CN112461752A - Method for accurately controlling thickness of adhesive layer in tensile shear test of heat-conducting adhesive - Google Patents

Method for accurately controlling thickness of adhesive layer in tensile shear test of heat-conducting adhesive Download PDF

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Publication number
CN112461752A
CN112461752A CN202011127465.5A CN202011127465A CN112461752A CN 112461752 A CN112461752 A CN 112461752A CN 202011127465 A CN202011127465 A CN 202011127465A CN 112461752 A CN112461752 A CN 112461752A
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CN
China
Prior art keywords
thickness
limiting block
adhesive
base material
adhesive layer
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202011127465.5A
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Chinese (zh)
Inventor
陈曲
吴晓宁
王淼
申永强
贾占辉
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Beijing Zhongshi Weiye Technology Yixing Co ltd
JONES TECH PLC
Wuxi Zhongshi Kuluojie Technology Co ltd
Beijing Jones Technology Wuxi Co ltd
Original Assignee
Beijing Zhongshi Weiye Technology Yixing Co ltd
JONES TECH PLC
Wuxi Zhongshi Kuluojie Technology Co ltd
Beijing Jones Technology Wuxi Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Beijing Zhongshi Weiye Technology Yixing Co ltd, JONES TECH PLC, Wuxi Zhongshi Kuluojie Technology Co ltd, Beijing Jones Technology Wuxi Co ltd filed Critical Beijing Zhongshi Weiye Technology Yixing Co ltd
Priority to CN202011127465.5A priority Critical patent/CN112461752A/en
Publication of CN112461752A publication Critical patent/CN112461752A/en
Pending legal-status Critical Current

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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N19/00Investigating materials by mechanical methods
    • G01N19/04Measuring adhesive force between materials, e.g. of sealing tape, of coating
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01BMEASURING LENGTH, THICKNESS OR SIMILAR LINEAR DIMENSIONS; MEASURING ANGLES; MEASURING AREAS; MEASURING IRREGULARITIES OF SURFACES OR CONTOURS
    • G01B5/00Measuring arrangements characterised by the use of mechanical techniques
    • G01B5/02Measuring arrangements characterised by the use of mechanical techniques for measuring length, width or thickness
    • G01B5/06Measuring arrangements characterised by the use of mechanical techniques for measuring length, width or thickness for measuring thickness
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N3/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N3/02Details
    • G01N3/04Chucks
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N3/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N3/08Investigating strength properties of solid materials by application of mechanical stress by applying steady tensile or compressive forces
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N3/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N3/24Investigating strength properties of solid materials by application of mechanical stress by applying steady shearing forces
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/0014Type of force applied
    • G01N2203/0016Tensile or compressive
    • G01N2203/0017Tensile
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/0014Type of force applied
    • G01N2203/0025Shearing

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  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Investigating Strength Of Materials By Application Of Mechanical Stress (AREA)

Abstract

The invention relates to a method for accurately controlling the thickness of a heat-conducting adhesive layer in a tensile shear test; the method comprises the following steps: step 1, coating an adhesive on one edge of a pretreated base material, wherein the thickness of the coated adhesive is slightly larger than H/2, and H is the thickness of a test adhesive layer to be controlled; step 2, attaching the first thickness limiting block to the first base material, aligning the edge with glue and the width, attaching the first thickness limiting block and the first base material to the bottom plate, and clamping and fixing the first thickness limiting block, the first base material and the bottom plate by using the first fixing clamp; step 3, referring to the step 1 and the step 2, attaching the second base material, the second thickness limiting block and the bottom plate, and clamping the second base material, the second thickness limiting block and the bottom plate by using the second fixing frame; step 4, pressing the components manufactured in the step 1, the step 2 and the step 3, and keeping the first fixing clamp and the second fixing clamp to be clamped tightly; the 2-piece thickness limiting blocks with precise thickness sizes are lapped with the bonded base material in a fixing mode through a fixing frame, and a thickness gap of the needed adhesive is formed so as to control the thickness of the adhesive.

Description

Method for accurately controlling thickness of adhesive layer in tensile shear test of heat-conducting adhesive
Technical Field
The invention relates to a method for accurately controlling the thickness of a glue layer in a tensile shear test of a heat-conducting adhesive.
Background
The heat-conducting adhesive is generally applied to the bonding fixation of a battery pack in the new energy lithium battery industry, the tensile shear test is a key performance test for evaluating the bonding performance of the heat-conducting adhesive, the thickness of a bonding adhesive layer is found to have a large influence on the tensile shear test result in the test, and if the thickness of the adhesive layer is not strictly controlled in the test process, the test result is often large in fluctuation, and even the condition that the specification requirement is not met is generated.
Disclosure of Invention
The invention aims to provide a method for accurately controlling the thickness of a heat-conducting adhesive tensile shear test adhesive layer so as to solve the problems in the background technology.
In order to achieve the purpose, the invention provides the following technical scheme: a method for accurately controlling the thickness of a glue layer in a tensile shear test of a heat-conducting adhesive comprises the following steps:
step 1, coating an adhesive on one edge of a pretreated base material, wherein the thickness of the coated adhesive is slightly larger than H/2, and H is the thickness of a test adhesive layer to be controlled;
step 2, attaching the first thickness limiting block to the first base material, aligning the edge with glue and the width, attaching the first thickness limiting block and the first base material to the bottom plate, and clamping and fixing the first thickness limiting block, the first base material and the bottom plate by using the first fixing clamp;
step 3, referring to the step 1 and the step 2, attaching the second base material, the second thickness limiting block and the bottom plate, and clamping the second base material, the second thickness limiting block and the bottom plate by using the second fixing frame;
and 4, pressing the components manufactured in the steps 1, 2 and 3, and keeping the first fixing clamp and the second fixing clamp clamped tightly.
Preferably, the floor is kept horizontal.
Preferably, the first thickness limiter and the second thickness limiter are kept horizontal.
Preferably, the thickness of the first thickness limiting block is consistent with that of the second thickness limiting block.
Preferably, the first thickness limiting block is also respectively abutted against the second base material and the adhesive.
Preferably, the second thickness limiting block is also respectively abutted against the first base material and the adhesive.
Preferably, the thickness of the adhesive is equal to the thickness of the first thickness limiting block minus the thickness of the first substrate.
The invention has the beneficial effects that: according to the method for accurately controlling the thickness of the adhesive layer in the tensile shear test of the heat-conducting adhesive, 2 thickness limiting blocks with precise thickness and size are overlapped with the bonded substrate in a fixing mode of the fixing frame to form a required thickness gap of the adhesive, so that the purpose of controlling the thickness of the adhesive is achieved, the thickness of the adhesive layer of the adhesive can be strictly controlled, a standardized sample preparation process is realized, and the accuracy and consistency of test results are improved.
Drawings
FIG. 1 is a schematic diagram illustrating an embodiment of a method for accurately controlling the thickness of a tensile shear test adhesive layer of a thermal conductive adhesive according to the present invention;
FIG. 2 is a schematic diagram illustrating an embodiment of a method for accurately controlling the thickness of a tensile shear test adhesive layer of a thermal conductive adhesive according to the present invention;
FIG. 3 is a schematic diagram illustrating an embodiment of a method for accurately controlling the thickness of a tensile shear test adhesive layer of a thermal conductive adhesive according to the present invention;
FIG. 4 is a schematic diagram illustrating an embodiment of a method for precisely controlling the thickness of a tensile shear test adhesive layer of a thermally conductive adhesive according to the present invention;
FIG. 5 is a schematic diagram illustrating an embodiment of a method for accurately controlling the thickness of a tensile shear test adhesive layer of a thermally conductive adhesive according to the present invention;
description of the drawings: 1. a first thickness limiting block; 2. a first fixing clamp; 3. an adhesive; 4. a second substrate; 5. A second thickness limiting block; 6. a base plate; 7. a first substrate; 8. and a second fixing clamp.
Detailed Description
The following description of the preferred embodiments of the present invention is provided for the purpose of illustration and description, and is in no way intended to limit the invention.
A method for accurately controlling the thickness of a glue layer in a tensile shear test of a heat-conducting adhesive comprises the following steps:
step 1, coating an adhesive 3 on the edge of a first pretreated substrate 7, wherein the thickness of the coated adhesive 3 is slightly larger than H/2, and H is the thickness of a test adhesive layer to be controlled, as shown in FIG. 2;
step 2, attaching the first thickness limiting block 1 to a first substrate 7, aligning the edges with glue and the widths, attaching the first thickness limiting block 1 and the first substrate 7 to a bottom plate 6, and clamping and fixing the first thickness limiting block 1, the first substrate 7 and the bottom plate 6 by using a first fixing clamp 2; as shown in fig. 3;
step 3, referring to the step 1 and the step 2, attaching the second base material 4, the second thickness limiting block 5 and the bottom plate 6, and clamping the second base material 4, the second thickness limiting block 5 and the bottom plate 6 by using a second fixing frame 8, as shown in fig. 4;
and 4, pressing the components manufactured in the steps 1, 2 and 3, and keeping the first fixing clamp 2 and the second fixing clamp 8 clamped tightly, as shown in fig. 5 and 1.
The floor 6 remains horizontal; the first thickness limiting block 1 and the second thickness limiting block 5 are both kept horizontal; the thickness of the first thickness limiting block 1 is consistent with that of the second thickness limiting block 5; the first thickness limiting block 1 is also abutted against the second base material 4 and the adhesive 3 respectively; the second thickness limiting block 5 is also abutted against the first base material 7 and the adhesive 3 respectively; the thickness of the adhesive 3 is equal to the thickness of the first thickness limiting block 1 minus the thickness of the first base material 7.
The method for accurately controlling the thickness of the adhesive layer in the tensile shear test of the heat-conducting adhesive realizes more accurate control of the thickness of the adhesive layer of the adhesive, ensures controllable errors in the product test process of the adhesive, realizes a standardized sample preparation process, and improves the accuracy and consistency of test results.
The above embodiments are preferred embodiments of the present invention, and those skilled in the art can make variations and modifications to the above embodiments, therefore, the present invention is not limited to the above embodiments, and any obvious improvements, substitutions or modifications made by those skilled in the art based on the present invention are within the protection scope of the present invention.

Claims (7)

1. A method for accurately controlling the thickness of a heat-conducting adhesive layer in a tensile shear test is characterized by comprising the following steps: the method comprises the following steps:
step 1, coating an adhesive (3) on the edge of a pretreated base material I (7), wherein the thickness of the coated adhesive (3) is slightly larger than H/2, and H is the thickness of a test adhesive layer to be controlled;
step 2, attaching the first thickness limiting block (1) to the first base material (7), aligning the edges with glue and the widths, attaching the first thickness limiting block (1) and the first base material (7) to the bottom plate (6), and clamping and fixing the first thickness limiting block (1), the first base material (7) and the bottom plate (6) by using a first fixing clamp (2);
step 3, referring to the step 1 and the step 2, attaching the second base material (4), the second thickness limiting block (5) and the bottom plate (6), and clamping the second base material (4), the second thickness limiting block (5) and the bottom plate (6) by using a second fixing frame (8);
and 4, pressing the components manufactured in the steps 1, 2 and 3, and keeping the first fixing clamp (2) and the second fixing clamp (8) clamped tightly.
2. The method for accurately controlling the thickness of the adhesive layer in the tensile shear test of the heat-conducting adhesive according to claim 1, is characterized in that: the floor (6) is kept horizontal.
3. The method for accurately controlling the thickness of the adhesive layer in the tensile shear test of the heat-conducting adhesive according to claim 1, is characterized in that: the first thickness limiting block (1) and the second thickness limiting block (5) are kept horizontal.
4. The method for accurately controlling the thickness of the adhesive layer in the tensile shear test of the heat-conducting adhesive according to claim 1, is characterized in that: the thickness of the first thickness limiting block (1) is consistent with that of the second thickness limiting block (5).
5. The method for accurately controlling the thickness of the adhesive layer in the tensile shear test of the heat-conducting adhesive according to claim 1, is characterized in that: the first thickness limiting block (1) is also abutted against the second base material (4) and the adhesive (3) respectively.
6. The method for accurately controlling the thickness of the adhesive layer in the tensile shear test of the heat-conducting adhesive according to claim 1, is characterized in that: the second thickness limiting block (5) is also abutted against the first base material (7) and the adhesive (3) respectively.
7. The method for accurately controlling the thickness of the adhesive layer in the tensile shear test of the heat-conducting adhesive according to claim 1, is characterized in that: the thickness of the adhesive (3) is equal to the thickness of the first thickness limiting block (1) minus the thickness of the first base material (7).
CN202011127465.5A 2020-10-20 2020-10-20 Method for accurately controlling thickness of adhesive layer in tensile shear test of heat-conducting adhesive Pending CN112461752A (en)

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CN202011127465.5A CN112461752A (en) 2020-10-20 2020-10-20 Method for accurately controlling thickness of adhesive layer in tensile shear test of heat-conducting adhesive

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102365410B1 (en) * 2021-05-26 2022-02-23 현대제철 주식회사 Evaluating method of adhesion property of metal plate

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2001289774A (en) * 2000-04-06 2001-10-19 Denki Kagaku Kogyo Kk Evaluation method for adhesive and bonding method
CN102954910A (en) * 2011-08-26 2013-03-06 航天科工防御技术研究试验中心 Heat-resistant coating tensile shear strength test model and production method thereof
CN204269449U (en) * 2014-12-16 2015-04-15 北京汽车股份有限公司 A kind of brace table device making shear test test piece
CN105014860A (en) * 2015-08-07 2015-11-04 上海交通大学 Glue joint structural part manufacturing tool adapting to different sizes
CN207923557U (en) * 2018-02-28 2018-09-28 浙江众泰汽车制造有限公司 Measure the sample preparation device of adhesive tensile shear strength
CN110132667A (en) * 2019-04-19 2019-08-16 东风汽车集团有限公司 A kind of adhesive tensile shear strength sample batch preparation tooling and method
CN209727573U (en) * 2019-02-28 2019-12-03 上纬新材料科技股份有限公司 A kind of tooling for cutting sample thickness uniformity for controlling bonding agent drawing

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2001289774A (en) * 2000-04-06 2001-10-19 Denki Kagaku Kogyo Kk Evaluation method for adhesive and bonding method
CN102954910A (en) * 2011-08-26 2013-03-06 航天科工防御技术研究试验中心 Heat-resistant coating tensile shear strength test model and production method thereof
CN204269449U (en) * 2014-12-16 2015-04-15 北京汽车股份有限公司 A kind of brace table device making shear test test piece
CN105014860A (en) * 2015-08-07 2015-11-04 上海交通大学 Glue joint structural part manufacturing tool adapting to different sizes
CN207923557U (en) * 2018-02-28 2018-09-28 浙江众泰汽车制造有限公司 Measure the sample preparation device of adhesive tensile shear strength
CN209727573U (en) * 2019-02-28 2019-12-03 上纬新材料科技股份有限公司 A kind of tooling for cutting sample thickness uniformity for controlling bonding agent drawing
CN110132667A (en) * 2019-04-19 2019-08-16 东风汽车集团有限公司 A kind of adhesive tensile shear strength sample batch preparation tooling and method

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102365410B1 (en) * 2021-05-26 2022-02-23 현대제철 주식회사 Evaluating method of adhesion property of metal plate

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Application publication date: 20210309