CN112891275A - Daily chemical detergent prepared based on peony active extract - Google Patents

Daily chemical detergent prepared based on peony active extract Download PDF

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Publication number
CN112891275A
CN112891275A CN202110208714.1A CN202110208714A CN112891275A CN 112891275 A CN112891275 A CN 112891275A CN 202110208714 A CN202110208714 A CN 202110208714A CN 112891275 A CN112891275 A CN 112891275A
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CN
China
Prior art keywords
parts
peony
extract
aqueous extract
active extract
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202110208714.1A
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Chinese (zh)
Inventor
李晓君
渠志灿
丁东源
梁锐
李建丽
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shanxi Na'an Biotechnology Co ltd
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Shanxi Na'an Biotechnology Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
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Priority to CN202110208714.1A priority Critical patent/CN112891275A/en
Publication of CN112891275A publication Critical patent/CN112891275A/en
Pending legal-status Critical Current

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Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9794Liliopsida [monocotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P17/00Drugs for dermatological disorders
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/005Antimicrobial preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/805Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/84Products or compounds obtained by lyophilisation, freeze-drying

Abstract

The invention discloses a daily chemical detergent prepared based on a peony active extract, and particularly relates to the field of plant extraction, wherein the daily chemical detergent comprises, by weight, 20-40 parts of the peony active extract, 15-30 parts of an entada aqueous extract, 5-30 parts of a photocatalyst and 10-20 parts of a crow's foot aqueous extract. The daily chemical cleaning agent provided by the invention has the advantages of less loss of active substances and less solvent residue.

Description

Daily chemical detergent prepared based on peony active extract
Technical Field
The invention relates to the field of plant extraction, and particularly relates to a daily chemical detergent prepared based on a peony active extract.
Background
Peony is a perennial deciduous shrub belonging to the genus Paeoniaceae, the class Dicotyledoneae. Peony has the effects of nourishing blood and liver, lowering blood pressure and relieving pain. The peony can be used for treating symptoms of irregular menstruation, menstrual abdominal pain, amenorrhea, facial chloasma, skin aging and the like of a human body. Although the traditional peony has extremely wide application in the field of medical care, the traditional peony has very little application in the field of daily chemical cleaning.
Moreover, some daily chemical detergents containing peony extracts on the market also have the problems of high active substance loss, poor extract solubility, solvent residue and the like, and the technical personnel are urgently required to solve the problems.
Disclosure of Invention
The invention provides a daily chemical cleanser prepared based on a peony active extract, and the daily chemical cleanser has the advantages of less loss of active substances and less solvent residue.
In order to achieve the purpose, the invention provides the following technical scheme:
the daily chemical detergent comprises, by weight, 20-40 parts of a peony active extract, 15-30 parts of an entada phaseoloides aqueous extract, 5-30 parts of a photocatalyst and 10-20 parts of a crow's-foot aqueous extract.
Preferably, the daily chemical cleanser further comprises at least one of sanguisorba officinalis, purslane and penthorum chinense pursh.
Preferably, the daily chemical detergent comprises, by weight, 20-40 parts of peony active extract, 15-30 parts of ketchun aqueous extract, 5-30 parts of photocatalyst, 10-20 parts of doodle aqueous extract, 1-5 parts of sanguisorba aqueous extract, 3-7 parts of purslane aqueous extract and 1-3 parts of penthorum aqueous extract.
Preferably, the preparation method of the peony active extract comprises the following steps:
s01, selecting the whole peony seedling of 2-3 years old, cleaning, drying, removing the main stem, and reserving peony leaves, peony roots and peony lateral branches, which are used as raw materials.
S02, placing the obtained raw materials and the extracting solution into an extracting container according to the material-liquid ratio of 1:8-1:15, and carrying out high-speed shearing on the raw materials for 3-5min by adopting a high-speed shearing machine to obtain a material mixture.
S03, performing solid-liquid separation on the material mixture by vacuum filtration equipment to obtain filtrate and residue.
S04, placing the filtrate in a stainless steel container, freezing for 10-15 h at the temperature of-8 to-12 ℃, thawing at room temperature after freezing, performing vacuum filtration by adopting medium-speed qualitative filter paper, and removing precipitates to obtain a filtrate.
And S05, concentrating the obtained suction filtration liquid by adopting membrane concentration equipment to obtain 1/3-1/4 of the original volume, further obtaining concentrated liquid, and freeze-drying the concentrated liquid at low temperature to obtain a finished product.
The traditional preparation method of the peony extract comprises the following steps: the problems of more active substance loss, poor extract solubility, solvent residue and the like exist in hot water extraction, solvent extraction and the like, and the application in the field of cleaning daily chemicals is inconvenient.
The method provided by the scheme has the following advantages:
1) said method comprises extracting at room temperature or a temperature below room temperature;
2) the above method does not employ organic solvent for extraction;
3) the method adopts freeze thawing method to remove the components which are not beneficial to dissolution,
4) the obtained product has high retention of active ingredients and no solvent residue, greatly improves the solubility, and can increase the use amount and make the efficacy of the product more easily exerted when applied to the field of cleaning daily chemicals.
5) The method adopts hydrogen-rich water as an extraction solvent, combines a high-speed shearing rapid extraction method, enables the pH (9.5-9.9) of the extracting solution to be kept at a slightly alkaline pH value in a short time, simultaneously enables the pH value of the extracting solution to be recovered to be neutral in a subsequent longer-time working section, and avoids damage to membrane concentration equipment during subsequent membrane concentration.
Of course, the pH can be adjusted by other inorganic bases, and the pH can be adjusted to be neutral by acid liquor after extraction, but corresponding inorganic salts are formed, and if the product contains high inorganic salts, the product has a large influence on the stability of daily chemical products when added as daily chemical products. The process can avoid the phenomenon.
The characteristics of the peony active extract are as follows: the total phenol content is 350-500mg/g, the total flavone content is 160-250mg/g, and the iron ion reduction amount is 35-40 mu mol.
Has no solvent residue and good solubility, and is suitable for application in the field of daily chemicals, especially for products with higher pH (7-8.5), such as cleaning products (face cleaning cream and bath lotion).
Preferably, in step S02, the ratio of the feed to the liquid is 1: 12.
Preferably, in step S04, the temperature condition is-10 ℃.
Preferably, in step S04, the frozen food is frozen for 12 hours.
Preferably, in step S05, the concentrated volume is 1/3 of the original volume.
The invention has the beneficial effects that:
in the invention, the peony active extract, the entada phaseoloides aqueous extract and the photocatalyst are added into the components, so that the effects of cleaning and bacteriostasis can be achieved. Meanwhile, the aqueous extract of the curvula vulgaris can repair damaged skin tissues and reduce the problems of pockmarks, large pores and the like on the surface of the skin. In addition, the skin care product is prepared from natural plant extracts, so that the skin care product is not easy to remain on the surface of skin tissues and is easy to clean.
Detailed Description
Example 1
The daily chemical detergent comprises, by weight, 20 parts of a peony active extract, 15 parts of an entada phaseoloides aqueous extract, 5 parts of a photocatalyst, 10 parts of a crow's-foot aqueous extract, 1 part of a sanguisorba aqueous extract, 3 parts of a purslane aqueous extract and 1 part of a penthorum aqueous extract.
The preparation method of the peony active extract comprises the following steps:
1. raw materials
2-3 years old peony, collecting the whole peony, cleaning, drying (drying in the shade), removing main stem, and retaining peony leaf, peony root, peony lateral branch, etc.
2. Raw material treatment
And (3) crushing the raw materials in the step (1) to 20-40 meshes for later use.
3. Preparation of the extract
Hydrogen-rich water with hydrogen content of 1.2-1.4ppm and pH of 9.5-9.9.
4. Extraction process
Adding the raw materials and the extracting solution into an extracting container according to the material-liquid ratio of 1:8-1: 15.
Rapidly (within 2 min) shearing the material at high speed for 3-5min by adopting a high-speed shearing machine (with the rotating speed of 12000-.
And (3) carrying out solid-liquid separation on the sheared material by adopting vacuum filtration equipment to obtain liquid 1 and residues, repeating the step 2) on the residues for extraction again, carrying out vacuum filtration to obtain liquid 2 after extraction is finished, and combining the two liquids to obtain an extracting solution.
Placing the extractive solution into stainless steel container, and freezing at-10 deg.C for 12 hr.
After freezing, melting at room temperature, vacuum-filtering with medium-speed qualitative filter paper to remove precipitate to obtain clear liquid, and repeating for 2 times to obtain filtrate.
Concentrating the prepared suction filtration liquid by adopting membrane concentration equipment to 1/3-1/4 in volume to obtain concentrated liquid;
and (5) freezing and drying the concentrated solution at low temperature to obtain a finished product.
Example 2
The daily chemical detergent prepared based on the peony active extract comprises, by weight, 30 parts of the peony active extract, 25 parts of an entada phaseoloides aqueous extract, 20 parts of a photocatalyst, 15 parts of an aqueous extract of a curdlan, 3 parts of an aqueous extract of sanguisorba officinalis, 4 parts of an aqueous extract of purslane and 2 parts of an aqueous extract of penthorum chinense pursh.
The preparation method of the peony active extract described in this example is the same as that of example 1.
Example 3
The daily chemical detergent comprises, by weight, 35 parts of a peony active extract, 25 parts of an entada phaseoloides aqueous extract, 26 parts of a photocatalyst, 18 parts of a crow's-foot aqueous extract, 4 parts of a sanguisorba aqueous extract, 6 parts of a purslane aqueous extract and 2 parts of a penthorum aqueous extract.
The preparation method of the peony active extract described in this example is the same as that of example 1.
Example 4
The daily chemical detergent comprises, by weight, 40 parts of a peony active extract, 30 parts of an entada phaseoloides aqueous extract, 30 parts of a photocatalyst, 20 parts of a crow's-foot aqueous extract, 5 parts of a sanguisorba aqueous extract, 7 parts of a purslane aqueous extract and 3 parts of a penthorum aqueous extract.
The preparation method of the peony active extract described in this example is the same as that of example 1.

Claims (10)

1. The daily chemical detergent prepared based on the peony active extract is characterized by comprising, by weight, 20-40 parts of the peony active extract, 15-30 parts of an entada aqueous extract, 5-30 parts of a photocatalyst and 10-20 parts of an aqueous extract of a crow's foot.
2. The peony active extract according to claim 1, further comprising at least one of sanguisorba officinalis, purslane and penthorum chinense.
3. The peony active extract according to claim 1, comprising, by weight, 20-40 parts of a peony active extract, 15-30 parts of an entada phaseoloides aqueous extract, 5-30 parts of a photocatalyst, 10-20 parts of an doodle aqueous extract, 1-5 parts of a sanguisorba aqueous extract, 3-7 parts of a purslane aqueous extract and 1-3 parts of a penthorum chinense aqueous extract.
4. The peony active extract according to claim 3, comprising 30 parts of peony active extract, 25 parts of entada phaseoloides aqueous extract, 20 parts of photocatalyst, 15 parts of doodle aqueous extract, 3 parts of sanguisorba aqueous extract, 4 parts of purslane aqueous extract and 2 parts of penthorum chinense aqueous extract in parts by weight.
5. The peony active extract according to claim 1, wherein the preparation method of the peony active extract comprises:
s01, selecting a 2-3 year old whole peony seedling, cleaning, drying, removing a main stem, and keeping peony leaves, peony roots and peony lateral branches, which are used as raw materials;
s02, placing the obtained raw materials and the extracting solution into an extracting container according to the material-liquid ratio of 1:8-1:15, and carrying out high-speed shearing on the raw materials for 3-5min by adopting a high-speed shearing machine to obtain a material mixture;
s03, performing solid-liquid separation on the material mixture by using vacuum filtration equipment to obtain filtrate and residues;
s04, placing the filtrate in a stainless steel container, freezing for 10-15 hours at the temperature of-8 to-12 ℃, thawing at room temperature after freezing, performing vacuum filtration by adopting medium-speed qualitative filter paper, and removing precipitates to obtain a filtrate;
and S05, concentrating the obtained suction filtration liquid by adopting membrane concentration equipment to obtain 1/3-1/4 of the original volume, further obtaining concentrated liquid, and freeze-drying the concentrated liquid at low temperature to obtain a finished product.
6. A peony active extract according to claim 5, wherein, in step S02, the ratio of material to liquid is 1: 12.
7. A peony active extract according to claim 5, wherein, in step S04, the temperature condition is-10 ℃.
8. A peony active extract according to claim 5, wherein, in step S04, it is frozen for 12 h.
9. A peony active extract according to claim 5, wherein in step S05, the volume after concentration is 1/3 of the original volume.
10. A peony active extract according to claim 5, wherein in step S02, the extract is selected from hydrogen-rich water, hydrogen content is 1.2-1.4ppm, and pH is 9.5-9.9.
CN202110208714.1A 2021-02-24 2021-02-24 Daily chemical detergent prepared based on peony active extract Pending CN112891275A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202110208714.1A CN112891275A (en) 2021-02-24 2021-02-24 Daily chemical detergent prepared based on peony active extract

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202110208714.1A CN112891275A (en) 2021-02-24 2021-02-24 Daily chemical detergent prepared based on peony active extract

Publications (1)

Publication Number Publication Date
CN112891275A true CN112891275A (en) 2021-06-04

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN202110208714.1A Pending CN112891275A (en) 2021-02-24 2021-02-24 Daily chemical detergent prepared based on peony active extract

Country Status (1)

Country Link
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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TWI229605B (en) * 1996-08-21 2005-03-21 Kao Corp Cosmetic method
JP2013159592A (en) * 2012-02-08 2013-08-19 Sansho Seiyaku Co Ltd External agent for preventing gray hair
CN106726932A (en) * 2016-12-19 2017-05-31 哈尔滨灵草舒生物科技有限公司 A kind of peony promoting blood circulation for regulating menstruation shower cream and preparation method thereof
CN110840777A (en) * 2019-12-10 2020-02-28 山西潞安矿业(集团)有限责任公司 Peony pore cleaning mask and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TWI229605B (en) * 1996-08-21 2005-03-21 Kao Corp Cosmetic method
JP2013159592A (en) * 2012-02-08 2013-08-19 Sansho Seiyaku Co Ltd External agent for preventing gray hair
CN106726932A (en) * 2016-12-19 2017-05-31 哈尔滨灵草舒生物科技有限公司 A kind of peony promoting blood circulation for regulating menstruation shower cream and preparation method thereof
CN110840777A (en) * 2019-12-10 2020-02-28 山西潞安矿业(集团)有限责任公司 Peony pore cleaning mask and preparation method thereof

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Application publication date: 20210604

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