CN112915057A - Compound coptis chinensis Chinese herbal medicine toothpaste and preparation method thereof - Google Patents
Compound coptis chinensis Chinese herbal medicine toothpaste and preparation method thereof Download PDFInfo
- Publication number
- CN112915057A CN112915057A CN202011242884.3A CN202011242884A CN112915057A CN 112915057 A CN112915057 A CN 112915057A CN 202011242884 A CN202011242884 A CN 202011242884A CN 112915057 A CN112915057 A CN 112915057A
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- China
- Prior art keywords
- paste
- extract
- total weight
- accounts
- decocting
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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- 239000000606 toothpaste Substances 0.000 title claims abstract description 96
- 229940034610 toothpaste Drugs 0.000 title claims abstract description 96
- 150000001875 compounds Chemical class 0.000 title claims abstract description 15
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- 241000411851 herbal medicine Species 0.000 title claims abstract description 12
- 241000037740 Coptis chinensis Species 0.000 title claims description 19
- 239000000284 extract Substances 0.000 claims abstract description 68
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 67
- 241001598107 Imperata Species 0.000 claims abstract description 25
- ZFXYFBGIUFBOJW-UHFFFAOYSA-N theophylline Chemical compound O=C1N(C)C(=O)N(C)C2=C1NC=N2 ZFXYFBGIUFBOJW-UHFFFAOYSA-N 0.000 claims abstract description 24
- 241000205585 Aquilegia canadensis Species 0.000 claims abstract description 19
- 235000007516 Chrysanthemum Nutrition 0.000 claims abstract description 19
- 240000000691 Houttuynia cordata Species 0.000 claims abstract description 19
- 241000123069 Ocyurus chrysurus Species 0.000 claims abstract description 19
- 235000005187 Taraxacum officinale ssp. officinale Nutrition 0.000 claims abstract description 18
- 235000013719 Houttuynia cordata Nutrition 0.000 claims abstract description 17
- 235000006679 Mentha X verticillata Nutrition 0.000 claims abstract description 17
- 235000002899 Mentha suaveolens Nutrition 0.000 claims abstract description 17
- 235000001636 Mentha x rotundifolia Nutrition 0.000 claims abstract description 17
- LRCFXGAMWKDGLA-UHFFFAOYSA-N dioxosilane;hydrate Chemical compound O.O=[Si]=O LRCFXGAMWKDGLA-UHFFFAOYSA-N 0.000 claims abstract description 13
- 229960004029 silicic acid Drugs 0.000 claims abstract description 13
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 claims abstract description 13
- 235000010234 sodium benzoate Nutrition 0.000 claims abstract description 13
- 239000004299 sodium benzoate Substances 0.000 claims abstract description 13
- FQENQNTWSFEDLI-UHFFFAOYSA-J sodium diphosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])([O-])=O FQENQNTWSFEDLI-UHFFFAOYSA-J 0.000 claims abstract description 13
- 235000019818 tetrasodium diphosphate Nutrition 0.000 claims abstract description 13
- PFTAWBLQPZVEMU-DZGCQCFKSA-N (+)-catechin Chemical compound C1([C@H]2OC3=CC(O)=CC(O)=C3C[C@@H]2O)=CC=C(O)C(O)=C1 PFTAWBLQPZVEMU-DZGCQCFKSA-N 0.000 claims abstract description 12
- 244000269722 Thea sinensis Species 0.000 claims abstract description 12
- ADRVNXBAWSRFAJ-UHFFFAOYSA-N catechin Natural products OC1Cc2cc(O)cc(O)c2OC1c3ccc(O)c(O)c3 ADRVNXBAWSRFAJ-UHFFFAOYSA-N 0.000 claims abstract description 12
- 235000005487 catechin Nutrition 0.000 claims abstract description 12
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- 239000008367 deionised water Substances 0.000 claims abstract description 12
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 12
- 150000008442 polyphenolic compounds Chemical class 0.000 claims abstract description 12
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- 229960000278 theophylline Drugs 0.000 claims abstract description 12
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims abstract description 11
- 235000019333 sodium laurylsulphate Nutrition 0.000 claims abstract description 11
- FTLYMKDSHNWQKD-UHFFFAOYSA-N (2,4,5-trichlorophenyl)boronic acid Chemical compound OB(O)C1=CC(Cl)=C(Cl)C=C1Cl FTLYMKDSHNWQKD-UHFFFAOYSA-N 0.000 claims abstract description 10
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims abstract description 10
- 239000001768 carboxy methyl cellulose Substances 0.000 claims abstract description 10
- 235000010948 carboxy methyl cellulose Nutrition 0.000 claims abstract description 10
- 229940085605 saccharin sodium Drugs 0.000 claims abstract description 10
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- 244000025254 Cannabis sativa Species 0.000 claims abstract description 8
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 claims abstract description 7
- 239000000686 essence Substances 0.000 claims abstract description 7
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims abstract description 4
- 239000011575 calcium Substances 0.000 claims abstract description 4
- 229910052791 calcium Inorganic materials 0.000 claims abstract description 4
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- 241000628997 Flos Species 0.000 claims description 12
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 claims description 10
- 239000000600 sorbitol Substances 0.000 claims description 10
- FUFJGUQYACFECW-UHFFFAOYSA-L calcium hydrogenphosphate Chemical compound [Ca+2].OP([O-])([O-])=O FUFJGUQYACFECW-UHFFFAOYSA-L 0.000 claims description 9
- 235000019700 dicalcium phosphate Nutrition 0.000 claims description 9
- 238000002156 mixing Methods 0.000 claims description 8
- 239000009513 Coptidis rhizoma extract Substances 0.000 claims description 7
- 238000011049 filling Methods 0.000 claims description 7
- UAJTZZNRJCKXJN-UHFFFAOYSA-M sodium;2-dodecoxy-2-oxoethanesulfonate Chemical compound [Na+].CCCCCCCCCCCCOC(=O)CS([O-])(=O)=O UAJTZZNRJCKXJN-UHFFFAOYSA-M 0.000 claims description 6
- 239000000463 material Substances 0.000 claims description 5
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- 239000004698 Polyethylene Substances 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 238000004806 packaging method and process Methods 0.000 claims description 3
- -1 polyethylene Polymers 0.000 claims description 3
- 229920000573 polyethylene Polymers 0.000 claims description 3
- CVHZOJJKTDOEJC-UHFFFAOYSA-N saccharin Chemical compound C1=CC=C2C(=O)NS(=O)(=O)C2=C1 CVHZOJJKTDOEJC-UHFFFAOYSA-N 0.000 claims description 3
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- 229940005608 hypericin Drugs 0.000 description 3
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Classifications
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Abstract
The invention provides compound coptis Chinese herbal medicine toothpaste and a preparation method thereof, wherein the compound coptis Chinese herbal medicine toothpaste comprises coptis cream, scutellaria cream, madder cream, houttuynia cordata cream, dandelion cream, honeysuckle cream, chrysanthemum cream, cogongrass rhizome cream, mint cream, catechin, theophylline, tea polyphenol, sorbitol (glucitol), deionized water, polydiethanol-8, sodium lauryl sulfate, edible essence, xanthan gum, cellulose gum, calcium hydrophosphate, hydrated silica, tetrasodium pyrophosphate, sodium benzoate and saccharin sodium. The compound coptis Chinese herbal medicine toothpaste and the preparation method thereof further enable the toothpaste to have the effects of clearing heat, removing toxicity and diminishing inflammation through the mutual matching of coptis extract, scutellaria extract, madder extract, houttuynia extract, dandelion extract, honeysuckle extract, chrysanthemum extract, lalang grass rhizome extract, mint extract, catechin, theophylline and tea polyphenol.
Description
Technical Field
The invention mainly relates to the technical field of toothpaste preparation, in particular to compound coptis chinensis Chinese herbal medicine toothpaste and a preparation method thereof.
Background
Toothpaste is a cleaning product commonly used in daily life, is a dentifrice, is usually smeared on a toothbrush, is used for cleaning teeth and keeping the teeth beautiful and bright, and has a long history, such as patent certificates with the following numbers: CN201711032407.2 patent, a method for preparing hypericin medicinal toothpaste, according to the weight portion, 10-20 portions of glycerin, 5-11 portions of sorbitol and 7-12 portions of deionized water are firstly stirred to be uniform; adding 1.5-3 parts of the medicinal extract, and stirring uniformly; and then respectively adding 40-50 parts of calcium carbonate, 10-20 parts of silicon dioxide and 2-3 parts of sodium dodecyl sulfate, stirring for 30 minutes, homogenizing and emulsifying for 10-20 minutes, and filling. The preparation method of the medicine extract comprises the following steps: taking the eucommia ulmoides leaves and the ardisia crenata sims according to the proportion of 3-27 parts of the eucommia ulmoides leaves and 4-20 parts of the ardisia crenata sims, adding 12 times of water, decocting for 3 times, 0.5h each time, combining decoction, and concentrating to obtain an extract with the relative density of 1.20-1.30 at the temperature of 45-55 ℃, thus obtaining a medicinal extract; the preparation method of the medicine solution comprises the following steps: 1-5 parts of hypericin is added into deionized water and 1-2 parts of hypericin is dissolved to obtain a medicine solution. Although the toothpaste has antibacterial function, it has poor anti-inflammatory effect.
Disclosure of Invention
The invention mainly provides compound coptis chinensis Chinese herbal medicine toothpaste and a preparation method thereof, which are used for solving the technical problems in the background technology.
The technical scheme adopted by the invention for solving the technical problems is as follows:
a compound Coptidis rhizoma Chinese herbal toothpaste comprises Coptidis rhizoma extract, Scutellariae radix extract, radix Rubiae extract, herba Houttuyniae extract, herba Taraxaci extract, flos Lonicerae extract, flos Chrysanthemi extract, lalang grass rhizome extract, herba Menthae extract, catechin, theophylline, tea polyphenols, sorbitol, deionized water, polydiethanol-8, sodium lauryl sulfate, edible essence, xanthan gum, cellulose gum, calcium hydrogen phosphate, hydrated silica, tetrasodium pyrophosphate, sodium benzoate, and saccharin sodium;
the usage of the coptis root paste accounts for 20-40% of the total weight of the toothpaste body;
the use of the scutellaria baicalensis paste accounts for 6-12% of the total weight of the toothpaste body;
the madder paste accounts for 4-8% of the total weight of the toothpaste body;
the houttuynia cordata paste accounts for 3% -6% of the total weight of the toothpaste body;
the dandelion paste accounts for 3% -6% of the total weight of the toothpaste body;
the honeysuckle paste accounts for 3-6% of the total weight of the toothpaste body;
the chrysanthemum paste accounts for 3-6% of the total weight of the toothpaste body;
the cogongrass rhizome paste accounts for 3-6% of the total weight of the toothpaste body;
the mint paste accounts for 3-6% of the total weight of the toothpaste body;
the catechin accounts for 0.8-1.4% of the total weight of the toothpaste body;
the usage of the theophylline accounts for 0.6 to 1.2 percent of the total weight of the toothpaste body;
the use of the tea polyphenol accounts for 0.6 to 1.2 percent of the total weight of the toothpaste body;
the sorbitol accounts for 2 to 5 percent of the total weight of the toothpaste body;
the deionized water accounts for 8-16% of the total weight of the toothpaste body;
the use of the polydiethylene glycol-8 accounts for 4-8% of the total weight of the toothpaste body;
the sodium lauryl sulfate accounts for 2-6% of the total weight of the toothpaste body;
the edible essence accounts for 0.4-1% of the total weight of the toothpaste body;
the use of the xanthan gum accounts for 5 to 10 percent of the total weight of the toothpaste body;
the use of the cellulose gum accounts for 3-6% of the total weight of the toothpaste body;
the calcium hydrophosphate is used in an amount which is 10 to 20 percent of the total weight of the toothpaste body;
the hydrated silica accounts for 7 to 12 percent of the total weight of the toothpaste body;
the tetrasodium pyrophosphate is used in an amount of 5-10% of the total weight of the toothpaste body;
the sodium benzoate accounts for 3-6% of the total weight of the toothpaste body;
the saccharin sodium accounts for 0.6-1% of the total weight of the toothpaste body.
Further, the calcium hydrogen phosphate, hydrated silica, tetrasodium pyrophosphate, sodium benzoate and sodium saccharin are ground by a grinder and sieved with 20000-and 30000-mesh sieve.
A preparation method of compound coptis chinensis Chinese herbal medicine toothpaste comprises the following steps:
1) preparing coptis chinensis paste, scutellaria baicalensis paste, madder paste, houttuynia cordata paste, dandelion paste, honeysuckle paste, chrysanthemum paste, cogongrass rhizome paste and mint paste:
rinsing and soaking the coptis chinensis, adding 4-8 times of water, decocting for 2-4 hours, filtering, adding 1-2 times of water into the decocted coptis chinensis again, decocting for 1-2 hours, filtering, combining the two filtrates, performing pressure filtration by using a 1000-plus 3000-mesh filter press, refluxing for 2-4 times at the temperature of 92-100 ℃, keeping the filtrate, and concentrating the filtrate into paste by using a jacketed kettle, thus obtaining the coptis chinensis paste;
rinsing and soaking scutellaria baicalensis, adding 4-8 times of water, decocting for 2-4 hours, filtering, adding 1-2 times of water into the decocted scutellaria baicalensis again, decocting for 1-2 hours, filtering, combining two filtrates, performing pressure filtration by using a 1000-plus 3000-mesh filter press, refluxing for 2-4 times at the temperature of 92-100 ℃, keeping the filtrate, and concentrating the filtrate into paste by using a jacketed kettle, namely the scutellaria baicalensis paste;
rinsing and soaking madder, adding 4-8 times of water, decocting for 2-4 hours, filtering, adding 1-2 times of water into the decocted madder again, decocting for 1-2 hours, filtering, combining two filtrates, performing pressure filtration by using a 1000-plus 3000-mesh filter press, refluxing for 2-4 times at 92-100 ℃, reserving the filtrate, and concentrating the filtrate into paste by using a jacketed kettle, namely the madder paste;
rinsing and soaking the houttuynia cordata, adding 4-8 times of water, decocting for 2-4 hours, filtering, adding 1-2 times of water into the decocted houttuynia cordata again, decocting for 1-2 hours, filtering, combining the two filtrates, performing pressure filtration by using a 1000-plus 3000-mesh filter press, refluxing for 2-4 times at the temperature of 92-100 ℃, keeping the filtrate, and concentrating the filtrate into paste by using a jacketed kettle, namely the houttuynia cordata paste;
rinsing and soaking the dandelion, adding 4-8 times of water, decocting for 2-4 hours, filtering, adding 1-2 times of water into the decocted dandelion again, decocting for 1-2 hours, filtering, combining the two filtrates, performing pressure filtration by using a 1000-plus 3000-mesh filter press, refluxing for 2-4 times at the temperature of 92-100 ℃, keeping the filtrate, and concentrating the filtrate into paste by using a jacketed kettle, thus obtaining the dandelion paste;
rinsing and soaking the honeysuckle, adding 4-8 times of water, decocting for 2-4 hours, filtering, adding 1-2 times of water into the decocted honeysuckle again, decocting for 1-2 hours, filtering, combining the two filtrates, performing pressure filtration by using a 1000-plus 3000-mesh filter press, refluxing for 2-4 times at 92-100 ℃, keeping the filtrate, and concentrating the filtrate into paste by using a jacketed kettle, namely the honeysuckle paste;
rinsing and soaking chrysanthemum, adding 4-8 times of water, decocting for 2-4 hours, filtering, adding 1-2 times of water into the decocted chrysanthemum again, decocting for 1-2 hours, filtering, combining the two filtrates, performing pressure filtration by using a 1000-plus 3000-mesh filter press, refluxing for 2-4 times at the temperature of 92-100 ℃, keeping the filtrate, and concentrating the filtrate into paste by using a jacketed kettle, namely the chrysanthemum paste;
rinsing and soaking the cogongrass rhizome, adding 4-8 times of water, decocting for 2-4 hours, filtering, adding 1-2 times of water into the decocted cogongrass rhizome again, decocting for 1-2 hours, filtering, combining the two filtrates, performing pressure filtration by using a 1000-plus 3000-mesh filter press, refluxing for 2-4 times at the temperature of 92-100 ℃, keeping the filtrate, and concentrating the filtrate into paste by using a jacketed kettle, namely cogongrass rhizome paste;
rinsing and soaking mint, adding 4-8 times of water, decocting for 2-4 hours, filtering, adding 1-2 times of water into the decocted mint again, decocting for 1-2 hours, filtering, combining two filtrates, performing pressure filtration by using a 1000-plus 3000-mesh filter press, refluxing for 2-4 times at 92-100 ℃, keeping the filtrate, and concentrating the filtrate into paste by using a jacketed kettle to obtain the mint paste;
2) and mixing materials:
mixing Coptidis rhizoma extract, Scutellariae radix extract, radix Rubiae extract, herba Houttuyniae extract, herba Taraxaci extract, flos Lonicerae extract, flos Chrysanthemi extract, lalang grass rhizome extract, herba Menthae extract, catechin, theophylline, tea polyphenols, sorbitol, deionized water, polyethylene glycol-8, sodium lauryl sulfate, edible essence, xanthan gum, cellulose gum and ground calcium hydrogen phosphate, hydrated silica, tetrasodium pyrophosphate, sodium benzoate, and saccharin sodium at a certain ratio to obtain paste;
3) and packaging:
and sterilizing and cooling the dry paste by a sterilizer, and filling by a full-automatic toothpaste filling machine.
The raw materials used in the invention have the following effects:
coptis chinensis: has the effects of clearing heat, eliminating dampness, purging pathogenic fire and removing toxic substances. Can be used for treating damp-heat distention and fullness, emesis, acid regurgitation, dysentery, hyperpyrexia, coma, vexation, insomnia, hematemesis, epistaxis, carbuncle, furuncle, conjunctival congestion, toothache, diabetes, eczema, and suppuration of ear canal.
Scutellaria baicalensis: clear heat and dry dampness, purge fire and remove toxicity, stop bleeding, prevent abortion.
Madder root: it is mainly used for treating hemorrhage due to recklessly blood flow due to blood heat, amenorrhea due to blood stasis, traumatic injury, and rheumatalgia.
Houttuynia cordata: clearing away heat and toxic material, curing abscess and discharging pus, inducing diuresis and treating stranguria.
Dandelion: the dandelion is cold in nature and bitter in taste, has the effects of clearing away heat and toxic materials, and inducing diuresis to reduce edema, and has the effects of regulating the stomach and liver.
Honeysuckle flower: clear heat and remove toxicity, disperse wind-heat.
Chrysanthemum: disperse wind-heat, calm liver yang, clear liver heat and improve vision, clear heat and remove toxicity.
Cogongrass rhizome: it is mainly used for treating hemorrhage due to blood heat, epistaxis, hemoptysis, hematuria, stranguria with blood, stranguria due to toxic heat, edema, jaundice due to damp-heat, emesis due to stomach heat, and cough and asthma due to lung heat.
Mint: disperse wind-heat, clear heat and improve eyesight, relieve sore throat and promote eruption, sooth liver and move qi.
Compared with the prior art, the invention has the beneficial effects that:
the compound coptis Chinese herbal medicine toothpaste and the preparation method thereof further enable the toothpaste to have the effects of clearing heat, removing toxicity and diminishing inflammation through the mutual matching of coptis extract, scutellaria extract, madder extract, houttuynia extract, dandelion extract, honeysuckle extract, chrysanthemum extract, lalang grass rhizome extract, mint extract, catechin, theophylline and tea polyphenol.
Detailed Description
The technical solutions in the embodiments of the present invention are clearly and completely described below with reference to specific embodiments, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, rather than all embodiments, and all other embodiments obtained by those skilled in the art without any creative work based on the embodiments of the present invention belong to the protection scope of the present invention.
Example 1
A compound Coptidis rhizoma Chinese herbal toothpaste comprises Coptidis rhizoma extract, Scutellariae radix extract, radix Rubiae extract, herba Houttuyniae extract, herba Taraxaci extract, flos Lonicerae extract, flos Chrysanthemi extract, lalang grass rhizome extract, herba Menthae extract, catechin, theophylline, tea polyphenols, sorbitol, deionized water, polydiethanol-8, sodium lauryl sulfate, edible essence, xanthan gum, cellulose gum, calcium hydrogen phosphate, hydrated silica, tetrasodium pyrophosphate, sodium benzoate, and saccharin sodium;
the usage of the coptis chinensis paste accounts for 20 percent of the total weight of the toothpaste body;
the use of the scutellaria baicalensis paste accounts for 6 percent of the total weight of the toothpaste body;
the madder paste accounts for 4% of the total weight of the toothpaste body;
the houttuynia cordata paste accounts for 3% of the total weight of the toothpaste body;
the dandelion paste accounts for 3% of the total weight of the toothpaste body;
the honeysuckle paste accounts for 3% of the total weight of the toothpaste body;
the chrysanthemum paste accounts for 3% of the total weight of the toothpaste body;
the cogongrass rhizome paste accounts for 3% of the total weight of the toothpaste body;
the mint paste accounts for 3% of the total weight of the toothpaste body;
the catechin accounts for 0.8% of the total weight of the toothpaste body;
the usage of the theophylline accounts for 0.6 percent of the total weight of the toothpaste body;
the usage of the tea polyphenol accounts for 0.6 percent of the total weight of the toothpaste body;
the sorbitol accounts for 2% of the total weight of the toothpaste body;
the deionized water accounts for 8% of the total weight of the toothpaste body;
the use of the polydiethylene glycol-8 accounts for 4% of the total weight of the toothpaste body;
the sodium lauryl sulfate accounts for 2% of the total weight of the toothpaste body;
the edible essence accounts for 0.4 percent of the total weight of the toothpaste body;
the use of the xanthan gum accounts for 5% of the total weight of the toothpaste body;
the use of the cellulose gum accounts for 3 percent of the total weight of the toothpaste body;
the calcium hydrophosphate is used in an amount which is 10 percent of the total weight of the toothpaste body;
the hydrated silica is used for 7 percent of the total weight of the toothpaste body;
the use of the tetrasodium pyrophosphate accounts for 5 percent of the total weight of the toothpaste body;
the sodium benzoate accounts for 3% of the total weight of the toothpaste body;
the saccharin sodium accounts for 0.6% of the total weight of the toothpaste body.
The dibasic calcium phosphate, hydrated silica, tetrasodium pyrophosphate, sodium benzoate and sodium saccharin were milled through a mill and sieved through a 25000 mesh sieve.
A preparation method of compound coptis chinensis Chinese herbal medicine toothpaste comprises the following steps:
1) preparing coptis chinensis paste, scutellaria baicalensis paste, madder paste, houttuynia cordata paste, dandelion paste, honeysuckle paste, chrysanthemum paste, cogongrass rhizome paste and mint paste:
rinsing Coptidis rhizoma, soaking, adding 4 times of water, decocting for 2 hr, filtering, adding 1 time of water again, decocting for 1 hr, filtering, mixing filtrates, press-filtering with 3000 mesh filter press, refluxing at 92 deg.C for 2 times, retaining filtrate, and concentrating the filtrate to paste with jacketed pan to obtain Coptidis rhizoma extract;
rinsing Scutellariae radix, soaking, adding 4 times of water, decocting for 2 hr, filtering, adding 1 time of water to the decocted Scutellariae radix, decocting for 1 hr, filtering, mixing filtrates, press-filtering with 3000 mesh filter press, refluxing at 92 deg.C for 2 times, retaining filtrate, and concentrating the filtrate to paste with jacketed pan to obtain Scutellariae radix extract;
rinsing and soaking madder, adding 4 times of water, decocting for 2 hours, filtering, adding 1 time of water into the decocted madder again, decocting for 1 hour, filtering, combining two filtrates, performing pressure filtration by using a 3000-mesh pressure filter, refluxing for 2 times at the temperature of 92 ℃, keeping the filtrate, and concentrating the filtrate into paste by using a jacketed kettle, namely the madder paste;
rinsing and soaking the houttuynia cordata, adding 4 times of water, decocting for 2 hours, filtering, adding 1 time of water into the decocted houttuynia cordata again, decocting for 1 hour, filtering, combining the two filtrates, performing filter pressing by using a 3000-mesh filter press, refluxing for 2 times at 92 ℃, keeping the filtrate, and concentrating the filtrate into paste by using a jacketed kettle, thus obtaining the houttuynia cordata paste;
rinsing and soaking the dandelion, adding 4 times of water, decocting for 2 hours, filtering, adding 1 time of water into the decocted dandelion again, decocting for 1 hour, filtering, combining the two filtrates, performing filter pressing by using a 3000-mesh filter press, refluxing for 2 times at 92 ℃, keeping the filtrate, and concentrating the filtrate into paste by using a jacketed kettle, thus obtaining the dandelion paste;
rinsing and soaking honeysuckle, adding 4 times of water, decocting for 2 hours, filtering, adding 1 time of water into the decocted honeysuckle again, decocting for 1 hour, filtering, combining the two filtrates, performing pressure filtration by using a 3000-mesh pressure filter, refluxing for 2 times at 92 ℃, keeping the filtrate, and concentrating the filtrate into paste by using a jacketed kettle, thus obtaining the honeysuckle extract;
rinsing and soaking chrysanthemum, adding 4 times of water, decocting for 2 hours, filtering, adding 1 time of water into the decocted chrysanthemum again, decocting for 1 hour, filtering, combining the two filtrates, performing pressure filtration by using a 3000-mesh pressure filter, refluxing for 2 times at 92 ℃, keeping the filtrate, and concentrating the filtrate into paste by using a jacketed kettle, thus obtaining chrysanthemum paste;
rinsing and soaking the cogongrass rhizome, adding 4 times of water, decocting for 2 hours, filtering, adding 1 time of water into the decocted cogongrass rhizome again, decocting for 1 hour, filtering, combining the two filtrates, performing pressure filtration by using a 3000-mesh pressure filter, refluxing for 2 times at the temperature of 92 ℃, keeping the filtrate, and concentrating the filtrate into paste by using a jacketed kettle to obtain cogongrass rhizome paste;
rinsing and soaking mint, adding 4 times of water, decocting for 2 hours, filtering, adding 1 time of water into the decocted mint again, decocting for 1 hour, filtering, combining two filtrates, performing pressure filtration by using a 3000-mesh pressure filter, refluxing for 2 times at 92 ℃, keeping the filtrate, and concentrating the filtrate into paste by using a jacketed kettle, thus obtaining the mint paste;
2) and mixing materials:
mixing Coptidis rhizoma extract, Scutellariae radix extract, radix Rubiae extract, herba Houttuyniae extract, herba Taraxaci extract, flos Lonicerae extract, flos Chrysanthemi extract, lalang grass rhizome extract, herba Menthae extract, catechin, theophylline, tea polyphenols, sorbitol, deionized water, polyethylene glycol-8, sodium lauryl sulfate, edible essence, xanthan gum, cellulose gum and ground calcium hydrogen phosphate, hydrated silica, tetrasodium pyrophosphate, sodium benzoate, and saccharin sodium at a certain ratio to obtain paste;
3) and packaging:
and sterilizing and cooling the dry paste by a sterilizer, and filling by a full-automatic toothpaste filling machine.
It will be evident to those skilled in the art that the invention is not limited to the details of the foregoing illustrative embodiments, and that the present invention may be embodied in other specific forms without departing from the spirit or essential attributes thereof, and it is therefore intended that the present embodiments be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein.
Furthermore, it should be understood that although the present description refers to embodiments, not every embodiment may contain only a single embodiment, and such description is for clarity only, and those skilled in the art should integrate the description, and the embodiments may be combined as appropriate to form other embodiments understood by those skilled in the art.
Claims (3)
1. A compound Coptidis rhizoma Chinese herbal toothpaste is characterized by comprising Coptidis rhizoma extract, Scutellariae radix extract, radix Rubiae extract, herba Houttuyniae extract, herba Taraxaci extract, flos Lonicerae extract, flos Chrysanthemi extract, lalang grass rhizome extract, herba Menthae extract, catechin, theophylline, tea polyphenols, sorbitol, deionized water, polydiethanol-8, sodium lauryl sulfate, edible essence, xanthan gum, cellulose gum, calcium hydrogen phosphate, hydrated silica, tetrasodium pyrophosphate, sodium benzoate, and saccharin sodium;
the usage of the coptis root paste accounts for 20-40% of the total weight of the toothpaste body;
the use of the scutellaria baicalensis paste accounts for 6-12% of the total weight of the toothpaste body;
the madder paste accounts for 4-8% of the total weight of the toothpaste body;
the houttuynia cordata paste accounts for 3% -6% of the total weight of the toothpaste body;
the dandelion paste accounts for 3% -6% of the total weight of the toothpaste body;
the honeysuckle paste accounts for 3-6% of the total weight of the toothpaste body;
the chrysanthemum paste accounts for 3-6% of the total weight of the toothpaste body;
the cogongrass rhizome paste accounts for 3-6% of the total weight of the toothpaste body;
the mint paste accounts for 3-6% of the total weight of the toothpaste body;
the catechin accounts for 0.8-1.4% of the total weight of the toothpaste body;
the usage of the theophylline accounts for 0.6 to 1.2 percent of the total weight of the toothpaste body;
the use of the tea polyphenol accounts for 0.6 to 1.2 percent of the total weight of the toothpaste body;
the sorbitol accounts for 2 to 5 percent of the total weight of the toothpaste body;
the deionized water accounts for 8-16% of the total weight of the toothpaste body;
the use of the polydiethylene glycol-8 accounts for 4-8% of the total weight of the toothpaste body;
the sodium lauryl sulfate accounts for 2-6% of the total weight of the toothpaste body;
the edible essence accounts for 0.4-1% of the total weight of the toothpaste body;
the use of the xanthan gum accounts for 5 to 10 percent of the total weight of the toothpaste body;
the use of the cellulose gum accounts for 3-6% of the total weight of the toothpaste body;
the calcium hydrophosphate is used in an amount which is 10 to 20 percent of the total weight of the toothpaste body;
the hydrated silica accounts for 7 to 12 percent of the total weight of the toothpaste body;
the tetrasodium pyrophosphate is used in an amount of 5-10% of the total weight of the toothpaste body;
the sodium benzoate accounts for 3-6% of the total weight of the toothpaste body;
the saccharin sodium accounts for 0.6-1% of the total weight of the toothpaste body.
2. The compound coptis chinensis Chinese herbal medicine toothpaste as claimed in claim 1, wherein the calcium hydrogen phosphate, the hydrated silica, the tetrasodium pyrophosphate, the sodium benzoate and the sodium saccharin are ground by a grinder and sieved by 20000-30000 mesh sieve.
3. The preparation method of the compound coptis chinensis Chinese herbal medicine toothpaste is characterized by comprising the following steps:
1) preparing coptis chinensis paste, scutellaria baicalensis paste, madder paste, houttuynia cordata paste, dandelion paste, honeysuckle paste, chrysanthemum paste, cogongrass rhizome paste and mint paste:
rinsing and soaking the coptis chinensis, adding 4-8 times of water, decocting for 2-4 hours, filtering, adding 1-2 times of water into the decocted coptis chinensis again, decocting for 1-2 hours, filtering, combining the two filtrates, performing pressure filtration by using a 1000-plus 3000-mesh filter press, refluxing for 2-4 times at the temperature of 92-100 ℃, keeping the filtrate, and concentrating the filtrate into paste by using a jacketed kettle, thus obtaining the coptis chinensis paste;
rinsing and soaking scutellaria baicalensis, adding 4-8 times of water, decocting for 2-4 hours, filtering, adding 1-2 times of water into the decocted scutellaria baicalensis again, decocting for 1-2 hours, filtering, combining two filtrates, performing pressure filtration by using a 1000-plus 3000-mesh filter press, refluxing for 2-4 times at the temperature of 92-100 ℃, keeping the filtrate, and concentrating the filtrate into paste by using a jacketed kettle, namely the scutellaria baicalensis paste;
rinsing and soaking madder, adding 4-8 times of water, decocting for 2-4 hours, filtering, adding 1-2 times of water into the decocted madder again, decocting for 1-2 hours, filtering, combining two filtrates, performing pressure filtration by using a 1000-plus 3000-mesh filter press, refluxing for 2-4 times at 92-100 ℃, reserving the filtrate, and concentrating the filtrate into paste by using a jacketed kettle, namely the madder paste;
rinsing and soaking the houttuynia cordata, adding 4-8 times of water, decocting for 2-4 hours, filtering, adding 1-2 times of water into the decocted houttuynia cordata again, decocting for 1-2 hours, filtering, combining the two filtrates, performing pressure filtration by using a 1000-plus 3000-mesh filter press, refluxing for 2-4 times at the temperature of 92-100 ℃, keeping the filtrate, and concentrating the filtrate into paste by using a jacketed kettle, namely the houttuynia cordata paste;
rinsing and soaking the dandelion, adding 4-8 times of water, decocting for 2-4 hours, filtering, adding 1-2 times of water into the decocted dandelion again, decocting for 1-2 hours, filtering, combining the two filtrates, performing pressure filtration by using a 1000-plus 3000-mesh filter press, refluxing for 2-4 times at the temperature of 92-100 ℃, keeping the filtrate, and concentrating the filtrate into paste by using a jacketed kettle, thus obtaining the dandelion paste;
rinsing and soaking the honeysuckle, adding 4-8 times of water, decocting for 2-4 hours, filtering, adding 1-2 times of water into the decocted honeysuckle again, decocting for 1-2 hours, filtering, combining the two filtrates, performing pressure filtration by using a 1000-plus 3000-mesh filter press, refluxing for 2-4 times at 92-100 ℃, keeping the filtrate, and concentrating the filtrate into paste by using a jacketed kettle, namely the honeysuckle paste;
rinsing and soaking chrysanthemum, adding 4-8 times of water, decocting for 2-4 hours, filtering, adding 1-2 times of water into the decocted chrysanthemum again, decocting for 1-2 hours, filtering, combining the two filtrates, performing pressure filtration by using a 1000-plus 3000-mesh filter press, refluxing for 2-4 times at the temperature of 92-100 ℃, keeping the filtrate, and concentrating the filtrate into paste by using a jacketed kettle, namely the chrysanthemum paste;
rinsing and soaking the cogongrass rhizome, adding 4-8 times of water, decocting for 2-4 hours, filtering, adding 1-2 times of water into the decocted cogongrass rhizome again, decocting for 1-2 hours, filtering, combining the two filtrates, performing pressure filtration by using a 1000-plus 3000-mesh filter press, refluxing for 2-4 times at the temperature of 92-100 ℃, keeping the filtrate, and concentrating the filtrate into paste by using a jacketed kettle, namely cogongrass rhizome paste;
rinsing and soaking mint, adding 4-8 times of water, decocting for 2-4 hours, filtering, adding 1-2 times of water into the decocted mint again, decocting for 1-2 hours, filtering, combining two filtrates, performing pressure filtration by using a 1000-plus 3000-mesh filter press, refluxing for 2-4 times at 92-100 ℃, keeping the filtrate, and concentrating the filtrate into paste by using a jacketed kettle to obtain the mint paste;
2) and mixing materials:
mixing Coptidis rhizoma extract, Scutellariae radix extract, radix Rubiae extract, herba Houttuyniae extract, herba Taraxaci extract, flos Lonicerae extract, flos Chrysanthemi extract, lalang grass rhizome extract, herba Menthae extract, catechin, theophylline, tea polyphenols, sorbitol, deionized water, polyethylene glycol-8, sodium lauryl sulfate, edible essence, xanthan gum, cellulose gum and ground calcium hydrogen phosphate, hydrated silica, tetrasodium pyrophosphate, sodium benzoate, and saccharin sodium at a certain ratio to obtain paste;
3) and packaging:
and sterilizing and cooling the dry paste by a sterilizer, and filling by a full-automatic toothpaste filling machine.
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| CN114983898A (en) * | 2022-07-05 | 2022-09-02 | 贵州苗老藤化妆品生产制造有限公司 | Chinese herbal medicine toothpaste and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN114983898A (en) * | 2022-07-05 | 2022-09-02 | 贵州苗老藤化妆品生产制造有限公司 | Chinese herbal medicine toothpaste and preparation method thereof |
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Application publication date: 20210608 |