CN112830764B - Manufacturing process of needle tube nixing decoration characteristic nixing pottery - Google Patents
Manufacturing process of needle tube nixing decoration characteristic nixing pottery Download PDFInfo
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- 238000004519 manufacturing process Methods 0.000 title claims abstract description 13
- 238000005034 decoration Methods 0.000 title description 2
- 238000010304 firing Methods 0.000 claims abstract description 33
- 239000000049 pigment Substances 0.000 claims abstract description 27
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 25
- 239000011268 mixed slurry Substances 0.000 claims abstract description 22
- 238000000034 method Methods 0.000 claims abstract description 21
- 238000001035 drying Methods 0.000 claims abstract description 17
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 15
- 239000010453 quartz Substances 0.000 claims abstract description 14
- 238000010422 painting Methods 0.000 claims abstract description 12
- 238000007580 dry-mixing Methods 0.000 claims abstract description 9
- 238000001125 extrusion Methods 0.000 claims abstract description 9
- 239000004372 Polyvinyl alcohol Substances 0.000 claims abstract description 7
- CWQXQMHSOZUFJS-UHFFFAOYSA-N molybdenum disulfide Chemical compound S=[Mo]=S CWQXQMHSOZUFJS-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229910052982 molybdenum disulfide Inorganic materials 0.000 claims abstract description 7
- 229920002451 polyvinyl alcohol Polymers 0.000 claims abstract description 7
- 238000002360 preparation method Methods 0.000 claims abstract description 3
- 239000002245 particle Substances 0.000 claims description 10
- 238000002156 mixing Methods 0.000 abstract description 21
- 238000000227 grinding Methods 0.000 abstract description 11
- RVTZCBVAJQQJTK-UHFFFAOYSA-N oxygen(2-);zirconium(4+) Chemical compound [O-2].[O-2].[Zr+4] RVTZCBVAJQQJTK-UHFFFAOYSA-N 0.000 abstract 2
- 229910001928 zirconium oxide Inorganic materials 0.000 abstract 2
- 230000018109 developmental process Effects 0.000 description 11
- 241001122767 Theaceae Species 0.000 description 9
- 238000009966 trimming Methods 0.000 description 8
- 238000007605 air drying Methods 0.000 description 7
- 238000000498 ball milling Methods 0.000 description 7
- 238000001816 cooling Methods 0.000 description 7
- 238000005336 cracking Methods 0.000 description 7
- 239000000706 filtrate Substances 0.000 description 7
- 238000007873 sieving Methods 0.000 description 7
- 239000002689 soil Substances 0.000 description 7
- 230000032683 aging Effects 0.000 description 6
- 238000004898 kneading Methods 0.000 description 6
- 238000003825 pressing Methods 0.000 description 6
- 239000004927 clay Substances 0.000 description 5
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 4
- USEGQPUGEPSVQL-UHFFFAOYSA-N [Pr].[Zr] Chemical compound [Pr].[Zr] USEGQPUGEPSVQL-UHFFFAOYSA-N 0.000 description 4
- 239000002932 luster Substances 0.000 description 4
- PUZPDOWCWNUUKD-UHFFFAOYSA-M sodium fluoride Chemical compound [F-].[Na+] PUZPDOWCWNUUKD-UHFFFAOYSA-M 0.000 description 4
- 230000000052 comparative effect Effects 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 239000000919 ceramic Substances 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000001103 potassium chloride Substances 0.000 description 2
- 235000011164 potassium chloride Nutrition 0.000 description 2
- 235000013024 sodium fluoride Nutrition 0.000 description 2
- 239000011775 sodium fluoride Substances 0.000 description 2
- 239000004575 stone Substances 0.000 description 2
- 239000006004 Quartz sand Substances 0.000 description 1
- 229910010413 TiO 2 Inorganic materials 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 238000003892 spreading Methods 0.000 description 1
- 239000002344 surface layer Substances 0.000 description 1
- SWGJCIMEBVHMTA-UHFFFAOYSA-K trisodium;6-oxido-4-sulfo-5-[(4-sulfonatonaphthalen-1-yl)diazenyl]naphthalene-2-sulfonate Chemical group [Na+].[Na+].[Na+].C1=CC=C2C(N=NC3=C4C(=CC(=CC4=CC=C3O)S([O-])(=O)=O)S([O-])(=O)=O)=CC=C(S([O-])(=O)=O)C2=C1 SWGJCIMEBVHMTA-UHFFFAOYSA-K 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/04—Clay; Kaolin
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
- C04B33/1305—Organic additives
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
- C04B33/131—Inorganic additives
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
- C04B33/14—Colouring matters
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/24—Manufacture of porcelain or white ware
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Dispersion Chemistry (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Inorganic Chemistry (AREA)
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Abstract
The invention discloses a manufacturing process of a needle tube nipu characteristic nixing pottery, which comprises the working procedures of blank preparation, blank forming, carving, needle tube nixing, drying and firing, wherein the needle tube nixing is prepared by mixing east mud, west mud and a pigment according to the weight ratio of 6: 4: 0.1-0.3 of dry mixing, superfine grinding, adding water, performing vacuum pugging and extrusion forming to obtain mixed slurry, injecting the mixed slurry into a groove formed by carving through a needle tube, flattening and compacting; the pigment comprises the following components in parts by weight: ZrO (zirconium oxide) 2 123 parts by weight of Pr 6 O 11 20-61 parts of quartz, 60-66 parts of quartz, 5-10 parts of polyvinyl alcohol and 1-5 parts of molybdenum disulfide. The mud painting has strong generating capacity and does not generate color spots.
Description
Technical Field
The invention relates to a manufacturing process of nixing ceramics, in particular to a manufacturing process of nixing ceramics with needle tube nipainting characteristics.
Background
The manufacturing process of the Qinzhou nixing pottery comprises the following steps: 1) preparing a blank: the blank is made of clay crossing Qinjiang east of Qinzhou city, commonly called east clay (soft clay, yellow-white in color, containing trace quartz sand, and having plasticity adjusted in the production process of nixing pottery for binding), and west clay (containing a small amount of K) of Qinjiang west region 2 O、NaO、CaO、MgO、Fe 2 0 3 、TiO 2 、MnO 2 The purple mud stone with high iron content is purple red, the surface layer has a small amount of iron dip-dyed and is hard clay, and the plasticity and the binding property are poor), and the purple mud stone and the purple mud are mixed according to the weight percentage of 40-60% of east mud and 40-60% of west mud, and are made into blanks through a series of processes such as grinding, dewatering and the like; 2) forming a blank body: preparing the blank into various blank bodies by adopting a plastic method or a grouting method; 3) trimming the blank: trimming the blank by using a plate knife and a semi-circular opening knife to meet the design requirement; 4) engraving: writing and drawing on the blank, picking out soil along the edges of two sides of the blank ink mark by a graver,removing all the parts with ink marks to form grooves with uniform bottoms; 5) and (3) drying: drying the green body by adopting an air drying method to remove the moisture of the green body; 6) and (3) firing the green body: and (3) putting the dried green body into a kiln for firing, controlling the firing temperature to be 1100-1200 ℃, controlling the firing time to be 10h, cooling and then taking out of the kiln. The needle tube nixing painting nixing pottery technology is a technology for painting mixed feed liquid filled with pug and pigment in a needle tube on a nixing pottery blank, namely, the mixed feed liquid is injected into a groove formed by carving through the needle tube, so that a nixing pottery finished product which has stronger stereoscopic impression, brighter color and better visual effect than the traditional nixing pottery relief, line carving and plain carving is obtained. However, the mud and the pigment are difficult to mix, and color spots are easy to form on the surface of the blank. If the color material is subjected to the ultramicro treatment, the color material can be uniformly mixed with the blank, but the color development capability of the color material is reduced, so that the color of the finished product is dull and lusterless.
Disclosure of Invention
The invention aims to provide a manufacturing process of a needle tube nixing pottery with characteristic nixing painting, which can realize uniform mixing of a pigment and a pug and has strong color development capability of the pigment.
The technical scheme provided by the invention is that the manufacturing process of the needle tube nixing pottery with the characteristic of nixing comprises the working procedures of blank preparation, blank forming, carving, needle tube nixing, drying and firing, wherein the needle tube nixing is prepared by mixing east mud, west mud and a pigment according to the weight ratio of 6: 4: 0.1-0.3 of dry mixing, superfine grinding, adding water, performing vacuum pugging and extrusion forming to obtain mixed slurry, injecting the mixed slurry into a groove formed by carving through a needle tube, flattening and compacting;
the pigment comprises the following components in parts by weight: ZrO (ZrO) 2 123 parts by weight of Pr 6 O 11 20-61 parts of quartz, 60-66 parts of quartz, 5-10 parts of polyvinyl alcohol and 1-5 parts of molybdenum disulfide.
The weight ratio of the east mud to the west mud is 6:4, and the weight ratio of the east mud to the west mud is the same as the weight ratio of the blank, so that the mixed mud is consistent with the mud ratio of the blank, the blank and the mud drawn by the needle tube are consistent in shrinkage in the firing process, and cracking or falling off is avoided.
And micronizing the mixture of the east mud, the west mud and the pigment to obtain the mixture with the particle size of 200-1000 nm. The mixture of the east mud, the west mud and the pigment is subjected to superfine grinding to 200-1000 nm, so that the pigment can be fully and uniformly mixed with the east mud and the west mud, the pigment agglomeration in the subsequent firing process is avoided, and color spots are avoided.
The water content of the mixed slurry is 30-40%. The water content of the mixed slurry is larger than that of the blank, so that the combination of the mixed slurry and the blank can be promoted, the mutual approaching and closing of the component particles are facilitated, and the bonding force is increased.
The water content of the blank is 15-20%.
The weight ratio of the east mud to the west mud in the blank is 6: 4.
compared with the prior art, the invention adopts superfine grinding to ensure that the east mud, the west mud and the pigment are fully mixed, thereby avoiding color spots. Secondly, the color development capability of the praseodymium-zirconium yellow is inevitably greatly reduced due to the superfine grinding, but the color development capability of the praseodymium-zirconium yellow is not influenced by the superfine grinding by adding the polyvinyl alcohol and the molybdenum disulfide, and the color development capability is still outstanding. Thirdly, the color development temperature of the praseodymium-zirconium yellow is about 800 ℃ under the conventional condition, and the color development capability is greatly reduced when the temperature is exceeded, but the color development capability is still good when the praseodymium-zirconium yellow is fired at 1100-1200 ℃.
Detailed Description
The following specific examples further illustrate the invention but are not intended to limit the invention thereto.
Example 1
1) Preparing a blank: mixing Dong mud and West mud according to the weight ratio of 6:4, mixing, performing ball milling for 8 hours, then sequentially sieving by a 40-mesh sieve and a 100-mesh sieve, pressing filtrate into mud strips, performing vacuum pugging, and aging for 15 days to obtain blanks.
2) Forming a blank body: the method comprises the steps of forming by pulling a blank by hand, putting the blank on a motor, starting the rotating speed of a speed regulator, and kneading 100 tea cups with the diameter of 30cm by using a plate cutter, a rubber plate and a rubber strip laying tool. Controlling the water content of the green body to be 15%.
3) Trimming the blank: and (4) thinning the excessively thick blank by using a plate knife and a semi-circular opening knife to meet the design requirement.
4) Engraving: writing and drawing on the blank body, picking out soil along the edges of two sides of the ink marks of the blank body by using a nicking tool, and completely removing the ink marks to form a groove with uniform bottom.
5) Needle tube mud painting: mixing Dong mud, West mud and pigment according to the weight ratio of 6: 4: 0.1, carrying out dry mixing, carrying out ultrafine grinding until the particle size is 200-1000 nm, adding water, carrying out vacuum pugging and extrusion forming to obtain mixed slurry with the water content of 30%, then injecting the mixed slurry into a groove formed by carving through a needle tube, flattening and compacting;
the pigment comprises the following components in parts by weight: ZrO (ZrO) 2 123 parts by weight of Pr 6 O 11 20 parts by weight of quartz, 60 parts by weight of quartz, 5 parts by weight of polyvinyl alcohol and 1 part by weight of molybdenum disulfide.
6) And (3) drying: and drying the green body by adopting an air drying method to remove the moisture of the green body.
7) Firing: and (3) putting the dried green body into a kiln for firing, controlling the firing temperature at 1100 ℃ and the firing time to be 10h, and taking the dried green body out of the kiln after cooling.
The finished product of the fired teacup has no shedding and cracking, and the perfectness rate is 100 percent. The mud painted part of the needle tube has good color development, bright yellow color, strong luster and no color spot.
Comparative example 1
1) Preparing a blank: mixing Dong mud and West mud according to the weight ratio of 6:4, mixing, performing ball milling for 8 hours, then sequentially sieving by a 40-mesh sieve and a 100-mesh sieve, pressing filtrate into mud strips, performing vacuum pugging, and aging for 15 days to obtain blanks.
2) Forming a blank body: the method comprises the steps of forming by pulling a blank by hand, putting the blank on a motor, starting the rotating speed of a speed regulator, and kneading 100 tea cups with the diameter of 30cm by using a plate cutter, a rubber plate and a rubber strip laying tool. Controlling the water content of the green body to be 15%.
3) Trimming the blank: and (4) thinning the excessively thick blank by using a plate knife and a semi-circular opening knife to meet the design requirement.
4) Engraving: writing and drawing on the blank, picking out soil along the edges of two sides of the ink marks of the blank by a graver, and completely removing the ink marks to form a groove with uniform bottom.
5) Needle tube mud painting: mixing Dong mud, West mud and pigment according to the weight ratio of 6: 4: 0.1, carrying out dry mixing, carrying out ultrafine grinding until the particle size is 200-1000 nm, adding water, carrying out vacuum pugging and extrusion forming to obtain mixed slurry with the water content of 30%, then injecting the mixed slurry into a groove formed by carving through a needle tube, flattening and compacting;
the pigment comprises the following components in parts by weight: ZrO (ZrO) 2 123 parts by weight of Pr 6 O 11 20 parts by weight of quartz and 60 parts by weight of quartz.
6) And (3) drying: and drying the green body by adopting an air drying method to remove the moisture of the green body.
7) And (3) firing: and (3) putting the dried green body into a kiln for firing, controlling the firing temperature at 1100 ℃ and the firing time at 10h, cooling and then taking out of the kiln.
The finished fired tea cup has no shedding and cracking, and the perfectness ratio is 100 percent. The color of the mud painted part of the needle tube is dark, and the mud painted part of the needle tube hardly presents yellow and has no color spots.
Comparative example 2
1) Preparing a blank: mixing Dong mud and West mud according to the weight ratio of 6:4, mixing, performing ball milling for 8 hours, then sequentially sieving by a 40-mesh sieve and a 100-mesh sieve, pressing filtrate into mud strips, performing vacuum pugging, and aging for 15 days to obtain blanks.
2) Forming a blank body: the method comprises the steps of forming by pulling a blank by hand, putting the blank on a motor, starting the rotating speed of a speed regulator, and kneading 100 tea cups with the diameter of 30cm by using a plate cutter, a rubber plate and a rubber strip laying tool. Controlling the water content of the green body to be 15%.
3) Trimming the blank: and (3) thinning the excessively thick blank by using a plate knife and a semi-circular opening knife to meet the design requirement.
4) Engraving: writing and drawing on the blank, picking out soil along the edges of two sides of the ink marks of the blank by a graver, and completely removing the ink marks to form a groove with uniform bottom.
5) Needle tube mud painting: mixing Dong mud, West mud and pigment according to the weight ratio of 6: 4: 0.1, carrying out dry mixing, carrying out ultrafine grinding until the particle size is 200-1000 nm, adding water, carrying out vacuum pugging and extrusion forming to obtain mixed slurry with the water content of 30%, then injecting the mixed slurry into a groove formed by carving through a needle tube, flattening and compacting;
the pigment comprises the following components in parts by weight: ZrO (ZrO) 2 123 parts by weight of Pr 6 O 11 20 parts by weight, 60 parts by weight of quartz, 3 parts by weight of sodium fluoride and 3 parts by weight of potassium chloride.
6) And (3) drying: and drying the green body by adopting an air drying method to remove the moisture of the green body.
7) Firing: and (3) putting the dried green body into a kiln for firing, controlling the firing temperature at 1100 ℃ and the firing time to be 10h, and taking the dried green body out of the kiln after cooling.
The finished product of the fired teacup has no shedding and cracking, and the perfectness rate is 100 percent. The color of the mud painted part of the needle tube is dark and has no luster and no color spot.
Comparative example 3
1) Preparing a blank: mixing Dong mud and West mud according to the weight ratio of 6:4, mixing, performing ball milling for 8 hours, then sequentially sieving by a 40-mesh sieve and a 100-mesh sieve, pressing filtrate into mud strips, performing vacuum pugging, and aging for 15 days to obtain blanks.
2) Forming a blank body: the method comprises the steps of forming by pulling a blank by hand, putting the blank on a motor, starting the rotating speed of a speed regulator, and kneading 100 tea cups with the diameter of 30cm by using a plate cutter, a rubber plate and a rubber strip laying tool. Controlling the water content of the green body to be 15%.
3) Trimming the blank: and (3) thinning the excessively thick blank by using a plate knife and a semi-circular opening knife to meet the design requirement.
4) Engraving: writing and drawing on the blank body, picking out soil along the edges of two sides of the ink marks of the blank body by using a nicking tool, and completely removing the ink marks to form a groove with uniform bottom.
5) Needle tube mud painting: mixing Dong mud, West mud and pigment according to the weight ratio of 6: 4: 0.1 dry mixing, adding water, ball milling, sieving by a 40-mesh sieve and a 100-mesh sieve, performing vacuum pugging and extrusion molding on filtrate to obtain mixed slurry with the water content of 30%, then injecting the mixed slurry into a groove formed by carving through a needle tube, flattening and compacting;
the pigment comprises the following components in parts by weight: ZrO (ZrO) 2 123 parts by weight of Pr 6 O 11 20 parts by weight of quartz 60 parts by weight3 parts of sodium fluoride and 3 parts of potassium chloride.
6) And (3) drying: and drying the green body by adopting an air drying method to remove the moisture of the green body.
7) Firing: and (3) putting the dried green body into a kiln for firing, controlling the firing temperature at 1100 ℃ and the firing time to be 10h, and taking the dried green body out of the kiln after cooling.
The finished fired tea cup has no shedding and cracking, and the perfectness ratio is 100 percent. The mud painted part of the needle tube has bright color, but can be seen in a plurality of color spots.
Example 2
1) Preparing a blank: mixing Dong mud and West mud according to the weight ratio of 6:4, mixing, performing ball milling for 8 hours, then sequentially sieving by a 40-mesh sieve and a 100-mesh sieve, pressing filtrate into mud strips, performing vacuum pugging, and aging for 15 days to obtain blanks.
2) Forming a blank body: the method comprises the steps of forming by pulling a blank by hand, putting the blank on a motor, starting the rotating speed of a speed regulator, and kneading 100 tea cups with the diameter of 30cm by using a plate cutter, a rubber plate and a rubber strip laying tool. Controlling the water content of the green body to be 20%.
3) Trimming the blank: and (3) thinning the excessively thick blank by using a plate knife and a semi-circular opening knife to meet the design requirement.
4) Engraving: writing and drawing on the blank, picking out soil along the edges of two sides of the ink marks of the blank by a graver, and completely removing the ink marks to form a groove with uniform bottom.
5) Needle tube mud painting: mixing Dong mud, West mud and pigment according to a weight ratio of 6: 4: 0.3, dry mixing, micronizing to obtain particles with the particle size of 200-1000 nm, adding water, performing vacuum pugging and extrusion molding to obtain mixed slurry with the water content of 40%, then injecting the mixed slurry into a groove formed by carving through a needle tube, flattening and compacting;
the pigment comprises the following components in parts by weight: ZrO (ZrO) 2 123 parts by weight of Pr 6 O 11 61 parts by weight, 66 parts by weight of quartz, 10 parts by weight of polyvinyl alcohol and 5 parts by weight of molybdenum disulfide.
6) And (3) drying: and drying the green body by adopting an air drying method to remove the moisture of the green body.
7) Firing: and (3) putting the dried green body into a kiln for firing, controlling the firing temperature at 1200 ℃ and the firing time at 10h, and taking the dried green body out of the kiln after cooling.
The finished fired tea cup has no shedding and cracking, and the perfectness ratio is 100 percent. The needle tube mud painting part has good color development, bright yellow, strong luster and no color spot.
Example 3
1) Preparing a blank: mixing Dong mud and West mud according to the weight ratio of 6:4, mixing, performing ball milling for 8 hours, then sequentially sieving by a 40-mesh sieve and a 100-mesh sieve, pressing filtrate into mud strips, performing vacuum pugging, and aging for 15 days to obtain blanks.
2) Forming a blank body: the method comprises the steps of hand-pulling a blank for molding, putting the blank on a motor, starting the rotating speed of a speed regulator, and kneading 100 tea cups with the diameter of 30cm by using a plate cutter, a rubber plate and a rubber strip spreading tool. Controlling the water content of the green body to be 15-20%.
3) Trimming the blank: and (4) thinning the excessively thick blank by using a plate knife and a semi-circular opening knife to meet the design requirement.
4) Engraving: writing and drawing on the blank, picking out soil along the edges of two sides of the ink marks of the blank by a graver, and completely removing the ink marks to form a groove with uniform bottom.
5) Needle tube mud painting: mixing Dong mud, West mud and pigment according to the weight ratio of 6: 4: 0.2, carrying out dry mixing, carrying out ultrafine grinding until the particle size is 200-1000 nm, adding water, carrying out vacuum pugging and extrusion forming to obtain mixed slurry with the water content of 35%, then injecting the mixed slurry into a groove formed by carving through a needle tube, flattening and compacting;
the pigment comprises the following components in parts by weight: ZrO (ZrO) 2 123 parts by weight of Pr 6 O 11 48 parts by weight, 63 parts by weight of quartz, 8 parts by weight of polyvinyl alcohol and 3 parts by weight of molybdenum disulfide.
6) And (3) drying: and drying the green body by adopting an air drying method to remove the moisture of the green body.
7) Firing: and (3) putting the dried green body into a kiln for firing, controlling the firing temperature to 1150 ℃ and the firing time to 10h, and taking the dried green body out of the kiln after cooling.
The finished product of the fired teacup has no shedding and cracking, and the perfectness rate is 100 percent. The mud painted part of the needle tube has good color development, bright yellow color, strong luster and no color spot.
Claims (4)
1. The manufacturing process of the needle tube nidraw characteristic nixing pottery comprises the working procedures of blank preparation, blank forming, carving, needle tube nidraw, drying and firing, and is characterized in that: the needle tube mud painting is that east mud, west mud and pigment are mixed according to the weight ratio of 6: 4: 0.1-0.3 of dry mixing, micronizing to obtain particles with the particle size of 200-1000 nm, adding water, performing vacuum pugging and extrusion forming to obtain mixed slurry, injecting the mixed slurry into a groove formed by carving through a needle tube, flattening and compacting; the pigment comprises the following components in parts by weight: ZrO (ZrO) 2 123 parts by weight of Pr 6 O 11 20-61 parts of quartz, 60-66 parts of quartz, 5-10 parts of polyvinyl alcohol and 1-5 parts of molybdenum disulfide.
2. The manufacturing process of the needle tube niploid characteristic nixing pottery as recited in claim 1, characterized in that: the water content of the mixed slurry is 30-40%.
3. The manufacturing process of the needle tube niploid characteristic nixing pottery as recited in claim 1, characterized in that: in the step of forming the blank body, the moisture content of the blank body is 15-20%.
4. The manufacturing process of the needle tube nixing-characteristic nixing pottery as claimed in claim 1, characterized in that: the blank is prepared from east mud and west mud according to the weight ratio of 6:4 in proportion.
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| CN202110088248.8A CN112830764B (en) | 2021-01-22 | 2021-01-22 | Manufacturing process of needle tube nixing decoration characteristic nixing pottery |
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| CN202110088248.8A CN112830764B (en) | 2021-01-22 | 2021-01-22 | Manufacturing process of needle tube nixing decoration characteristic nixing pottery |
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