for 3 hours, filtering to obtain a boiling extract, adding 145 kg of purified water into the filter residue, stirring, boiling and extracting for 3 hours under the condition of heating to 100 ℃, filtering to obtain a boiling extract, and combining the boiling extracts for 2 times;
(V) combining the juice obtained in the step (III) and the decoction obtained in the step (IV), performing centrifugal separation by using a horizontal spiral centrifuge, and collecting supernate at the centrifugal rotation speed of 15000 rpm;
sixthly, adding 1.45 kg of diatomite into the supernatant obtained in the fifth step, fully stirring and uniformly mixing, and filtering by using a diatomite filter to obtain filtrate;
seventhly, concentrating the filtrate obtained in the sixth step into 5 kg of clear paste by using a vacuum rotary evaporator under the conditions of 70 ℃ and-0.075 MPa;
(eighthly), adding 5 kg of clear paste obtained in the seventh step into 45 kg of distillate obtained in the second step, and fully and uniformly containing 50 kg of traditional Chinese medicine extracting solution;
mixing 50 kg of the traditional Chinese medicine extracting solution obtained in the step (VIII) with 550 kg of yellow wine, and uniformly stirring;
and (ten) aging the wine liquid obtained in the step (nine) at 1 ℃ for 30 days, filtering by using an organic membrane tubular ultrafiltration device with the membrane aperture of 0.18 mu m at 1 ℃, and subpackaging to obtain the Zhibai Dihuang yellow wine product.
Example 30
Firstly, weighing 8 kg of processed and qualified clean medicinal materials of prepared rehmannia root, 4 kg of cornus officinalis (prepared), 4 kg of Chinese yam, 3 kg of tree peony bark, 3 kg of poria cocos, 3 kg of rhizoma alismatis, 2 kg of rhizoma anemarrhenae and 2 kg of golden cypress, grinding six materials of Chinese yam, tree peony bark, poria cocos, rhizoma alismatis, rhizoma anemarrhenae and golden cypress into coarse powder, mixing the coarse powder with the prepared rehmannia root and the cornus officinalis, smashing the mixture together, placing the mixture in an oven, fully drying the mixture at 75 ℃, taking the mixture out, cooling the mixture, crushing the mixture, and sieving the powder by a 75-mesh sieve to obtain Chinese medicinal mixed powder;
secondly, putting the mixed powder of the traditional Chinese medicines obtained in the first step into a sandwich reaction pot, adding 145 kg of edible alcohol with the concentration of 40% V/V, uniformly mixing, sealing, introducing steam through a sandwich layer for heating, keeping the temperature of the feed liquid at 50 ℃, stirring and leaching for 12 hours, then carrying out reduced pressure distillation under the conditions of-0.085 MPa and the distillation temperature of 85 ℃, and collecting 45 kg of distillate for later use;
(III) pouring out the residual liquid and the material residues after the distillation in the step (II), and squeezing by using a wrapping type squeezer to respectively obtain juice and the material residues, wherein the juice is stored in another device, and the material residues are reserved;
adding 145 kg of purified water into the material residue in the third step, heating to 100 ℃, stirring, boiling and extracting for 3 hours, filtering to obtain a boiling extract, adding 145 kg of purified water into the filter residue, stirring, boiling and extracting for 3 hours under the condition of heating to 100 ℃, filtering to obtain a boiling extract, and combining the boiling extracts for 2 times;
(V) combining the juice obtained in the step (III) and the decoction obtained in the step (IV), performing centrifugal separation by using a horizontal spiral centrifuge, and collecting supernate at the centrifugal rotation speed of 16000 rpm;
sixthly, adding 1.45 kg of diatomite into the supernatant obtained in the fifth step, fully stirring and uniformly mixing, and filtering by using a diatomite filter to obtain filtrate;
seventhly, concentrating the filtrate obtained in the sixth step into 5 kg of clear paste by using a vacuum rotary evaporator under the conditions of 70 ℃ and-0.075 MPa;
(eighthly), adding 5 kg of clear paste obtained in the seventh step into 45 kg of distillate obtained in the second step, and fully and uniformly containing 50 kg of traditional Chinese medicine extracting solution;
mixing 50 kg of the Chinese medicine extracting solution obtained in the step (eight) with 1000 kg of white spirit, and uniformly stirring;
and (ten) aging the wine liquid obtained in the step (nine) at 1 ℃ for 30 days, filtering by using an organic membrane tubular ultrafiltration device with the membrane aperture of 0.18 mu m at 1 ℃, and subpackaging to obtain the Zhibai Dihuang health care wine product.

Claims (10)

1. The processing method of the Zhibai Dihuang health wine is characterized in that eight traditional Chinese medicine raw materials, namely prepared rehmannia root, cornus officinalis (prepared), Chinese yam, tree peony bark, tuckahoe, rhizoma alismatis, rhizoma anemarrhenae and phellodendron are used, and the weight ratio of the raw materials is that the prepared rehmannia root: fructus Corni (prepared): chinese yam: moutan bark: tuckahoe, poria cocos: rhizoma alismatis: rhizoma anemarrhenae: phellodendron = 8-16: 4-8: 4-8: 3-6: 3-6: 3-6: 2-4: 2-4, preparing a traditional Chinese medicine extracting solution according to the proportion of the traditional Chinese medicine extracting solution: the weight ratio of the wine is 50: the preparation method comprises the following specific steps of preparing the raw materials in a ratio of 500-1000:
firstly, weighing qualified processed clean medicinal materials, grinding the Chinese yam, the tree peony bark, the poria cocos, the rhizoma alismatis, the rhizoma anemarrhenae and the golden cypress into coarse powder, then smashing the coarse powder together with the prepared rehmannia root and the dogwood pulp, placing the smashed mixture into an oven, drying the mixture at 75-85 ℃, taking out the dried mixture, cooling the dried mixture, and crushing the cooled mixture into 65-75-mesh powder to obtain mixed Chinese medicinal powder;
placing the traditional Chinese medicine mixed powder obtained in the step (I) into a sandwich reaction pot, adding edible alcohol with concentration content of 40-45% V/V, which is 5 times of the weight of the traditional Chinese medicine raw materials, uniformly mixing and sealing, introducing steam through a sandwich layer, heating, stirring and leaching for 12-18 hours at the temperature of 45-50 ℃, distilling under reduced pressure at-0.055 MPa to-0.085 MPa and the distillation temperature of 65-85 ℃, and collecting 45 kg of distillate for later use;
pouring out residual liquid and material residues distilled in the step (II), squeezing to obtain juice and material residues, and storing the juice and the material residues in another juice extractor; material slag is reserved;
adding purified water which is 5 times of the weight of the raw materials into the material residues in the step (three), heating to 100 ℃, stirring, boiling and extracting for 2 times, boiling and extracting for 3 hours each time, and combining the boiling and extracting solutions;
step five, combining the squeezed juice obtained in the step three and the decoction obtained in the step four, performing centrifugal separation at a centrifugal rotation speed of 12000-16000 rpm, and collecting supernatant;
filtering the supernatant obtained in the step (five) to obtain filtrate;
step seven, concentrating the filtrate obtained in the step six to 5 kg of clear paste at the temperature of between 50 and 75 ℃ and under the pressure of between-0.06 and-0.1 MPa;
adding the 5 kg of the fluid extracts obtained in the step (seven) into 45 kg of the distillate obtained in the step (two), and completely and uniformly metering to 50 kg of the distillate to obtain Chinese herbal medicine extracting solution;
step (nine), the traditional Chinese medicine extracting solution obtained in the step (eight) is prepared according to the following traditional Chinese medicine extracting solution: wine = 50: mixing at a mass ratio of 500-1000, and stirring and mixing uniformly;
placing the wine liquid obtained in the step (nine) at a temperature of between 2 ℃ below zero and 2 ℃, aging for 30 days, and then carrying out fine filtration and subpackage at a temperature of between 2 ℃ below zero and 2 ℃ to obtain a product; the wine is white spirit, wine, yellow wine, beer or fruit wine.
2. The method of claim 1, wherein: a wrapping type presser is selected for pressing in the step (III); the centrifugal separation in the step (five) is preferably performed by using a horizontal spiral centrifuge.
3. The method of claim 1, wherein: and (5) filtering the filtrate in the step (six) by using kieselguhr.
4. The method of claim 1, wherein: the concentration in the step (VII) is performed by using a vacuum rotary evaporator, a tubular evaporation concentrator or a plate evaporation concentrator; the concentration conditions are preferably 55 ℃ to 70 ℃ and-0.075 MPa to-0.095 MPa.
5. The method of claim 1, wherein: and (iv) filtering the fine filter in the step (ten) by using a membrane with the pore size of less than 0.20 mu m.
6. The method of claim 1, wherein: and (iv) filtering the fine filter in the step (ten) by using a rotary vacuum filter.
7. The method as claimed in claim 1, wherein the composition is prepared from eight Chinese medicinal materials including prepared rehmannia root, cornus officinalis (prepared), Chinese yam, moutan bark, poria cocos, alisma orientale, anemarrhena asphodeloides bunge and phellodendron bark, the weight ratio of the raw materials is prepared rehmannia root: fructus Corni (prepared): chinese yam: moutan bark: tuckahoe, poria cocos: rhizoma alismatis: rhizoma anemarrhenae: phellodendron = 16: 8: 8: 6: 6: 6: 4: 4, preparing the traditional Chinese medicine extracting solution according to the mass ratio: the wine is 50: the adhesive is prepared by mixing the components in a ratio of 500-1000, and comprises the following specific steps:
firstly, weighing qualified processed clean medicinal materials, grinding the Chinese yam, the tree peony bark, the poria cocos, the rhizoma alismatis, the rhizoma anemarrhenae and the golden cypress into coarse powder, then smashing the coarse powder together with the prepared rehmannia root and the dogwood pulp, placing the smashed mixture into an oven, drying the mixture at 75-85 ℃, taking out the dried mixture, cooling the dried mixture, and crushing the cooled mixture into 65-75-mesh powder to obtain mixed Chinese medicinal powder;
placing the traditional Chinese medicine mixed powder obtained in the step (I) into a sandwich reaction pot, adding edible alcohol with concentration content of 40-45% V/V, which is 5 times of the weight of the traditional Chinese medicine raw materials, uniformly mixing and sealing, introducing steam through a sandwich layer, heating, stirring and leaching for 12-18 hours at the temperature of 45-50 ℃, distilling under reduced pressure at-0.055 MPa to-0.085 MPa and the distillation temperature of 65-85 ℃, and collecting 45 kg of distillate for later use;
pouring out residual liquid and material residues distilled in the step (II), squeezing to obtain juice and material residues, and storing the juice and the material residues in another juice extractor; material slag is reserved;
adding purified water which is 5 times of the weight of the raw materials into the material residues in the step (three), heating to 100 ℃, stirring, boiling and extracting for 2 times, boiling and extracting for 3 hours each time, and combining the boiling and extracting solutions;
step five, combining the squeezed juice obtained in the step three and the decoction obtained in the step four, performing centrifugal separation at a centrifugal rotation speed of 12000-16000 rpm, and collecting supernatant;
filtering the supernatant obtained in the step (five) to obtain filtrate;
step seven, concentrating the filtrate obtained in the step six to 5 kg of clear paste at the temperature of between 50 and 75 ℃ and under the pressure of between-0.06 and-0.1 MPa;
and (eight), adding the 5 kg of the fluid extracts obtained in the step (seven) into the 45 kg of the distillate obtained in the step (two), and fully and uniformly metering to 50 kg of the Chinese herbal medicine extract.
8. The method as claimed in claim 1, wherein the composition is prepared from eight Chinese medicinal materials including prepared rehmannia root, cornus officinalis (prepared), Chinese yam, moutan bark, poria cocos, alisma orientale, anemarrhena asphodeloides bunge and phellodendron bark, the weight ratio of the raw materials is prepared rehmannia root: fructus Corni (prepared): chinese yam: moutan bark: tuckahoe, poria cocos: rhizoma alismatis: rhizoma anemarrhenae: phellodendron = 12: 6: 6: 4.5: 4.5: 4.5: 3: 3, preparing the traditional Chinese medicine extracting solution according to the mass ratio: the wine is 50: the adhesive is prepared by mixing the components in a ratio of 500-1000, and comprises the following specific steps:
firstly, weighing qualified processed clean medicinal materials, grinding the Chinese yam, the tree peony bark, the poria cocos, the rhizoma alismatis, the rhizoma anemarrhenae and the golden cypress into coarse powder, then smashing the coarse powder together with the prepared rehmannia root and the dogwood pulp, placing the smashed mixture into an oven, drying the mixture at 75-85 ℃, taking out the dried mixture, cooling the dried mixture, and crushing the cooled mixture into 65-75-mesh powder to obtain mixed Chinese medicinal powder;
placing the traditional Chinese medicine mixed powder obtained in the step (I) into a sandwich reaction pot, adding edible alcohol with concentration content of 40-45% V/V, which is 5 times of the weight of the traditional Chinese medicine raw materials, uniformly mixing and sealing, introducing steam through a sandwich layer, heating, stirring and leaching for 12-18 hours at the temperature of 45-50 ℃, distilling under reduced pressure at-0.055 MPa to-0.085 MPa and the distillation temperature of 65-85 ℃, and collecting 45 kg of distillate for later use;
pouring out residual liquid and material residues distilled in the step (II), squeezing to obtain juice and material residues, and storing the juice and the material residues in another juice extractor; material slag is reserved;
adding purified water which is 5 times of the weight of the raw materials into the material residues in the step (three), heating to 100 ℃, stirring, boiling and extracting for 2 times, boiling and extracting for 3 hours each time, and combining the boiling and extracting solutions;
step five, combining the squeezed juice obtained in the step three and the decoction obtained in the step four, performing centrifugal separation at a centrifugal rotation speed of 12000-16000 rpm, and collecting supernatant;
filtering the supernatant obtained in the step (five) to obtain filtrate;
step seven, concentrating the filtrate obtained in the step six to 5 kg of clear paste at the temperature of between 50 and 75 ℃ and under the pressure of between-0.06 and-0.1 MPa;
and (eight), adding the 5 kg of the fluid extracts obtained in the step (seven) into the 45 kg of the distillate obtained in the step (two), and fully and uniformly metering to 50 kg of the Chinese herbal medicine extract.
9. The method as claimed in claim 1, wherein the composition is prepared from eight Chinese medicinal materials including prepared rehmannia root, cornus officinalis (prepared), Chinese yam, moutan bark, poria cocos, alisma orientale, anemarrhena asphodeloides bunge and phellodendron bark, the weight ratio of the raw materials is prepared rehmannia root: fructus Corni (prepared): chinese yam: moutan bark: tuckahoe, poria cocos: rhizoma alismatis: rhizoma anemarrhenae: phellodendron = 8: 4: 4: 3: 3: 3: 2: 2, preparing the traditional Chinese medicine extracting solution according to the mass ratio: the wine is 50: the adhesive is prepared by mixing the components in a ratio of 500-1000, and comprises the following specific steps:
firstly, weighing qualified processed clean medicinal materials, grinding the Chinese yam, the tree peony bark, the poria cocos, the rhizoma alismatis, the rhizoma anemarrhenae and the golden cypress into coarse powder, then smashing the coarse powder together with the prepared rehmannia root and the dogwood pulp, placing the smashed mixture into an oven, drying the mixture at 75-85 ℃, taking out the dried mixture, cooling the dried mixture, and crushing the cooled mixture into 65-75-mesh powder to obtain mixed Chinese medicinal powder;
placing the traditional Chinese medicine mixed powder obtained in the step (I) into a sandwich reaction pot, adding edible alcohol with concentration content of 40-45% V/V, which is 5 times of the weight of the traditional Chinese medicine raw materials, uniformly mixing and sealing, introducing steam through a sandwich layer, heating, stirring and leaching for 12-18 hours at the temperature of 45-50 ℃, distilling under reduced pressure at-0.055 MPa to-0.085 MPa and the distillation temperature of 65-85 ℃, and collecting 45 kg of distillate for later use;
pouring out residual liquid and material residues distilled in the step (II), squeezing to obtain juice and material residues, and storing the juice and the material residues in another juice extractor; material slag is reserved;
adding purified water which is 5 times of the weight of the raw materials into the material residues in the step (three), heating to 100 ℃, stirring, boiling and extracting for 2 times, boiling and extracting for 3 hours each time, and combining the boiling and extracting solutions;
step five, combining the squeezed juice obtained in the step three and the decoction obtained in the step four, performing centrifugal separation at a centrifugal rotation speed of 12000-16000 rpm, and collecting supernatant;
filtering the supernatant obtained in the step (five) to obtain filtrate;
step seven, concentrating the filtrate obtained in the step six to 5 kg of clear paste at the temperature of between 50 and 75 ℃ and under the pressure of between-0.06 and-0.1 MPa;
and (eight), adding the 5 kg of the fluid extracts obtained in the step (seven) into the 45 kg of the distillate obtained in the step (two), and fully and uniformly metering to 50 kg of the Chinese herbal medicine extract.
10. A health wine containing Anemarrhena asphodeloides and rehmannia prepared by the method of any one of claims 1-6.
CN202110540151.6A 2021-05-18 2021-05-18 Processing method of Zhibai rehmannia health wine Withdrawn CN113265316A (en)

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Application publication date: 20210817