CN112457060A - Glue dry particle archaized brick and preparation method thereof - Google Patents
Glue dry particle archaized brick and preparation method thereof Download PDFInfo
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- CN112457060A CN112457060A CN202011484813.4A CN202011484813A CN112457060A CN 112457060 A CN112457060 A CN 112457060A CN 202011484813 A CN202011484813 A CN 202011484813A CN 112457060 A CN112457060 A CN 112457060A
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/89—Coating or impregnation for obtaining at least two superposed coatings having different compositions
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
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Abstract
A glue dry particle archaized brick and a preparation method thereof, the preparation method of the glue dry particle archaized brick comprises the following steps: step (1): printing glue on the green brick according to a set pattern by an ink-jet printer, wherein the pattern part of the pattern is coated with the glue, and the line part is arranged in a vacant way; step (2): arranging dry particles of the antique brick on the surface of a green brick; and (3): blowing dry grains of the archaized bricks along the line part in the green bricks away from the surfaces of the green bricks by using a fan; and (4): sintering the green brick at a sintering temperature not higher than the melting point of the dry particles of the archaized brick; and (5): half polishing the green brick, and polishing the dry particles of the archaized brick of the green brick in a standing state; glue dry particle archaizing brick, including: green bricks, bonding layers and dry grain layers of the antique bricks. According to the preparation method of the antique brick with the dry glue particles, the ink-jet printing glue is combined with the dry glue particles of the antique brick, the size and the position of the dry glue particles can be controlled by ink-jet on the surface, the hand feeling of the antique dry particles is achieved, and controllable concave-convex textures are achieved.
Description
Technical Field
The invention relates to the technical field of archaized bricks, in particular to a glue dry particle archaized brick and a preparation method thereof.
Background
Along with the increasing living standard of people, the requirements of people on the environment are also increased, for example, the requirements of decorative archaized bricks are relatively increased. The prior archaized brick has certain improvement in appearance, color, hardness, water absorption, abrasion resistance and other aspects; but the improvement of the performance leads to the improvement of the production cost of the antique brick; meanwhile, in the preparation process of the existing antique brick, the preparation method is complex, the concave-convex feeling of the preparation is not controllable, the concave-convex feeling can not be designed according to the user requirement, generally, when the brick body is provided with a concave-convex structure, the brick body is not easy to have glossiness, namely, the concave-convex feeling and the glossiness can not be simultaneously met.
Disclosure of Invention
The invention aims to provide a preparation method of an archaized brick with dry glue particles, which combines ink-jet printing glue with the dry particles of the archaized brick.
The invention also provides a glue dry particle archaized brick which is prepared by the preparation method.
In order to achieve the purpose, the invention adopts the following technical scheme:
a preparation method of a glue dry particle archaized brick comprises the following steps:
step (1): printing glue on the green brick according to a set pattern by an ink-jet printer, wherein the pattern part of the pattern is coated with the glue, and the line part is arranged in a vacant way;
step (2): arranging dry particles of the antique brick on the surface of a green brick;
and (3): blowing dry grains of the archaized bricks along the line part in the green bricks away from the surfaces of the green bricks by using a fan;
and (4): sintering the green brick at a sintering temperature not higher than the melting point of the dry particles of the archaized brick;
and (5): and (4) half polishing the green brick, and polishing the dry particles of the archaized brick of the green brick in the standing state.
Preferably, the difference between the melting point of the dried particles of the antique bricks and the sintering temperature in the step (4) is 10-30 ℃.
Preferably, the raw materials of the dry particles of the archaized brick comprise the following oxides of elements in percentage by mass: 50-55% of silicon, 15-20% of aluminum, 0.01-0.1% of iron, 0.01-0.1% of titanium, 7-9% of calcium, 1-2% of magnesium, 2-3% of potassium, 2-4% of sodium, 5-6% of zinc, 7-8% of barium and the balance of impurities.
Preferably, the raw materials of the dry particles of the archaized brick comprise the following oxides of elements in percentage by mass: 52.3% silicon, 17.0% aluminum, 0.1% iron, 0.02% titanium, 8.8% calcium, 1.1% magnesium, 2.4% potassium, 4.0% sodium, 5.6% zinc, 7.2% barium, and the balance impurities;
the melting point of the archaized brick dry particles is 1200 ℃; the sintering temperature in the step (4) is 1180 ℃.
Preferably, in the step (3), the frequency of the fan is 28-32 Hz.
Preferably, in the step (3), the output end of the fan is connected with the duckbill air outlet, and the duckbill air outlet is obliquely aligned with the line part.
Preferably, in the step (1), the surface of the green brick is provided with a surface glaze layer.
A glue dry particle archaized brick, comprising: green bricks, bonding layers and dry grain layers of the antique bricks;
the archaized brick dry particle layer is adhered to the surface of the green brick through the bonding layer.
The invention has the beneficial effects that:
according to the preparation method of the antique brick with the dry glue particles, the ink-jet printing glue is combined with the dry glue particles of the antique brick, the size and the position of the dry glue particles can be controlled by ink-jet on the surface, the hand feeling of the antique dry particles is achieved, and controllable concave-convex textures are achieved.
Detailed Description
The technical solution of the present invention is further explained by the following embodiments.
A preparation method of a glue dry particle archaized brick comprises the following steps:
step (1): printing glue on the green brick according to a set pattern by an ink-jet printer, wherein the pattern part of the pattern is coated with the glue, and the line part is arranged in a vacant way;
the glue has adhesiveness, the ink-jet printer designs the pattern according to the requirement of the user before distributing the glue, wherein the pattern part in the pattern prints the glue, and the line part is set for leaving empty (namely not spreading glue), the surface of the adobe finally forms the adhesive linkage formed by the set pattern;
step (2): arranging dry particles of the antique brick on the surface of a green brick;
the glue is arranged along the pattern part, and the line part is arranged to be left empty, so that the dry particles of the antique brick positioned at the pattern part can be adhered to the surface of the green brick, and the dry particles of the antique brick positioned at the line part are in a loose state;
and (3): blowing dry grains of the archaized bricks along the line part in the green bricks away from the surfaces of the green bricks by using a fan;
because the dry particles of the antique bricks at the line part are in a loose state, when the fan blows the dry particles of the antique bricks, the dry particles of the antique bricks at the position can fall off and are distributed along the line part in the pattern to form an obvious separation line with the pattern part with the dry particles of the antique bricks, so that the attractiveness is improved;
and (4): sintering the green brick at a sintering temperature not higher than the melting point of the dry particles of the archaized brick;
the sintering temperature is lower than the melting point of the archaized brick dry particles, so that the archaized brick dry particles are prevented from being melted during the sintering of the brick blank, the archaized brick dry particles cannot stand upright, the semi-polishing process in the step (5) cannot be matched, and the effect of the archaized brick cannot be achieved.
And (5): and (4) half polishing the green brick, and polishing the dry particles of the archaized brick of the green brick in the standing state.
Because the sintering temperature is not higher than the melting point of the dry particles of the antique brick, the dry particles of the antique brick are not easy to melt, and can stand on the surface of a brick blank under the condition that the sintering temperature is not large, and then the dry particles of the antique brick are ground flat through a half-polishing step, so that the pattern part is processed into slightly small concave-convex feeling and certain brightness, and the attractiveness of a finished brick body is improved. As is well understood, in general, tile surfaces appear flat and when bright are fully polished; the surface of the ceramic tile is slightly concave-convex and is partially polished by half polishing.
According to the preparation method of the antique brick with the dry glue particles, the ink-jet printing glue is combined with the dry glue particles of the antique brick, the size and the position of the dry glue particles can be controlled by ink-jet on the surface, the hand feeling of the antique dry particles is achieved, and controllable concave-convex textures are achieved.
Preferably, the difference between the melting point of the dried particles of the antique bricks and the sintering temperature in the step (4) is 10-30 ℃.
The sintering temperature is not higher than the melting point of the dry particles of the antique brick, the difference value between the sintering temperature and the melting point is controlled to be 10-30 ℃, the sintering temperature can not influence the dry particles of the antique brick even in the fluctuation range, and the upright state of the dry particles is kept.
Preferably, the raw materials of the dry particles of the archaized brick comprise the following oxides of elements in percentage by mass: 50-55% of silicon, 15-20% of aluminum, 0.01-0.1% of iron, 0.01-0.1% of titanium, 7-9% of calcium, 1-2% of magnesium, 2-3% of potassium, 2-4% of sodium, 5-6% of zinc, 7-8% of barium and the balance of impurities.
The preparation method takes the oxides containing more silicon, aluminum, iron, titanium, calcium, magnesium, potassium, sodium, zinc and barium as the raw materials of the dry particles of the antique brick, and the content of each oxide is blended and can be fully combined with glue to improve the performance of the dry particles of the antique brick, so that the Mohs hardness and acid and alkali resistance of the brick body are improved after the brick body is sintered. Meanwhile, the melting point of the dry particles of the antique brick is preferably 1150-1250 ℃, so that enterprises can process the dry particles at a sinterable temperature, and the sintering cost is reduced.
Preferably, the raw materials of the dry particles of the archaized brick comprise the following oxides of elements in percentage by mass: 52.3% silicon, 17.0% aluminum, 0.1% iron, 0.02% titanium, 8.8% calcium, 1.1% magnesium, 2.4% potassium, 4.0% sodium, 5.6% zinc, 7.2% barium, and the balance impurities;
the melting point of the archaized brick dry particles is 1200 ℃; the sintering temperature in the step (4) is 1180 ℃.
Preferably, in the step (3), the frequency of the fan is 28-32 Hz.
The frequency of the fan is not too high or too low, and too high can blow away dry particles of the antique brick of the pattern part; and the frequency of the fan is too low, so that dry particles of the antique brick in the line part are not easy to separate, or the separation efficiency is low, and the separation speed is slow.
Preferably, in the step (3), the output end of the fan is connected with the duckbill air outlet, and the duckbill air outlet is obliquely aligned with the line part.
The duckbilled air outlet is provided with a long diameter port and a short diameter port, the short diameter port is connected with the output end of the fan, and the long diameter port is aligned with the line part, so that the air supply area to the line part can be increased; meanwhile, when the duckbill air outlet is obliquely aligned with the line part, the broken dry particles of the antique brick are not easy to influence the pattern part.
Preferably, in the step (1), the surface of the green brick is provided with a surface glaze layer.
The glue can directly act on the surface glaze layer, and the surface glaze layer is used as a bearing interface between the surface of the brick body and the glue, so that the bonding capability of the glue on the surface of the brick body can be improved, and the stability of the dry particles of the antique brick on the surface of the brick body is further improved.
A glue dry particle archaized brick, comprising: green bricks, bonding layers and dry grain layers of the antique bricks;
the archaized brick dry particle layer is adhered to the surface of the green brick through the bonding layer.
And (3) performance testing:
appearance: the surface of the brick body is observed to be glossy; and obvious concave-convex feeling can be achieved when the touch is carried out by hands.
Acid and alkali resistance: according to GB/T3810.13-2016 ceramic tile test method part 13: determination of chemical resistance the surface of the tile was subjected to a performance test.
Mohs hardness: the brick body was tested using a mohs hardness tester to obtain mohs hardness.
Example A:
step (1): printing glue on the green brick according to a set pattern by an ink-jet printer, wherein the pattern part of the pattern is coated with the glue, and the line part is arranged in a vacant way;
step (2): arranging dry particles of the antique brick on the surface of a green brick; the raw materials of the dry particles of the antique brick comprise the following oxides of the following elements in percentage by mass: 52.3% silicon, 17.0% aluminum, 0.1% iron, 0.02% titanium, 8.8% calcium, 1.1% magnesium, 2.4% potassium, 4.0% sodium, 5.6% zinc, 7.2% barium, and the balance impurities; the melting point of the archaized brick dry particles is 1200 ℃;
and (3): blowing dry grains of the archaized bricks along the line part in the green bricks away from the surfaces of the green bricks by using a fan; the frequency of the fan is 30 Hz.
And (4): sintering the green brick at a sintering temperature not higher than the melting point of the dry particles of the archaized brick; the sintering temperature was 1180 ℃.
And (5): and (5) semi-polishing the green brick to polish the dry particles of the archaized brick in the standing state of the green brick flat.
Comparative example a 1:
step (1): printing glue on the green brick according to a set pattern by an ink-jet printer, wherein the pattern part of the pattern is coated with the glue, and the line part is arranged in a vacant way;
step (2): arranging dry particles of the antique brick on the surface of a green brick; the raw materials of the dry particles of the antique brick comprise the following oxides of the following elements in percentage by mass: 52.3% silicon, 17.0% aluminum, 0.1% iron, 0.02% titanium, 8.8% calcium, 1.1% magnesium, 2.4% potassium, 4.0% sodium, 5.6% zinc, 7.2% barium, and the balance impurities; the melting point of the archaized brick dry particles is 1200 ℃;
and (3): blowing dry grains of the archaized bricks along the line part in the green bricks away from the surfaces of the green bricks by using a fan; the frequency of the fan is 30 Hz.
And (4): sintering the green brick at a sintering temperature not higher than the melting point of the dry particles of the archaized brick; the sintering temperature was 1180 ℃.
Comparative example a 2:
step (1): printing glue on the green brick according to a set pattern by an ink-jet printer, wherein the pattern part of the pattern is coated with the glue, and the line part is arranged in a vacant way;
step (2): arranging dry particles of the antique brick on the surface of a green brick; the raw materials of the dry particles of the antique brick comprise the following oxides of the following elements in percentage by mass: 52.3% silicon, 20.0% aluminum, 0.1% iron, 0.02% titanium, 8.8% calcium, 1.1% magnesium, 2.0% potassium, 2.0% sodium, 6.0% zinc, 7.0% barium, and the balance impurities; the melting point of the archaized brick dry particles is 1243 ℃;
and (3): blowing dry grains of the archaized bricks along the line part in the green bricks away from the surfaces of the green bricks by using a fan; the frequency of the fan is 30 Hz.
And (4): sintering the green brick at a sintering temperature not higher than the melting point of the dry particles of the archaized brick; the sintering temperature is 1240 ℃ and 1250 ℃.
And (5): and (5) semi-polishing the green brick.
Example A, comparative examples A1-A2 were individually tested for performance as shown in Table 1.
TABLE 1 Performance testing of example A
Description of the drawings:
1. as can be seen from the comparison between example A and comparative example A1, comparative example A1 does not polish the dried particles of the archaized tile after sintering; as can be seen from the performance of the comparative example A1, the surface of the tile is dull, the concave-convex feeling is rough, the height of the dry grains of the antique tile is uneven when the dry grains are erected, and the user is easy to be hurt; meanwhile, since the acid and alkali resistance of the comparative example No. A1 is only B grade, and the alkali resistance is only C grade, the test solution is easy to corrode the unpolished brick, which is not favorable for the acid and alkali resistance of the brick. And embodiment A then carries out half polishing to the dry grain sintering back of archaizing brick, controls the dry grain of archaizing brick on ceramic tile surface effectively, has both kept the roughness of the dry grain of archaizing brick in order to improve acid and alkali resistance, makes the ceramic tile have the glossiness again.
2. As can be seen from the comparison between the example B and the comparative example A2, in the comparative example A2, the sintering temperature of the green brick is adjusted to be equal to or higher than the melting point of the dry particles of the archaized brick, and at this time, the dry particles of the archaized brick are unstable in vertical state and have certain fluidity, which is not beneficial to maintaining the vertical state of the dry particles of the archaized brick, so that the ceramic finished product has no concave-convex feeling, and the acid and alkali resistance is reduced; and the Mohs hardness of the antique brick is reduced to 5 grade due to the fact that the upright state of dry particles of the antique brick is damaged. And the sintering temperature is not higher than the melting point of the dry particles of the archaized brick in the embodiment A, so that the upright state of the dry particles of the archaized brick is effectively kept, and the stability of the dry particles of the archaized brick is improved.
Example B:
step (1): the surface of the green brick is provided with a surface glaze layer, glue is printed on the green brick according to a set pattern through an ink-jet printer, the pattern part of the pattern is coated with the glue, and the line part is arranged in a vacant way;
step (2): arranging dry particles of the antique brick on the surface of a green brick; the raw materials of the dry particles of the antique brick comprise the following oxides of the following elements in percentage by mass: 55% of silicon, 15% of aluminum, 0.01% of iron, 0.1% of titanium, 9% of calcium, 2% of magnesium, 2% of potassium, 2% of sodium, 6% of zinc, 7% of barium and the balance impurities; the melting point of the archaized brick dry particles is 1243 ℃;
and (3): blowing dry grains of the archaized bricks along the line part in the green bricks away from the surfaces of the green bricks by using a fan; the frequency of the fan is 25 Hz; the output end of the fan is connected with the duckbill air outlet;
and (4): sintering the green brick at a sintering temperature not higher than the melting point of the dry particles of the archaized brick; the sintering temperature was 1223 ℃.
And (5): and (5) semi-polishing the green brick to polish the dry particles of the archaized brick in the standing state of the green brick flat.
Example C:
step (1): the surface of the green brick is provided with a surface glaze layer, glue is printed on the green brick according to a set pattern through an ink-jet printer, the pattern part of the pattern is coated with the glue, and the line part is arranged in a vacant way;
step (2): arranging dry particles of the antique brick on the surface of a green brick; the raw materials of the dry particles of the antique brick comprise the following oxides of the following elements in percentage by mass: 55% of silicon, 20% of aluminum, 0.01% of iron, 0.1% of titanium, 7% of calcium, 1% of magnesium, 2% of potassium, 2% of sodium, 5% of zinc, 7% of barium and the balance impurities; the melting point of the archaized brick dry particles is 1252 ℃;
and (3): blowing dry grains of the archaized bricks along the line part in the green bricks away from the surfaces of the green bricks by using a fan; the frequency of the fan is 32 Hz; the output end of the fan is connected with the duckbill air outlet;
and (4): sintering the green brick at a sintering temperature not higher than the melting point of the dry particles of the archaized brick; the sintering temperature was 1232 ℃.
And (5): and (5) semi-polishing the green brick to polish the dry particles of the archaized brick in the standing state of the green brick flat.
Example B and example C were tested for performance as in table 2.
TABLE 2 Performance testing of examples B and C
The technical principle of the present invention is described above in connection with specific embodiments. The description is made for the purpose of illustrating the principles of the invention and should not be construed in any way as limiting the scope of the invention. Based on the explanations herein, those skilled in the art will be able to conceive of other embodiments of the present invention without inventive effort, which would fall within the scope of the present invention.
Claims (8)
1. A preparation method of a glue dry particle archaized brick is characterized by comprising the following steps:
step (1): printing glue on the green brick according to a set pattern by an ink-jet printer, wherein the pattern part of the pattern is coated with the glue, and the line part is arranged in a vacant way;
step (2): arranging dry particles of the antique brick on the surface of a green brick;
and (3): blowing dry grains of the archaized bricks along the line part in the green bricks away from the surfaces of the green bricks by using a fan;
and (4): sintering the green brick at a sintering temperature not higher than the melting point of the dry particles of the archaized brick;
and (5): and (4) half polishing the green brick, and polishing the dry particles of the archaized brick of the green brick in the standing state.
2. The method according to claim 1, wherein the difference between the melting point of the dried particles of the antique brick and the sintering temperature in the step (4) is 10-30 ℃.
3. The preparation method according to claim 1 or 2, wherein the raw material of the archaized brick dry particles comprises the following oxides of elements in percentage by mass: 50-55% of silicon, 15-20% of aluminum, 0.01-0.1% of iron, 0.01-0.1% of titanium, 7-9% of calcium, 1-2% of magnesium, 2-3% of potassium, 2-4% of sodium, 5-6% of zinc, 7-8% of barium and the balance of impurities.
4. The preparation method of the archaized brick is characterized in that the raw materials of the archaized brick dry particles comprise the following oxides of elements in percentage by mass: 52.3% silicon, 17.0% aluminum, 0.1% iron, 0.02% titanium, 8.8% calcium, 1.1% magnesium, 2.4% potassium, 4.0% sodium, 5.6% zinc, 7.2% barium, and the balance impurities;
the melting point of the archaized brick dry particles is 1200 ℃; the sintering temperature in the step (4) is 1180 ℃.
5. The manufacturing method according to claim 3, wherein in the step (3), the frequency of the blower is 28 to 32 Hz.
6. The method according to claim 5, wherein in the step (3), the output end of the fan is connected with the duckbill outlet, and the duckbill outlet is obliquely aligned with the line pattern part.
7. The method according to claim 1, wherein in the step (1), the surface of the green brick is provided with a glaze layer.
8. The glue dry particle archaized brick prepared by the preparation method of any one of claims 1 to 7, which comprises the following steps: green bricks, bonding layers and dry grain layers of the antique bricks;
the archaized brick dry particle layer is adhered to the surface of the green brick through the bonding layer.
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| CN115215548A (en) * | 2022-08-08 | 2022-10-21 | 佛山市典石釉科技有限公司 | Dry grain glaze for ceramic tiles and preparation method thereof, ceramic tiles and preparation method thereof |
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