CN113025151B - 一种底盘装甲涂料及其制备方法 - Google Patents

一种底盘装甲涂料及其制备方法 Download PDF

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CN113025151B
CN113025151B CN201911246535.6A CN201911246535A CN113025151B CN 113025151 B CN113025151 B CN 113025151B CN 201911246535 A CN201911246535 A CN 201911246535A CN 113025151 B CN113025151 B CN 113025151B
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陈炳耀
董颖
姚荣茂
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GUANGDONG SANVO CHEMICAL INDUSTRY TECHNOLOGY CO LTD
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Abstract

一种底盘装甲涂料，其主要成分按照重量比包括：复合树脂22‑4、环保溶剂35‑55、500‑2500目功能填料7‑16、纳米石墨烯1‑7、阻燃剂4‑15、200‑2000目重防护抗锈剂5‑12、二元乙丙橡胶1‑5、氯磺化橡胶1‑7、分散防沉剂0.7‑5、抗裂剂1‑6、色浆显色剂0.6‑7、环保抛射剂12～35；本发明还公开了一种底盘装甲涂料的制备方法。发明具有优点：1.产品性能好；2.施工方便；3.复合树脂与橡胶体系强化，耐老化性能优异，4.扩展阻燃与抗锈产品性能。

Description

一种底盘装甲涂料及其制备方法
技术领域
本发明涉及一种底盘装甲涂料，具体是一种气雾型汽车底盘涂料，本发明还涉及了上述气雾型涂料的制备方法；具体涉及一种气雾型用于汽车底盘涂料或类似用途的保护涂料及其制备方法。
背景技术
气雾型涂料，又名自喷漆或手摇自动喷漆。气雾型涂料是把树脂、溶剂、颜填料、抛射剂等装入气雾罐中，通过阀门释放装置控制，使混合物以气溶胶形式喷出的自加压包装形式的产品。气雾漆具有施工操作灵活简单、携带方便、喷涂雾化效果好、喷出率高等特点，打破了传统涂料的施工方法，轻松解决了传统涂料在户内外施工困难的难题
底盘涂料（又名底盘装甲），可以有效防护路面砂石对汽车车辆底盘的击打，防止轻微的拖底磨擦；预防酸、碱、盐对底盘铁板的腐蚀；防止底盘螺丝的松脱；降低行驶时噪音的传导，增加驾驶宁静感；阻止底盘铁板热传导，使驾驶室内冬暖夏凉。目前，市面上的底盘装甲主要为各种沥青类涂料，沥青涂料虽然具有优异的防腐性能，但是其缺点同样明显，主要表现在沥青在夏天车底温度高时容易滴落，散发出有害气体渗入车厢危害车主的健康，沥青漆膜在后期易脆化变硬脱落，耐老化性能差，不耐汽油，沥青材料易燃，车辆高速行驶时，对碎石撞击声、风噪的隔声效果较差。
发明内容
本发明的一个目的是提供一种底盘装甲涂料及其制备方法，以克服常规气雾漆所述的技术缺陷，和应用领域受限等问题。本发明的另一个目的是提供该涂料及其制备方法，以解决上述现有普通沥青类涂料存在的问题。
技术方案如下：
一种底盘装甲涂料，其主要成分按照重量比包括：
复合树脂22-45
环保溶剂 35-55
500-2500目功能填料7-16
纳米石墨烯1-7
阻燃剂4-15
偶联剂 1-3
200-2000目重防护抗锈剂5-12
二元乙丙橡胶1-5
氯磺化橡胶1-7
分散防沉剂0.7-5
抗裂剂1-6
色浆显色剂0.6-7
环保抛射剂 12～35；
所述的复合树脂为氢化SIS、氢化SBS、氢化柏油=0-9︰2-7︰1-8；
所述的环保溶剂为乙二醇二醋酸酯(EGDA)、二元醇酯(YPC)、D80溶剂油中的至少一种；
所述的500-2500目功能填料为空心微珠︰矿物粉=1-9︰2-7，空心微珠为500-2500目空心玻璃微珠、500-2000目中空陶瓷微粒中的至少一种，矿物粉为500-2500目珍珠岩、500-2500目云母粉、500-2500目硅微粉、500-2500目石墨粉中的至少一种；
所述的阻燃剂为氢氧化镁、二苯基砜磺酸盐、改性氢氧化铝、十溴二苯醚、MCA阻燃剂中的至少一种；
所述的偶联剂为KH-550硅烷偶联剂、KH-551硅烷偶联剂、KH-560硅烷偶联剂、KH-570硅烷偶联剂中至少一种。
所述的200-2000目重防护抗锈剂为锌粉︰铝粉︰铁红粉=1-10︰0-7︰0-6；
所述的氯磺化橡胶为氯磺化聚乙烯、改性氯磺化聚乙烯、氯磺化聚丙烯中的至少一种；
所述的分散防沉剂为Efka FA 4663、YRFC-02、FS-01、DA—50中的至少一种；
所述的抗裂剂为40-1500目玻璃纤维粉、0.05-0.5MM聚丙烯纤维、0.05-0.5MM聚乙烯纤维中的至少一种；
所述的色浆显色剂为上海银客化工热敏色浆、东莞腾达变色涂料公司热敏色浆、3,3-双(N-辛基-2-甲基吲哚)邻苯二甲内酯(红色素-16)CK-16、广州科迪油性色浆色精、苏州世名科技的油性色浆色精中的至少一种；
所述的环保抛射剂为R141B、134a、152a、HFO1234yf、HFO1234ze中的至少一种。
所述一种气雾型汽车底盘涂料的制备方法：包括以下步骤：按重量份配比，将500-2500目功能填料、纳米石墨烯、抗裂剂加热60-85度，真空脱水加入偶联剂并分散均匀，冷却常温；将复合树脂、环保溶剂、阻燃剂、200-2000目重防护抗锈剂、二元乙丙橡胶、氯磺化橡胶、分散防沉剂、色浆显色剂依次加入混合搅拌均匀浆料；按规定重量份比例分装浆料到气雾罐中，然后装上雌阀阀门并封口，用气雾剂灌封机按规定重量份配比，填充相应环保抛射剂，包装即得成品。
本发明的一种气雾型汽车底盘涂料与市场上同类产品对比的优点有：
1. 产品性能好，功能填料与纳米石墨烯补强，内聚力与粘接强度高；
2.施工方便，快干环保溶剂体系，固含量高，低VOC；
3.复合树脂与橡胶体系强化，氯磺化橡胶与乙丙橡胶补强，耐老化性能优异，可满足耐候使用需求；
4.扩展阻燃与抗锈产品性能，使用阻燃剂与重防护阻燃剂。
具体实施方式：
以下实施例对本发明进行说明，但本发明并不受这些实施例所限制。对本发明的具体实施方式进行修改或者对部分技术特征进行等同替换，而不脱离本发明方案的精神，其均应涵盖在本发明请求保护的技术方案范围当中。
实施例1
按重量份配比，将500-2500目目空心玻璃微珠3份、500-2500目珍珠岩2份、500-2500目云母粉4份、纳米石墨烯3份、40-1500目玻璃纤维粉0.5份、0.05-0.5MM聚丙烯纤维0.5份、加热60-85度，真空脱水加入KH-550硅烷偶联剂1份、KH-551硅烷偶联剂2份并分散均匀，冷却常温；将氢化SIS 5份、氢化SBS 10份、氢化柏油15份、乙二醇二醋酸酯(EGDA)10份、二元醇酯(YPC)25份、氢氧化镁2份、二苯基砜磺酸盐份3份、锌粉3份、铝粉3份、铁红粉1份、二元乙丙橡胶1份、氯磺化橡胶2份、Efka FA 4663 0.5份、YRFC-02 0.5份、上海银客化工热敏色浆2份、3,3-双(N-辛基-2-甲基吲哚)邻苯二甲内酯(红色素-16)CK-16 1份、依次加入混合搅拌均匀浆料依次加入混合搅拌均匀浆料；按规定重量份比例分装浆料到气雾罐中，然后装上雌阀阀门并封口，用气雾剂灌封机按规定重量份配比，填充R141B︰134a︰152a=2︰5:1环保抛射剂30g，包装即得成品。
实施例2
按重量份配比，空心微珠为500-2500目空心玻璃微珠2份、500-2500目云母粉2份、500-2500目硅微粉3份、纳米石墨烯4份、0.05-0.5MM聚丙烯纤维1份、加热60-85度，真空脱水加入KH-550硅烷偶联剂1份、KH-551硅烷偶联剂2份并分散均匀，冷却常温；将氢化SIS 10份、氢化SBS 6份、氢化柏油7份、二元醇酯(YPC)17份、D80溶剂油23份、二苯基砜磺酸盐2份、改性氢氧化铝份2份、锌粉2份︰铝粉3份、二元乙丙橡胶4份、氯磺化橡胶3份、YRFC-02 1份、FS-01 2份、东莞腾达变色涂料公司热敏色浆2份、广州科迪油性色浆色精1份、依次加入混合搅拌均匀浆料依次加入混合搅拌均匀浆料；按规定重量份比例分装浆料到气雾罐中，然后装上雌阀阀门并封口，用气雾剂灌封机按规定重量份配比，填充相应R141B︰134a︰HFO1234yf =3︰7:1环保抛射剂30g，包装即得成品。
实施例3
按重量份配比，空心微珠为500-2500目空心玻璃微珠2份、500-2000目中空陶瓷微粒1份， 500-2500目珍珠岩3份、500-2500目硅微粉2份、纳米石墨烯3份、40-1500目玻璃纤维粉1份、0.05-0.5MM聚丙烯纤维1份加热60-85度，真空脱水加入KH-550硅烷偶联剂1份、KH-570硅烷偶联剂2份并分散均匀，冷却常温；将氢化SIS 5份、氢化SBS 10份、氢化柏油10份、乙二醇二醋酸酯(EGDA)25份、D80溶剂油15份、十溴二苯醚1份、MCA阻燃剂3份、锌粉3份、铁红粉3份、二元乙丙橡胶2份、氯磺化橡胶4份、FS-01 0.5份、DA—50 0.5份、上海银客化工热敏色浆1.5份、苏州世名科技的油性色浆色精0.5份依次加入混合搅拌均匀浆料依次加入混合搅拌均匀浆料；按规定重量份比例分装浆料到气雾罐中，然后装上雌阀阀门并封口，用气雾剂灌封机按规定重量份配比，填充相应HFO1234yf︰HFO1234ze=1︰1环保抛射剂，包装即得成品。
实施例4
按重量份配比，500-2000目中空陶瓷微粒7份、500-2500目硅微粉1份、500-2500目石墨粉1份、纳米石墨烯1份、0.05-0.5MM聚乙烯纤维2份加热60-85度，真空脱水加入KH-550硅烷偶联剂1份、KH-560硅烷偶联剂2份并分散均匀，冷却常温；将氢化SIS 15份、氢化SBS 3份、氢化柏油5份、乙二醇二醋酸酯(EGDA)17份、二元醇酯(YPC)18份、D80溶剂油5份、二苯基砜磺酸盐3份、MCA阻燃剂2份、锌粉2份、铝粉3份、铁红粉2份、二元乙丙橡胶2.5份、氯磺化橡胶4.5份、Efka FA 4663 1份、FS-01 1份、东莞腾达变色涂料公司热敏色浆0.7、苏州世名科技的油性色浆色精0.3份依次加入混合搅拌均匀浆料依次加入混合搅拌均匀浆料；按规定重量份比例分装浆料到气雾罐中，然后装上雌阀阀门并封口，用气雾剂灌封机按规定重量份配比，填充相应R141B环保抛射剂30g，包装即得成品。
表1气雾型汽车底盘涂料主要性能测试结果：
Figure DEST_PATH_IMAGE001
由测试结果可见，本发明一种气雾型汽车底盘涂料产品性能优良，具有干燥速度快、耐候性好等特点。

Claims (12)

1.一种底盘装甲涂料，其特征在于，其主要成分按照重量份配比包括：
复合树脂 22-45
环保溶剂 35-55
500-2500目功能填料 7-16
纳米石墨烯 1-7
阻燃剂 4-15
偶联剂 1-3
200-2000目重防护抗锈剂 5-12
二元乙丙橡胶 1-5
氯磺化橡胶 1-7
分散防沉剂 0.7-5
抗裂剂 1-6
色浆显色剂 0.6-7
环保抛射剂 12～35；
所述的复合树脂为氢化SIS：氢化SBS：氢化柏油=0-9︰2-7︰1-8；
所述的环保抛射剂为R141B、134a、152a、HFO1234yf、HFO1234ze中的至少一种。
2.如权利要求1所述的一种底盘装甲涂料，其特征在于，所述的环保溶剂为乙二醇二醋酸酯、二元醇酯、D80溶剂油中的至少一种。
3.如权利要求1所述的一种底盘装甲涂料，其特征在于，所述的500-2500目功能填料为空心微珠︰矿物粉=1-9︰2-7。
4.如权利要求3所述的一种底盘装甲涂料，其特征在于，所述的空心微珠为500-2500目空心玻璃微珠、500-2000目中空陶瓷微粒中的至少一种。
5.如权利要求3所述的一种底盘装甲涂料，其特征在于，所述的矿物粉为500-2500目珍珠岩、500-2500目云母粉、500-2500目硅微粉、500-2500目石墨粉中的至少一种。
6.如权利要求1所述的一种底盘装甲涂料，其特征在于，所述的阻燃剂为氢氧化镁、二苯基砜磺酸盐、改性氢氧化铝、十溴二苯醚、MCA阻燃剂中的至少一种。
7.如权利要求1所述的一种底盘装甲涂料，其特征在于，所述的偶联剂为KH-550硅烷偶联剂、KH-551硅烷偶联剂、KH-560硅烷偶联剂、KH-570硅烷偶联剂中的至少一种。
8.如权利要求1所述的一种底盘装甲涂料，其特征在于，所述的200-2000目重防护抗锈剂为锌粉︰铝粉︰铁红粉=1-10︰0-7︰0-6。
9.如权利要求1所述的一种底盘装甲涂料，其特征在于，所述的氯磺化橡胶为氯磺化聚乙烯、改性氯磺化聚乙烯、氯磺化聚丙烯中的至少一种。
10. 如权利要求1所述的一种底盘装甲涂料，其特征在于，所述的分散防沉剂为EfkaFA4663、YRFC-02、FS-01、DA—50中的至少一种。
11.如权利要求1所述的一种底盘装甲涂料，其特征在于，所述的色浆显色剂为上海银客化工热敏色浆、东莞腾达变色涂料公司热敏色浆、3,3-双(N-辛基-2-甲基吲哚)邻苯二甲内酯、广州科迪油性色浆色精、苏州世名科技的油性色浆色精中的至少一种。
12.如权利要求1所述的一种底盘装甲涂料，其特征在于，所述底盘装甲涂料的制备方法包括以下步骤：按重量份配比，将500-2500目功能填料、纳米石墨烯、抗裂剂加热60-85度，真空脱水加入偶联剂并分散均匀，冷却常温；将复合树脂、环保溶剂、阻燃剂、200-2000目重防护抗锈剂、二元乙丙橡胶、氯磺化橡胶、分散防沉剂、色浆显色剂依次加入混合搅拌均匀浆料；按规定重量份比例分装浆料到气雾罐中，然后装上雌阀阀门并封口，用气雾剂灌封机按规定重量份配比，填充相应环保抛射剂，包装即得成品。
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