CN112641673A - Aqueous environment-friendly nail polish - Google Patents
Aqueous environment-friendly nail polish Download PDFInfo
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- CN112641673A CN112641673A CN201910956847.XA CN201910956847A CN112641673A CN 112641673 A CN112641673 A CN 112641673A CN 201910956847 A CN201910956847 A CN 201910956847A CN 112641673 A CN112641673 A CN 112641673A
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- polyurethane
- nail polish
- aqueous
- raw material
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/87—Polyurethanes
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q3/00—Manicure or pedicure preparations
- A61Q3/02—Nail coatings
Abstract
The invention provides a water-based environment-friendly nail polish which is characterized by comprising the following raw material components in parts by weight: 60-90 parts by weight of an aqueous polyurethane dispersion, wherein the aqueous polyurethane dispersion comprises polyurethane-35, polyurethane-10, polyurethane-11 and polyurethane-2. The nail polish is an environment-friendly healthy nail polish which has good self-drying performance, lasting appearance, capability of being peeled off and makeup removed in a whole piece and no odor. The invention also provides a preparation method of the nail polish, which is characterized by comprising the following steps: mixing various aqueous polyurethane dispersions according to a formula to obtain a basic dispersion liquid; step two, stirring the basic dispersion liquid, measuring and adjusting the solid content to keep the solid content at 40-45%; and step three, adding other raw material components into the basic dispersion liquid, uniformly mixing, and testing the brushing performance and the raw material stability on the nail.
Description
Technical Field
The invention relates to the technical field of cosmetics, in particular to a water-based environment-friendly nail polish.
Background
The nail polish belongs to the function of beautifying and decorating nails, and the nail polish used by people at present is divided into traditional solvent type nail polish and emerging water-based nail polish.
Conventional solvent-based nail polish products include make-up nail polish and nail polish remover, which contain a large amount of volatile organic solvents and are therefore unsuitable for use in many situations and environmentally unfriendly. In addition, solvent-based nail polishes and nail polish removers tend to yellow and crisp the nails, which can damage the nails. The emerging aqueous nail polish mainly comprises an aqueous film forming agent, a chemical auxiliary agent, a coloring agent and water. Compared with the traditional solvent type nail polish product, the water-based nail polish has the advantages of health and environmental protection, but a part of organic solvent and chemical agent harmful to skin are still used in the components.
With the development of industrial technology, chemical solvent-free aqueous polymer resin dispersions have been widely used in many fields, especially aqueous polyurethane dispersions, which are very suitable for use as raw materials of aqueous nail polish due to their properties of self-drying, film-forming, flexibility, scratch resistance, gloss, safety, etc. The molecular structure of the polyurethane dispersion also contains a plurality of functional groups, and the polyurethane dispersion can provide leveling, wetting, thickening and other performances for a product formula, so that the use of other chemical auxiliary agents in the nail polish formula is reduced, and the safety of the nail polish product is improved.
Disclosure of Invention
The invention aims to solve the problems, adopts a plurality of aqueous polyurethane dispersions with different chemical characteristics as main raw materials, and aims to provide the aqueous environment-friendly nail polish.
The invention provides a water-based environment-friendly nail polish which is characterized by comprising the following raw material components in parts by weight: 60-90 parts by weight of an aqueous polyurethane dispersion, wherein the aqueous polyurethane dispersion comprises polyurethane-35, polyurethane-10, polyurethane-11 and polyurethane-2.
The water-based environment-friendly nail polish provided by the invention can also have the following characteristics: wherein the weight part of polyurethane-35 in the aqueous polyurethane dispersion is 1-30, the weight part of polyurethane-10 is 15-45, the weight part of polyurethane-11 is 15-40, and the weight part of polyurethane-2 is 1-5.
The water-based environment-friendly nail polish provided by the invention can also have the following characteristics: the water-based environment-friendly nail polish also comprises the following raw material components: 2-5 parts of a dispersing agent and 0.2-5 parts of a suspending agent, wherein the dispersing agent is alkyl glycoside, and the suspending agent comprises at least one of carrageenan, xanthan gum and natural cellulose.
The water-based environment-friendly nail polish provided by the invention can also have the following characteristics: the nail polish also comprises the following raw material components: 1 to 15 parts by weight of a colorant.
The water-based environment-friendly nail polish provided by the invention can also have the following characteristics: wherein, various raw material components are included in the catalogue of names of used cosmetic raw materials (2015 edition).
The invention provides a preparation method of water-based environment-friendly nail polish, which is characterized by comprising the following steps of: mixing various aqueous polyurethane dispersions according to a formula to obtain a basic dispersion liquid; step two, stirring the basic dispersion liquid, measuring and adjusting the solid content of the basic dispersion liquid to keep the solid content at 40-45%; and step three, adding other raw material components into the basic dispersion liquid, stirring, uniformly mixing, testing the brushing performance (self-drying, leveling property, stripping property and the like) and the raw material stability on the nail, carrying out micro-adjustment, and then filtering and carrying out microbial inspection.
Action and Effect of the invention
According to the water-based environment-friendly nail polish, the nail polish comprises the following raw material components in parts by weight: 60-90 parts by weight of an aqueous polyurethane dispersion, wherein the aqueous polyurethane dispersion comprises polyurethane-35, polyurethane-10, polyurethane-11 and polyurethane-2, and the polyurethane-10 has the functions of emulsification, dispersion, leveling and film formation; the polyurethane-11 has the functions of film forming, hardness, luster, dispersion, wetting and leveling; the polyurethane-35 has the functions of film forming, hardness, gloss and fastness; the polyurethane-2 has the functions of solubilization, thickening, suspension, rheological property and the like, so that the dispersoid formed by mixing the four kinds of waterborne polyurethane can form a bionic film with the effects of moisturizing and ventilating on the surface of the human nail. Moreover, by adjusting the formula of the 4 polyurethane raw materials, the waterborne polyurethane dispersion coated on the nail can be quickly dried by air at the natural room temperature (25-30 ℃), has no odor, and is suitable for various people to use conveniently in any occasion. The nail polish product has the makeup removing performance that the whole piece can be torn off, is convenient for a user to remove makeup at any time, and does not need to use nail polish remover. The nail polish of the invention has no damage to nails and no pollution to environment.
In conclusion, the nail polish developed by the invention is an odorless environment-friendly healthy nail polish which has good self-drying performance and lasting appearance and can be peeled off and removed integrally.
Detailed Description
The various raw material components related to the invention are recorded in a used cosmetic raw material name catalogue (2015 edition), so that the safety of the product is ensured.
The invention provides a water-based environment-friendly nail polish which comprises the following raw material components in parts by weight: 60-90 parts by weight of an aqueous polyurethane dispersion and water, the water being used to make up 100 parts by weight.
An aqueous polyurethane dispersion comprising: 1-30 parts of polyurethane-35, 15-45 parts of polyurethane-10, 15-40 parts of polyurethane-11 and 1-5 parts of polyurethane-2. The components enable the raw material formula to have good dispersing, leveling, stabilizing, thickening and other properties, and provide the characteristics of self-drying, luster, durability, stripping and the like of film forming of the product.
The water-based environment-friendly nail polish can also comprise 2-5 parts by weight of a dispersing agent, 0.2-5 parts by weight of a suspending agent and 1-15 parts by weight of a coloring agent.
The dispersant may be an alkyl glycoside. The suspending agent comprises at least one of carrageenan, xanthan gum and natural cellulose. The suspending agent in the invention is derived from natural plant extraction, and the function of the suspending agent is to ensure the dispersibility and stability of a product system.
The water-based environment-friendly nail polish can also comprise 1-15 parts by weight of a coloring agent. The colorant in the present invention includes at least one of an organic pigment, an inorganic pigment, and a pearlescent pigment, and functions to provide a color tone and a diversified appearance of the product. Wherein the organic pigment can be CI15850:1, CI15850:2, CI15880:1, CI73900, CI73915, CI12370, CI74160, CI74260, CI11710, CI21108 and the like. The inorganic pigment can be CI 77891 (titanium dioxide), CI 77266 (carbon black), CI77491 (red iron oxide), CI77499 (black iron oxide), CI77492 (yellow iron oxide), CI77007 (ultramarine), silica, CI77820 (silver powder), CI77000 (aluminum powder), CI77163 (bismuth oxychloride), CI77400 (bronze powder) and the like. The pearlescent pigment can be mica, and glitter powder (polyethylene terephthalate).
The preparation process of the aqueous environment-friendly nail polish comprises the following steps:
mixing various aqueous polyurethane dispersions according to a formula to obtain a basic dispersion liquid;
step two, stirring the basic dispersion liquid, measuring and adjusting the solid content of the basic dispersion liquid to keep the solid content at 40-45%;
the determination method of the solid content comprises the following steps: firstly, weighing a certain amount of basic dispersion liquid in an aluminum foil dish, baking the part of basic dispersion liquid in an oven at 110-120 ℃ for 2-3 hours, weighing the weight of residues, wherein the weight ratio of the residues to the basic dispersion liquid is the solid content in the basic dispersion liquid.
When the solid content is too high, adjusting by adding pure water into the basic dispersion liquid; when the solid content is too low, the base dispersion is heated over water with hot water at 60 to 80 ℃ to evaporate water.
And step three, adding other raw material components except the water-based polyurethane dispersion in the nail polish into the adjusted dispersion liquid, stirring, uniformly mixing, and testing the brushing performance (self-drying, leveling, stripping and the like) on the nail. And (3) placing the liquid with qualified test results and color tones in the shade for more than 1 week, observing the stability of the liquid, carrying out micro-adjustment, then filtering, collecting the filtrate, carrying out microbial inspection (according to the national standard of cosmetics), wherein the liquid with qualified inspection is the finished nail polish raw material capable of being canned.
The brushing performance is qualified, namely the self-drying property, the leveling property and the stripping property are all qualified. The self-drying property is qualified, namely the surface is naturally dried (no impression is made by touching a finger) within 1 minute after a layer of liquid is coated on the surface of the human nail at 25 ℃; the leveling property is qualified, namely, at 25 ℃, a layer of the liquid is coated on the surface of the human nail, and after 1 minute, a layer is coated again, and the surface is observed to be smooth without painting marks; the qualified tearing property means that one or two layers of nail polish are coated on the nail surface after the nail surface is cleaned by alcohol cleaning cotton, and the self-dried film can be torn off from the nail surface in a whole piece after 30 minutes.
In order to make the technical means, the creation characteristics, the achievement purposes and the effects of the invention easy to understand, the following embodiments are combined to specifically describe the water-based environment-friendly nail polish of the invention.
< example 1>
The embodiment provides a red aqueous nail polish, which comprises the following raw material components in a specific implementation:
30g of polyurethane-10, 25g of polyurethane-11, 20g of polyurethane-35, 2g of polyurethane-2, 2g of CI73915 (red), 5g of CI 77891 (titanium dioxide), 5g of mica, 3g of alkyl glycoside, 0.2g of xanthan gum and the balance of deionized water to 100 g.
The procedure for preparing a red aqueous nail enamel according to the above formulation of this example was:
step one, mixing 30g of polyurethane-10, 25g of polyurethane-11, 20g of polyurethane-35 and 2g of polyurethane-2 to obtain a base dispersion.
And step two, mechanically stirring the mixed basic dispersion liquid uniformly, measuring and adjusting the solid content of the mixed basic dispersion liquid, and controlling the solid content of the basic dispersion liquid to be 40-45% to obtain the adjusted dispersion liquid.
And step three, adding a dispersing agent (3g of alkyl glycoside) and a suspending agent (0.2g of xanthan gum) into the treated dispersion, then adding a coloring agent (2g of CI73915, 5g of CI 77891 and 5g of mica), mechanically stirring for 4 hours, then toning, and testing the brushing performance (self-drying, leveling, stripping and the like) of the waterborne nail polish on a nail to obtain a semi-finished waterborne nail polish raw material with qualified tone and brushing performance. Placing the semi-finished nail polish with qualified brushing performance in shade for more than 1 week, filtering, collecting filtrate, and performing microorganism inspection (according to national standard of cosmetics), wherein the qualified liquid is the raw material of canned red nail polish.
The red aqueous nail polish prepared in this example was tested in relation to commercially available similar colored aqueous nail polish products and oily nail polish products.
Wherein, the water nail polish mainly comprises acrylic acid and polyurethane water dispersoid (the content is about 60 percent), and contains about 15 percent of chemical auxiliary agent (alcohol cosolvent, wetting agent, flatting agent, suspending agent, etc.); commercially available oily nail polishes are composed primarily of nitrocellulose and butyl acetate.
The volunteers of the experiment are normal office workers aged 20-30 years, the experiment is carried out in an indoor environment, and the body sensing temperature is 24-26 ℃.
The test method comprises the following steps:
(1) self-drying: coating a layer of nail polish on the surface of a human nail, touching the surface of the nail polish with fingers every 1 minute until no obvious mark exists, and recording the time.
(2) Durability: after a layer of nail polish is coated on the surface of a human nail, the time that the film at the tip of the nail is not lifted is recorded.
(3) Tearing and stripping performance: the surface of a human nail was coated with a layer of nail polish and the extent of the peel of the whole piece was tested after 30 minutes.
(4) Odor: the bottle cap was opened 5 cm from the mouth of the bottle and the odor was smelled with a nose for 2 seconds, and the presence or absence of a noticeable odor was recorded.
The test results are shown in table 1.
Table 1 red water-based nail polish performance test table
As shown in table 1, the red aqueous nail polish of this example 1 is superior to the commercially available aqueous nail polish in self-drying property, durability and stripping property, and the red aqueous nail polish film layer of this example is capable of being stripped off in one piece, while the commercially available aqueous nail polish layer is not capable of being stripped off in one piece and has odor.
The red aqueous nail polish in this example also performed better than the commercial oil nail polish. Commercially available oil nail polishes, while best in durability, have significant weaknesses such as being longest in dry time, completely non-peelable, and having an irritating odor.
The results of the above tests show that the colored nail polish of example 1 has fast self-drying, long-lasting, ability to be peeled off in one piece and odorless properties, and is superior to commercially available water-based and oil-based nail polishes. The aqueous polyurethane dispersion content of the nail polish in example 1 was 77%, while the acrylic and polyurethane aqueous dispersions in the commercially available aqueous nail polish contained 60% and about 15% of chemical auxiliaries (alcohol cosolvents, wetting agents, leveling agents, suspending agents, etc.), so that the overall release performance was poor and there was a certain odor. The commercial oil nail polish has the best durability, but has the advantages of pungent smell, difficult makeup removal and environmental pollution, so the comprehensive performance is inferior to that of the embodiment and the commercial water nail polish.
< example 2>
The embodiment provides a transparent top layer nail polish, which comprises the following specific formula:
40g of polyurethane-10, 40g of polyurethane-11, 5g of polyurethane-35, 1g of polyurethane-2 and the balance of deionized water to 100 g.
The procedure for preparing nail polish according to the above formulation of this example was:
step one, mixing 40g of polyurethane-10, 40g of polyurethane-11, 5g of polyurethane-35 and 1g of polyurethane-2 to obtain a basic dispersion liquid.
And step two, mechanically stirring the mixed basic dispersion liquid for 3 hours, measuring the solid content of the mixed basic dispersion liquid, and controlling the solid content of the basic dispersion liquid to be 40-45% to obtain the transparent top-layer semi-finished nail polish raw material.
And step three, testing the brushing performance (self-drying, leveling, stripping and the like) of the semi-finished nail polish on the nails, then filtering, collecting filtrate, carrying out microbial inspection (according to the national standard of cosmetics), and obtaining qualified liquid which is the finished transparent top-layer nail polish raw material capable of being canned.
The clear top-layer nail polish prepared in this example was subjected to performance testing experiments in relation to commercially available clear aqueous nail polish and commercially available clear oily nail polish.
Wherein, the water nail polish mainly comprises acrylic acid and polyurethane water dispersoid (the content is about 60 percent), and contains about 15 percent of chemical auxiliary agent (alcohol cosolvent, wetting agent, flatting agent, suspending agent, etc.); commercially available oily nail polishes are composed primarily of nitrocellulose and butyl acetate.
The volunteers of the experiment are normal office workers aged 20-30 years, the experiment is carried out in an indoor environment, and the body sensing temperature is 24-26 ℃.
In example 2, the same test items as in example 1 were tested in the same manner as in example 1, and the other test items were tested in the following manners:
(5) gloss retention: the above-mentioned persons keep a normal life (e.g., office, housework, bath, etc.) for 24 hours after applying different types of nail varnishes, and then observe whether the gloss of the surface of the nail coating layer is maintained.
(6) Scratch resistance test: the above-mentioned persons keep a normal life (e.g., office, housework, bath, etc.) for 24 hours after applying different types of nail varnishes, and then observe whether or not there is a significant scratch on the surface of the nail coating layer.
The test results are shown in table 2.
Table 2 transparent top layer nail polish performance test table
As shown by the results in table 2, the nail polish of example 2 is fast self-drying, long lasting, capable of being peeled off in one piece and odorless, and outperforms both commercially available water and oil nail polishes. In addition, the scratch resistance of the embodiment is obviously superior to that of the commercially available transparent water-based nail polish and transparent oil-based nail polish. Although there was no difference in appearance compared to the commercial clear aqueous nail enamel, the gloss retention of this example was better than the commercial clear aqueous nail enamel. Since the aqueous polyurethane dispersion in this example is up to 87% and contains no other chemical additives, while the commercially available aqueous nail polish contains 20% of chemical additives (leveling agent, gloss agent, etc.), this example is also significantly superior to similar products in terms of environmental protection and safety of the product.
The above embodiments are preferred examples of the present invention, and are not intended to limit the scope of the present invention.
Claims (6)
1. The water-based environment-friendly nail polish is characterized by comprising the following raw material components in parts by weight:
60 to 90 parts by weight of an aqueous polyurethane dispersion,
wherein the aqueous polyurethane dispersion comprises polyurethane-35, polyurethane-10, polyurethane-11 and polyurethane-2.
2. The aqueous environment-friendly nail polish according to claim 1, wherein:
the weight portion of the polyurethane-35 in the aqueous polyurethane dispersion is 1-30, the weight portion of the polyurethane-10 is 15-45, the weight portion of the polyurethane-11 is 15-40, and the weight portion of the polyurethane-2 is 1-5.
3. The aqueous environment-friendly nail polish as claimed in claim 1, wherein the raw material components of the aqueous environment-friendly nail polish further comprise:
2 to 5 parts by weight of a dispersant and 0.2 to 5 parts by weight of a suspending agent,
wherein the dispersant is alkyl glycoside,
the suspending agent comprises at least one of carrageenan, xanthan gum and natural cellulose.
4. The aqueous environment-friendly nail polish as claimed in claim 1, wherein the raw material components of the aqueous environment-friendly nail polish further comprise:
1 to 15 parts by weight of a colorant.
5. The aqueous environment-friendly nail polish according to claim 1, wherein:
wherein the ingredient component is selected from a list of names of used cosmetic ingredients (2015 edition).
6. The preparation method of the water-based environment-friendly nail polish is characterized by comprising the following steps:
mixing various aqueous polyurethane dispersions according to a formula to obtain a basic dispersion liquid;
step two, stirring the basic dispersion liquid, measuring and adjusting the solid content of the basic dispersion liquid to keep the solid content at 40-45%;
adding other raw material components into the basic dispersion, stirring, uniformly mixing, testing the brushing performance (self-drying, leveling property, stripping property and the like) and the raw material stability on the nail, carrying out micro-adjustment, then filtering and carrying out microbial inspection,
the water-based environment-friendly nail polish as claimed in any one of claims 1 to 5.
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| CN201910956847.XA CN112641673A (en) | 2019-10-10 | 2019-10-10 | Aqueous environment-friendly nail polish |
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| CN201910956847.XA CN112641673A (en) | 2019-10-10 | 2019-10-10 | Aqueous environment-friendly nail polish |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113730271A (en) * | 2021-10-13 | 2021-12-03 | 齐鲁工业大学 | Edible wolfberry nail polish and preparation method thereof |
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| CN113730271A (en) * | 2021-10-13 | 2021-12-03 | 齐鲁工业大学 | Edible wolfberry nail polish and preparation method thereof |
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