CN113109521A - Production detection device of fluorine-containing chemical intermediate - Google Patents
Production detection device of fluorine-containing chemical intermediate Download PDFInfo
- Publication number
- CN113109521A CN113109521A CN202110512311.6A CN202110512311A CN113109521A CN 113109521 A CN113109521 A CN 113109521A CN 202110512311 A CN202110512311 A CN 202110512311A CN 113109521 A CN113109521 A CN 113109521A
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- CN
- China
- Prior art keywords
- outer shell
- fluorine
- cover plate
- reaction tanks
- detection device
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Links
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 title claims abstract description 31
- 229910052731 fluorine Inorganic materials 0.000 title claims abstract description 31
- 239000011737 fluorine Substances 0.000 title claims abstract description 31
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 21
- 238000001514 detection method Methods 0.000 title claims abstract description 20
- 239000000126 substance Substances 0.000 title claims abstract description 18
- 238000006243 chemical reaction Methods 0.000 claims abstract description 60
- 239000007788 liquid Substances 0.000 claims abstract description 46
- 239000003153 chemical reaction reagent Substances 0.000 claims abstract description 9
- 238000005192 partition Methods 0.000 claims description 13
- 239000011521 glass Substances 0.000 claims description 3
- 230000000149 penetrating effect Effects 0.000 claims description 3
- 238000000926 separation method Methods 0.000 claims description 3
- 239000000543 intermediate Substances 0.000 abstract description 16
- -1 benzene series compounds Chemical class 0.000 description 3
- 235000017166 Bambusa arundinacea Nutrition 0.000 description 2
- 235000017491 Bambusa tulda Nutrition 0.000 description 2
- 241001330002 Bambuseae Species 0.000 description 2
- 235000015334 Phyllostachys viridis Nutrition 0.000 description 2
- 239000011425 bamboo Substances 0.000 description 2
- 238000009434 installation Methods 0.000 description 2
- 239000000376 reactant Substances 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 150000002391 heterocyclic compounds Chemical class 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
Images
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
Abstract
The invention discloses a production detection device of a fluorine-containing chemical intermediate, which comprises: the reactor comprises an outer shell, a reaction tank and a reaction tank, wherein the outer shell is of a cylindrical structure with a closed lower end, a plurality of mutually independent reaction tanks are arranged inside the outer shell, the reaction tanks are distributed along the circumferential direction of the outer shell, and the openings of the reaction tanks are upward; the cover plate is provided with a plurality of liquid outlets, and when the cover plate is arranged at the upper port of the outer shell, the liquid outlets are in one-to-one correspondence with the reaction tanks; and the liquid supply assembly is fixedly arranged above the cover plate and is used for conveying a reaction reagent to the liquid outlet. The reactions in different reaction tanks are carried out synchronously, so that a user can conveniently compare and observe the reaction conditions among different samples, and the characteristics of different fluorine-containing organic intermediates can be more intuitively compared and observed.
Description
Technical Field
The invention belongs to the technical field of detection of fluorine-containing organic intermediates, and particularly relates to a production detection device for a fluorine-containing chemical intermediate.
Background
The fluorine-containing organic intermediates currently developed in China are roughly divided into four large series, namely benzene series compounds, toluene series compounds, aliphatic fluorides and heterocyclic compounds, according to the starting materials or chemical structures.
Fluorine-containing organic midbody need detect its characteristic after production is accomplished, but current production detection device for fluorine-containing organic midbody can only detect a fluorine-containing organic midbody simultaneously, can't realize the contrast and detect, and then inconvenient user contrasts the detection reaction result of different fluorine-containing organic midbodies.
Disclosure of Invention
The invention provides a production detection device of a fluorine-containing chemical intermediate, which aims to solve the technical problems in the background technology.
In order to achieve the purpose, the invention adopts the following technical scheme:
a production detection device of fluorine-containing chemical intermediate comprises:
the reactor comprises an outer shell, a reaction tank and a reaction tank, wherein the outer shell is of a cylindrical structure with a closed lower end, a plurality of mutually independent reaction tanks are arranged inside the outer shell, the reaction tanks are distributed along the circumferential direction of the outer shell, and the openings of the reaction tanks are upward;
the cover plate is provided with a plurality of liquid outlets, and when the cover plate is arranged at the upper port of the outer shell, the liquid outlets are in one-to-one correspondence with the reaction tanks;
and the liquid supply assembly is fixedly arranged above the cover plate and is used for conveying a reaction reagent to the liquid outlet.
Preferably, a plurality of mounting ports are formed in the cover plate, transparent glass is fixedly mounted in the mounting ports to form observation windows, and the observation windows are in one-to-one correspondence with the reaction tanks.
Preferably, the liquid supply assembly includes a plurality of liquid distribution pipes and an adding cylinder with a lower end sealed, a plurality of liquid distribution pipes and a plurality of liquid outlets one-to-one, the lower end of the liquid distribution pipe is fixedly connected with the cover plate and communicated with the corresponding liquid outlets, and the upper end of the liquid distribution pipe is fixedly connected with the lower end of the adding cylinder and communicated with the inside of the adding cylinder.
Preferably, be provided with the partition subassembly in the shell body, the partition subassembly includes erection column and a plurality of baffle, the erection column with the shell body is coaxial to be set up, and fixed configuration in the shell body middle part, it is a plurality of the baffle is followed shell body circumference evenly distributed, just baffle self is followed the shell body radially extends to separate into a plurality of independence with shell body inside the reaction tank.
Preferably, a vertically arranged fixing column is fixedly arranged in the middle of the lower side of the cover plate, the cross section of the fixing column is a regular polygon, the number of the side edges of the fixing column is equal to that of the reaction grooves, and a fixing groove with the same shape as the fixing column is arranged at the upper end of the mounting column.
Preferably, the cover plate is detachably connected with the outer shell through a fixing piece.
Preferably, the connecting piece is a threaded column, a threaded hole matched with the threaded column is formed in the lower end of the fixing column, a mounting hole penetrating through the bottom of the outer shell is also formed in the bottom wall of the fixing groove, the threaded column is installed in the threaded hole and the mounting hole in a threaded mode, the lower end of the threaded column is fixedly arranged in the rotating block, and a stand column is fixedly arranged at the bottom of the outer shell.
Compared with the prior art, the invention has the beneficial effects that:
when needs contrast detection fluorine-containing organic midbody sample, get its part as the sample with the fluorine-containing organic midbody that various different production were accomplished, place respectively in the reaction tank of difference, then cover the apron, corresponding reactant is added to the rethread liquid supply subassembly, reactant gets into in each different reaction tank through different liquid outlets, thereby make the reaction in the different reaction tanks go on in step, and then the reaction condition between the different samples of convenient to use person contrast observation, thereby can more audio-visually carry out comparison observation to the characteristic of the fluorine-containing organic midbody of difference.
Drawings
FIG. 1 is a schematic view of a top-view perspective structure of a production detection device for fluorine-containing chemical intermediates according to the present invention;
FIG. 2 is a schematic bottom perspective view of a device for detecting the production of fluorine-containing chemical intermediates according to the present invention;
fig. 3 is a schematic view of a vertical cross-sectional structure of a production detection device for a fluorine-containing chemical intermediate provided by the invention.
In the figure: the device comprises an outer shell 1, an upright column 2, a partition plate 3, a reaction tank 4, a mounting column 5, a cover plate 6, an adding cylinder 7, a liquid separating pipe 8, an observation window 9, a liquid outlet 10, a fixing column 11, a fixing piece 12 and a threaded hole 13.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments.
In the description of the present invention, it is to be understood that the terms "upper", "lower", "front", "rear", "left", "right", "top", "bottom", "inner", "outer", and the like, indicate orientations or positional relationships based on the orientations or positional relationships shown in the drawings, are merely for convenience in describing the present invention and simplifying the description, and do not indicate or imply that the device or element being referred to must have a particular orientation, be constructed and operated in a particular orientation, and thus, should not be construed as limiting the present invention.
Referring to fig. 1 to 3, a production detection apparatus for a fluorine-containing chemical intermediate includes:
the reactor comprises an outer shell 1, wherein the outer shell 1 is of a cylindrical structure with a closed lower end, a plurality of mutually independent reaction tanks 4 are arranged inside the outer shell 1, the plurality of reaction tanks 4 are distributed along the circumferential direction of the outer shell 1, and the notches of the reaction tanks 4 are upward;
a cover plate 6, wherein a plurality of liquid outlets 10 are arranged on the cover plate 6, and when the cover plate 6 is arranged at the upper port of the outer shell 1, the liquid outlets 10 correspond to the reaction tanks 4 one by one;
and the liquid supply assembly is fixedly arranged above the cover plate 6 and is used for conveying a reaction reagent to the liquid outlet 10.
In the embodiment applying the technical scheme, the reaction tank 4 is used for providing a space for reacting a fluorine-containing organic intermediate sample with a reaction reagent, when the fluorine-containing organic intermediate sample needs to be contrastively detected, parts of various fluorine-containing organic intermediates after production are taken as samples and are respectively placed in different reaction tanks 4, then the cover plate 6 is covered, corresponding reaction reagents are added through the liquid supply assembly, the reaction reagents enter different reaction tanks 4 through different liquid outlets 10, so that the reactions in different reaction tanks 4 are synchronously carried out, and further, a user can conveniently contrast and observe the reaction conditions among different samples, thereby more intuitively comparing and observing the characteristics of different fluorine-containing organic intermediates.
According to the preferable technical scheme in the embodiment, the cover plate 6 is provided with a plurality of mounting ports, transparent glass is fixedly mounted in the mounting ports, so that the observation windows 9 are formed, and the plurality of observation windows 9 correspond to the plurality of reaction tanks 4 one to one; particularly, the observation window 9 is arranged, so that a user can conveniently observe the reaction condition in the reaction tank 4.
In the preferred technical scheme of the embodiment, the liquid supply assembly comprises a plurality of liquid separating pipes 8 and an adding cylinder 7 with the lower end sealed, the liquid separating pipes 8 correspond to the liquid outlets 10 one by one, the lower ends of the liquid separating pipes 8 are fixedly connected with the cover plate 6 and are communicated with the corresponding liquid outlets 10, and the upper ends of the liquid separating pipes 8 are fixedly connected with the lower end of the adding cylinder 7 and are communicated with the inside of the adding cylinder; in specific this embodiment, during the use, operating personnel adds reaction reagent to adding a section of thick bamboo 7 in, add in a section of thick bamboo 7 reaction reagent reposition of redundant personnel to each divides in the liquid pipe 8, and then flows to different reaction tanks 4 through each liquid outlet 10.
In the preferred technical scheme in this embodiment, a partition assembly is arranged in an outer shell 1, the partition assembly includes a mounting column 5 and a plurality of partition plates 3, the mounting column 5 and the outer shell 1 are coaxially arranged and fixedly disposed in the middle of the outer shell 1, the plurality of partition plates 3 are uniformly distributed along the circumferential direction of the outer shell 1, and the partition plates 3 extend along the radial direction of the outer shell 1, so as to partition the interior of the outer shell 1 into a plurality of independent reaction tanks 4; in this embodiment, the inner side of the partition board 3 is fixedly connected to the mounting post 5, the outer side is fixedly connected to the inner wall of the outer casing 1, and the lower side is fixedly connected to the bottom wall of the outer casing 1.
According to the preferable technical scheme in the embodiment, the middle part of the lower side of the cover plate 6 is fixedly provided with the vertically arranged fixing columns 11, the cross sections of the fixing columns 11 are regular polygons, the number of the side edges of the fixing columns is the same as that of the reaction tanks 4, and the upper ends of the mounting columns 5 are provided with fixing grooves with the same shapes as the fixing columns 11; in this embodiment, when the cover plate 6 is disposed on the upper end of the outer casing 1, the mounting posts 5 are inserted into the fixing slots, and due to the shape limitation of the fixing slots and the fixing posts 11, the horizontal position of the cover plate 6 relative to the outer casing 1 is locked, and further the relative position of the liquid outlet 10 and the reaction tank 4 is locked.
In the preferred technical scheme of the embodiment, the cover plate 6 is detachably connected with the outer shell 1 through a fixing piece 12; specifically, the fixing piece 12 is arranged to connect the cover plate 6 with the outer shell 1, so that the cover plate and the outer shell can be stably connected in the reaction process, accidental separation is avoided, and the cover plate 6 can be detached and separated after the reaction is completed.
According to a further preferable technical scheme, the connecting piece is a threaded column, a threaded hole 13 matched with the threaded column is formed in the lower end of the fixing column 11, an installation hole penetrating through the bottom of the outer shell 1 is also formed in the bottom wall of the fixing groove, the threaded column is installed in the threaded hole 13 and the installation hole in a threaded mode, the lower end of the threaded column is fixedly arranged in the rotating block, and the upright column 2 is fixedly arranged at the bottom of the outer shell 1; in particular, in this embodiment, the operator can rotate the screw post through the rotating block, and when the screw post is disengaged from the screw hole 13, the cover plate 6 can be separated from the outer casing 1.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.
Claims (7)
1. The utility model provides a production detection device of fluorine-containing chemical industry midbody which characterized in that includes:
the reactor comprises an outer shell (1), wherein the outer shell (1) is of a cylindrical structure with a closed lower end, a plurality of mutually independent reaction tanks (4) are arranged inside the outer shell (1), the plurality of reaction tanks (4) are distributed along the circumferential direction of the outer shell (1), and the notches of the reaction tanks (4) are upward;
the cover plate (6) is provided with a plurality of liquid outlets (10), and when the cover plate (6) is arranged at the upper end of the outer shell (1), the liquid outlets (10) correspond to the reaction tanks (4) one by one;
the liquid supply assembly is fixedly arranged above the cover plate (6) and used for conveying reaction reagents to the liquid outlet (10).
2. The production detection device for the fluorine-containing chemical intermediate according to claim 1, wherein a plurality of mounting ports are formed in the cover plate (6), transparent glass is fixedly mounted in the mounting ports to form the observation windows (9), and the plurality of observation windows (9) correspond to the plurality of reaction tanks (4) one by one.
3. The production detection device of fluorine-containing chemical intermediate according to claim 1, wherein the liquid supply assembly comprises a plurality of liquid distribution pipes (8) and an addition cylinder (7) with a sealed lower end, the plurality of liquid distribution pipes (8) correspond to the plurality of liquid outlets (10) one by one, the lower end of the liquid distribution pipe (8) is fixedly connected with the cover plate (6) and communicated with the corresponding liquid outlets (10), and the upper end of the liquid distribution pipe (8) is fixedly connected with the lower end of the addition cylinder (7) and communicated with the inside of the addition cylinder.
4. The fluorine-containing chemical intermediate production detection device according to claim 1, wherein a separation assembly is arranged in the outer shell (1), the separation assembly comprises a mounting column (5) and a plurality of partition plates (3), the mounting column (5) and the outer shell (1) are coaxially arranged and fixedly arranged in the middle of the outer shell (1), the plurality of partition plates (3) are uniformly distributed along the circumferential direction of the outer shell (1), and the partition plates (3) extend along the radial direction of the outer shell (1) to separate the interior of the outer shell (1) into a plurality of independent reaction tanks (4).
5. The production detection device of the fluorine-containing chemical intermediate according to claim 4, wherein a vertically arranged fixing column (11) is fixedly arranged at the middle part of the lower side of the cover plate (6), the cross section of the fixing column (11) is a regular polygon, the number of the side edges of the fixing column is the same as that of the reaction tanks (4), and a fixing groove with the same shape as that of the fixing column (11) is arranged at the upper end of the mounting column (5).
6. The production detection device of fluorine-containing chemical intermediate as claimed in claim 5, wherein the cover plate (6) is detachably connected to the outer casing (1) via a fixing member (12).
7. The production detection device of the fluorine-containing chemical intermediate according to claim 6, wherein the connecting member is a threaded post, a threaded hole (13) for fitting the threaded post is formed in a lower end of the fixed post (11), a mounting hole penetrating through a bottom of the outer housing (1) is also formed in a bottom wall of the fixed groove, the threaded post is threadedly mounted in the threaded hole (13) and the mounting hole, the lower end is fixedly arranged on the rotating block, and the upright post (2) is fixedly arranged at the bottom of the outer housing (1).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110512311.6A CN113109521A (en) | 2021-05-11 | 2021-05-11 | Production detection device of fluorine-containing chemical intermediate |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110512311.6A CN113109521A (en) | 2021-05-11 | 2021-05-11 | Production detection device of fluorine-containing chemical intermediate |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN113109521A true CN113109521A (en) | 2021-07-13 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202110512311.6A Pending CN113109521A (en) | 2021-05-11 | 2021-05-11 | Production detection device of fluorine-containing chemical intermediate |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN113109521A (en) |
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Application publication date: 20210713 |