CN112662492A - Artemisia argyi degerming perfumed soap - Google Patents
Artemisia argyi degerming perfumed soap Download PDFInfo
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- CN112662492A CN112662492A CN202011603903.0A CN202011603903A CN112662492A CN 112662492 A CN112662492 A CN 112662492A CN 202011603903 A CN202011603903 A CN 202011603903A CN 112662492 A CN112662492 A CN 112662492A
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- 239000000344 soap Substances 0.000 title claims abstract description 64
- 241001435059 Artemisia argyi Species 0.000 title description 2
- 235000010894 Artemisia argyi Nutrition 0.000 title description 2
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 57
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 52
- 235000003261 Artemisia vulgaris Nutrition 0.000 claims abstract description 42
- 235000009051 Ambrosia paniculata var. peruviana Nutrition 0.000 claims abstract description 39
- 235000003097 Artemisia absinthium Nutrition 0.000 claims abstract description 39
- 235000017731 Artemisia dracunculus ssp. dracunculus Nutrition 0.000 claims abstract description 39
- 239000001138 artemisia absinthium Substances 0.000 claims abstract description 39
- KDYFGRWQOYBRFD-UHFFFAOYSA-N succinic acid Chemical compound OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 claims abstract description 39
- 240000004307 Citrus medica Species 0.000 claims abstract description 31
- 239000004094 surface-active agent Substances 0.000 claims abstract description 31
- 235000013399 edible fruits Nutrition 0.000 claims abstract description 29
- 239000001522 artemisia absinthium l. herb extract Substances 0.000 claims abstract description 20
- 229940119569 wormwood extract Drugs 0.000 claims abstract description 20
- 235000019864 coconut oil Nutrition 0.000 claims abstract description 17
- 239000003240 coconut oil Substances 0.000 claims abstract description 17
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims abstract description 13
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 13
- 239000011734 sodium Substances 0.000 claims abstract description 13
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims abstract description 13
- 239000004711 α-olefin Substances 0.000 claims abstract description 13
- 239000002994 raw material Substances 0.000 claims abstract description 12
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 8
- 230000002087 whitening effect Effects 0.000 claims abstract description 7
- 240000001851 Artemisia dracunculus Species 0.000 claims abstract 11
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical group O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 28
- 238000002156 mixing Methods 0.000 claims description 22
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 20
- 238000003756 stirring Methods 0.000 claims description 18
- 238000009210 therapy by ultrasound Methods 0.000 claims description 18
- 238000001035 drying Methods 0.000 claims description 17
- 239000004744 fabric Substances 0.000 claims description 17
- 239000000706 filtrate Substances 0.000 claims description 16
- 238000001914 filtration Methods 0.000 claims description 16
- 239000000843 powder Substances 0.000 claims description 16
- 238000007873 sieving Methods 0.000 claims description 16
- 238000010298 pulverizing process Methods 0.000 claims description 14
- 239000004408 titanium dioxide Substances 0.000 claims description 14
- 238000002360 preparation method Methods 0.000 claims description 12
- 230000001954 sterilising effect Effects 0.000 claims description 11
- 239000007788 liquid Substances 0.000 claims description 10
- 238000001816 cooling Methods 0.000 claims description 9
- 238000010438 heat treatment Methods 0.000 claims description 9
- 238000007789 sealing Methods 0.000 claims description 9
- 239000008149 soap solution Substances 0.000 claims description 8
- OQWBLDGADMLCSE-UHFFFAOYSA-N 2-[2-[4-phenyl-1-[2-(2-sulfophenyl)ethenyl]cyclohexa-2,4-dien-1-yl]ethenyl]benzenesulfonic acid Chemical group OS(=O)(=O)C1=CC=CC=C1C=CC1(C=CC=2C(=CC=CC=2)S(O)(=O)=O)C=CC(C=2C=CC=CC=2)=CC1 OQWBLDGADMLCSE-UHFFFAOYSA-N 0.000 claims description 4
- 238000000034 method Methods 0.000 claims description 3
- 238000004659 sterilization and disinfection Methods 0.000 claims description 2
- KJIOQYGWTQBHNH-UHFFFAOYSA-N undecanol Chemical compound CCCCCCCCCCCO KJIOQYGWTQBHNH-UHFFFAOYSA-N 0.000 abstract description 11
- 238000005187 foaming Methods 0.000 abstract description 4
- 230000000844 anti-bacterial effect Effects 0.000 abstract description 3
- 239000002131 composite material Substances 0.000 abstract description 3
- 230000000694 effects Effects 0.000 abstract description 3
- 239000000126 substance Substances 0.000 abstract description 3
- 230000009044 synergistic interaction Effects 0.000 abstract description 2
- 240000006891 Artemisia vulgaris Species 0.000 description 31
- 238000000605 extraction Methods 0.000 description 14
- 229910052799 carbon Inorganic materials 0.000 description 12
- 230000000052 comparative effect Effects 0.000 description 6
- 238000012360 testing method Methods 0.000 description 4
- 238000004140 cleaning Methods 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- 241000196324 Embryophyta Species 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 206010000234 Abortion spontaneous Diseases 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- 206010011224 Cough Diseases 0.000 description 1
- 241000628997 Flos Species 0.000 description 1
- 206010020751 Hypersensitivity Diseases 0.000 description 1
- 206010061218 Inflammation Diseases 0.000 description 1
- 239000004721 Polyphenylene oxide Substances 0.000 description 1
- 150000001447 alkali salts Chemical class 0.000 description 1
- 208000026935 allergic disease Diseases 0.000 description 1
- 230000007815 allergy Effects 0.000 description 1
- 239000003945 anionic surfactant Substances 0.000 description 1
- 208000006673 asthma Diseases 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000000740 bleeding effect Effects 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 238000004332 deodorization Methods 0.000 description 1
- 239000003599 detergent Substances 0.000 description 1
- 230000003467 diminishing effect Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000001804 emulsifying effect Effects 0.000 description 1
- 239000003925 fat Substances 0.000 description 1
- 235000019197 fats Nutrition 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 230000004054 inflammatory process Effects 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 208000015994 miscarriage Diseases 0.000 description 1
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- 230000004048 modification Effects 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- 235000012830 plain croissants Nutrition 0.000 description 1
- 229920000570 polyether Polymers 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 235000002639 sodium chloride Nutrition 0.000 description 1
- 208000000995 spontaneous abortion Diseases 0.000 description 1
- 238000011282 treatment Methods 0.000 description 1
- 125000002948 undecyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Landscapes
- Detergent Compositions (AREA)
Abstract
The invention discloses a wormwood degerming soap. The composite material comprises the following raw materials in parts by weight: 30-80 parts of coconut oil, 8-18 parts of sodium hydroxide, 15-35 parts of water, 5-18 parts of wormwood extract, 5-18 parts of citron fruit extract, 3-5 parts of surfactant and 0.5-2 parts of whitening agent. The wormwood degerming perfumed soap adopts the wormwood extract and the citron fruit extract as bactericidal substances, and has the effect of keeping clothes whiteness. The foaming power of the degerming soap is improved by adopting the alpha-olefin sodium sulfonate and the undecanol polyether-9 composite surfactant, and the alpha-olefin sodium sulfonate and the undecanol polyether-9 are interacted to realize synergistic interaction.
Description
Technical Field
The invention belongs to the technical field of soap preparation, and particularly relates to a wormwood degerming soap and a preparation method thereof.
Background
The toilet soap is a widely accepted personal cleaning product, has strong cleaning capability and low price, and becomes a necessity for life of people. Toilet soaps are alkali salts of pH 9.5-10 consisting of fats, oils and salts, the simplest anionic surfactants, which cleanse the skin surface material by emulsifying it by forming soap salts. With the improvement of living standard of people, not only the function of cleaning skin but also some new functions of beauty treatment, sterilization, deodorization, etc. are required.
The mugwort is a perennial herb or a slightly semi-shrub plant, and the plant has strong fragrance. The whole herb is used as a medicine and has the functions of warming channels, removing dampness, dispelling cold, stopping bleeding, diminishing inflammation, relieving asthma, relieving cough, preventing miscarriage, resisting allergy and the like. The mugwort leaves are dried in the sun and smashed to obtain mugwort floss which is used for moxibustion and can also be used as a raw material of inkpad. It has been reported that moxa is added to soap raw materials for preparing soap to prepare soap with bactericidal effect.
The citron belongs to shrubs or small trees with irregular branches, and the fruits of the citron are citron fruits which are oval, nearly round or spindle-shaped with two narrow ends, the weight of the citron fruits can reach 2000 g, the peels are light yellow, coarse and difficult to peel, the pulp is colorless, nearly transparent or light creamy yellow, and the citron is crisp and tasty and sour or slightly sweet.
At present, no report exists that the extract essence of wormwood and citron fruit is added into soap to prepare functional perfumed soap.
Disclosure of Invention
The invention aims to provide a wormwood degerming soap and a preparation method thereof.
The wormwood degerming soap comprises the following raw materials in parts by weight: 30-80 parts of coconut oil, 8-18 parts of sodium hydroxide, 15-35 parts of water, 5-18 parts of wormwood extract, 5-18 parts of citron fruit extract, 3-5 parts of surfactant and 0.5-2 parts of whitening agent.
The extraction method of the wormwood extract comprises the following steps: pulverizing folium Artemisiae Argyi, sieving with 60-80 mesh sieve, mixing 100-150g folium Artemisiae Argyi powder with 1200-1600mL water, ultrasonic treating for 35-55min, filtering with filter cloth, decolorizing with activated carbon to obtain decolorized filtrate, and concentrating under reduced pressure at 50-80 deg.C until the water content is less than 20% to obtain folium Artemisiae Argyi extract.
The ultrasonic treatment conditions are as follows: the ultrasonic temperature is 60-75 ℃, the ultrasonic power is 150-220W, and the ultrasonic frequency is 15-25 kHz.
The extraction method of the citron fruit extract comprises the following steps: drying citron fruits, crushing, sieving by a 60-80 mesh sieve, uniformly mixing 100-150g of citron fruit powder with 1000-1500mL of water, carrying out ultrasonic treatment for 30-45min, filtering by using filter cloth, decoloring by using activated carbon to obtain decolored filtrate, and concentrating under reduced pressure at 50-80 ℃ until the water content is less than 20% to obtain the citron fruit extract.
The ultrasonic treatment conditions are as follows: the ultrasonic temperature is 60-70 ℃, the ultrasonic power is 150-.
The surfactant is prepared from alpha-olefin sodium sulfonate and undecanol polyether-9 according to a mass ratio of 1: 1 mixed surfactant.
The whitening agent is titanium dioxide or 4, 4-bis (2-sulfostyryl) -1, 1-biphenyl.
The preparation method of the wormwood sterilizing perfumed soap comprises the following steps:
(1) according to the parts by weight, 8-18 parts of sodium hydroxide and 15-35 parts of water are taken and evenly mixed;
(2) heating to 65-85 deg.C, adding 30-80 parts of oleum Cocois under stirring, and reacting for 25-35 min;
(3) cooling to 45-55 deg.C, adding folium Artemisiae Argyi extract 5-18 parts, fructus Citri extract 5-18 parts, surfactant 3-5 parts, and whitening agent 0.5-2 parts, stirring for 10-20min to obtain mixed soap solution;
(4) pouring the mixed soap liquid into a mold, sealing, standing at 30-40 deg.C for 24-48 hr, demolding, and drying at 40-50 deg.C for 4-8 hr to obtain the wormwood sterilized soap.
The invention has the beneficial effects that: the wormwood degerming perfumed soap adopts the wormwood extract and the citron fruit extract as bactericidal substances, and has the effect of keeping clothes whiteness. The foaming power of the degerming soap is improved by adopting the alpha-olefin sodium sulfonate and the undecanol polyether-9 composite surfactant, and the alpha-olefin sodium sulfonate and the undecanol polyether-9 are interacted to realize synergistic interaction.
Detailed Description
In order that the invention may be more fully understood, reference will now be made to the following description. This invention may, however, be embodied in many different forms and should not be construed as limited to the embodiments set forth herein. Rather, these embodiments are provided so that this disclosure will be thorough and complete.
Example 1
The wormwood degerming soap comprises the following raw materials in parts by weight: 50 parts of coconut oil, 12 parts of sodium hydroxide, 25 parts of water, 12 parts of wormwood extract, 12 parts of citron fruit extract, 4 parts of surfactant and 1 part of titanium dioxide; the surfactant is prepared from alpha-olefin sodium sulfonate and undecanol polyether-9 according to a mass ratio of 1: 1 mixed surfactant.
The extraction method of the wormwood extract comprises the following steps: pulverizing folium Artemisiae Argyi, sieving with 70 mesh sieve, mixing 120g folium Artemisiae Argyi powder and 1400mL water, ultrasonic treating for 45min, filtering with filter cloth, decolorizing with active carbon to obtain decolorized filtrate, and concentrating under reduced pressure at 70 deg.C until the water content is less than 20% to obtain folium Artemisiae Argyi extract; the ultrasonic treatment conditions are as follows: the ultrasonic temperature is 70 ℃, the ultrasonic power is 180W, and the ultrasonic frequency is 20 kHz.
The extraction method of the citron fruit extract comprises the following steps: sun drying fructus Citri, pulverizing, sieving with 70 mesh sieve, mixing 120g fructus Citri powder and 1300mL water, ultrasonic treating for 35min, filtering with filter cloth, decolorizing with active carbon to obtain decolorized filtrate, and concentrating under reduced pressure at 70 deg.C until the water content is less than 20% to obtain fructus Citri extract. The ultrasonic treatment conditions are as follows: the ultrasonic temperature is 65 ℃, the ultrasonic power is 180W, and the ultrasonic frequency is 15 kHz.
The preparation method of the wormwood degerming soap comprises the following steps:
(1) according to the weight portion, taking 12 portions of sodium hydroxide and 25 portions of water, and uniformly mixing;
(2) heating to 70 ℃, adding 50 parts of coconut oil while stirring, and reacting for 30 min;
(3) cooling to 50 deg.C, adding folium Artemisiae Argyi extract 12 parts, fructus Citri extract 12 parts, surfactant 4 parts, and titanium dioxide 1 parts, stirring for 15min to obtain mixed soap solution;
(4) pouring the mixed soap liquid into a mould, sealing, standing at 35 ℃ for 36 hours, demoulding, and drying at 45 ℃ for 6 hours to obtain the wormwood sterilizing soap.
Example 2
The wormwood degerming soap comprises the following raw materials in parts by weight: 35 parts of coconut oil, 10 parts of sodium hydroxide, 16 parts of water, 6 parts of wormwood extract, 6 parts of citron fruit extract, 3 parts of surfactant and 0.5 part of 4, 4-bis (2-sulfostyryl) -1, 1-biphenyl; the surfactant is prepared from alpha-olefin sodium sulfonate and undecanol polyether-9 according to a mass ratio of 1: 1 mixed surfactant.
The extraction method of the wormwood extract comprises the following steps: pulverizing folium Artemisiae Argyi, sieving with 60 mesh sieve, mixing 100g folium Artemisiae Argyi powder and 1200mL water, ultrasonic treating for 35min, filtering with filter cloth, decolorizing with active carbon to obtain decolorized filtrate, and concentrating under reduced pressure at 60 deg.C until the water content is less than 20% to obtain folium Artemisiae Argyi extract; the ultrasonic treatment conditions are as follows: the ultrasonic temperature is 65 ℃, the ultrasonic power is 150W, and the ultrasonic frequency is 15 kHz.
The extraction method of the citron fruit extract comprises the following steps: sun-drying fructus Citri, pulverizing, sieving with 60 mesh sieve, mixing 100g fructus Citri powder and 1000mL water, ultrasonic treating for 30min, filtering with filter cloth, decolorizing with active carbon to obtain decolorized filtrate, and concentrating under reduced pressure at 50 deg.C until the water content is less than 20% to obtain fructus Citri extract; the ultrasonic treatment conditions are as follows: the ultrasonic temperature is 60 ℃, the ultrasonic power is 150W, and the ultrasonic frequency is 13 kHz.
The preparation method of the wormwood degerming soap comprises the following steps:
(1) according to the weight portion, 10 portions of sodium hydroxide and 16 portions of water are taken and evenly mixed;
(2) heating to 65 ℃, adding 35 parts of coconut oil while stirring, and reacting for 28 min;
(3) cooling to 45 deg.C, adding folium Artemisiae Argyi extract 6 parts, fructus Citri extract 6 parts, surfactant 3 parts, and 4, 4-bis (2-sulfostyryl) -1, 1-biphenyl 0.5 parts, stirring for 12min to obtain mixed soap solution;
(4) pouring the mixed soap liquid into a mould, sealing, standing for 24 hours at 30 ℃, demoulding, and drying for 8 hours at 40 ℃ to obtain the wormwood sterilizing soap.
Example 3
The wormwood degerming soap comprises the following raw materials in parts by weight: 80 parts of coconut oil, 18 parts of sodium hydroxide, 35 parts of water, 16 parts of wormwood extract, 16 parts of citron fruit extract, 5 parts of surfactant and 2 parts of titanium dioxide; the surfactant is prepared from alpha-olefin sodium sulfonate and undecanol polyether-9 according to a mass ratio of 1: 1 mixed surfactant.
The extraction method of the wormwood extract comprises the following steps: pulverizing folium Artemisiae Argyi, sieving with 80 mesh sieve, mixing 150g folium Artemisiae Argyi powder and 1600mL water, ultrasonic treating for 53min, filtering with filter cloth, decolorizing with active carbon to obtain decolorized filtrate, and concentrating under reduced pressure at 80 deg.C until the water content is less than 20% to obtain folium Artemisiae Argyi extract; the ultrasonic treatment conditions are as follows: the ultrasonic temperature is 75 ℃, the ultrasonic power is 220W, and the ultrasonic frequency is 25 kHz.
The extraction method of the citron fruit extract comprises the following steps: sun-drying fructus Citri, pulverizing, sieving with 80 mesh sieve, mixing 150g fructus Citri powder and 1500mL water, ultrasonic treating for 45min, filtering with filter cloth, decolorizing with active carbon to obtain decolorized filtrate, and concentrating under reduced pressure at 80 deg.C until the water content is less than 20% to obtain fructus Citri extract; the ultrasonic treatment conditions are as follows: the ultrasonic temperature is 70 ℃, the ultrasonic power is 200W, and the ultrasonic frequency is 20 kHz.
The preparation method of the wormwood degerming soap comprises the following steps:
(1) taking 18 parts of sodium hydroxide and 35 parts of water according to parts by weight, and uniformly mixing;
(2) heating to 85 ℃, adding 80 parts of coconut oil while stirring, and reacting for 35 min;
(3) cooling to 55 deg.C, adding folium Artemisiae Argyi extract 16 parts, fructus Citri extract 16 parts, surfactant 5 parts, and titanium dioxide 2 parts, and stirring for 20min to obtain mixed soap solution;
(4) pouring the mixed soap liquid into a mould, sealing, standing for 48 hours at 40 ℃, demoulding, and drying for 8 hours at 50 ℃ to obtain the wormwood sterilizing soap.
Comparative example 1
The wormwood degerming soap comprises the following raw materials in parts by weight: 50 parts of coconut oil, 12 parts of sodium hydroxide, 25 parts of water, 12 parts of wormwood extract, 12 parts of citron fruit extract, 4 parts of alpha-olefin sodium sulfonate and 1 part of titanium dioxide.
The extraction method of the wormwood extract comprises the following steps: pulverizing folium Artemisiae Argyi, sieving with 70 mesh sieve, mixing 120g folium Artemisiae Argyi powder and 1400mL water, ultrasonic treating for 45min, filtering with filter cloth, decolorizing with active carbon to obtain decolorized filtrate, and concentrating under reduced pressure at 70 deg.C until the water content is less than 20% to obtain folium Artemisiae Argyi extract; the ultrasonic treatment conditions are as follows: the ultrasonic temperature is 70 ℃, the ultrasonic power is 180W, and the ultrasonic frequency is 20 kHz.
The extraction method of the citron fruit extract comprises the following steps: sun drying fructus Citri, pulverizing, sieving with 70 mesh sieve, mixing 120g fructus Citri powder and 1300mL water, ultrasonic treating for 35min, filtering with filter cloth, decolorizing with active carbon to obtain decolorized filtrate, and concentrating under reduced pressure at 70 deg.C until the water content is less than 20% to obtain fructus Citri extract. The ultrasonic treatment conditions are as follows: the ultrasonic temperature is 65 ℃, the ultrasonic power is 180W, and the ultrasonic frequency is 15 kHz.
The preparation method of the wormwood degerming soap comprises the following steps:
(1) according to the weight portion, taking 12 portions of sodium hydroxide and 25 portions of water, and uniformly mixing;
(2) heating to 70 ℃, adding 50 parts of coconut oil while stirring, and reacting for 30 min;
(3) cooling to 50 deg.C, adding folium Artemisiae Argyi extract 12 parts, fructus Citri extract 12 parts, sodium alpha-olefin sulfonate 4 parts, and titanium dioxide 1 part, stirring for 15min to obtain mixed soap solution;
(4) pouring the mixed soap liquid into a mould, sealing, standing at 35 ℃ for 36 hours, demoulding, and drying at 45 ℃ for 6 hours to obtain the wormwood sterilizing soap.
Comparative example 2
The wormwood degerming soap comprises the following raw materials in parts by weight: 50 parts of coconut oil, 12 parts of sodium hydroxide, 25 parts of water, 12 parts of wormwood extract, 12 parts of citron fruit extract, 94 parts of undecanol polyether and 1 part of titanium dioxide.
The extraction method of the wormwood extract comprises the following steps: pulverizing folium Artemisiae Argyi, sieving with 70 mesh sieve, mixing 120g folium Artemisiae Argyi powder and 1400mL water, ultrasonic treating for 45min, filtering with filter cloth, decolorizing with active carbon to obtain decolorized filtrate, and concentrating under reduced pressure at 70 deg.C until the water content is less than 20% to obtain folium Artemisiae Argyi extract; the ultrasonic treatment conditions are as follows: the ultrasonic temperature is 70 ℃, the ultrasonic power is 180W, and the ultrasonic frequency is 20 kHz.
The extraction method of the citron fruit extract comprises the following steps: sun drying fructus Citri, pulverizing, sieving with 70 mesh sieve, mixing 120g fructus Citri powder and 1300mL water, ultrasonic treating for 35min, filtering with filter cloth, decolorizing with active carbon to obtain decolorized filtrate, and concentrating under reduced pressure at 70 deg.C until the water content is less than 20% to obtain fructus Citri extract. The ultrasonic treatment conditions are as follows: the ultrasonic temperature is 65 ℃, the ultrasonic power is 180W, and the ultrasonic frequency is 15 kHz.
The preparation method of the wormwood degerming soap comprises the following steps:
(1) according to the weight portion, taking 12 portions of sodium hydroxide and 25 portions of water, and uniformly mixing;
(2) heating to 70 ℃, adding 50 parts of coconut oil while stirring, and reacting for 30 min;
(3) cooling to 50 deg.C, adding folium Artemisiae Argyi extract 12 parts, fructus Citri extract 12 parts, undecyl polyether-94 parts, and titanium dioxide 1 parts, stirring for 15min to obtain mixed soap solution;
(4) pouring the mixed soap liquid into a mould, sealing, standing at 35 ℃ for 36 hours, demoulding, and drying at 45 ℃ for 6 hours to obtain the wormwood sterilizing soap.
Comparative example 3
The wormwood degerming soap comprises the following raw materials in parts by weight: 50 parts of coconut oil, 12 parts of sodium hydroxide, 25 parts of water, 12 parts of citron fruit extract, 4 parts of surfactant and 1 part of titanium dioxide; the surfactant is prepared from alpha-olefin sodium sulfonate and undecanol polyether-9 according to a mass ratio of 1: 1 mixed surfactant.
The extraction method of the citron fruit extract comprises the following steps: sun drying fructus Citri, pulverizing, sieving with 70 mesh sieve, mixing 120g fructus Citri powder and 1300mL water, ultrasonic treating for 35min, filtering with filter cloth, decolorizing with active carbon to obtain decolorized filtrate, and concentrating under reduced pressure at 70 deg.C until the water content is less than 20% to obtain fructus Citri extract. The ultrasonic treatment conditions are as follows: the ultrasonic temperature is 65 ℃, the ultrasonic power is 180W, and the ultrasonic frequency is 15 kHz.
The preparation method of the wormwood degerming soap comprises the following steps:
(1) according to the weight portion, taking 12 portions of sodium hydroxide and 25 portions of water, and uniformly mixing;
(2) heating to 70 ℃, adding 50 parts of coconut oil while stirring, and reacting for 30 min;
(3) cooling to 50 deg.C, adding fructus Citri extract 12 parts, surfactant 4 parts, and titanium dioxide 1 parts, stirring for 15min to obtain mixed soap solution;
(4) pouring the mixed soap liquid into a mould, sealing, standing at 35 ℃ for 36 hours, demoulding, and drying at 45 ℃ for 6 hours to obtain the wormwood sterilizing soap.
Comparative example 4
The wormwood degerming soap comprises the following raw materials in parts by weight: 50 parts of coconut oil, 12 parts of sodium hydroxide, 25 parts of water, 12 parts of wormwood extract, 4 parts of surfactant and 1 part of titanium dioxide; the surfactant is prepared from alpha-olefin sodium sulfonate and undecanol polyether-9 according to a mass ratio of 1: 1 mixed surfactant.
The extraction method of the wormwood extract comprises the following steps: pulverizing folium Artemisiae Argyi, sieving with 70 mesh sieve, mixing 120g folium Artemisiae Argyi powder and 1400mL water, ultrasonic treating for 45min, filtering with filter cloth, decolorizing with active carbon to obtain decolorized filtrate, and concentrating under reduced pressure at 70 deg.C until the water content is less than 20% to obtain folium Artemisiae Argyi extract; the ultrasonic treatment conditions are as follows: the ultrasonic temperature is 70 ℃, the ultrasonic power is 180W, and the ultrasonic frequency is 20 kHz.
The preparation method of the wormwood degerming soap comprises the following steps:
(1) according to the weight portion, taking 12 portions of sodium hydroxide and 25 portions of water, and uniformly mixing;
(2) heating to 70 ℃, adding 50 parts of coconut oil while stirring, and reacting for 30 min;
(3) cooling to 50 ℃, adding 12 parts of wormwood extract, 4 parts of surfactant and 1 part of titanium dioxide, and stirring for 15min to obtain mixed soap liquid;
(4) pouring the mixed soap liquid into a mould, sealing, standing at 35 ℃ for 36 hours, demoulding, and drying at 45 ℃ for 6 hours to obtain the wormwood sterilizing soap.
Experimental example 1: foaming force test
1g of the sterilized soap prepared in examples 1 to 3 and comparative examples 1 to 4 was dissolved in 99g of water to prepare a 1% solution, and the foaming power of the sterilized soap was tested at 25 ℃ according to 5.5 in QB/T2486-2008 laundry soap. The test results are shown in table 1:
TABLE 1
Note: represents P <0.05 compared to the example 1 group.
Experimental example 2: washing effect test
The solutions prepared in examples 1 to 3 and comparative examples 1 to 4 were prepared to 1000ppm, and the solutions were prepared according to "research on application of anti-redeposition agents to laundry detergents such as siemens and croissant", science of daily chemicals, 2011, 34 (10): the method in 21 was tested to test the whiteness of the white cotton knitted fabric and calculate the whiteness maintenance value.
TABLE 2
Note: represents P <0.05 compared to the example 1 group.
The above-mentioned embodiments only express several embodiments of the present invention, and the description thereof is more specific and detailed, but not construed as limiting the scope of the invention. It should be noted that, for a person skilled in the art, several variations and modifications can be made without departing from the inventive concept, which falls within the scope of the present invention. Therefore, the protection scope of the present patent shall be subject to the appended claims.
Claims (8)
1. The wormwood degerming soap is characterized by comprising the following raw materials in parts by weight: 30-80 parts of coconut oil, 8-18 parts of sodium hydroxide, 15-35 parts of water, 5-18 parts of wormwood extract, 5-18 parts of citron fruit extract, 3-5 parts of surfactant and 0.5-2 parts of whitening agent.
2. The wormwood sterilization soap according to claim 1, wherein the wormwood extract is extracted by a method comprising: pulverizing folium Artemisiae Argyi, sieving with 60-80 mesh sieve, mixing 100-150g folium Artemisiae Argyi powder with 1200-1600mL water, ultrasonic treating for 35-55min, filtering with filter cloth, decolorizing with activated carbon to obtain decolorized filtrate, and concentrating under reduced pressure at 50-80 deg.C until the water content is less than 20% to obtain folium Artemisiae Argyi extract.
3. The wormwood degerming soap according to claims 1-2, wherein the ultrasonic treatment conditions are as follows: the ultrasonic temperature is 60-75 ℃, the ultrasonic power is 150-220W, and the ultrasonic frequency is 15-25 kHz.
4. The wormwood degerming soap according to claim 1, wherein the citron fruit extract is extracted by a method comprising: drying citron fruits, crushing, sieving by a 60-80 mesh sieve, uniformly mixing 100-150g of citron fruit powder with 1000-1500mL of water, carrying out ultrasonic treatment for 30-45min, filtering by using filter cloth, decoloring by using activated carbon to obtain decolored filtrate, and concentrating under reduced pressure at 50-80 ℃ until the water content is less than 20% to obtain the citron fruit extract.
5. The wormwood degerming soap according to claim 4, wherein the ultrasonic treatment conditions are as follows: the ultrasonic temperature is 60-70 ℃, the ultrasonic power is 150-.
6. The wormwood degerming soap according to claim 1, wherein the surfactant is sodium alpha-olefin sulfonate and undecaneth-9 in a mass ratio of 1: 1 mixed surfactant.
7. The wormwood degerming soap according to claim 1, wherein the whitening agent is titanium dioxide or 4, 4-bis (2-sulfostyryl) -1, 1-biphenyl.
8. The preparation method of the wormwood sterilizing soap as claimed in claim 1, which is characterized by comprising the following steps:
(1) according to the parts by weight, 8-18 parts of sodium hydroxide and 15-35 parts of water are taken and evenly mixed;
(2) heating to 65-85 deg.C, adding 30-80 parts of oleum Cocois under stirring, and reacting for 25-35 min;
(3) cooling to 45-55 deg.C, adding folium Artemisiae Argyi extract 5-18 parts, fructus Citri extract 5-18 parts, surfactant 3-5 parts, and whitening agent 0.5-2 parts, stirring for 10-20min to obtain mixed soap solution;
(4) pouring the mixed soap liquid into a mold, sealing, standing at 30-40 deg.C for 24-48 hr, demolding, and drying at 40-50 deg.C for 4-8 hr to obtain the wormwood sterilized soap.
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Application publication date: 20210416 Assignee: ANHUI LMZ-FANGCAO Co.,Ltd. Assignor: LIANGMIANZHEN (JIANGSU) INDUSTRIAL CO.,LTD. Contract record no.: X2024990000279 Denomination of invention: Mugwort antibacterial soap Granted publication date: 20220208 License type: Exclusive License Record date: 20240611 |