CN112494983A - Extraction process method and extraction equipment of phytosterol - Google Patents

Extraction process method and extraction equipment of phytosterol Download PDF

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Publication number
CN112494983A
CN112494983A CN202011319812.4A CN202011319812A CN112494983A CN 112494983 A CN112494983 A CN 112494983A CN 202011319812 A CN202011319812 A CN 202011319812A CN 112494983 A CN112494983 A CN 112494983A
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CN
China
Prior art keywords
stirring
fixed
standing
driving motor
filtering
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Pending
Application number
CN202011319812.4A
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Chinese (zh)
Inventor
杨品红
易晓千
邢浩男
李璟
张芳玲
夏杭静
莫亚琼
宁悦
类延菊
徐文思
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Hunan University of Arts and Science
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Hunan University of Arts and Science
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Publication date
Application filed by Hunan University of Arts and Science filed Critical Hunan University of Arts and Science
Priority to CN202011319812.4A priority Critical patent/CN112494983A/en
Publication of CN112494983A publication Critical patent/CN112494983A/en
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D11/00Solvent extraction
    • B01D11/02Solvent extraction of solids
    • B01D11/0215Solid material in other stationary receptacles
    • B01D11/0253Fluidised bed of solid materials
    • B01D11/0257Fluidised bed of solid materials using mixing mechanisms, e.g. stirrers, jets
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D36/00Filter circuits or combinations of filters with other separating devices
    • B01D36/04Combinations of filters with settling tanks
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07JSTEROIDS
    • C07J9/00Normal steroids containing carbon, hydrogen, halogen or oxygen substituted in position 17 beta by a chain of more than two carbon atoms, e.g. cholane, cholestane, coprostane

Abstract

The invention discloses a process for extracting phytosterol and extraction equipment thereof, which relate to the technical field of fine chemical engineering, the process comprises the steps of placing plant raw materials in an organic solvent, heating for dissolving, standing for layering, keeping constant temperature for carrying out crystal growing operation on the standing stock solution, filtering the stock solution after standing for a certain time, recovering filtrate, placing filter residues in a place with the external temperature of 10-30 ℃ for air drying, adding 2-5 times of volume of an extracting agent into the recovered filtrate, stirring and extracting at the position of 10-40 ℃ at the stirring speed of 100-400r/min, standing for layering, washing with water and an alkaline ethanol solution for multiple times, recovering the extraction liquid, drying to obtain the sterol, solving the problems that the traditional extraction method needs a large amount of organic solvent and wastes the organic solvent, and the traditional purification process is easy to cause the problem that the purity of the sterol is relatively low.

Description

Extraction process method and extraction equipment of phytosterol
Technical Field
The invention relates to the technical field of fine chemical engineering, in particular to a process method for extracting phytosterol and extraction equipment thereof.
Background
Sterols (also called sterols), which are a class of steroids, are hydroxyl-containing steroids. They are called steroid compounds because they have a basic structure of cyclopentanoperhydrophenanthrene and contain hydroxyl groups. The lipid in animal and plant tissues is extracted by alkaline solution, wherein the lipid is often a substance which is not saponified by alkali in different amounts. Steroid compounds are widely distributed in the biological world. Such as cholesterol, are important components of higher animal cells. It forms cholesteryl esters with long chain fatty acids, an important component of plasma lipoproteins and cell membranes. Plant cell membranes contain other sterols such as stigmasterol and sitosterol. Fungi and yeasts contain sterols.
The traditional extraction method of the phytosterol has certain defects, a large amount of organic solvent is needed in the traditional extraction method, the waste of the organic solvent is caused, and the traditional purification process easily causes the relatively low purity of the sterol.
Disclosure of Invention
Aiming at the defects of the prior art, the invention provides a process and equipment for extracting phytosterol, which solves the problems that a large amount of organic solvent is needed in the traditional extraction method, so that the organic solvent is wasted, and the traditional purification process is easy to cause relatively low purity of the phytosterol.
In order to achieve the purpose, the invention is realized by the following technical scheme: a phytosterol extraction device comprises a bottom bracket, wherein a side bracket is fixedly arranged on the upper side of the bottom bracket, an upper bracket is fixedly arranged on the upper side of the side bracket, an upper driving motor is fixedly arranged on the surface of the upper side of the upper bracket, a stirring rod assembly is fixedly arranged on a driving shaft of the upper driving motor through a coupler, a bearing block is fixedly arranged at the middle section of the surface of the side bracket, a control panel is fixedly arranged on the upper side of the side wall of the side bracket, a motor fixing frame is fixedly arranged on the outer part of one side of the side bracket, a side driving motor is arranged in the motor fixing frame, a stirring tank body is rotatably arranged in the side bracket through the bearing block, a limiting rod and a rotating shaft are fixedly arranged on the surface of the side wall of the stirring tank body, a liquid outlet is arranged on the surface of the bottom of the stirring tank, and a lower collecting box is arranged on the upper surface of the bottom support.
Furthermore, the stirring tank body is connected with the bearing block through a rotating shaft in a rotating mode, and the side driving motor is fixedly connected with one end of the rotating shaft through a coupler.
Further, the stirring rod subassembly includes the stirring bull stick, the stirring bull stick crisscross fixed a plurality of branches that are provided with on the surface, the stirring bull stick be provided with a plurality of panels through branch is fixed on the surface.
Further, the filter tank comprises a filter tank main body fixed on the side support, and the bottom inside the filter tank main body is fixedly provided with an adjusting filter;
the adjusting filter comprises an internal filtering screen fixed at the bottom of the filtering tank main body, and an external filtering screen is rotatably arranged outside the internal filtering screen.
Further, the filter tank main body is a combined frame member with a hollow interior.
Furthermore, the extraction equipment of the extraction process method of the phytosterol further comprises a tiling mechanism, the tiling mechanism comprises a platform fixed on an external base body, hydraulic cylinders are fixedly arranged at four corners of the surface of the platform, an upper substrate is fixedly arranged on the driving end of each hydraulic cylinder, and an upper driving motor is fixedly arranged on the upper surface of the upper substrate.
Further, go up through shaft coupling fixedly connected with side pivot on driving motor's the drive end, be provided with the threaded rod through the fixed connecting block down on the upper and lower end of side pivot, the side pivot slide on the surface and be provided with the connecting piece, the connecting piece slides and sets up on the threaded rod.
Further, the threaded rod is provided with the restriction nut with the screw thread mode on the surface, the fixed mounting bracket that is provided with in one side of connecting piece, the inside of mounting bracket is rotated and is provided with the tiling roller bearing.
The invention also provides an extraction process method of the phytosterol, which comprises the following steps:
step S1: placing plant raw materials in an organic solvent, heating for dissolving, and then standing for layering;
step S2: keeping constant temperature to carry out crystal growing operation on the standing stock solution;
step S3: filtering the stock solution which is kept standing for a certain time in the step S2, recovering the filtrate, and air-drying the filter residue at the outside temperature of 10-30 ℃;
step S4: adding 2-5 times of volume of extractant into the recovered filtrate in the step S3, stirring and extracting at the position of 10-40 ℃ at the stirring speed of 100-400r/min, adding the stock solution into the stirring tank from the feed pipe, stirring under the action of the stirring rod assembly, and turning over the stock solution in the stirring tank under the action of the rotating shaft and the side driving motor;
step S5: standing for layering, washing with water and alkaline ethanol solution for multiple times, recovering the extract, discharging the solution from the outlet of the stirring tank, filtering, collecting the filtrate in the lower collecting tank, and drying to obtain sterol.
Further, the organic solvent in step S1 is acetone, and the volume ratio of the plant material to the organic solvent is 1: 10-30 g/ml.
Further, the temperature of the heating dissolution in the step S1 is 40 to 80 ℃.
Further, the standing time in the step S3 is 60-120 min.
Advantageous effects
The invention provides a process method for extracting phytosterol and extraction equipment thereof. Compared with the prior art, the method has the following beneficial effects:
1. a process for extracting phytosterol from plant material includes such steps as putting the plant material in organic solvent, heating for dissolving, standing for layering, keeping constant temperature for crystal growing, standing for a certain time for filtering, recovering filtrate, air drying the filter residue at 10-30 deg.C, adding 2-5 times of extractant into the recovered filtrate, stirring and extracting at 10-40 deg.C at stirring speed of 100-400r/min, standing for layering, washing with water and alkaline ethanol solution for several times, and the extraction liquid is recovered, and then the sterol is obtained by drying, so that the problems that a large amount of organic solvent is needed in the traditional extraction method, the organic solvent is wasted, and the traditional purification process easily causes relatively low purity of the sterol are solved.
2. A phytosterol extraction process and extraction equipment thereof, wherein a side bracket is fixedly arranged on the upper side of a bottom bracket, an upper bracket is fixedly arranged on the upper side of the side bracket, an upper driving motor is fixedly arranged on the surface of the upper side of the upper bracket, a stirring rod assembly is fixedly arranged on a driving shaft of the upper driving motor through a coupling, a bearing block is fixedly arranged at the middle section of the surface of the side bracket, a control panel is fixedly arranged on the upper side of the side wall of the side bracket, a motor fixing bracket is fixedly arranged on the outer part of one side of the side bracket, a side driving motor is arranged in the motor fixing bracket, a stirring tank body is rotatably arranged in the side bracket through the bearing block, a limiting rod and a rotating shaft are fixedly arranged on the surface of the side wall of the stirring tank body, a liquid outlet is arranged on the surface of the bottom of the stirring, the stirring and filtering device can efficiently stir and filter when in use, and is integrated equipment, so that the waste of time and the waste of stock solution caused by transfer equipment are avoided.
3. A process for extracting phytosterol and its extraction equipment, comprises a platform fixed on the external base body by a tiling mechanism, hydraulic cylinders are fixed at four corners of the surface of the platform, an upper base plate is fixed on the driving end of each hydraulic cylinder, an upper driving motor is fixed on the upper surface of the upper base plate, a square rotating shaft is fixedly connected on the driving end of the upper driving motor by a coupler, a threaded rod is fixedly arranged on the upper and lower ends of the square rotating shaft by a lower connecting block, a connecting piece is slidably arranged on the surface of the square rotating shaft, a limiting nut is arranged on the surface of the threaded rod in a threaded manner, a mounting frame is fixedly arranged on one side of the connecting piece, a tiling roller is rotatably arranged in the mounting frame, the dried raw material can be flatly laid and can be adjusted in height according to the amount.
Drawings
FIG. 1 is a schematic structural view of the present invention;
FIG. 2 is a front view of the present invention;
FIG. 3 is a side view of the structure of the present invention;
FIG. 4 is a rear view of the structure of the present invention;
FIG. 5 is a top view of the structure of the present invention;
FIG. 6 is a schematic view of the construction of the stirring rod assembly of the present invention;
FIG. 7 is a schematic view of a canister according to the present invention;
FIG. 8 is a schematic view of a conditioning filter according to the present invention;
FIG. 9 is a top view of a canister construction according to the present invention;
fig. 10 is a schematic structural diagram of the tiling mechanism of the present invention.
In the figure: 1. an upper drive motor; 2. an upper bracket; 3. a feed pipe; 4. a stirring rod assembly; 41. a stirring rotating rod; 42. a strut; 43. a panel; 5. a stirring tank body; 6. a restraining bar; 7. a bearing block; 8. a rotating shaft; 10. a liquid outlet; 11. a side bracket; 12. a filter tank; 121. a canister body; 122. adjusting the filter; 1221. a filtering net cover is arranged outside; 1222. a filtering net cover is arranged in the filter; 13. a lower collection box; 14. a bottom bracket; 15. a flat laying mechanism; 151. an upper drive motor; 152. an upper substrate; 153. a hydraulic cylinder; 154. a threaded rod; 155. a connecting member; 156. a restraining nut; 157. a lower connecting block; 158. a platform; 159. a mounting frame; 1510. flatly laying the rolling shafts; 1511. a square rotating shaft; 16. a side drive motor; 17. a motor fixing frame; 18. a control panel.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Referring to fig. 1-10, an extraction apparatus for phytosterol comprises a bottom bracket 14, a side bracket 11 is fixedly arranged on the upper side of the bottom bracket 14, an upper bracket 2 is fixedly arranged on the upper side of the side bracket 11, an upper driving motor 1 is fixedly arranged on the surface of the upper side of the upper bracket 2, a stirring rod assembly 4 is fixedly arranged on a driving shaft of the upper driving motor 1 through a coupling, a bearing block 7 is fixedly arranged at the middle section of the surface of the side bracket 11, a control panel 18 is fixedly arranged on the upper side of the side wall of the side bracket 11, a motor fixing frame 17 is fixedly arranged on the outer portion of one side of the side bracket 11, a side driving motor 16 is arranged inside the motor fixing frame 17, a stirring tank body 5 is rotatably arranged inside the side bracket 11 through the bearing block 7, a limiting rod 6 and a rotating shaft 8 are fixedly arranged on the surface of the side wall, a filter tank 12 is fixedly arranged on the bottom side wall of the side bracket 11, and a lower collecting box 13 is arranged on the upper surface of the bottom bracket 14.
As a preferred embodiment of the present invention: the stirring tank body 5 is rotatably connected with the bearing block 7 through the rotating shaft 8, and the side driving motor 16 is fixedly connected with one end of the rotating shaft 8 through a coupler.
As a preferred embodiment of the present invention: the stirring rod assembly 4 comprises a stirring rotating rod 41, a plurality of support rods 42 are fixedly arranged on the surface of the stirring rotating rod 41 in a staggered mode, and a plurality of panels 43 are fixedly arranged on the surface of the stirring rotating rod 41 through the support rods 42.
As a preferred embodiment of the present invention: the filtering tank 12 comprises a filtering tank main body 121 fixed on the side bracket 11, the filtering tank main body 121 is a hollow combined frame member, the bottom inside the filtering tank main body 121 is fixedly provided with an adjusting filter 122, the adjusting filter 122 comprises an internal filtering mesh cover 1222 fixed at the bottom of the filtering tank main body 121, and the external filtering mesh cover 1221 is rotatably arranged outside the internal filtering mesh cover 1222.
As a preferred embodiment of the present invention: still include tiling mechanism 15, tiling mechanism 15 is including fixing the platform 158 on external base member, the fixed pneumatic cylinder 153 that is provided with in surface four corners department of platform 158, all the fixed upper substrate 152 that is provided with on the drive end of every pneumatic cylinder 153, the fixed driving motor 151 that is provided with on the upper surface of upper substrate 152, go up through shaft coupling fixedly connected with side pivot 1511 on the drive end of driving motor 151, be provided with threaded rod 154 through lower connecting block 157 is fixed on the upper and lower end of side pivot 1511, the side pivot 1511 slides on the surface and is provided with connecting piece 155, connecting piece 155 slides and sets up on threaded rod 154, threaded rod 154 is provided with limiting nut 156 with the screw thread mode on the surface, the fixed mounting bracket 159 that is provided with in one side of connecting piece 155, the inside of mounting bracket 159 rotates and.
The embodiment of the invention also provides an extraction process method of the phytosterol, which comprises the following steps:
step S1: placing plant raw materials in an organic solvent, heating for dissolving, and then standing for layering;
step S2: keeping constant temperature to carry out crystal growing operation on the standing stock solution;
step S3: filtering the stock solution which is kept standing for a certain time in the step S2, recovering the filtrate, and air-drying the filter residue at the outside temperature of 10-30 ℃;
step S4: adding 2-5 times of volume of the extracting agent into the recovered filtrate in the step S3 and performing stirring extraction at a position of 10-40 ℃ at a stirring speed of 100-400r/min, adding the stock solution into the stirring tank body 5 from the feeding pipe 3, and performing stirring under the action of the stirring rod assembly 4, and simultaneously turning over the stock solution in the stirring tank body 5 under the action of the rotating shaft 8 and the side driving motor 16;
step S5: standing for layering, washing with water and alkaline ethanol solution for multiple times, recovering the extract, discharging the solution in the stirring tank 5 from the liquid outlet 10, allowing the solution to enter the filtering tank 12, filtering, allowing the solution to flow to the lower collecting tank 13, and drying to obtain sterol.
When the extraction equipment and the extraction method of the extraction process method of the phytosterol are used, the stock solution which is heated and dissolved in the step S1 enters the stirring tank body 5 from the feeding pipe 3, the upper driving motor 1 is started at the same time, the upper driving motor 1 drives the stirring rod assembly 4 to rotate, the supporting rod 42 and the panel 43 on the stirring rod assembly 4 fully stir the whole stock solution in the stirring tank body 5 to help the dissolution effect to be stable, the side driving motor 16 can help the whole stirring tank body 5 to slightly rotate transversely to increase the effect, then the stock solution comes out of the liquid outlet 10 and enters the filtering tank 12, and the difference of the separation effect is ensured by controlling the gap value between the external filtering mesh enclosure 1221 and the internal filtering mesh 1222;
through the effect of last driving motor 151, offer the square pivot 1511 and rotate under last driving motor 151, the cross-section of square pivot 1511 is the rectangle component, and the fixed threaded rod 154 structure that is provided with on the square pivot 1511, connecting piece 155 slides on the square pivot 1511, and confirm the position of tiling roller 1510 on the square pivot 1511, after the solution that comes out from crossing filter tank 12 department enters lower collecting box 13, take out lower collecting box 13 and place to tiling mechanism 15, adjust the height of pneumatic cylinder 153 and place lower collecting box 13 in the bottom of square pivot 1511, and roll through the rotation of tiling roller 1510 and tile dry powder, make things convenient for subsequent high-efficient drying.
It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims (9)

1. The utility model provides an extraction equipment of phytosterol, includes bottom support (14), the fixed collateral branch frame (11) that is provided with of upside of bottom support (14), the fixed upper bracket (2) that is provided with of upside of collateral branch frame (11), its characterized in that, the upside of upper bracket (2) is fixed on the surface and is provided with driving motor (1), it is provided with stirring rod subassembly (4) through the shaft coupling is fixed in the drive shaft of driving motor (1) to go up, the fixed bearing block (7) that is provided with in the middle section of the surface of collateral branch frame (11), the fixed control panel (18) that is provided with of lateral wall upside of collateral branch frame (11), fixed motor mount (17) that is provided with on one side outside of collateral branch frame (11), the inside of motor mount (17) is provided with side driving motor (16), the inside of collateral branch frame (11) is provided with agitator tank body (5) through bearing block (, the side wall surface of the stirring tank body (5) is fixedly provided with a limiting rod (6) and a rotating shaft (8), the bottom surface of the stirring tank body (5) is provided with a liquid outlet (10), the bottom side wall of the side support (11) is fixedly provided with a filtering tank (12), and the upper surface of the bottom support (14) is provided with a lower collecting box (13).
2. The plant sterol extracting apparatus according to claim 1, wherein: the stirring tank body (5) is connected with the bearing block (7) in a rotating mode through the rotating shaft (8), and the side driving motor (16) is fixedly connected with one end of the rotating shaft (8) through the coupler.
3. The plant sterol extracting apparatus according to claim 1, wherein: the stirring rod assembly (4) comprises a stirring rotating rod (41), a plurality of supporting rods (42) are fixedly arranged on the surface of the stirring rotating rod (41) in a staggered mode, and a plurality of panels (43) are fixedly arranged on the surface of the stirring rotating rod (41) through the supporting rods (42).
4. The plant sterol extracting apparatus according to claim 1, wherein: the filter tank (12) comprises a filter tank main body (121) fixed on the side bracket (11), and the bottom inside the filter tank main body (121) is fixedly provided with an adjusting filter (122);
the adjusting filter (122) comprises an internal filtering net cover (1222) fixed at the bottom of the filtering tank main body (121), and an external filtering net cover (1221) is rotatably arranged outside the internal filtering net cover (1222).
5. The plant sterol extraction apparatus according to claim 4, wherein: the filter tank main body (121) is a combined frame member with a hollow interior.
6. The plant sterol extracting apparatus according to claim 1, wherein: still including tiling mechanism (15), tiling mechanism (15) are including fixing platform (158) on external base member, the fixed pneumatic cylinder (153) that is provided with in surface four corners department of platform (158), every all fixed upper substrate (152) that is provided with on the drive end of pneumatic cylinder (153), fixed driving motor (151) of being provided with on the upper surface of upper substrate (152).
7. The plant sterol extracting apparatus according to claim 6, wherein: go up through shaft coupling fixedly connected with side pivot (1511) on the drive end of driving motor (151), the upper and lower end of side pivot (1511) is gone up and is provided with threaded rod (154) through lower connecting block (157) is fixed, the side pivot (1511) slide on the surface and be provided with connecting piece (155), connecting piece (155) slide and set up on threaded rod (154).
8. The plant sterol extracting apparatus according to claim 7, wherein: the threaded rod (154) is provided with a limiting nut (156) on the surface in a threaded mode, one side of the connecting piece (155) is fixedly provided with a mounting rack (159), and the inside of the mounting rack (159) is rotatably provided with a tiled rolling shaft (1510).
9. A process for extracting phytosterol is characterized by comprising the following steps:
step S1: placing plant raw materials in an organic solvent, heating for dissolving, and then standing for layering;
step S2: keeping constant temperature to carry out crystal growing operation on the standing stock solution;
step S3: filtering the stock solution which is kept standing for a certain time in the step S2, recovering the filtrate, and air-drying the filter residue at the outside temperature of 10-30 ℃;
step S4: adding 2-5 times of volume of the extracting agent into the recovered filtrate in the step S3 and performing stirring extraction at a position of 10-40 ℃ at a stirring speed of 100-400r/min, adding the stock solution into the stirring tank body (5) from the feeding pipe (3), stirring by the stirring rod assembly (4), and simultaneously overturning the stock solution in the stirring tank body (5) under the actions of the rotating shaft (8) and the side driving motor (16);
step S5: standing for layering, washing for multiple times by using water and an alkaline ethanol solution, recovering the extract, discharging the solution in the stirring tank body (5) from a liquid outlet (10), entering the inside of a filtering tank (12), filtering, flowing to a lower collecting box (13) after completion, and drying to obtain the sterol.
CN202011319812.4A 2020-11-23 2020-11-23 Extraction process method and extraction equipment of phytosterol Pending CN112494983A (en)

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CN202011319812.4A CN112494983A (en) 2020-11-23 2020-11-23 Extraction process method and extraction equipment of phytosterol

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Application Number Priority Date Filing Date Title
CN202011319812.4A CN112494983A (en) 2020-11-23 2020-11-23 Extraction process method and extraction equipment of phytosterol

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CN112494983A true CN112494983A (en) 2021-03-16

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CN112999690A (en) * 2021-03-27 2021-06-22 合肥九茗信息科技有限公司 Extraction sub-component for extracting Chinese medicinal materials by using ethanol organic solvent
CN113519880A (en) * 2021-07-23 2021-10-22 赣州市倞华菲尔雪食品有限公司 Cake stoste multi-angle stirring and standing separation equipment

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112999690A (en) * 2021-03-27 2021-06-22 合肥九茗信息科技有限公司 Extraction sub-component for extracting Chinese medicinal materials by using ethanol organic solvent
CN113519880A (en) * 2021-07-23 2021-10-22 赣州市倞华菲尔雪食品有限公司 Cake stoste multi-angle stirring and standing separation equipment

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Application publication date: 20210316