CN112588243A - Synthesis device and synthesis method of biomass hydrogen production composite catalyst - Google Patents
Synthesis device and synthesis method of biomass hydrogen production composite catalyst Download PDFInfo
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- CN112588243A CN112588243A CN202011527394.8A CN202011527394A CN112588243A CN 112588243 A CN112588243 A CN 112588243A CN 202011527394 A CN202011527394 A CN 202011527394A CN 112588243 A CN112588243 A CN 112588243A
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- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
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- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0073—Sealings
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
- B01J19/20—Stationary reactors having moving elements inside in the form of helices, e.g. screw reactors
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- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B9/00—Cleaning hollow articles by methods or apparatus specially adapted thereto
- B08B9/08—Cleaning containers, e.g. tanks
- B08B9/093—Cleaning containers, e.g. tanks by the force of jets or sprays
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
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Abstract
The invention discloses a device and a method for synthesizing a biomass hydrogen production composite catalyst, which comprises a shell, wherein the top of the shell is movably connected with a cover plate, the surface of the shell is fixedly sleeved with a cover body, the right side of the inner cavity of the cover body is fixedly connected with a heating wire, the left side of the inner cavity of the cover body is fixedly connected with a semiconductor refrigerating sheet, the inner wall of the cover body is movably sleeved with a gear ring, the tops of two sides of the gear ring are fixedly connected with stirring rods, and the right side of the bottom of the cover body is fixedly connected with a first. The invention solves the problems that the existing synthesis device of the biomass hydrogen production composite catalyst has poor stirring effect, is not fully mixed and stirred uniformly, has large difference between the upper raw material and the lower raw material, relatively insufficient and slow reaction process, is mostly heated by an internal resistance wire during synthesis, and has the defects of insufficient reaction, inconvenient cleaning and influence on next use due to nonuniform heating although rapid heating.
Description
Technical Field
The invention relates to the technical field of biomass hydrogen production, in particular to a device and a method for synthesizing a biomass hydrogen production composite catalyst.
Background
The reaction temperature required by the hydrogen production from the garbage is about 1000 ℃, the required high-temperature heat energy is transmitted from the outside of the pyrolysis chamber and the catalytic reforming chamber, the garbage hydrogen production furnace is required to have high heat utilization efficiency, the furnace wall material can bear the high temperature of 1000 ℃, and a catalyst is required for catalysis when the hydrogen production from the biomass is carried out, so that the yield and the quality of pyrolysis feed gas are improved, the residual carbon discharged from the pyrolysis chamber is reduced, and the tar content in the feed gas is reduced; catalytic reforming with the feed gas as much as possible turns into hydrogen, the catalyst is synthesized through synthesizer, but current living beings hydrogen manufacturing composite catalyst synthesizer stirring effect is poor, do not fully mix the stirring, upper and lower raw materials differ great, the reaction process is abundant and comparatively slow inadequately relatively, and heat through inside resistance wire mostly when synthesizing, though the heating is rapid, but the heating is inhomogeneous, make the reaction insufficient, and be not convenient for wash, influence next use.
Disclosure of Invention
The invention aims to provide a synthesis device and a synthesis method of a biomass hydrogen production composite catalyst, which have the advantages of good stirring effect, rapid and uniform heating and convenient cleaning, and solve the problems that the existing synthesis device of the biomass hydrogen production composite catalyst has poor stirring effect, is not fully mixed and uniformly stirred, has large difference between upper and lower raw materials, relatively insufficient and slow reaction process, is mostly heated by an internal resistance wire during synthesis, and has the defects of insufficient reaction, inconvenient cleaning and influence on next use due to rapid heating but nonuniform heating.
In order to achieve the purpose, the invention provides the following technical scheme: a biomass hydrogen production composite catalyst synthesis device comprises a shell, wherein the top of the shell is movably connected with a cover plate, the surface of the shell is fixedly sleeved with a cover body, the right side of an inner cavity of the cover body is fixedly connected with a heating wire, the left side of the inner cavity of the cover body is fixedly connected with a semiconductor refrigerating sheet, the inner wall of the cover body is movably sleeved with a gear ring, the tops of two sides of the gear ring are both fixedly connected with a stirring rod, the right side of the bottom of the cover body is fixedly connected with a first motor, the top of a rotating shaft of the first motor penetrates through the inner cavity of the cover body and is fixedly connected with a circular gear, the circular gear is meshed with the gear ring, the left side of the top of the cover plate is fixedly communicated with an inlet pipe, the top of the inlet pipe is movably connected with a cover through a rotating shaft, the left end of the rotating shaft of the second motor penetrates through the inner cavity of the box body and is fixedly connected with a first bevel gear, the bottom of the inner cavity of the shell is fixedly connected with a vertical pipe through a bracket, the bottom of the inner cavity of the box is provided with a rotating pipe in a penetrating way, the bottom of the rotating pipe penetrates through the inner cavities of the box body and the cover plate extending shell in sequence and is fixedly connected with a rotating rod, the bottom of the rotating rod penetrates to the bottom of the vertical pipe, the bottom of the surface of the rotating pipe is provided with a one-way valve, the bottom of the right side of the rotating pipe is fixedly communicated with a transverse pipe, the bottom of the transverse pipe is fixedly communicated with a spray head, the surface of the rotating rod is fixedly connected with a helical blade, the tops of both sides of the rotating rod are fixedly connected with connecting rods, the fixed surface that is located box inner chamber one end of runner pipe is equipped with second conical gear, first conical gear and second conical gear meshing.
Preferably, the left side fixedly connected with temperature sensor of casing inner chamber, the fixed intercommunication of bottom of casing has row material pipe, the bottom on row material pipe surface is provided with the valve.
Preferably, the support fixedly connected with condenser is passed through on the right side at apron top, the intake pipe of condenser and the fixed intercommunication in right side at apron top, the bottom movable sleeve on standpipe surface is equipped with the plectane, the connecting rod is kept away from the one end of bull stick and the top fixed connection of plectane, be provided with first ball between standpipe and the plectane.
Preferably, a second ball is arranged between the gear ring and the cover body, and the bottom of the cover body is fixedly connected with a supporting leg.
Preferably, the left side at lid top is seted up flutedly, there is the L template in the left side of inlet pipe through pivot swing joint, and the top of L template is run through and is provided with the threaded rod, and the bottom of threaded rod runs through to the bottom of L template and has the base through bearing swing joint, and the bottom of base extends to the inner chamber of recess, threaded rod and L template threaded connection, the top fixedly connected with handle of threaded rod.
Preferably, a bearing is arranged between the rotating pipe and the cover plate, and the bearing is sleeved on the surface of the rotating pipe.
Preferably, the right side of the top of the cover body is fixedly communicated with an oil inlet pipe, and a sealing cover is sleeved on the top thread of the surface of the oil inlet pipe.
Preferably, the top of apron is run through and is provided with the bolt, and the bottom of bolt runs through lid and casing in proper order and extends to the outside of casing, and the bottom screw thread cover on bolt surface is equipped with the nut.
Preferably, the synthesis method of the composite catalyst synthesis device for hydrogen production from biomass comprises the following steps:
A) with device through wire external power supply and controller, will advance the water pipe and pass through the external water supply installation of pipeline, pass through the external cooling water of pipeline with the condenser, open the lid and add the casing with the raw materials through the inlet pipe, cover the rotation handle with the lid, the rotation of handle drives the rotation of threaded rod and down removes, makes the base remove and carries out fixed seal to the lid in the recess.
B) The operation of controller control second motor, the rotation of second motor shaft drives first bevel gear, second bevel gear, the bull stick, the connecting rod, stirring rake and helical blade's rotation, the rotation of connecting rod and stirring rake stirs the mixing reaction to the raw materials, helical blade's rotation constantly carries the lower part through the standpipe with the raw materials on upper portion in the casing simultaneously, the raw materials of lower part is carried toward upper portion to circulate, realize fully stirring mixing reaction.
C) The operation of controller control heater strip and first motor, the operation of heater strip heats the conduction oil that covers the internal, the rotation of first motor shaft drives circular gear, the rotation of ring gear and puddler, the rotation of puddler stirs the conduction oil, make the more even of the internal conduction oil temperature of cover, thereby carry out the even heating reaction to the raw materials in the casing, feedback through temperature sensor, the controller is through the operation and the closing of control heater strip and semiconductor refrigeration piece, make the raw materials in the casing keep the constancy of temperature in certain scope.
D) When the synthesis device needs to be cleaned, the water supply device supplies water to enter the box body, the water is sprayed out from the spray head through the rotating pipe and the transverse pipe, and the components in the shell are cleaned under the rotating effect of the spray head.
Compared with the prior art, the invention has the following beneficial effects:
1. the invention matches the shell, the cover body, the heating wires, the semiconductor refrigeration sheet, the gear ring, the stirring rod, the first motor, the circular gear, the feeding pipe, the box body, the water inlet pipe, the second motor, the first bevel gear, the vertical pipe, the rotating rod, the horizontal pipe, the spray head, the spiral blade, the connecting rod, the stirring paddle and the second bevel gear, has the advantages of good stirring effect, rapid and uniform heating and convenient cleaning, solves the problems that the existing synthesis device for the biomass composite hydrogen production catalyst has poor stirring effect, does not fully mix and stir uniformly, has large difference between the upper raw material and the lower raw material, relatively insufficient and slow reaction process, and mostly heats through the internal resistance wire during synthesis, although the heating is rapid, the heating is not uniform, so that the reaction is not sufficient, and the cleaning is inconvenient, which affects the next use.
2. According to the invention, the temperature sensor is arranged, so that the temperature in the shell can be conveniently monitored and regulated, the condenser is arranged, the gas in the shell is condensed into liquid backflow, the circular plate and the first ball are arranged, so that the connecting rod and the stirring paddle are more stable in rotation, the second ball is arranged, the gear ring is fixed and the gear ring is more smooth in rotation, the cover is fixed by arranging the groove, the L-shaped plate, the threaded rod, the base and the handle, the cover can be conveniently opened, the oil inlet pipe and the sealing cover are arranged, so that heat conducting oil can be conveniently supplemented into the cover body in time, the cover plate is fixed by arranging the bolt and the nut, and the cover plate can be conveniently taken down to deeply clean the inside of the shell.
Drawings
FIG. 1 is a schematic structural view of the present invention;
FIG. 2 is an enlarged top plan view of the ring gear of the present invention;
FIG. 3 is an enlarged front sectional view of the housing of the present invention;
FIG. 4 is an enlarged top view of a standpipe of the present invention.
In the figure: the device comprises a shell 1, a cover plate 2, a cover body 3, a heating wire 4, a semiconductor refrigerating sheet 5, a gear ring 6, a stirring rod 7, a first motor 8, a circular gear 9, a feeding pipe 10, a cover 11, a box 12, a water inlet pipe 13, a second motor 14, a first bevel gear 15, a vertical pipe 16, a rotating pipe 17, a rotating rod 18, a check valve 19, a transverse pipe 20, a spray head 21, a spiral blade 22, a connecting rod 23, a stirring paddle 24, a second bevel gear 25, a temperature sensor 26, a discharge pipe 27, a valve 28, a condenser 29 and a circular plate 30.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
In the description of the present invention, it should be noted that the terms "upper", "lower", "inner", "outer", "front", "rear", "both ends", "one end", "the other end", and the like indicate orientations or positional relationships based on the orientations or positional relationships shown in the drawings, and are only for convenience of describing the present invention and simplifying the description, but do not indicate or imply that the referred device or element must have a specific orientation, be configured in a specific orientation, and operate, and thus, should not be construed as limiting the present invention. Furthermore, the terms "first" and "second" are used for descriptive purposes only and are not to be construed as indicating or implying relative importance.
In the description of the present invention, it is to be noted that, unless otherwise explicitly specified or limited, the terms "mounted," "disposed," "connected," and the like are to be construed broadly, such as "connected," which may be fixedly connected, detachably connected, or integrally connected; can be mechanically or electrically connected; they may be connected directly or indirectly through intervening media, or they may be interconnected between two elements. The specific meanings of the above terms in the present invention can be understood in specific cases to those skilled in the art.
Referring to fig. 1-4, a composite catalyst synthesis device for hydrogen production from biomass comprises a shell 1, a cover plate 2 is movably connected to the top of the shell 1, a cover body 3 is fixedly sleeved on the surface of the shell 1, a heating wire 4 is fixedly connected to the right side of the inner cavity of the cover body 3, a semiconductor refrigerating sheet 5 is fixedly connected to the left side of the inner cavity of the cover body 3, a gear ring 6 is movably sleeved on the inner wall of the cover body 3, stirring rods 7 are fixedly connected to the tops of the two sides of the gear ring 6, a first motor 8 is fixedly connected to the right side of the bottom of the cover body 3, the top of the rotating shaft of the first motor 8 penetrates through the inner cavity of the cover body 3 and is fixedly connected with a circular gear 9, the circular gear 9 is meshed with the gear ring 6, a feed pipe 10 is fixedly communicated to the left side of the top of the cover plate, a second motor 14 is fixedly connected to the right side of the box 12, the left end of the rotating shaft of the second motor 14 penetrates through the inner cavity of the box 12 and is fixedly connected with a first bevel gear 15, the bottom of the inner cavity of the shell 1 is fixedly connected with a vertical pipe 16 through a support, a rotating pipe 17 penetrates through the bottom of the inner cavity of the box 12, the bottom of the rotating pipe 17 sequentially penetrates through the box 12 and the cover plate 2, extends out of the inner cavity of the shell 1 and is fixedly connected with a rotating rod 18, the bottom of the rotating rod 18 penetrates through the bottom of the vertical pipe 16, a one-way valve 19 is arranged at the bottom of the surface of the rotating pipe 17, a transverse pipe 20 is fixedly communicated with the bottom of the right side of the rotating pipe 17, a spray nozzle 21 is fixedly communicated with the bottom of the transverse pipe 20, helical blades 22 are fixedly connected with the surface of the rotating rod 18, connecting rods 23 are fixedly connected with the tops of both sides of the, the first bevel gear 15 is meshed with the second bevel gear 25, the left side of the inner cavity of the shell 1 is fixedly connected with a temperature sensor 26, the bottom of the shell 1 is fixedly communicated with a material discharging pipe 27, the bottom of the surface of the material discharging pipe 27 is provided with a valve 28, the temperature sensor 26 is arranged to facilitate monitoring and regulation of the temperature in the shell 1, the right side of the top of the cover plate 2 is fixedly connected with a condenser 29 through a bracket, an air inlet pipe of the condenser 29 is fixedly communicated with the right side of the top of the cover plate 2, the bottom of the surface of the vertical pipe 16 is movably sleeved with a circular plate 30, one end, far away from the rotating rod 18, of the connecting rod 23 is fixedly connected with the top of the circular plate 30, a first ball is arranged between the vertical pipe 16 and the circular plate 30, the condenser 29 is arranged to condense the gas in the shell 1 into liquid backflow, and the, a second ball is arranged between the gear ring 6 and the cover body 3, the bottom of the cover body 3 is fixedly connected with a supporting leg, the gear ring 6 is enabled to rotate more smoothly while being fixed by arranging the second ball, the left side of the top of the cover 11 is provided with a groove, the left side of the feeding pipe 10 is movably connected with an L-shaped plate through a rotating shaft, the top of the L-shaped plate is provided with a threaded rod in a penetrating way, the bottom of the threaded rod penetrates to the bottom of the L-shaped plate and is movably connected with a base through a bearing, the bottom of the base extends to the inner cavity of the groove, the threaded rod is in threaded connection with the L-shaped plate, the top of the threaded rod is fixedly connected with a handle, by arranging the groove, the L-shaped plate, the threaded rod, the base and the handle, the cover 11 is fixed, meanwhile, the cover 11 is convenient to open, the, the top thread bush on the surface of the oil inlet pipe is provided with a sealing cover, the oil inlet pipe and the sealing cover are arranged, heat conducting oil is convenient to supplement into the cover body 3 in time, the top of the cover plate 2 is provided with a bolt in a penetrating way, the bottom of the bolt sequentially penetrates through the cover 11 and the shell 1 and extends to the outside of the shell 1, the bottom thread bush on the surface of the bolt is provided with a nut, the cover plate 2 is fixed by arranging the bolt and the nut, meanwhile, the cover plate is convenient to take down and deeply clean the inside of the shell 1, the cover body 3, the heating wire 4, the semiconductor refrigeration sheet 5, the gear ring 6, the stirring rod 7, the first motor 8, the circular gear 9, the inlet pipe 10, the box body 12, the inlet pipe 13, the second motor 14, the first bevel gear 15, the vertical pipe 16, the rotating pipe 17, the rotating rod 18, the transverse pipe 20, possess the stirring effect good, the heating is rapidly even and the abluent advantage of being convenient for, it is poor to have solved current living beings hydrogen manufacturing composite catalyst synthesizer stirring effect, do not fully mix the stirring, upper and lower raw materials differ great, the reaction process is abundant and comparatively slow inadequately relatively, and heat through inside resistance wire mostly when synthesizing, though the heating is rapid, but the heating is inhomogeneous, make the reaction insufficient, and be not convenient for wash, influence the problem of next use.
A synthetic method of a biomass hydrogen production composite catalyst synthetic device comprises the following steps:
A) with the device through wire external power supply and controller, with inlet tube 13 through the external water supply installation of pipeline, with condenser 29 through the external cooling water of pipeline, open lid 11 and add the casing 1 with the raw materials through inlet pipe 10 in, cover lid 11 and rotate the handle, the rotation of handle drives the rotation of threaded rod and down removes, makes the base remove and carries out fixed seal to lid 11 in the recess.
B) The operation of controller control second motor 14, the rotation of the pivot of second motor 14 drives first bevel gear 15, second bevel gear 25, the bull stick 17, bull stick 18, connecting rod 23, stirring rake 24 and helical blade 22's rotation, the rotation of connecting rod 23 and stirring rake 24 stirs the mixing reaction to the raw materials, helical blade 22's rotation is constantly carried the lower part through standpipe 16 with the raw materials on upper portion in the casing 1 simultaneously, the raw materials of lower part are carried toward upper portion, thereby circulate, realize the intensive mixing reaction.
C) Controller control heater strip 4 and first motor 8's operation, heater strip 4's operation heats the conduction oil that covers in the body 3, the rotation of first motor 8 pivot drives circular gear 9, ring gear 6 and puddler 7's rotation, puddler 7's rotation is stirred the conduction oil, make the more even of the conduction oil temperature in the cover body 3, thereby carry out the even heating reaction to the raw materials in the casing 1, feedback through temperature sensor 26, the controller is through the operation and the closing of control heater strip 4 and semiconductor refrigeration piece 5, make the raw materials in the casing 1 keep the constancy of temperature in certain scope.
D) When the synthesis apparatus needs to be cleaned, the water supply apparatus supplies water into the tank 12, and the water is discharged from the spray head 21 through the rotary pipe 17 and the horizontal pipe 20, and the components in the casing 1 are cleaned by the rotation of the spray head 21.
All parts used in the application document are standard parts and can be purchased from the market, and the specific connection mode of all parts adopts conventional means such as bolts, rivets, welding and the like mature in the prior art, and detailed description is not given here.
In summary, the following steps: the device and the method for synthesizing the biomass hydrogen production composite catalyst are characterized in that a shell 1, a cover body 3, a heating wire 4, a semiconductor refrigerating sheet 5, a gear ring 6, a stirring rod 7, a first motor 8, a circular gear 9, a feeding pipe 10, a box body 12, a water inlet pipe 13, a second motor 14, a first bevel gear 15, a vertical pipe 16, a rotating pipe 17, a rotating rod 18, a horizontal pipe 20, a spray head 21, a spiral blade 22, a connecting rod 23, a stirring paddle 24 and a second bevel gear 25 are matched, so that the problems that the existing device for synthesizing the biomass hydrogen production composite catalyst is poor in stirring effect, uniform mixing and stirring are not sufficiently performed, the difference between upper and lower raw materials is large, the reaction process is relatively insufficient and slow are solved, and most of resistance wires are heated through the inner part during synthesis, although the heating is rapid, the heating is not uniform, the reaction is not sufficient, affecting the next use.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (9)
1. The utility model provides a living beings hydrogen manufacturing composite catalyst synthesizer, includes casing (1), its characterized in that: the top swing joint of casing (1) has apron (2), the fixed surface cover of casing (1) is equipped with cover body (3), the right side fixedly connected with heater strip (4) of cover body (3) inner chamber, the left side fixedly connected with semiconductor refrigeration piece (5) of cover body (3) inner chamber, the inner wall movable sleeve of cover body (3) is equipped with ring gear (6), the equal fixedly connected with puddler (7) in top of ring gear (6) both sides, the right side fixedly connected with first motor (8) of cover body (3) bottom, the top of first motor (8) pivot is run through to the inner chamber of cover body (3) and fixedly connected with circular gear (9), circular gear (9) and ring gear (6) meshing, the left side fixed intercommunication at apron (2) top has inlet pipe (10), the top of inlet pipe (10) has lid (11) through pivot swing joint, the top of the cover plate (2) is fixedly connected with a box body (12), the top of the box body (12) is fixedly communicated with a water inlet pipe (13), the right side of the box body (12) is fixedly connected with a second motor (14), the left end of a rotating shaft of the second motor (14) penetrates through an inner cavity of the box body (12) and is fixedly connected with a first bevel gear (15), the bottom of the inner cavity of the shell body (1) is fixedly connected with a vertical pipe (16) through a support, the bottom of the inner cavity of the box body (12) is provided with a rotating pipe (17) in a penetrating manner, the bottom of the rotating pipe (17) sequentially penetrates through the inner cavity of the box body (12) and the cover plate (2) extending shell body (1) and is fixedly connected with a rotating rod (18), the bottom of the rotating rod (18) penetrates through the bottom of the vertical pipe (16), the bottom of the surface of the rotating pipe (17) is provided with a one, the fixed intercommunication in bottom of violently managing (20) has shower nozzle (21), the fixed surface of bull stick (18) is connected with helical blade (22), the equal fixedly connected with connecting rod (23) in top of bull stick (18) both sides, the fixed surface of connecting rod (23) is connected with stirring rake (24), the fixed cover in surface that bull stick (17) are located box (12) inner chamber one end is equipped with second conical gear (25), first conical gear (15) and second conical gear (25) meshing.
2. The composite catalyst synthesis device for hydrogen production from biomass as claimed in claim 1, wherein: the left side fixedly connected with temperature sensor (26) of casing (1) inner chamber, the fixed intercommunication in bottom of casing (1) has row material pipe (27), the bottom on row material pipe (27) surface is provided with valve (28).
3. The composite catalyst synthesis device for hydrogen production from biomass as claimed in claim 1, wherein: support fixedly connected with condenser (29) is passed through on the right side at apron (2) top, the intake pipe of condenser (29) and the fixed intercommunication in right side at apron (2) top, the bottom movable sleeve on standpipe (16) surface is equipped with plectane (30), the top fixed connection of the one end of bull stick (18) and plectane (30) is kept away from in connecting rod (23), be provided with first ball between standpipe (16) and plectane (30).
4. The composite catalyst synthesis device for hydrogen production from biomass as claimed in claim 1, wherein: a second ball is arranged between the gear ring (6) and the cover body (3), and the bottom of the cover body (3) is fixedly connected with a supporting leg.
5. The composite catalyst synthesis device for hydrogen production from biomass as claimed in claim 1, wherein: the left side at lid (11) top is seted up flutedly, there is the L template in the left side of inlet pipe (10) through pivot swing joint, and the top of L template is run through and is provided with the threaded rod, and the bottom of threaded rod runs through to the bottom of L template and has the base through bearing swing joint, and the bottom of base extends to the inner chamber of recess, threaded rod and L template threaded connection, the top fixedly connected with handle of threaded rod.
6. The composite catalyst synthesis device for hydrogen production from biomass as claimed in claim 1, wherein: a bearing is arranged between the rotating pipe (17) and the cover plate (2), and the bearing is sleeved on the surface of the rotating pipe (17).
7. The composite catalyst synthesis device for hydrogen production from biomass as claimed in claim 1, wherein: the right side of the top of the cover body (3) is fixedly communicated with an oil inlet pipe, and a sealing cover is sleeved on the top thread of the surface of the oil inlet pipe.
8. The composite catalyst synthesis device for hydrogen production from biomass as claimed in claim 1, wherein: the top of apron (2) is run through and is provided with the bolt, and the bottom of bolt runs through lid (11) and casing (1) in proper order and extends to the outside of casing (1), and the bottom screw thread cover on bolt surface is equipped with the nut.
9. The synthesis method of the composite catalyst synthesis device for hydrogen production from biomass according to any one of claims 1 to 8, characterized in that: the method comprises the following steps:
A) with device through wire external power supply and controller, with inlet tube (13) through the external water supply installation of pipeline, with condenser (29) through the external cooling water of pipeline, open lid (11) and add the raw materials into casing (1) through inlet pipe (10), cover lid (11) and rotate the handle, the rotation of handle drives the rotation of threaded rod and down removes, makes the base remove and carries out fixed seal to lid (11) in the recess.
B) The operation of controller control second motor (14), the rotation of second motor (14) pivot drives first bevel gear (15), second bevel gear (25), revolving pipe (17), bull stick (18), connecting rod (23), the rotation of stirring rake (24) and helical blade (22), the rotation of connecting rod (23) and stirring rake (24) stirs the mixing reaction to the raw materials, helical blade (22) rotate simultaneously and constantly carry the lower part through standpipe (16) with the raw materials on upper portion in casing (1), the raw materials of lower part are carried toward upper portion, thereby circulate, realize the intensive mixing reaction.
C) Operation of controller control heater strip (4) and first motor (8), the operation of heater strip (4) heats the conduction oil in the cover body (3), the rotation of first motor (8) pivot drives circular gear (9), the rotation of ring gear (6) and puddler (7), the rotation of puddler (7) stirs the conduction oil, make the more even of heat conduction oil temperature in the cover body (3), thereby carry out the even heating reaction to the raw materials in casing (1), feedback through temperature sensor (26), the operation and the closing of controller through control heater strip (4) and semiconductor refrigeration piece (5), make the raw materials in casing (1) keep the constancy of temperature in certain scope.
D) When the synthesis device needs to be cleaned, the water supply device supplies water into the box body (12), the water is sprayed out from the spray head (21) through the rotary pipe (17) and the transverse pipe (20), and the components in the shell (1) are cleaned under the action of the rotation of the spray head (21).
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| CN202011527394.8A CN112588243A (en) | 2020-12-22 | 2020-12-22 | Synthesis device and synthesis method of biomass hydrogen production composite catalyst |
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| CN113231001A (en) * | 2021-05-18 | 2021-08-10 | 焦顺利 | Constant temperature treatment process for producing leather auxiliary agent |
| CN114324194A (en) * | 2022-01-24 | 2022-04-12 | 河北北方学院 | Grape gray mold monitoring device |
| CN114452905A (en) * | 2022-03-09 | 2022-05-10 | 技源生物制品(徐州)有限公司 | Liquid raw material conveying device |
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Application publication date: 20210402 |