CN112812595A - Inorganic magic color liquid particle and preparation method thereof - Google Patents
Inorganic magic color liquid particle and preparation method thereof Download PDFInfo
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- CN112812595A CN112812595A CN202110079841.6A CN202110079841A CN112812595A CN 112812595 A CN112812595 A CN 112812595A CN 202110079841 A CN202110079841 A CN 202110079841A CN 112812595 A CN112812595 A CN 112812595A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D1/00—Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances
- C09D1/02—Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances alkali metal silicates
- C09D1/04—Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances alkali metal silicates with organic additives
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D1/00—Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses an inorganic magic color liquid particle and a preparation method thereof, wherein the inorganic magic color liquid particle comprises an inorganic gel A and an inorganic component B which are uniformly mixed, and the inorganic gel A comprises the following components in parts by mass: 90-95 parts of deionized water and 5-10 parts of inorganic gel solution; the inorganic component B comprises the following components in percentage by mass: 10-35 parts of deionized water, 0.1-0.2 part of multifunctional auxiliary agent, 0.1-0.2 part of wetting agent, 0.2-0.3 part of dispersing agent, 0.2-0.4 part of preservative, 0.2-0.4 part of defoaming agent, 0.6-1.2 parts of film-forming auxiliary agent, 10-15 parts of inorganic silicon resin, 15-25 parts of potassium silicate, 1-3 parts of reactant and 1-2 parts of pigment. The invention overcomes the defects of poor weather resistance and stain resistance of the existing product, and is harmless and pollution-free to the environment; not only the decorative effect of the stone is kept, but also the excellent fire resistance is provided, so that the coating can reach the A-level fire resistance.
Description
Technical Field
The invention belongs to the technical field of building decoration materials, and particularly relates to inorganic multicolor liquid particles and a preparation method thereof.
Background
With the rapid development of economy in China, people have higher and higher requirements on environmental protection of building decoration materials. Meanwhile, the stone-like coating is widely applied because the decorative effect of the stone-like coating is close to that of natural stone. But the weather resistance, the stain resistance, the heat preservation and the fire resistance of the composite material have certain defects.
Disclosure of Invention
The invention aims to overcome the defects of the prior art, provide inorganic magic color liquid particles which not only keep the decorative effect of stone, but also provide excellent fire resistance, and enable a coating to achieve the grade A fire resistance, and provide a preparation method of the inorganic magic color liquid particles.
The purpose of the invention is realized by the following technical scheme: an inorganic magic color liquid particle comprises an inorganic gel A and an inorganic component B which are uniformly mixed, wherein the mass ratio of the inorganic gel A to the inorganic component B is 8: 1-10: 1; the inorganic gel A comprises the following components in parts by mass: 90-95 parts of deionized water and 5-10 parts of inorganic gel solution; the inorganic component B comprises the following components in percentage by mass: 10-35 parts of deionized water, 0.1-0.2 part of multifunctional auxiliary agent, 0.1-0.2 part of wetting agent, 0.2-0.3 part of dispersing agent, 0.2-0.4 part of preservative, 0.2-0.4 part of defoaming agent, 0.6-1.2 parts of film-forming auxiliary agent, 10-15 parts of inorganic silicon resin, 15-25 parts of potassium silicate, 1-3 parts of reactant and 1-2 parts of pigment.
Further, the inorganic gel solution in the inorganic gel agent A is a divalent or trivalent metal ion solution.
Further, the dispersing agent is sodium polyphosphate or ammonium polyacrylate, the wetting agent is fatty alcohol sulfosuccinate anionic type, the preservative is isothiazolinone derivatives, the defoaming agent is a defoaming agent mineral oil defoaming agent, the film-forming aid is carbon dodecyl alcohol, the multifunctional aid is 2-amino-2-methyl-1-propanol, the inorganic silicone resin is self-drying resin, potassium silicate is modified stabilized potassium silicate, the reactant is a hydroxyl compound capable of providing a coordination reaction with divalent or trivalent ions, and the pigment is an inorganic pigment.
Further, the divalent or trivalent ions in the inorganic gelling agent A and the hydroxyl compound in the inorganic component B are subjected to coordination reaction to generate a crosslinking compound.
The invention also aims to provide a preparation method of the inorganic magic color liquid particles, which comprises the following steps:
s1, preparing an inorganic gel A: weighing deionized water and an inorganic gel solution according to a certain proportion, adding the deionized water and the inorganic gel solution into a mixer, and fully and uniformly mixing to obtain an inorganic reaction gel A;
s2, preparing an inorganic component B: weighing deionized water, a multifunctional additive, a wetting agent, a dispersing agent, a preservative, a defoaming agent, a reactant, a film-forming additive, inorganic silicon resin and potassium silicate according to a proportion, adding the materials into a mixer, fully and uniformly mixing, adding a pigment, and uniformly mixing to obtain an inorganic component B;
s3, preparing inorganic colorful liquid particles: adding the inorganic component B prepared in the step S2 into the inorganic gel A prepared in the step S1, and fully and uniformly mixing; then slicing the uniformly mixed gel to obtain liquid particles; wherein the mass ratio of the inorganic gel A to the inorganic component B is 8: 1-10: 1.
The invention has the beneficial effects that: the film forming material is inorganic silicon resin and potassium silicate, which are inorganic substances, and has the advantages of good weather resistance and stain resistance; and the inorganic material is a non-combustible material, so the liquid particle has good fire resistance, and a coating prepared by using the liquid particle can reach the A-level fire resistance, is harmless and pollution-free to the environment, and is a real inorganic environment-friendly product.
Detailed Description
The technical scheme of the invention is further explained by combining specific examples.
Example 1
An inorganic magic color liquid particle comprises an inorganic gel A and an inorganic component B which are uniformly mixed, wherein the mass ratio of the inorganic gel A to the inorganic component B is 8: 1; the inorganic gel A comprises the following components in parts by mass: 90 parts of deionized water and 5 parts of inorganic gel solution; the inorganic component B comprises the following components in percentage by mass: 10 parts of deionized water, 0.1 part of multifunctional auxiliary agent, 0.1 part of wetting agent, 0.2 part of dispersing agent, 0.2 part of preservative, 0.2 part of defoaming agent, 0.6 part of film-forming auxiliary agent, 10 parts of inorganic silicon resin, 15 parts of potassium silicate, 1 part of reactant and 1 part of pigment.
The inorganic gel solution in the inorganic gel agent A is a divalent or trivalent metal ion solution, such as a magnesium ion or calcium ion solution.
The dispersing agent is sodium polyphosphate or ammonium polyacrylate, the wetting agent is fatty alcohol succinate anionic, the preservative is an isothiazolinone derivative, the defoaming agent is a mineral oil defoaming agent, the film-forming aid is carbon dodecyl alcohol, the multifunctional aid is 2-amino-2-methyl-1-propanol, the inorganic silicon resin is self-drying resin, potassium silicate is modified stabilized potassium silicate, the reactant is a hydroxyl compound capable of providing a coordination reaction with divalent or trivalent ions, and the pigment is an inorganic pigment.
And carrying out coordination reaction on divalent or trivalent ions in the inorganic gel A and a hydroxyl compound in the inorganic component B to generate a cross-linked compound.
The preparation method of the inorganic magic color liquid particle comprises the following steps:
s1, preparing an inorganic gel A: weighing deionized water and an inorganic gel solution according to a certain proportion, adding the deionized water and the inorganic gel solution into a mixer, and fully and uniformly mixing to obtain an inorganic reaction gel A;
s2, preparing an inorganic component B: weighing deionized water, a multifunctional additive, a wetting agent, a dispersing agent, a preservative, a defoaming agent, a reactant, a film-forming additive, inorganic silicon resin and potassium silicate according to a proportion, adding the materials into a mixer, fully and uniformly mixing, adding a pigment, and uniformly mixing to obtain an inorganic component B;
s3, preparing inorganic colorful liquid particles: adding the inorganic component B prepared in the step S2 into the inorganic gel A prepared in the step S1, and fully and uniformly mixing; then slicing the uniformly mixed gel to obtain liquid particles; wherein the mass ratio of the inorganic gel A to the inorganic component B is 8: 1.
Example 2
An inorganic magic color liquid particle comprises an inorganic gel A and an inorganic component B which are uniformly mixed, wherein the mass ratio of the inorganic gel A to the inorganic component B is 9: 1; the inorganic gel A comprises the following components in parts by mass: 92 parts of deionized water and 8 parts of inorganic gel solution; the inorganic component B comprises the following components in percentage by mass: 20 parts of deionized water, 0.15 part of multifunctional auxiliary agent, 0.15 part of wetting agent, 0.25 part of dispersing agent, 0.3 part of preservative, 0.3 part of defoaming agent, 0.9 part of film-forming auxiliary agent, 12 parts of inorganic silicon resin, 20 parts of potassium silicate, 2 parts of reactant and 1.5 parts of pigment.
The inorganic gel solution in the inorganic gel agent A is a divalent or trivalent metal ion solution, such as a magnesium ion or calcium ion solution.
Further, the dispersing agent is sodium polyphosphate or ammonium polyacrylate, the wetting agent is fatty alcohol sulfosuccinate anionic type, the preservative is isothiazolinone derivatives, the defoaming agent is a defoaming agent mineral oil defoaming agent, the film-forming aid is carbon dodecyl alcohol, the multifunctional aid is 2-amino-2-methyl-1-propanol, the inorganic silicone resin is self-drying resin, potassium silicate is modified stabilized potassium silicate, the reactant is a hydroxyl compound capable of providing a coordination reaction with divalent or trivalent ions, and the pigment is an inorganic pigment.
Further, the divalent or trivalent ions in the inorganic gelling agent A and the hydroxyl compound in the inorganic component B are subjected to coordination reaction to generate a crosslinking compound.
The preparation method of the inorganic multicolor liquid particles comprises the following steps:
s1, preparing an inorganic gel A: weighing deionized water and an inorganic gel solution according to a certain proportion, adding the deionized water and the inorganic gel solution into a mixer, and fully and uniformly mixing to obtain an inorganic reaction gel A;
s2, preparing an inorganic component B: weighing deionized water, a multifunctional additive, a wetting agent, a dispersing agent, a preservative, a defoaming agent, a reactant, a film-forming additive, inorganic silicon resin and potassium silicate according to a proportion, adding the materials into a mixer, fully and uniformly mixing, adding a pigment, and uniformly mixing to obtain an inorganic component B;
s3, preparing inorganic colorful liquid particles: adding the inorganic component B prepared in the step S2 into the inorganic gel A prepared in the step S1, and fully and uniformly mixing; then slicing the uniformly mixed gel to obtain liquid particles; wherein the mass ratio of the inorganic gel A to the inorganic component B is 9: 1.
Example 3
An inorganic magic color liquid particle comprises an inorganic gel A and an inorganic component B which are uniformly mixed, wherein the mass ratio of the inorganic gel A to the inorganic component B is 10: 1; the inorganic gel A comprises the following components in parts by mass: 95 parts of deionized water and 10 parts of inorganic gel solution; the inorganic component B comprises the following components in percentage by mass: 35 parts of deionized water, 0.2 part of multifunctional auxiliary agent, 2 parts of wetting agent, 0.3 part of dispersing agent, 0.4 part of preservative, 0.4 part of defoaming agent, 1.2 parts of film-forming auxiliary agent, 15 parts of inorganic silicon resin, 25 parts of potassium silicate, 3 parts of reactant and 2 parts of pigment.
The inorganic gel solution in the inorganic gel agent A is a divalent or trivalent metal ion solution, such as a magnesium ion or calcium ion solution.
Further, the dispersing agent is sodium polyphosphate or ammonium polyacrylate, the wetting agent is fatty alcohol sulfosuccinate anionic type, the preservative is isothiazolinone derivatives, the defoaming agent is a defoaming agent mineral oil defoaming agent, the film-forming aid is carbon dodecyl alcohol, the multifunctional aid is 2-amino-2-methyl-1-propanol, the inorganic silicone resin is self-drying resin, potassium silicate is modified stabilized potassium silicate, the reactant is a hydroxyl compound capable of providing a coordination reaction with divalent or trivalent ions, and the pigment is an inorganic pigment.
Further, the divalent or trivalent ions in the inorganic gelling agent A and the hydroxyl compound in the inorganic component B are subjected to coordination reaction to generate a crosslinking compound.
The preparation method of the inorganic multicolor liquid particles comprises the following steps:
s1, preparing an inorganic gel A: weighing deionized water and an inorganic gel solution according to a certain proportion, adding the deionized water and the inorganic gel solution into a mixer, and fully and uniformly mixing to obtain an inorganic reaction gel A;
s2, preparing an inorganic component B: weighing deionized water, a multifunctional additive, a wetting agent, a dispersing agent, a preservative, a defoaming agent, a reactant, a film-forming additive, inorganic silicon resin and potassium silicate according to a proportion, adding the materials into a mixer, fully and uniformly mixing, adding a pigment, and uniformly mixing to obtain an inorganic component B;
s3, preparing inorganic colorful liquid particles: adding the inorganic component B prepared in the step S2 into the inorganic gel A prepared in the step S1, and fully and uniformly mixing; then slicing the uniformly mixed gel to obtain liquid particles; wherein the mass ratio of the inorganic gel A to the inorganic component B is 10: 1.
Example 4
An inorganic magic color liquid particle comprises an inorganic gel A and an inorganic component B which are uniformly mixed, wherein the mass ratio of the inorganic gel A to the inorganic component B is 9: 1; the inorganic gel A comprises the following components in parts by mass: 90 parts of deionized water and 8 parts of inorganic gel solution; the inorganic component B comprises the following components in percentage by mass: 30 parts of deionized water, 0.2 part of multifunctional auxiliary agent, 0.1 part of wetting agent, 0.3 part of dispersing agent, 0.3 part of preservative, 0.2 part of defoaming agent, 1 part of film-forming auxiliary agent, 15 parts of inorganic silicon resin, 20 parts of potassium silicate, 2 parts of reactant and 2 parts of pigment.
The inorganic gel solution in the inorganic gel agent A is a divalent or trivalent metal ion solution, such as a magnesium ion or calcium ion solution.
Further, the dispersing agent is sodium polyphosphate or ammonium polyacrylate, the wetting agent is fatty alcohol sulfosuccinate anionic type, the preservative is isothiazolinone derivatives, the defoaming agent is a defoaming agent mineral oil defoaming agent, the film-forming aid is carbon dodecyl alcohol, the multifunctional aid is 2-amino-2-methyl-1-propanol, the inorganic silicone resin is self-drying resin, potassium silicate is modified stabilized potassium silicate, the reactant is a hydroxyl compound capable of providing a coordination reaction with divalent or trivalent ions, and the pigment is an inorganic pigment.
Further, the divalent or trivalent ions in the inorganic gelling agent A and the hydroxyl compound in the inorganic component B are subjected to coordination reaction to generate a crosslinking compound.
The preparation method of the inorganic multicolor liquid particles comprises the following steps:
s1, preparing an inorganic gel A: weighing deionized water and an inorganic gel solution according to a certain proportion, adding the deionized water and the inorganic gel solution into a mixer, and fully and uniformly mixing to obtain an inorganic reaction gel A;
s2, preparing an inorganic component B: weighing deionized water, a multifunctional additive, a wetting agent, a dispersing agent, a preservative, a defoaming agent, a reactant, a film-forming additive, inorganic silicon resin and potassium silicate according to a proportion, adding the materials into a mixer, fully and uniformly mixing, adding a pigment, and uniformly mixing to obtain an inorganic component B;
s3, preparing inorganic colorful liquid particles: adding the inorganic component B prepared in the step S2 into the inorganic gel A prepared in the step S1, and fully and uniformly mixing; then slicing the uniformly mixed gel to obtain liquid particles; wherein the mass ratio of the inorganic gel A to the inorganic component B is 9: 1.
It will be appreciated by those of ordinary skill in the art that the embodiments described herein are intended to assist the reader in understanding the principles of the invention and are to be construed as being without limitation to such specifically recited embodiments and examples. Those skilled in the art can make various other specific changes and combinations based on the teachings of the present invention without departing from the spirit of the invention, and these changes and combinations are within the scope of the invention.
Claims (5)
1. The inorganic magic color liquid particle is characterized by comprising an inorganic gel agent A and an inorganic component B which are uniformly mixed, wherein the mass ratio of the inorganic gel agent A to the inorganic component B is 8: 1-10: 1; the inorganic gel A comprises the following components in parts by mass: 90-95 parts of deionized water and 5-10 parts of inorganic gel solution; the inorganic component B comprises the following components in percentage by mass: 10-35 parts of deionized water, 0.1-0.2 part of multifunctional auxiliary agent, 0.1-0.2 part of wetting agent, 0.2-0.3 part of dispersing agent, 0.2-0.4 part of preservative, 0.2-0.4 part of defoaming agent, 0.6-1.2 parts of film-forming auxiliary agent, 10-15 parts of inorganic silicon resin, 15-25 parts of potassium silicate, 1-3 parts of reactant and 1-2 parts of pigment.
2. The inorganic magic color liquid particle as claimed in claim 1, wherein the inorganic gel solution in the inorganic gel agent A is a divalent or trivalent metal ion solution.
3. The inorganic magic color liquid particle as claimed in claim 2, wherein the dispersant is sodium polyphosphate or ammonium polyacrylate, the wetting agent is fatty alcohol sulfosuccinate anion, the preservative is isothiazolinone derivative, the defoamer is mineral oil defoamer, the film forming aid is carbon dodecyl alcohol, the multifunctional aid is 2-amino-2-methyl-1-propanol, the inorganic silicone resin is self-drying resin, the potassium silicate is modified stabilized potassium silicate, the reactant is hydroxyl compound capable of providing coordination reaction with divalent or trivalent ion, and the pigment is inorganic pigment.
4. The liquid crystal of claim 3, wherein the divalent or trivalent ion of the inorganic gelling agent A is coordinated with the hydroxyl compound of the inorganic component B to form a crosslinked compound.
5. The method for preparing inorganic magic color liquid particle as claimed in any one of claims 1 to 4, characterized by comprising the following steps:
s1, preparing an inorganic gel A: weighing deionized water and an inorganic gel solution according to a certain proportion, adding the deionized water and the inorganic gel solution into a mixer, and fully and uniformly mixing to obtain an inorganic reaction gel A;
s2, preparing an inorganic component B: weighing deionized water, a multifunctional additive, a wetting agent, a dispersing agent, a preservative, a defoaming agent, a reactant, a film-forming additive, inorganic silicon resin and potassium silicate according to a proportion, adding the materials into a mixer, fully and uniformly mixing, adding a pigment, and uniformly mixing to obtain an inorganic component B;
s3, preparing inorganic colorful liquid particles: adding the inorganic component B prepared in the step S2 into the inorganic gel A prepared in the step S1, and fully and uniformly mixing; then slicing the uniformly mixed gel to obtain liquid particles; wherein the mass ratio of the inorganic gel A to the inorganic component B is 8: 1-10: 1.
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2021
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| CN108264789A (en) * | 2017-12-29 | 2018-07-10 | 上海墙特节能材料有限公司 | A kind of water-in-water multicolor coating and preparation method thereof |
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Application publication date: 20210518 |