CN113069978A - Water-soluble fertilizer mixing production equipment and water-soluble fertilizer preparation method - Google Patents

Water-soluble fertilizer mixing production equipment and water-soluble fertilizer preparation method Download PDF

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Publication number
CN113069978A
CN113069978A CN202110319630.5A CN202110319630A CN113069978A CN 113069978 A CN113069978 A CN 113069978A CN 202110319630 A CN202110319630 A CN 202110319630A CN 113069978 A CN113069978 A CN 113069978A
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motor
soluble fertilizer
rotating shaft
water
shaft
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CN113069978B (en
Inventor
杨恒哲
闫涛
解学仕
王婷婷
张淑敏
高进华
白静
李元峰
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Chengde Lihe Fertilizer Co ltd
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Shandong Aodelu Biotechnology Co ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00Other mixers; Mixing plants; Combinations of mixers
    • B01F33/80Mixing plants; Combinations of mixers
    • B01F33/82Combinations of dissimilar mixers
    • B01F33/821Combinations of dissimilar mixers with consecutive receptacles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/10Maintenance of mixers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/181Preventing generation of dust or dirt; Sieves; Filters
    • B01F35/184Preventing generation of dust
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/71Feed mechanisms
    • B01F35/714Feed mechanisms for feeding predetermined amounts
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/79Preventing lumping, or comminuting lumps, during feeding or discharging, e.g. by means of vibrations, or by scrapers
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05BPHOSPHATIC FERTILISERS
    • C05B7/00Fertilisers based essentially on alkali or ammonium orthophosphates
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F2101/00Mixing characterised by the nature of the mixed materials or by the application field
    • B01F2101/32Mixing fertiliser ingredients
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/40Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Fertilizers (AREA)

Abstract

The invention discloses water-soluble fertilizer mixing production equipment, which comprises a paddle mixer, a quantitative feeder, a conveyor and a continuous forced mixer; the quantitative feeder is positioned below the paddle mixer; the conveyor is positioned at one end of the quantitative feeder; the continuous forced mixer is positioned at one end of the conveyor; the paddle mixer comprises a box body, an access cover, a first motor, a feeding hole, a first oil cylinder, a hopper lifter, a partition plate and a first rotating shaft; the hopper lifter comprises a first rotating roller, a conveyor belt, a second rotating roller and a second motor; the continuous forced mixer comprises a third motor, a cylinder, a second rotating shaft and a vibrating mechanism; the vibration mechanism comprises a fourth motor, a half-moon-shaped top plate, a guide shaft and a spring. The invention can realize continuous production to quickly and uniformly mix materials and elements, and can remove annual caking of fertilizers on the inner wall of equipment and reduce fertilizer wall adhesion.

Description

Water-soluble fertilizer mixing production equipment and water-soluble fertilizer preparation method
Technical Field
The invention belongs to the technical field of water-soluble fertilizer production and processing equipment, and particularly relates to water-soluble fertilizer mixing production equipment.
Background
In recent years, the water and fertilizer integration technology is popularized by the nation, the domestic powder water-soluble fertilizer product is developed rapidly, but the current powder water-soluble fertilizer in the market generally has the phenomenon of uneven nutrients, and products of various companies have unqualified random inspection events for many times. Through research and analysis, the uneven nutrition of the powder water-soluble fertilizer is mainly caused by the technical defects of the production process, and the main production process at present is shown in the attached figures 6 and 7;
the proportion of trace elements in the powder water-soluble fertilizer is small, 1-10kg of trace elements are added in each ton of product, the proportion is only a few per thousand, and various materials are difficult to uniformly mix by the conventional continuous mixing process. The intermittent mixing process can uniformly mix materials by prolonging the mixing time theoretically, but because the equipment is closed, heat is gathered in the mixing process, meanwhile, moisture absorption is obvious, the physical properties of the materials are greatly changed under the comprehensive action, the phenomena of fertilizer agglomeration and wall sticking can occur, and the intermittent mixing process has the defect of low production efficiency;
this patent improves current process equipment on technology and equipment, solves water-soluble fertile nutrient homogeneity problem, can realize continuous production simultaneously.
Disclosure of Invention
The invention aims to overcome the defects in the prior art, and provides water-soluble fertilizer mixing production equipment, which can realize continuous production to quickly and uniformly mix materials and elements, and can remove annual caking of fertilizers on the inner wall of the equipment and reduce fertilizer wall adhesion.
In order to achieve the purpose, the invention adopts the technical scheme that:
a water soluble fertilizer mixing production device comprises a paddle mixer, a quantitative feeder, a conveyor and a continuous forced mixer; the quantitative feeder is positioned below the paddle mixer; the conveyor is positioned at one end of the quantitative feeder; a continuous forced mixer is located at one end of the conveyor.
The paddle mixer comprises a box body, an access cover, a first motor, a feeding hole, a first oil cylinder, a hopper lifter, a partition plate and a first rotating shaft; the access cover is arranged at the top of the box body; the first motor and the feed inlet are arranged at the top of the box body, and the output shaft end of the first motor is provided with a chain wheel; the partition plate is arranged in the box body to form two material bins; the bottom of the clapboard is provided with a gate.
The first rotating shaft is arranged on the other side of the partition plate; a chain wheel is arranged at the top end of the first rotating shaft; the first rotating shaft body is provided with a plurality of groups of first spiral sheets and first blades, and the material stirring directions of the first spiral sheets and the first blades are opposite; the first motor shaft end chain wheel is connected with the first rotating shaft end chain wheel through a chain; the bottom of the box body is provided with a first sealing plate and is arranged at the gate; the first oil cylinder is arranged on one side of the bottom of the box body; the top shaft of the first oil cylinder is connected with a first sealing plate; the second sealing plate is arranged at a discharge port at the bottom of the box body; the shaft end of the top shaft of the second oil cylinder is connected with a second sealing plate.
The hopper hoister is arranged on one side of the partition plate; the hopper lifter comprises a first rotating roller, a conveyor belt, a second rotating roller and a second motor; the first rotating roller is fixed at the bottom of the box body through a rotating shaft, and a chain wheel is arranged at the rotating shaft; the second rotating roller is fixed at the top of the box body through a rotating shaft; the conveying belt is connected with the first rotating roller and the second rotating roller; the conveyer belt is provided with a hopper; the second motor is fixed on the outer side of the box body, and a chain wheel is arranged at the output shaft end of the second motor and connected with the chain wheel at the first rotating roller through a chain.
The continuous forced mixer comprises a third motor, a cylinder, a second rotating shaft and a vibrating mechanism; the third motor is fixed at one end of the cylinder; the bottom of the cylinder body is provided with a fixing frame for fixing the cylinder body; the top of the cylinder body is provided with a feeding port and a breathing port, and the breathing port is sealed by a PPS fiber cloth bag; a discharge hole is formed in one end of the bottom of the cylinder body; the second rotating shaft is arranged in the cylinder body; one end of the second rotating shaft is connected with an output shaft of a third motor through a coupler; a second spiral plate, a third spiral plate and a second blade are arranged on the second rotating shaft; the second spiral sheet is arranged at one end of the second rotating shaft and corresponds to the position of the feeding port; the third spiral sheet is positioned at the other end of the second rotating shaft and corresponds to the discharge hole; the rotation directions of the second spiral piece and the third spiral piece are opposite; the second blades are uniformly arranged between the second spiral sheet and the third spiral sheet; the materials are put into the cylinder body through the feed opening.
The vibration mechanism is fixed on the fixed frame; the vibration mechanism comprises a fourth motor, a half-moon-shaped top plate, a guide shaft and a spring; the fourth motor is fixed on the fixing frame; the half-moon-shaped top plate is fixed on the output shaft of the fourth motor; one end of the guide shaft is provided with a vibrating plate, and the other end of the guide shaft is provided with a limiting plate; the guide shaft penetrates through the cylinder body and is movably connected with the cylinder body, and the vibration plate is arranged in the cylinder body; the spring is sleeved with the guide shaft; one end of the spring is propped against the outer wall of the cylinder body, and the other end of the spring is propped against the limiting plate at one end of the guide shaft; and the half-moon-shaped top plate is abutted against the limiting plate at the end of the guide shaft.
A water soluble fertilizer and a mixed preparation method thereof, the 20-20-20 water soluble fertilizer contains trace elements, the contents of which are respectively 0.06-0.07% of boron, 0.09-0.15% of iron, 0.04-0.05% of zinc, 0.05-0.65% of manganese and 0.01-0.02% of molybdenum,
the mixed preparation method of the water-soluble fertilizer comprises the following steps: calculating the component proportion, preparing materials, premixing trace elements and finally mixing all material elements;
1) calculating the weight of the material elements according to the component proportion and preparing ingredients;
the water-soluble fertilizer has the following specific formula:
212 parts of urea (powder, 46-0-0), 38-334 parts of monoammonium phosphate (12-61-0), 442 parts of potassium nitrate (13-0-46), 3.0-4.0 parts of boric acid (containing 17% of boron), 7.0-8.5 parts of EDTA chelated iron (containing 13% of iron), 3.0-3.5 parts of EDTA chelated zinc (containing 15% of zinc), 3.5-4.5 parts of EDTA chelated manganese (containing 13% of manganese), and 0.15-0.25 part of ammonium molybdate heptahydrate (containing 54% of molybdenum);
2) firstly, premixing trace elements, namely premixing boric acid, EDTA chelated iron, EDTA chelated zinc, EDTA chelated manganese and ammonium molybdate heptahydrate containing the trace elements and potassium nitrate in proportion by a paddle mixer, wherein the premixing time is only 2-3 min;
3) the other elements and the premixed trace elements are simultaneously put into a continuous forced mixer, so that the trace elements and the other elements are secondarily mixed.
Compared with the prior art, the invention has the beneficial effects that:
1) a baffle plate is arranged in the paddle mixer, and two material bins are formed on two sides of the baffle plate; a hopper lifter is arranged on one side of the partition plate, and a first rotating shaft is arranged on the other side of the partition plate; the first rotating shaft is provided with a first spiral blade and a first paddle, the first spiral blade and the first paddle are fixed at intervals, the stirring direction and the material conveying direction are opposite, and the materials can be repeatedly mixed up and down during mixing, so that the materials are prevented from sinking to the bottom in the first time, and cannot be quickly and uniformly mixed in a short time; the mixed raw materials enter the other side of the partition plate through the partition plate gate, and are sent back to one side of the first rotating shaft through the hopper lifting machine, so that the positions of the raw materials at the bottom and the top of the paddle mixer are exchanged, and then the raw materials are mixed by the first paddle and the first spiral slice to be fully and uniformly mixed;
2) a second rotating shaft is arranged in the continuous forced mixer, a second spiral blade and a third spiral blade are respectively arranged at two ends of the second rotating shaft, and a plurality of second blades which are uniformly distributed are arranged between the second rotating shaft and the third spiral blade; the raw materials are conveyed to one end of the cylinder under the action of the second spiral piece, then under the action of the second paddle, the materials are lifted and continue to move rightwards, and the whole process has the functions of conveying and mixing until the materials are conveyed to the discharge hole; the third spiral sheet and the second spiral sheet have opposite material guiding directions, and the raw materials accumulated at the end part of the cylinder body are reversely conveyed into the discharging hole, so that the accumulation of the raw materials is avoided;
3) be equipped with the mouth of breathing on the barrel, the mouth of breathing uses PPS fiber material sack to seal, plays the effect of the inside atmospheric pressure of balanced equipment for the dust is not excessive. The whole mixing equipment comprises a feed port and a discharge port which are in a closed state, and dust removing equipment is not required to be additionally arranged;
4) the inside vibrations mechanism that is equipped with of barrel promotes the guiding axle through half moon type roof, then guiding axle hand spring force resets rapidly and forms vibrations to the barrel, makes the raw materials that the barrel inner wall bonded drop fast, avoids excessive bonding.
Drawings
FIG. 1 is a schematic structural diagram of a water-soluble fertilizer mixing production device and a mixing production device in a water-soluble fertilizer preparation method;
FIG. 2 is a schematic structural diagram of a paddle mixer in mixing production equipment in the water-soluble fertilizer mixing production equipment and the water-soluble fertilizer preparation method;
FIG. 3 is a schematic sectional structure view of a cylinder in the water-soluble fertilizer mixing production equipment and the water-soluble fertilizer preparation method of the invention;
FIG. 4 is a schematic structural diagram of a vibration mechanism in the water-soluble fertilizer mixing production equipment and the water-soluble fertilizer preparation method;
FIG. 5 is a schematic structural diagram of a vibration mechanism in the water-soluble fertilizer mixing production equipment;
FIG. 6 is a schematic process diagram of comparative example 1 of a water-soluble fertilizer mixing production apparatus and a water-soluble fertilizer preparation method of the present invention;
FIG. 7 is a schematic process diagram of comparative example 1 of a water-soluble fertilizer mixing production apparatus and a water-soluble fertilizer preparation method of the present invention;
in the figure: 1. a paddle mixer; 101. a box body; 1011. a first seal plate; 1012. a second seal plate; 1013. a second cylinder; 102. an access cover; 103. a first motor; 104. a feed inlet; 105. a first cylinder; 106. a hopper elevator; 1061. a first rotating roller; 1062. a conveyor belt; 10621. a hopper; 1063. a second rotating roller; 1064. a second motor; 107. a partition plate; 1071. a gate opening; 108. a first rotating shaft; 1081. a first helical flight; 1082. a first blade; 2. a constant feeder; 3. a conveyor; 4. a continuous forced mixer; 401. a third motor; 402. a barrel; 4021. a feeding port; 4022. a breathing port; 4023. a discharging port; 4024. a fixed mount; 403. a second rotating shaft; 4031. a second flight; 4032. a second blade; 4033. a third flight; 404. a vibration mechanism; 4041. a fourth motor; 4042. a half-moon shaped top plate; 4043. a guide shaft; 40431. a vibration plate; 4044. a spring.
Detailed Description
For the convenience of understanding of those skilled in the art, the technical solution of the present invention will be further described in detail with reference to fig. 1 to 7.
A water soluble fertilizer mixing production device comprises a paddle mixer 1, a quantitative feeder 2, a conveyor 3 and a continuous forced mixer 4; the constant feeder 2 is positioned below the paddle mixer 1; the conveyor 3 is positioned at one end of the quantitative feeder 2; a continuous forced mixer 4 is located at one end of the conveyor 3.
The paddle mixer 1 comprises a box body 101, an access cover 102, a first motor 103, a feeding hole 104, a first oil cylinder 105, a hopper lifter 106, a partition plate 107 and a first rotating shaft 108; the access cover 102 is arranged at the top of the box body 101 and used for opening and closing the box body 101 to access the internal protection structure; the first motor 103 and the feed inlet 104 are arranged at the top of the box body 101, and the output shaft end of the first motor 103 is provided with a chain wheel; the partition plate 107 is arranged in the box body 101 to form two material bins; the bottom of the partition 107 is provided with a gate 1071 for transferring the material on both sides of the partition 107.
The first rotating shaft 108 is arranged on the other side of the partition plate 107; a chain wheel is arranged at the top end of the first rotating shaft 108; the first rotating shaft 108 is provided with a plurality of groups of first spiral pieces 1081 and first blades 1082 on the shaft body, the material stirring directions of the first spiral pieces 1081 and the first blades 1082 are opposite, namely the first spiral pieces 1081 downwards stir materials, the materials are upwards turned and gushed by turning the first blades 1082, the first spiral pieces 1081 and the first blades are arranged at intervals to form an up-and-down mixing and stirring effect, the materials are more uniform in the stirring and mixing process, and the situation that the materials are difficult to be uniformly mixed in a short time due to the fact that the materials settle at the bottom of the box 101 in the first time is avoided; the first motor 103 shaft end chain wheel is connected with the first rotating shaft 108 shaft end chain wheel through a chain; the first motor 103 provides power to drive the first rotating shaft 108 to rotate so as to mix and stir the materials; the bottom of the box body 101 is provided with a first sealing plate 1011 and arranged at the gate 1071; the first oil cylinder 105 is arranged on one side of the bottom of the box body 101; the top shaft of the first oil cylinder 105 is connected with a first closing plate 1011; the opening and closing of the first closing plate 1011 are controlled by the first oil cylinder 105; the second sealing plate 1012 is arranged at the discharge port at the bottom of the box body 101; the top shaft end of the second oil cylinder 1013 is connected with a second sealing plate 1012, and the opening and closing of the discharge port is controlled by the second oil cylinder 1013.
The hopper lifter 106 is arranged on one side of the partition plate 107; the hopper elevator 106 comprises a first rotating roller 1061, a conveyor belt 1062, a second rotating roller 1063 and a second motor 1064; the first rotating roller 1061 is fixed at the bottom of the box 101 through a rotating shaft, and a sprocket is arranged at the rotating shaft; the second rotating roller 1063 is fixed on the top of the box 101 through a rotating shaft; the conveyor belt 1062 connects the first rotating roller 1061 and the second rotating roller 1063; a hopper 10621 is arranged on the conveyor belt 1062; the second motor 1064 is fixed on the outer side of the box body 101, and a sprocket is arranged at the output shaft end of the second motor 1064 and is connected with a sprocket at the first rotating roller 1061 through a chain; the second motor 1064 provides power to drive the conveyor belt 1062 to run, and the material is conveyed to the other side of the top pouring partition 107 through the hopper 10621; the materials are circularly stirred in the material bins at the two sides of the partition plate 107, so that the materials are mixed more uniformly.
The continuous forced mixer 4 comprises a third motor 401, a cylinder 402, a second rotating shaft 403 and a vibrating mechanism 404; the third motor 401 is fixed at one end of the cylinder 402; the bottom of the cylinder 402 is provided with a fixing frame 4024 for fixing the cylinder 402; the top of the barrel 402 is provided with a feeding port 4021 and a breathing port 4022, and the breathing port 4022 is sealed by a PPS fiber cloth bag, so that the air pressure in the equipment is balanced, and dust is prevented from overflowing; a discharging hole 4023 is formed in one end of the bottom of the cylinder 402; the second rotating shaft 403 is arranged inside the cylinder 402; one end of the second rotating shaft 403 is connected with an output shaft of the third motor 401 through a coupler; a second spiral piece 4031, a third spiral piece 4033 and a second blade 4032 are arranged on the second rotating shaft 403; the second spiral plate 4031 is arranged at one end of the second rotating shaft 403 and corresponds to the feeding port 4021; the third spiral plate 4033 is positioned at the other end of the second rotating shaft 403 and corresponds to the discharge hole 4023; the second spiral piece 4031 and the third spiral piece 4033 rotate in opposite directions; second paddle 4032 is uniformly arranged between second spiral piece 4031 and third spiral piece 4033; materials are fed into the cylinder 402 through the feeding port 4021, the third motor 401 provides power to drive the second rotating shaft 403 to rotate, the second spiral piece 4031 pushes the materials to be conveyed to the discharging port 4023, and the second blade 4032 continues to stir and mix the materials and simultaneously lifts the materials to continue to convey the materials to the right; the third spiral 4033 reversely transfers the material accumulated at the bottom end of the barrel 402 to the discharge port 4023 for discharging to avoid accumulation.
The vibration mechanism 404 is fixed on the fixing frame 4024; the vibration mechanism 404 includes a fourth motor 4041, a half-moon-shaped top plate 4042, a guide shaft 4043, and a spring 4044; the fourth motor 4041 is fixed on the fixing frame 4024; a half-moon-shaped top plate 4042 is fixed on an output shaft of the fourth motor 4041; a vibration plate 40431 is arranged at one end of the guide shaft 4043, and a limit plate is arranged at the other end; the guide shaft 4043 penetrates the cylinder 402 and is movably connected with the cylinder 402, and the vibration plate 40431 is arranged inside the cylinder 402; a spring 4044 is sleeved on the guide shaft 4043; one end of the spring 4044 is pressed against the outer wall of the cylinder 402, and the other end is pressed against the limit plate at one end of the guide shaft 4043; the half-moon-shaped top plate 4042 is abutted against a limit plate at the end of the guide shaft 4043; in order to prevent the inner wall of the cylinder 402 from being bonded by the material, the stirring machine is stopped after the stirring operation of the cylinder 402 is finished, then the fourth motor 4041 drives the half-moon-shaped top plate 4042 to rotate to push the guide shaft 4043, when the half-moon-shaped top plate 4042 crosses the topmost end, the guide shaft 4043 is pushed by the elastic force of the spring 4044 to reset rapidly, the vibration plate 40431 knocks the inner wall of the cylinder 402 to generate vibration, and the material bonding block on the inner wall of the cylinder 402 falls off.
A water soluble fertilizer and a mixed preparation method thereof, the 20-20-20 water soluble fertilizer contains trace elements, the contents of which are respectively 0.06-0.07% of boron, 0.09-0.15% of iron, 0.04-0.05% of zinc, 0.05-0.65% of manganese and 0.01-0.02% of molybdenum,
the mixed preparation method of the water-soluble fertilizer comprises the following steps: calculating the component proportion, preparing materials, premixing trace elements and finally mixing all material elements;
example 1: as shown in fig. 5;
1) calculating the weight of the material elements according to the component proportion and preparing ingredients;
the water-soluble fertilizer has the following specific formula:
212 portions of urea (powder, 46-0-0), 38-334 portions of monoammonium phosphate (12-61-0), 442 portions of potassium nitrate (13-0-46), 3.0-4.0 portions of boric acid (containing 17% of boron), 7.0-8.5 portions of EDTA chelated iron (containing 13% of iron), 3.0-3.5 portions of EDTA chelated zinc (containing 15% of zinc), 3.5-4.5 portions of EDTA chelated manganese (containing 13% of manganese), and 0.15-0.25 portion of ammonium molybdate heptahydrate (containing 54% of molybdenum).
2) And (3) premixing trace elements, namely premixing 3.5 parts of boric acid containing the trace elements, 8.0 parts of EDTA chelated iron, 3.3 parts of EDTA chelated zinc, 4.0 parts of EDTA chelated manganese and 0.2 part of ammonium heptahydrate with 440 potassium nitrate in a paddle mixer in proportion, wherein the premixing time is only 2 min.
3) The other elements and the premixed trace elements are simultaneously put into a continuous forced mixer, so that the trace elements and the other elements are secondarily mixed.
As shown in fig. 5, the specific operation is that 211 parts of urea is put into a buffer bin from a feeding port 1, and then enters an integral mixing bin after being measured by a constant feeder; 330 parts of monoammonium phosphate are put into the buffer bin from the feed inlet 2, and then enter the integral mixing bin after being measured by the constant feeder; 440 parts of potassium nitrate, 3.5 parts of boric acid, 8.0 parts of EDTA chelated iron, 3.3 parts of EDTA chelated zinc, 4.0 parts of EDTA chelated manganese and 0.2 part of ammonium molybdate heptahydrate are all simultaneously thrown into the feed inlet 4 and then enter a paddle mixer to be stirred and mixed for 2 min.
The raw materials are measured and conveyed to a continuous forced mixer: the materials are fed into the equipment from a feeding port and conveyed to the right under the action of a fourth motor and a third spiral piece. Then, under the effect of second paddle, the material is picked up and continues to the right, and whole process plays the function of carrying, mixing, and until the material conveys the drain hole, then packs. The barrel is fixed, and the mouth of respiration uses PPS fiber material sack to seal, plays the effect of balanced equipment inside atmospheric pressure for the dust is not excessive.
Comparative example 1: as shown in fig. 6;
the specific formula is unchanged from the example 1, and all the materials are directly put into the system through the feed ports in sequence, wherein the trace elements are independently put into the system through the feed ports of the same feed port, mixed by a drum mixer and then packaged;
specifically, 211 parts of urea is fed into a buffer bin from a feeding port 1 and then is metered by a constant feeder and then enters an integral mixing bin; 330 parts of monoammonium phosphate are put into the buffer bin from the feed inlet 2, and then enter the integral mixing bin after being measured by the constant feeder; 440 parts of potassium nitrate is put into the buffer bin from the feeding port 3 and enters the integral mixing bin after being measured by the quantitative feeder; after 3.5 parts of boric acid, 8.0 parts of EDTA chelated iron, 3.3 parts of EDTA chelated zinc, 4.0 parts of EDTA chelated manganese and 0.2 part of ammonium molybdate heptahydrate are simultaneously fed from a feeding port 4, the materials are metered by a quantitative feeder to enter an integral mixing bunker, the integral mixing bunker is connected with a rotary drum mixer, and the materials are discharged after being mixed by a rotary drum and then packaged.
Comparative example 2: as shown in fig. 7;
in the same way as example 1, a premixing process was added, a 1000L paddle mixer was used to premix trace elements with one of the macroelements in proportion, a drum mixer was used to mix the materials entering the equipment, and then packaging was performed. Because the feed inlet can not be completely sealed, the dust is large, and a bag-type dust remover is required to be additionally arranged;
specifically, 211 parts of urea is fed into a buffer bin from a feeding port 1 and then is metered by a constant feeder and then enters an integral mixing bin; 330 parts of monoammonium phosphate are put into the buffer bin from the feed inlet 2, and then enter the integral mixing bin after being measured by the constant feeder; 440 parts of potassium nitrate, 3.5 parts of boric acid, 8.0 parts of EDTA chelated iron, 3.3 parts of EDTA chelated zinc, 4.0 parts of EDTA chelated manganese and 0.2 part of ammonium molybdate heptahydrate are all simultaneously thrown into the feed inlet 4, enter a paddle mixer and are stirred and mixed for 2min, then a discharge valve is opened, and the mixed material enters a buffer bin and enters an integral mixing bin through the metering of a quantitative feeder. The whole mixing bin is connected with the rotary drum mixer, and is discharged after being mixed by the rotary drum, and then is packaged.
The nutrient stability and uniformity of the 20-20-20 water-soluble fertilizers produced in the examples 1, 1 and 2 are determined by sampling at regular time in the process of producing the 20-20-20 water-soluble fertilizers (containing trace elements and respectively containing 0.06% of boron, 0.1% of iron, 0.05% of zinc, 0.05% of manganese and 0.01% of molybdenum) by three water-soluble fertilizer production process equipment in the examples 1, 1 and 2, sampling at a discharge port for 6 times every 1 hour after stable discharge of the three processes, and determining the nutrient content of the samples for 6 times. The results of the measurements are shown in tables 1-6 below:
TABLE 13 Water soluble fertilizer produced by the process samples taken at each time interval of the available nitrogen content unit (%)
Treatment of 1 2 3 4 5 6
Example 1 19.98 20.03 20.01 19.88 20.46 20.33
Comparative example 1 18.2 22.96 23.25 18.14 19.15 24.03
Comparative example 2 17.23 20.55 21.89 18.42 23.05 18.16
As can be seen from Table 1, in the process of 6 times of sampling, the nitrogen content fluctuation of example 1 is minimum, the nitrogen content is qualified, the nitrogen content fluctuation between the sampling of comparative example 1 and the sampling of comparative example 2 is large, and even the single nutrient is unqualified (GB15063-2009 Compound Fertilizer) states that the single nutrient content of nitrogen, phosphorus and potassium is controlled to be +/-1.5).
TABLE 23 effective phosphorus content (%)
Treatment of 1 2 3 4 5 6
Example 1 20.01 19.89 20.11 20.04 19.96 20.22
Comparative example 1 23.11 17.63 21.55 18.36 19.45 22.68
Comparative example 2 18.44 22.63 17.06 22.59 16.42 21.66
As can be seen from Table 2, the phosphorus content in example 1 fluctuates minimally and is acceptable in the 6 times of sampling, and the phosphorus content in comparative example 1 and comparative example 2 fluctuates greatly and even the single nutrient is unacceptable (GB15063-2009 Compound Fertilizer) states that the single nutrient content of NPK is controlled to be +/-1.5).
TABLE 33 quick-acting potassium content (%) -based samples of water-soluble fertilizers produced by the process at various time intervals
Treatment of 1 2 3 4 5 6
Example 1 20.02 20.31 19.94 19.78 20.06 20.15
Comparative example 1 18.64 22.65 16.65 17.15 21.88 23.75
Comparative example 2 20.42 17.65 19.58 21.43 16.45 23.64
As can be seen from Table 3, in the 6 sampling processes, the fluctuation of the potassium content in example 1 is minimum, the potassium content is qualified, the fluctuation of the potassium content in each sampling of comparative example 1 and comparative example 2 is large, and even single nutrient is unqualified (GB15063-2009 Compound Fertilizer) states that the single nutrient content of nitrogen, phosphorus and potassium is controlled to be +/-1.5).
TABLE 43 boron content units (%)
Treatment of 1 2 3 4 5 6
Example 1 0.06 0.065 0.064 0.062 0.068 0.0615
Comparative example 1 0.1 0.04 0.12 0.2 0.65 0.68
Comparative example 2 0.06 0.03 0.07 0.08 0.01 0.07
As can be seen from Table 4, in the 6 sampling processes, the fluctuation of the boron content in example 1 is minimum, and the boron content is qualified, and the fluctuation of the boron content in each sampling of comparative example 1 and comparative example 2 is large, which does not meet the quality requirement.
TABLE 53 iron content units (%) -of samples taken at various time intervals of water-soluble fertilizers produced by the process
Treatment of 1 2 3 4 5 6
Example 1 0.1 0.09 0.11 0.12 0.09 0.95
Comparative example 1 0.03 0.18 0.06 0.2 0.1 0.08
Comparative example 2 0.06 0.09 0.13 0.04 0.21 0.2
As can be seen from Table 5, in the course of 6 times of sampling, the fluctuation of the iron content in example 1 was minimal, and the iron content was acceptable, while the fluctuation of the iron content between the sampling in comparative examples 1 and 2 was large, and the quality was not satisfactory.
TABLE 63 Water-soluble fertilizers produced by the process sampling zinc content units (%)
Treatment of 1 2 3 4 5 6
Example 1 0.05 0.045 0.052 0.048 0.055 0.046
Comparative example 1 0.02 0.1 0.32 0.04 0.05 0.18
Comparative example 2 0.01 0.09 0.045 0.21 0.64 0.08
As can be seen from Table 6, in the 6 sampling processes, the zinc content fluctuation of example 1 is minimum, and the zinc content is qualified, and the zinc content fluctuation between the sampling of comparative example 1 and the sampling of comparative example 2 is large, which does not meet the quality requirement.
TABLE 73 Water-soluble fertilizer produced by the process manganese content unit (%)
Treatment of 1 2 3 4 5 6
Example 1 0.05 0.055 0.62 0.06 0.52 0.05
Comparative example 1 0.055 0.04 0.12 0.22 0.07 0.02
Comparative example 2 0.1 0.12 0.04 0.2 0.05 0.02
As can be seen from Table 7, in the 6 sampling processes, the manganese content fluctuation of example 1 is minimum, the manganese content is qualified, and the manganese content fluctuation between the sampling of comparative example 1 and the sampling of comparative example 2 is large, which does not meet the quality requirement.
TABLE 83 molybdenum content (%) -in samples taken at various time intervals of water-soluble fertilizer produced by process
Treatment of 1 2 3 4 5 6
Example 1 0.012 0.012 0.16 0.14 0.15 0.14
Comparative example 1 0.01 0 0.08 0.1 0.15 0.12
Comparative example 2 0.02 0.09 0 0.10 0.20 0.03
As can be seen from Table 8, in the 6 sampling processes, the fluctuation of the molybdenum content in example 1 is minimal, and the molybdenum content is acceptable, while the fluctuation of the molybdenum content in each sampling of comparative example 1 and comparative example 2 is large, and the quality requirements are not met.
The foregoing is merely exemplary and illustrative of the present invention and various modifications, additions and substitutions may be made by those skilled in the art to the specific embodiments described without departing from the scope of the present invention as defined in the accompanying claims.

Claims (9)

1. A water soluble fertilizer mixing production device comprises a paddle mixer, a quantitative feeder, a conveyor and a continuous forced mixer; it is characterized in that the constant feeder is positioned below the paddle mixer; the conveyor is positioned at one end of the quantitative feeder; the continuous forced mixer is positioned at one end of the conveyor;
the paddle mixer comprises a box body, an access cover, a first motor, a feeding hole, a first oil cylinder, a hopper lifter, a partition plate and a first rotating shaft; the access cover is arranged at the top of the box body; the first motor and the feed inlet are arranged at the top of the box body, and the output shaft end of the first motor is provided with a chain wheel; the partition plate is arranged in the box body to form two material bins; the bottom of the clapboard is provided with a gate.
2. The water-soluble fertilizer mixing production equipment as claimed in claim 1, wherein the first rotating shaft is arranged at the other side of the partition plate; a chain wheel is arranged at the top end of the first rotating shaft; the first rotating shaft body is provided with a plurality of groups of first spiral sheets and first blades, and the material stirring directions of the first spiral sheets and the first blades are opposite; the first motor shaft end chain wheel is connected with the first rotating shaft end chain wheel through a chain; the bottom of the box body is provided with a first sealing plate and is arranged at the gate; the first oil cylinder is arranged on one side of the bottom of the box body; the top shaft of the first oil cylinder is connected with a first sealing plate; the second sealing plate is arranged at a discharge port at the bottom of the box body; the shaft end of the top shaft of the second oil cylinder is connected with a second sealing plate.
3. The water-soluble fertilizer mixing production equipment according to claim 1, wherein the hopper elevator is arranged on one side of the partition plate; the hopper lifter comprises a first rotating roller, a conveyor belt, a second rotating roller and a second motor; the first rotating roller is fixed at the bottom of the box body through a rotating shaft, and a chain wheel is arranged at the rotating shaft; the second rotating roller is fixed at the top of the box body through a rotating shaft; the conveying belt is connected with the first rotating roller and the second rotating roller; the conveyer belt is provided with a hopper; the second motor is fixed on the outer side of the box body, and a chain wheel is arranged at the output shaft end of the second motor and connected with the chain wheel at the first rotating roller through a chain.
4. The mixing production equipment of the water-soluble fertilizer as claimed in claim 1, wherein the continuous forced mixer comprises a third motor, a cylinder, a second rotating shaft and a vibrating mechanism; the third motor is fixed at one end of the cylinder; the bottom of the cylinder body is provided with a fixing frame for fixing the cylinder body; the top of the cylinder body is provided with a feeding port and a breathing port, and the breathing port is sealed by a PPS fiber cloth bag; a discharge hole is formed in one end of the bottom of the cylinder body; the second rotating shaft is arranged in the cylinder body; one end of the second rotating shaft is connected with an output shaft of a third motor through a coupler; a second spiral plate, a third spiral plate and a second blade are arranged on the second rotating shaft; the second spiral sheet is arranged at one end of the second rotating shaft and corresponds to the position of the feeding port; the third spiral sheet is positioned at the other end of the second rotating shaft and corresponds to the discharge hole; the rotation directions of the second spiral piece and the third spiral piece are opposite; the second blades are uniformly arranged between the second spiral sheet and the third spiral sheet; the materials are put into the cylinder body through the feed opening.
5. The mixing production equipment of the water soluble fertilizer as claimed in claim 1, wherein the vibration mechanism is fixed on a fixing frame; the vibration mechanism comprises a fourth motor, a half-moon-shaped top plate, a guide shaft and a spring; the fourth motor is fixed on the fixing frame; the half-moon-shaped top plate is fixed on the output shaft of the fourth motor; one end of the guide shaft is provided with a vibrating plate, and the other end of the guide shaft is provided with a limiting plate; the guide shaft penetrates through the cylinder body and is movably connected with the cylinder body, and the vibration plate is arranged in the cylinder body; the spring is sleeved with the guide shaft; one end of the spring is propped against the outer wall of the cylinder body, and the other end of the spring is propped against the limiting plate at one end of the guide shaft; and the half-moon-shaped top plate is abutted against the limiting plate at the end of the guide shaft.
6. A water soluble fertilizer and a mixed preparation method thereof, which is characterized in that the water soluble fertilizer 20-20-20 contains trace elements, the content of which is respectively 0.06-0.07% of boron, 0.09-0.15% of iron, 0.04-0.05% of zinc, 0.05-0.65% of manganese and 0.01-0.02% of molybdenum,
the mixed preparation method of the water-soluble fertilizer comprises the following steps: calculating the component proportion, preparing materials, premixing trace elements and finally mixing all material elements.
7. The water soluble fertilizer and the mixing preparation method thereof according to claim 6, wherein the weight of the raw material elements is calculated according to the component proportion and ingredients are prepared;
the water-soluble fertilizer has the following specific formula:
212 portions of urea (powder, 46-0-0), 38-334 portions of monoammonium phosphate (12-61-0), 442 portions of potassium nitrate (13-0-46), 3.0-4.0 portions of boric acid (containing 17% of boron), 7.0-8.5 portions of EDTA chelated iron (containing 13% of iron), 3.0-3.5 portions of EDTA chelated zinc (containing 15% of zinc), 3.5-4.5 portions of EDTA chelated manganese (containing 13% of manganese), and 0.15-0.25 portion of ammonium molybdate heptahydrate (containing 54% of molybdenum).
8. The water-soluble fertilizer and the mixing preparation method thereof as claimed in claim 6, characterized in that firstly, the trace elements are premixed, boric acid containing trace elements, EDTA chelated iron, EDTA chelated zinc, EDTA chelated manganese, ammonium molybdate heptahydrate and potassium nitrate are premixed in proportion by a paddle mixer, and the premixing time is only 2-3 min.
9. The water soluble fertilizer and the mixing preparation method thereof as claimed in claim 6, wherein the other elements and the premixed trace elements are simultaneously fed into the continuous forced mixer to complete the secondary mixing of the trace elements and the other elements.
CN202110319630.5A 2021-03-25 2021-03-25 Water-soluble fertilizer mixing production equipment and water-soluble fertilizer preparation method Active CN113069978B (en)

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CN206935292U (en) * 2017-07-27 2018-01-30 滁州市腾鑫新材料有限公司 Powder continuous mixer is used in pressure sensitive adhesive production
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CN114100464B (en) * 2021-12-01 2024-05-07 宁波欣元环保科技有限公司 Chemical fertilizer mixing device

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