CN112586726A - Preparation method of yang-strengthening food capable of retaining biological activity to the maximum extent - Google Patents
Preparation method of yang-strengthening food capable of retaining biological activity to the maximum extent Download PDFInfo
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- CN112586726A CN112586726A CN202011408495.3A CN202011408495A CN112586726A CN 112586726 A CN112586726 A CN 112586726A CN 202011408495 A CN202011408495 A CN 202011408495A CN 112586726 A CN112586726 A CN 112586726A
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- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L13/00—Meat products; Meat meal; Preparation or treatment thereof
- A23L13/20—Meat products; Meat meal; Preparation or treatment thereof from offal, e.g. rinds, skins, marrow, tripes, feet, ears or snouts
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Abstract
The invention discloses a preparation method of yang-strengthening food capable of retaining bioactivity to the maximum extent, which comprises the following specific steps: s1: preparing the male deer plasma freeze-dried powder; s2: preparing a donkey penis gelatin hollow capsule; s3: preparing yang-strengthening food. The invention relates to a preparation method of a penis equi gelatin hollow capsule, which comprises the steps of freeze-drying deer blood plasma into powder by a freeze-drying technology, keeping the complete yang-strengthening biological function of the deer blood plasma, reasonably matching donkey penis collagen peptide and edible gelatin by adding a plasticizer and a surfactant to prepare the penis equi gelatin hollow capsule, keeping the complete yang-strengthening biological function of the donkey penis, and then filling the male deer blood plasma freeze-dried powder with a certain proportion into the penis equi gelatin hollow capsule to prepare a yang-strengthening food with biological activity, thereby exerting the medical health-care value of deer blood and donkey penis for double yang strengthening to the maximum extent.
Description
Technical Field
The invention relates to the technical field of yang-strengthening foods, in particular to a preparation method of a yang-strengthening food capable of retaining biological activity to the maximum extent.
Background
With the continuous improvement of the living standard of people, the problem of how to delay aging and keep the vitality of body functions is generally concerned by people, and the body functions of middle-aged and old people are continuously aged along with the increase of the age, so that the symptoms of weakened disease resistance, decline of sexual function and the like appear. The yang-strengthening food is a kind of food, and has the main function of regulating the functions of a human body so as to be suitable for specific people to eat. Although the yang-strengthening food is different from common food, the yang-strengthening food also has the functions of food such as color, fragrance, taste, shape and the like; meanwhile, since yang-strengthening food is a nutritional supplement, the optimal yang-strengthening food should have active ingredients and content ratios suitable for specific people, as well as taste and appearance. The prior yang-tonifying food has the disadvantages of poor functional effect and slow absorption rate due to the rough preparation process, which greatly reduces the bioactivity.
Disclosure of Invention
The invention aims to provide a preparation method of yang-tonifying food capable of retaining biological activity to the maximum extent, and aims to solve the problems that the biological activity of the existing yang-tonifying food is greatly reduced due to a rough preparation process, the functional effect is poor and the absorption speed is slow in the background technology.
In order to achieve the purpose, the invention provides the following technical scheme:
a preparation method of yang-strengthening food capable of retaining biological activity to the maximum extent comprises the following specific steps:
s1: preparing the male deer plasma freeze-dried powder;
s2: preparing a donkey penis gelatin hollow capsule;
s3: preparing yang-strengthening food.
Preferably, the specific steps for preparing the male deer plasma freeze-dried powder are as follows:
s11: taking fresh male deer blood, and mixing the fresh male deer blood with an anticoagulant according to the ratio of 6: 1, filtering after mixing, adding an equal volume of 0.9% NaCl aqueous solution into the filtered blood for washing, adding the blood into a centrifugal machine, controlling the rotating speed to 3000 and 3500rpm for centrifuging for 10-15min, removing supernatant, repeatedly washing for 2-3 times, and discarding lower layer red blood cells;
s12: packaging the upper layer plasma in a clean sterile container, placing in a temperature control box, and sterilizing at 70-75 deg.C for 1-1.5 hr;
s13: controlling the temperature in the temperature control box, pre-freezing for 30-60min after cooling to-20 ℃, and then rapidly cooling to-80 ℃ for rapid freezing and solidification;
s14: freezing and solidifying the blood plasma for 1-2h, and freeze drying and sterilizing to obtain the blood plasma freeze-dried powder.
Preferably, the specific steps for preparing the donkey penis gelatin empty capsule are as follows:
s21: cutting donkey penis into blocks, soaking in alkali liquor, cleaning, removing fishy smell, placing in distilled water, heating and boiling, adding concentrated alkali to adjust pH to 10-13, soaking for 35-40h, taking out donkey penis, soaking in distilled water, cleaning, simultaneously adding active carbon, soaking for 2-2.5h, repeatedly washing with distilled water, filtering, and draining;
s22: cleaning the processed donkey penis, crushing, adjusting the pH value to 8.0 by NaOH, adding 4.8-5.5% of papain and trypsin, heating to 50 ℃, keeping the temperature for 4 hours, and performing ultrasonic-assisted enzymolysis for 1-5 hours under the condition of 200-500W;
s23: after complete enzymolysis, rapidly heating to 100 deg.C, boiling for 15-20min for inactivation, cooling to room temperature, filtering with 0.45 μm filter membrane to remove bacteria and impurities, and spray drying the filtrate to obtain donkey penis collagen polypeptide;
s24: mixing gelatin, glycerol, sorbitol and water at room temperature in proportion, placing the mixture in a heating tank, setting the temperature at 70-75 deg.C, vacuum heating and stirring for 30-40min until the gel blocks melt to obtain gelatin solution;
s25: placing donkey penis collagen peptide in water at room temperature according to the weight ratio of 1: 1, mixing, heating to 60-65 ℃ in vacuum, and stirring for 40-45min until the mixture is melted;
s26: mixing the prepared gelatin solution and donkey penis collagen peptide according to the ratio of 8: 2, and simultaneously adding 0.1-30% of plasticizer and 0.001-10% of surfactant according to the mass percentage, and stirring in a stirring tank preheated to 60 ℃ to fully and uniformly mix the components;
s27: placing the glue solution in a constant-temperature water bath kettle at the temperature of 40-70 ℃ and stirring until a uniform flowing glue solution is formed;
s28: performing ultrasonic degassing on the prepared glue solution in an ultrasonic processor with the frequency of 20kHz-120kHz, and then placing the glue solution under the vacuum pressure of 0.08-0.09MPa until the solution becomes clear and transparent to form a uniform shell material;
s29: transferring the degassed shell material into a preheated holding tank, setting the temperature at 60-65 deg.C for 4-4.5h, using for subsequent encapsulation, immersing the die rod of the capsule grinding tool in mustard oil for sufficient lubrication to coat a layer of semen Brassicae Junceae oil layer on the surface, immersing the lubricated die rod of the capsule grinding tool in the glue solution for 5-20s, slowly lifting the mold, turning over for 3-7 times to uniformly distribute the glue solution on the surface of the mold, rapidly solidifying with cold water, transferring the solidified capsule into a constant temperature dryer, setting the drying temperature at 40-60 deg.C, and drying for 40-45 min;
s210: pulling out the blastocyst after moisture regaining, cutting according to the required proportion size, combining the cut capsule body and the cut capsule cap to obtain a capsule shell finished product, and sterilizing the prepared capsule shell finished product by adopting an ozone sterilization method, wherein the ozone pressure is 0.2MPa, and the sterilization time is 1-10 min.
Preferably, the particle size of the pulverized donkey penis in step S22 is 70-80 mesh.
Preferably, in step S22, papain and trypsin are added in a ratio of 1: 1.
preferably, the gelatin solution comprises the following raw materials in percentage by weight: 35-45% of gelatin, 10-15% of glycerol and 10-15% of sorbitol, and the balance of water.
Preferably, the gelatin solution comprises the following raw materials in percentage by weight: 40% of gelatin, 12% of glycerol, 15% of sorbitol and 33% of water.
Preferably, the gelatin solution comprises the following raw materials in percentage by weight: 35% of gelatin, 15% of glycerol, 15% of sorbitol and 35% of water.
Preferably, the gelatin solution comprises the following raw materials in percentage by weight: 45% of gelatin, 10% of glycerol, 14% of sorbitol and 31% of water.
Preferably, the specific steps for preparing the yang-strengthening food are as follows: the male deer blood plasma freeze-dried powder with a certain proportion is filled into the donkey penis gelatin hollow capsule to prepare the yang-strengthening food with biological activity, and the amount of the male deer blood plasma freeze-dried powder added is two thirds to four fifths of the volume of the donkey penis gelatin hollow capsule.
Compared with the prior art, the invention has the beneficial effects that:
1. deer blood has strong yang-strengthening effects of tonifying deficiency, benefiting essence and blood and the like, and deer blood plasma is used as a main functional component of the deer blood effect and has active proteins such as various biological enzymes, growth factors and the like. The method adopts freeze drying technology to freeze dry deer blood plasma into powder, and retains the complete yang-strengthening biological function.
2. The donkey penis also has strong yang-strengthening efficacy, the donkey penis collagen polypeptide is obtained by processing the donkey penis collagen polypeptide through a biological enzyme preparation, the donkey penis collagen polypeptide can be digested within 3 hours, the digestion speed is high, the molecular weight can be smaller than or equal to 3000Da, meanwhile, donkey penis collagen peptide and edible gelatin are reasonably matched, not only the active ingredients of collagen are retained, but also the donkey penis collagen polypeptide can be molded for different purposes, and the gas in the mixed sol can be further removed by simultaneously using ultrasonic and vacuum treatment, so that the donkey penis collagen capsule is more uniform after molding, and the donkey penis collagen capsule is prepared, and is convenient to take while the complete yang-strengthening medicinal value of the donkey penis collagen capsule is retained.
3. The invention fills the lyophilized powder of the male deer blood plasma in a certain proportion into the donkey penis gelatin hollow capsule to prepare the yang-strengthening food with biological activity, and can furthest exert the medical health-care value of the double yang-strengthening of the deer blood and the donkey penis.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The invention provides the following technical scheme:
example 1
A preparation method of yang-strengthening food capable of retaining biological activity to the maximum extent comprises the following specific steps:
s1: preparing the male deer plasma freeze-dried powder;
s2: preparing a donkey penis gelatin hollow capsule;
s3: preparing yang-strengthening food.
The specific steps for preparing the male deer plasma freeze-dried powder in the embodiment are as follows:
s11: taking fresh male deer blood, and mixing the fresh male deer blood with an anticoagulant according to the ratio of 6: 1, filtering after mixing, adding an isovolumetric 0.9% NaCl aqueous solution into filtered blood for washing, adding into a centrifuge, controlling the rotating speed to 3000rpm for centrifuging for 10min, removing supernatant, repeatedly washing for 2 times, and removing lower layer red blood cells;
s12: packaging the upper layer plasma in a clean sterile container, placing in a temperature control box, controlling the temperature at 70 deg.C, and sterilizing for 1 hr;
s13: controlling the temperature in the temperature control box, pre-freezing for 30min after cooling to-20 ℃, and then rapidly cooling to-80 ℃ for rapid freezing and solidification;
s14: freezing and solidifying the blood plasma for 1h, and freeze-drying and sterilizing to obtain the blood plasma freeze-dried powder.
The specific steps for preparing the donkey penis gelatin empty capsule in the embodiment are as follows:
s21: cutting donkey penis into blocks, soaking in alkali liquor, cleaning, removing fishy smell, placing in distilled water, heating and boiling, adding concentrated alkali to adjust pH to 10, soaking for 35h, taking out donkey penis, soaking in distilled water, cleaning, simultaneously adding active carbon, soaking for 2h, repeatedly washing with distilled water, filtering, and draining;
s22: cleaning the processed donkey penis, crushing, adjusting the pH to 8.0 by NaOH, adding 4.8% of papain and trypsin, heating to 50 ℃, keeping the temperature for 4 hours, and performing ultrasonic-assisted enzymolysis for 2.5 hours under the condition of 200W;
s23: after complete enzymolysis, rapidly heating to 100 deg.C, boiling for 15min for inactivation, cooling to room temperature, filtering with 0.45 μm filter membrane to remove bacteria and impurities, and spray drying the filtrate to obtain collagen polypeptide of testis Et penis equi;
s24: mixing gelatin, glycerol, sorbitol and water at room temperature in proportion, placing the mixture in a heating tank, setting the temperature at 75 deg.C, vacuum heating and stirring for 30-40min until the gel blocks melt to obtain gelatin solution;
s25: placing donkey penis collagen peptide in water at room temperature according to the weight ratio of 1: 1, mixing, heating to 65 ℃ in vacuum, and stirring for 40min until the mixture is melted;
s26: mixing the prepared gelatin solution and donkey penis collagen peptide according to the ratio of 8: 2, and adding 10 percent of plasticizer and 5 percent of surfactant into a stirring tank preheated to 60 ℃ according to the mass percentage, and stirring to fully and uniformly mix;
s27: placing the glue solution in a constant-temperature water bath kettle at the temperature of 40 ℃ and stirring until a uniform flowing glue solution is formed;
s28: performing ultrasonic degassing on the prepared glue solution in an ultrasonic processor with the frequency of 40kHz, and then placing the glue solution under the vacuum pressure of 0.08MPa until the solution becomes clear and transparent to form a uniform shell material;
s29: transferring the degassed shell material into a preheated holding tank, setting the temperature at 60 ℃ for 4h, using for subsequent encapsulation, immersing the die rod of the capsule grinding tool into mustard oil for sufficient lubrication, uniformly covering a layer of mustard oil layer on the surface of the die rod, immersing the lubricated die rod of the capsule grinding tool into glue solution for 10s, slowly lifting the die, turning over for 6 times to uniformly distribute the glue solution on the surface of the die, rapidly solidifying with cold water, transferring the solidified capsule into a constant temperature dryer, setting the temperature for drying at 40 ℃, and drying for 45 min;
s210: pulling out the blastocyst after moisture regaining, cutting according to the required proportion size, combining the cut capsule body and the cut capsule cap to obtain a capsule shell finished product, and sterilizing the prepared capsule shell finished product by adopting an ozone sterilization method, wherein the ozone pressure is 0.2MPa, and the sterilization time is 3 min.
Specifically, the particle size of the pulverized donkey penis in step S22 is 70 mesh sieve, and the ratio of papain and trypsin added in step S22 is 1: 1.
it is worth to be noted that the gelatin solution comprises the following raw materials in percentage by weight: 40% of gelatin, 12% of glycerol, 15% of sorbitol and 33% of water.
The specific steps for preparing the yang-strengthening food in this embodiment are as follows: the male deer blood plasma freeze-dried powder with a certain proportion is filled into the donkey penis gelatin hollow capsule to prepare the yang-strengthening food with biological activity, and the amount of the male deer blood plasma freeze-dried powder added is two thirds to four fifths of the volume of the donkey penis gelatin hollow capsule.
Example 2
A preparation method of yang-strengthening food capable of retaining biological activity to the maximum extent comprises the following specific steps:
s1: preparing the male deer plasma freeze-dried powder;
s2: preparing a donkey penis gelatin hollow capsule;
s3: preparing yang-strengthening food.
The specific steps for preparing the male deer plasma freeze-dried powder in the embodiment are as follows:
s11: taking fresh male deer blood, and mixing the fresh male deer blood with an anticoagulant according to the ratio of 6: 1, filtering after mixing, adding an isovolumetric 0.9% NaCl aqueous solution into filtered blood for washing, adding into a centrifuge, controlling the rotating speed to be 3200rpm for centrifugation for 12min, removing supernatant, repeatedly washing for 3 times, and removing lower layer red blood cells;
s12: packaging the upper layer plasma in a clean sterile container, and placing in a temperature control box, controlling the temperature at 73 ℃, and sterilizing for 1.2 h;
s13: controlling the temperature in the temperature control box, pre-freezing for 40min after cooling to-20 ℃, and then rapidly cooling to-80 ℃ for rapid freezing and solidification;
s14: freezing the blood plasma for 1.5h, and freeze drying and sterilizing to obtain the blood plasma freeze-dried powder.
The specific steps for preparing the donkey penis gelatin empty capsule in the embodiment are as follows:
s21: cutting donkey penis into blocks, soaking in alkali liquor, cleaning, removing fishy smell, placing in distilled water, heating and boiling, adding concentrated alkali to adjust pH to 12, soaking for 37h, taking out donkey penis, soaking in distilled water, cleaning, simultaneously adding active carbon, soaking for 2.2h, repeatedly washing with distilled water, filtering, and draining;
s22: cleaning the processed donkey penis, crushing, adjusting the pH to 8.0 by NaOH, adding 5% of papain and trypsin, heating to 50 ℃, keeping the temperature for 4 hours, and performing ultrasonic-assisted enzymolysis for 2 hours under the condition of 300W;
s23: after complete enzymolysis, rapidly heating to 100 deg.C, boiling for 18min for inactivation, cooling to room temperature, filtering with 0.45 μm filter membrane to remove bacteria and impurities, and spray drying the filtrate to obtain collagen polypeptide of testis Et penis equi;
s24: mixing gelatin, glycerol, sorbitol and water at room temperature in proportion, placing the mixture in a heating tank, setting the temperature at 72 deg.C, vacuum heating and stirring for 35min until the gel blocks are melted to obtain gelatin solution;
s25: placing donkey penis collagen peptide in water at room temperature according to the weight ratio of 1: mixing at a ratio of 1, heating to 62 ℃ in vacuum, and stirring for 42min to melt;
s26: mixing the prepared gelatin solution and donkey penis collagen peptide according to the ratio of 8: 2, and adding 15% of plasticizer and 8% of surfactant into a stirring tank preheated to 60 ℃ according to the mass percentage, and stirring to fully and uniformly mix;
s27: placing the glue solution in a constant-temperature water bath kettle at the temperature of 50 ℃ and stirring until a uniform flowing glue solution is formed;
s28: performing ultrasonic degassing on the prepared glue solution in an ultrasonic processor with the frequency of 60kHz, and then placing the glue solution under the vacuum pressure of 0.09MPa until the solution becomes clear and transparent to form a uniform shell material;
s29: transferring the degassed shell material into a preheated holding tank, setting the temperature at 65 deg.C for 4.5h for subsequent encapsulation, soaking the die rod of the capsule grinding tool in mustard oil for sufficient lubrication to uniformly coat a layer of semen Brassicae Junceae oil layer on the surface, soaking the lubricated die rod of the capsule grinding tool in glue solution for 15s, slowly lifting the die, turning over for 3 times to uniformly distribute the glue solution on the surface of the die, rapidly solidifying with cold water, transferring the solidified capsule into a constant temperature drier, setting the drying temperature at 50 deg.C, and drying for 46 min;
s210: pulling out the blastocyst after moisture regaining, cutting according to the required proportion size, combining the cut capsule body and the cut capsule cap to obtain a capsule shell finished product, and sterilizing the prepared capsule shell finished product by adopting an ozone sterilization method, wherein the ozone pressure is 0.2MPa, and the sterilization time is 5 min.
Specifically, the particle size of the pulverized donkey penis in step S22 is 75 meshes, and the ratio of papain to trypsin added in step S22 is 1: 1.
it is worth to be noted that the gelatin solution comprises the following raw materials in percentage by weight: 35% of gelatin, 15% of glycerol, 15% of sorbitol and 35% of water.
The specific steps for preparing the yang-strengthening food in this embodiment are as follows: the male deer blood plasma freeze-dried powder with a certain proportion is filled into the donkey penis gelatin hollow capsule to prepare the yang-strengthening food with biological activity, and the amount of the male deer blood plasma freeze-dried powder added is two thirds to four fifths of the volume of the donkey penis gelatin hollow capsule.
Example 3
A preparation method of yang-strengthening food capable of retaining biological activity to the maximum extent comprises the following specific steps:
s1: preparing the male deer plasma freeze-dried powder;
s2: preparing a donkey penis gelatin hollow capsule;
s3: preparing yang-strengthening food.
The specific steps for preparing the male deer plasma freeze-dried powder in the embodiment are as follows:
s11: taking fresh male deer blood, and mixing the fresh male deer blood with an anticoagulant according to the ratio of 6: 1, filtering after mixing, adding an isovolumetric 0.9% NaCl aqueous solution into the filtered blood for washing, adding into a centrifuge, controlling the rotating speed to be 3500rpm for centrifuging for 10min, removing supernatant, repeatedly washing for 2 times, and removing lower layer red blood cells;
s12: packaging the upper layer plasma in a clean sterile container, placing in a temperature control box, controlling the temperature at 75 ℃, and sterilizing for 1 h;
s13: controlling the temperature in the temperature control box, pre-freezing for 50min after cooling to-20 ℃, and then rapidly cooling to-80 ℃ for rapid freezing and solidification;
s14: freezing and solidifying the blood plasma for 2h, and freeze-drying and sterilizing to obtain the blood plasma freeze-dried powder.
The specific steps for preparing the donkey penis gelatin empty capsule in the embodiment are as follows:
s21: cutting donkey penis into blocks, soaking in alkali liquor, cleaning, removing fishy smell, placing in distilled water, heating and boiling, adding concentrated alkali to adjust pH to 13, soaking for 35h, taking out donkey penis, soaking in distilled water, cleaning, simultaneously adding active carbon, soaking for 2.5h, repeatedly washing with distilled water, filtering, and draining;
s22: cleaning the processed donkey penis, crushing, adjusting the pH value to 8.0 by NaOH, adding 5.5% of papain and trypsin, heating to 50 ℃, keeping the temperature for 4 hours, and performing ultrasonic-assisted enzymolysis for 2 hours under the condition of 400W;
s23: after complete enzymolysis, rapidly heating to 100 deg.C, boiling for 15min for inactivation, cooling to room temperature, filtering with 0.45 μm filter membrane to remove bacteria and impurities, and spray drying the filtrate to obtain collagen polypeptide of testis Et penis equi;
s24: mixing gelatin, glycerol, sorbitol and water at room temperature in proportion, placing the mixture in a heating tank, setting the temperature at 70 deg.C, vacuum heating and stirring for 40min until the gel blocks melt to obtain gelatin solution;
s25: placing donkey penis collagen peptide in water at room temperature according to the weight ratio of 1: 1, mixing, heating to 65 ℃ in vacuum, and stirring for 40min until the mixture is melted;
s26: mixing the prepared gelatin solution and donkey penis collagen peptide according to the ratio of 8: 2, and simultaneously adding 20% of plasticizer and 5% of surfactant according to the mass percentage, and stirring in a stirring tank preheated to 60 ℃ to fully and uniformly mix the mixture;
s27: placing the glue solution in a constant-temperature water bath kettle at the temperature of 40-70 ℃ and stirring until a uniform flowing glue solution is formed;
s28: performing ultrasonic degassing on the prepared glue solution in an ultrasonic processor with the frequency of 20kHz-120kHz, and then placing the glue solution under the vacuum pressure of 0.08-0.09MPa until the solution becomes clear and transparent to form a uniform shell material;
s29: transferring the degassed shell material into a preheated holding tank, setting the temperature at 65 deg.C for 4.55h for subsequent encapsulation, soaking the die rod of the capsule grinding tool in mustard oil for sufficient lubrication to uniformly coat a layer of semen Brassicae Junceae oil layer on the surface, soaking the lubricated die rod of the capsule grinding tool in glue solution for 15s, slowly lifting the die, turning over for 6 times to uniformly distribute the glue solution on the surface of the die, rapidly solidifying with cold water, transferring the solidified capsule into a constant temperature drier, setting the drying temperature at 45 deg.C, and drying for 42 min;
s210: pulling out the blastocyst after moisture regaining, cutting according to the required proportion size, combining the cut capsule body and the cut capsule cap to obtain a capsule shell finished product, and sterilizing the prepared capsule shell finished product by adopting an ozone sterilization method, wherein the ozone pressure is 0.2MPa, and the sterilization time is 5 min.
Specifically, the particle size of the pulverized donkey penis in step S22 is 70 mesh sieve, and the ratio of papain and trypsin added in step S22 is 1: 1.
it is worth to be noted that the gelatin solution comprises the following raw materials in percentage by weight: 45% of gelatin, 10% of glycerol, 14% of sorbitol and 31% of water.
The specific steps for preparing the yang-strengthening food in this embodiment are as follows: the male deer blood plasma freeze-dried powder with a certain proportion is filled into the donkey penis gelatin hollow capsule to prepare the yang-strengthening food with biological activity, and the amount of the male deer blood plasma freeze-dried powder added is two thirds to four fifths of the volume of the donkey penis gelatin hollow capsule.
Compared with the existing yang-tonifying food, the digestion speed, the functional effect and the molecular weight of the capsule wall materials of the pigskin collagen produced by the preparation method of the yang-tonifying food which maintains the biological activity to the maximum extent in the three embodiments are shown in the following table.
| Contrast parameter | Digestion speed of capsule wall material/h | Functional effects | Molecular weight/Da |
| Example 1 | 1.58-2.69 | Invigorating kidney, strengthening body constitution, and strengthening tendons and bones | ≤3000 |
| Example 2 | 1.85-2.72 | Invigorating kidney, strengthening body constitution, and strengthening tendons and bones | ≤3000 |
| Example 3 | 1.97-2.57 | Invigorating kidney, strengthening body constitution, and strengthening tendons and bones | ≤3000 |
| Existing | 6.36-7.25 | Is free of | ＞3500 |
As can be seen from the above table, the preparation method of the yang-strengthening food capable of furthest retaining the biological activity can retain the active ingredients of the collagen and can also be shaped for different purposes by adding the plasticizer and the surfactant, can further remove the gas existing in the mixed sol by simultaneously using ultrasonic treatment and vacuum treatment so as to ensure that the mixed sol is more uniform after being shaped, combines the donkey penis capsule shell and the freeze-dried deer plasma dry powder to prepare the capsule, can furthest combine the medicinal values of the donkey penis capsule and the freeze-dried deer plasma dry powder simultaneously, further enhances the medicinal value of the donkey penis capsule, can be digested within 3 hours, has high digestion speed, has the molecular weight less than or equal to 3000Da, reasonably matches the donkey penis collagen peptide with edible gelatin, retains the active ingredients of the collagen, can also be shaped for different purposes, and has good kidney tonifying and body strengthening effects, Has effects of strengthening tendons and bones, and the edible gelatin is also beneficial to the digestion of food, and the combination of the two can further strengthen the respective effects.
The foregoing shows and describes the general principles, essential features, and advantages of the invention. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, and the preferred embodiments of the present invention are described in the above embodiments and the description, and are not intended to limit the present invention. The scope of the invention is defined by the appended claims and equivalents thereof.
Claims (10)
1. A preparation method of yang-strengthening food capable of retaining biological activity to the maximum extent is characterized in that: the method comprises the following specific steps:
s1: preparing the male deer plasma freeze-dried powder;
s2: preparing a donkey penis gelatin hollow capsule;
s3: preparing yang-strengthening food.
2. The method for preparing yang-invigorating food with maximum retention of bioactivity according to claim 1, wherein the method comprises the following steps: the preparation method of the male deer plasma freeze-dried powder comprises the following specific steps:
s11: taking fresh male deer blood, and mixing the fresh male deer blood with an anticoagulant according to the ratio of 6: 1, filtering after mixing, adding an equal volume of 0.9% NaCl aqueous solution into the filtered blood for washing, adding the blood into a centrifugal machine, controlling the rotating speed to 3000 and 3500rpm for centrifuging for 10-15min, removing supernatant, repeatedly washing for 2-3 times, and discarding lower layer red blood cells;
s12: packaging the upper layer plasma in a clean sterile container, placing in a temperature control box, and sterilizing at 70-75 deg.C for 1-1.5 hr;
s13: controlling the temperature in the temperature control box, pre-freezing for 30-60min after cooling to-20 ℃, and then rapidly cooling to-80 ℃ for rapid freezing and solidification;
s14: freezing and solidifying the blood plasma for 1-2h, and freeze drying and sterilizing to obtain the blood plasma freeze-dried powder.
3. The method for preparing yang-invigorating food with maximum retention of bioactivity according to claim 1, wherein the method comprises the following steps: the preparation method of the donkey penis gelatin hollow capsule comprises the following specific steps:
s21: cutting donkey penis into blocks, soaking in alkali liquor, cleaning, removing fishy smell, placing in distilled water, heating and boiling, adding concentrated alkali to adjust pH to 10-13, soaking for 35-40h, taking out donkey penis, soaking in distilled water, cleaning, simultaneously adding active carbon, soaking for 2-2.5h, repeatedly washing with distilled water, filtering, and draining;
s22: cleaning the processed donkey penis, crushing, adjusting the pH value to 8.0 by NaOH, adding 4.8-5.5% of papain and trypsin, heating to 50 ℃, keeping the temperature for 4 hours, and performing ultrasonic-assisted enzymolysis for 1-5 hours under the condition of 200-500W;
s23: after complete enzymolysis, rapidly heating to 100 deg.C, boiling for 15-20min for inactivation, cooling to room temperature, filtering with 0.45 μm filter membrane to remove bacteria and impurities, and spray drying the filtrate to obtain donkey penis collagen polypeptide;
s24: mixing gelatin, glycerol, sorbitol and water at room temperature in proportion, placing the mixture in a heating tank, setting the temperature at 70-75 deg.C, vacuum heating and stirring for 30-40min until the gel blocks melt to obtain gelatin solution;
s25: placing donkey penis collagen peptide in water at room temperature according to the weight ratio of 1: 1, mixing, heating to 60-65 ℃ in vacuum, and stirring for 40-45min until the mixture is melted;
s26: mixing the prepared gelatin solution and donkey penis collagen peptide according to the ratio of 8: 2, and simultaneously adding 0.1-30% of plasticizer and 0.001-10% of surfactant according to the mass percentage, and stirring in a stirring tank preheated to 60 ℃ to fully and uniformly mix the components;
s27: placing the glue solution in a constant-temperature water bath kettle at the temperature of 40-70 ℃ and stirring until a uniform flowing glue solution is formed;
s28: performing ultrasonic degassing on the prepared glue solution in an ultrasonic processor with the frequency of 20kHz-120kHz, and then placing the glue solution under the vacuum pressure of 0.08-0.09MPa until the solution becomes clear and transparent to form a uniform shell material;
s29: transferring the degassed shell material into a preheated holding tank, setting the temperature at 60-65 deg.C for 4-4.5h, using for subsequent encapsulation, immersing the die rod of the capsule grinding tool in mustard oil for sufficient lubrication to coat a layer of semen Brassicae Junceae oil layer on the surface, immersing the lubricated die rod of the capsule grinding tool in the glue solution for 5-20s, slowly lifting the mold, turning over for 3-7 times to uniformly distribute the glue solution on the surface of the mold, rapidly solidifying with cold water, transferring the solidified capsule into a constant temperature dryer, setting the drying temperature at 40-60 deg.C, and drying for 40-45 min;
s210: pulling out the blastocyst after moisture regaining, cutting according to the required proportion size, combining the cut capsule body and the cut capsule cap to obtain a capsule shell finished product, and sterilizing the prepared capsule shell finished product by adopting an ozone sterilization method, wherein the ozone pressure is 0.2MPa, and the sterilization time is 1-10 min.
4. The method for preparing yang-invigorating food with maximum retention of bioactivity according to claim 3, wherein the food comprises: in the step S22, the crushed donkey penis has the particle size of being sieved by a sieve of 70-80 meshes.
5. The method for preparing yang-invigorating food with maximum retention of bioactivity according to claim 3, wherein the food comprises: in step S22, papain and trypsin are added in a ratio of 1: 1.
6. the method for preparing yang-invigorating food with maximum retention of bioactivity according to claim 3, wherein the food comprises: the gelatin solution comprises the following raw materials in percentage by weight: 35-45% of gelatin, 10-15% of glycerol and 10-15% of sorbitol, and the balance of water.
7. The method for preparing yang-invigorating food with maximum retention of biological activity according to claim 6, wherein: the gelatin solution comprises the following raw materials in percentage by weight: 40% of gelatin, 12% of glycerol, 15% of sorbitol and 33% of water.
8. The method for preparing yang-invigorating food with maximum retention of biological activity according to claim 6, wherein: the gelatin solution comprises the following raw materials in percentage by weight: 35% of gelatin, 15% of glycerol, 15% of sorbitol and 35% of water.
9. The method for preparing yang-invigorating food with maximum retention of biological activity according to claim 6, wherein: the gelatin solution comprises the following raw materials in percentage by weight: 45% of gelatin, 10% of glycerol, 14% of sorbitol and 31% of water.
10. The method for preparing yang-invigorating food with maximum retention of bioactivity according to claim 1, wherein the method comprises the following steps: the specific steps for preparing the yang-strengthening food are as follows: the male deer blood plasma freeze-dried powder with a certain proportion is filled into the donkey penis gelatin hollow capsule to prepare the yang-strengthening food with biological activity, and the amount of the male deer blood plasma freeze-dried powder added is two thirds to four fifths of the volume of the donkey penis gelatin hollow capsule.
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