CN112386523A - Low-odor low-irritation black eyelash beautifying gel for eyelash adhesion - Google Patents
Low-odor low-irritation black eyelash beautifying gel for eyelash adhesion Download PDFInfo
- Publication number
- CN112386523A CN112386523A CN201910756621.5A CN201910756621A CN112386523A CN 112386523 A CN112386523 A CN 112386523A CN 201910756621 A CN201910756621 A CN 201910756621A CN 112386523 A CN112386523 A CN 112386523A
- Authority
- CN
- China
- Prior art keywords
- low
- eyelash
- black
- irritation
- odor
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 210000000720 eyelash Anatomy 0.000 title claims abstract description 50
- 239000006229 carbon black Substances 0.000 claims abstract description 19
- 229920001651 Cyanoacrylate Polymers 0.000 claims abstract description 17
- 229920003229 poly(methyl methacrylate) Polymers 0.000 claims abstract description 17
- 239000004926 polymethyl methacrylate Substances 0.000 claims abstract description 17
- GRVDJDISBSALJP-UHFFFAOYSA-N methyloxidanyl Chemical group [O]C GRVDJDISBSALJP-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000003381 stabilizer Substances 0.000 claims abstract description 14
- 239000002318 adhesion promoter Substances 0.000 claims abstract description 11
- 239000003292 glue Substances 0.000 claims description 18
- 230000007794 irritation Effects 0.000 claims description 15
- 239000002994 raw material Substances 0.000 claims description 8
- RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical group O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 claims description 6
- -1 crown ether compound Chemical class 0.000 claims description 6
- 239000000463 material Substances 0.000 claims description 6
- 238000004513 sizing Methods 0.000 claims description 6
- 239000000499 gel Substances 0.000 claims description 4
- 239000000654 additive Substances 0.000 claims description 3
- 238000001035 drying Methods 0.000 claims description 3
- 235000015110 jellies Nutrition 0.000 claims description 3
- 239000008274 jelly Substances 0.000 claims description 3
- 239000011812 mixed powder Substances 0.000 claims description 3
- AUONHKJOIZSQGR-UHFFFAOYSA-N oxophosphane Chemical compound P=O AUONHKJOIZSQGR-UHFFFAOYSA-N 0.000 claims description 3
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims description 3
- 239000000843 powder Substances 0.000 claims description 3
- 238000002360 preparation method Methods 0.000 claims 1
- 230000007547 defect Effects 0.000 abstract description 2
- 239000000853 adhesive Substances 0.000 abstract 1
- 230000001070 adhesive effect Effects 0.000 abstract 1
- 230000002045 lasting effect Effects 0.000 description 4
- 230000000638 stimulation Effects 0.000 description 4
- 206010020751 Hypersensitivity Diseases 0.000 description 3
- 206010023644 Lacrimation increased Diseases 0.000 description 3
- 208000026935 allergic disease Diseases 0.000 description 3
- 230000007815 allergy Effects 0.000 description 3
- 230000004317 lacrimation Effects 0.000 description 3
- 238000004040 coloring Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000003595 mist Substances 0.000 description 2
- 230000003796 beauty Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
- 125000000956 methoxy group Chemical group [H]C([H])([H])O* 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/10—Preparations containing skin colorants, e.g. pigments for eyes, e.g. eyeliner, mascara
Abstract
The invention aims to overcome the technical defects and provide the low-odor and low-irritation black eyelash adhesive for bonding eyelashes, which comprises @ -cyanoacrylate ethyl, methoxyl, polymethyl methacrylate, carbon black, an adhesion promoter, a stabilizer, a photoinitiator and an accelerant.
Description
Technical Field
The invention particularly relates to low-odor and low-irritation black eyelash beauty glue for eyelash sticking.
Background
As the mascara glue in the market is prepared from single @ -cyanoacrylate as a main raw material, the mascara glue is characterized by high irritation, and the phenomenon of lacrimation and even allergy can be caused when a customer carries out grafting operation, so that the mascara glue is not good for health. Since @ -cyanoacrylate is easily oxidized by air when exposed to air, it easily generates a layer of white mist, referred to as white mist, around eyelashes, thus limiting the application thereof.
Eyelash need use the dryer to continuously blow with higher speed glue solidification after the grafting is accomplished, can not freely open the eye before the glue is not totally solidified, and this causes very big inconvenience to customer experience.
Therefore, the safe, quick, lasting and effective eyelash beautifying gel provided by the invention can be applied to eyelash grafting, and can be completely cured quickly and effectively by using LED ultraviolet rays after grafting is finished. And has excellent durability and flexibility, and has a low odor and low irritation.
Disclosure of Invention
The invention aims to overcome the technical defects and provide safe, quick, lasting and effective eyelash beautifying glue which can be applied to eyelash grafting and can be quickly, effectively and completely cured by using LED ultraviolet rays after grafting is finished. And has excellent durability and flexibility, and has a low odor and low irritation.
According to one aspect of the present invention, there is provided a low-odor, low-irritation black mascara for eyelash sticking use, comprising @ -cyanoacryiate ethyl, methoxy, polymethylmethacrylate, carbon black, adhesion promoter, stabilizer, photoinitiator, and accelerator.
Further, according to the black eyelash glue for eyelash sticking with low odor and low irritation, the weight ratio of the raw materials is as follows: comprises 10-20% of @ -cyanoacrylate ethyl, 40-60% of methoxyl, 20-10% of polymethyl methacrylate, 5-10% of carbon black, 0.10-2% of adhesion promoter, 0.01-1% of stabilizer, 0.1-4% of photoinitiator and 0.10-2% of promoter.
Further, according to the black eyelash glue for eyelash binding use, which is low in smell and stimulation, the weight ratio of the raw materials is as follows: comprises 15% of @ -cyanoacrylate ethyl, 58% of methoxyl, 15% of polymethyl methacrylate, 8% of carbon black, 1% of adhesion promoter, 0.05% of stabilizer, 2% of photoinitiator and 0.5% of promoter.
Further, the stabilizer is sulfur dioxide.
Further, the photoinitiator is phenyl bis (2, 4, 6 trimethylformyl) phosphine oxide.
Further, the accelerator is a crown ether compound.
According to another aspect of the present invention, there is provided a method for preparing a low-odor and low-irritation black mascara for eyelash sticking use, comprising the steps of:
1: selecting a proper amount of @ -cyanoacrylate ethyl and methoxyl groups, and fully mixing in a reaction kettle;
2: selecting a proper amount of polymethyl methacrylate and carbon black, baking at the temperature of 80 ℃ for 12-24 hours, and drying the moisture content of the product;
3: physically mixing the dried polymethyl methacrylate and the carbon black;
4: adding the fully mixed powder into a reaction kettle and a sizing material for constant-temperature reaction;
5: adding other additives during the reaction;
6: until the powder is completely dissolved in the sizing material, ending;
7: the obtained black low-odor and low-irritation eyelash jelly.
The invention has the beneficial effects that: the safe, quick, lasting and effective eyelash beautifying gel disclosed by the invention can be applied to eyelash grafting, and can be quickly, effectively and completely cured by utilizing LED ultraviolet rays after grafting is finished. And has excellent durability and flexibility. Due to the characteristics of moderate methoxyl and low irritation, the eye care product well cares for the eyes of customers, and avoids lacrimation and allergy. Because the strength of the single methoxyl is too low, the invention mixes a certain amount of @ -cyanoacrylate ethyl in the methoxyl to increase the strength, and simultaneously controls the dosage on the premise of not generating stimulation. The product looks more full and bright black by coloring with carbon black. The product can achieve excellent durability in eyelash grafting applications.
Detailed Description
The invention is further described below with reference to specific embodiments.
The invention provides a black eyelash glue for eyelash bonding with low odor and low irritation, which comprises @ -cyanoacrylate ethyl, methoxyl, polymethyl methacrylate, carbon black, adhesion promoter, stabilizer, photoinitiator and promoter.
Further, according to the black eyelash glue for eyelash sticking with low odor and low irritation, the weight ratio of the raw materials is as follows: comprises 10-20% of @ -cyanoacrylate ethyl, 40-60% of methoxyl, 20-10% of polymethyl methacrylate, 5-10% of carbon black, 0.10-2% of adhesion promoter, 0.01-1% of stabilizer, 0.1-4% of photoinitiator and 0.10-2% of promoter.
Further, according to the black eyelash glue for eyelash binding use, which is low in smell and stimulation, the weight ratio of the raw materials is as follows: comprises 15% of @ -cyanoacrylate ethyl, 58% of methoxyl, 15% of polymethyl methacrylate, 8% of carbon black, 1% of adhesion promoter, 0.05% of stabilizer, 2% of photoinitiator and 0.5% of promoter.
Further, according to the black eyelash glue for eyelash sticking with low odor and low irritation, the weight ratio of the raw materials is as follows: comprises 18 percent of @ -cyanoacrylate ethyl, 49 percent of methoxyl, 18 percent of polymethyl methacrylate, 9 percent of carbon black, 1.5 percent of adhesion promoter, 0.8 percent of stabilizer, 2.2 percent of photoinitiator and 1.5 percent of promoter.
Further, the stabilizer is sulfur dioxide.
Further, the photoinitiator is phenyl bis (2, 4, 6 trimethylformyl) phosphine oxide.
Further, the accelerator is a crown ether compound.
According to another aspect of the present invention, there is provided a method for preparing a low-odor and low-irritation black mascara for eyelash sticking use, comprising the steps of:
1: selecting a proper amount of @ -cyanoacrylate ethyl and methoxyl groups, and fully mixing in a reaction kettle;
2: selecting a proper amount of polymethyl methacrylate and carbon black, baking at the temperature of 80 ℃ for 12-24 hours, and drying the moisture content of the product;
3: physically mixing the dried polymethyl methacrylate and the carbon black;
4: adding the fully mixed powder into a reaction kettle and a sizing material for constant-temperature reaction;
5: adding other additives during the reaction;
6: until the powder is completely dissolved in the sizing material, ending;
7: the obtained black low-odor and low-irritation eyelash jelly.
The eyelash beautifying glue is safe, quick, lasting and effective to the traditional eyelash beautifying glue, can be applied to eyelash grafting, and can be completely cured quickly and effectively by using LED ultraviolet rays after grafting is completed. And has excellent durability and flexibility. Due to the characteristics of moderate methoxyl and low irritation, the eye care product well cares for the eyes of customers, and avoids lacrimation and allergy. Because the strength of the single methoxyl is too low, the invention mixes a certain amount of @ -cyanoacrylate ethyl in the methoxyl to increase the strength, and simultaneously controls the dosage on the premise of not generating stimulation. The product looks more full and bright black by coloring with carbon black. The product can achieve excellent durability in eyelash grafting applications.
It should be noted that the above-mentioned embodiments illustrate rather than limit the invention, and that those skilled in the art will be able to design alternative embodiments without departing from the scope of the appended claims. In the claims, any reference signs placed between parentheses shall not be construed as limiting the claim. The word "comprising" does not exclude the presence of elements or operations not listed in a claim.
Claims (7)
1. A black eyelash gel for eyelash sticking application with low odor and low irritation is characterized by comprising @ -cyanoacrylate ethyl, methoxyl, polymethyl methacrylate, carbon black, adhesion promoter, stabilizer, photoinitiator and promoter.
2. The black eyelash glue for eyelash binding of low odor and low irritation according to claim 1, wherein the weight ratio of the raw materials is: comprises 10-20% of @ -cyanoacrylate ethyl, 40-60% of methoxyl, 20-10% of polymethyl methacrylate, 5-10% of carbon black, 0.10-2% of adhesion promoter, 0.01-1% of stabilizer, 0.1-4% of photoinitiator and 0.10-2% of promoter.
3. The black eyelash glue for eyelash binding of low odor and low irritation according to claim 1, wherein the weight ratio of the raw materials is: comprises 15% of @ -cyanoacrylate ethyl, 58% of methoxyl, 15% of polymethyl methacrylate, 8% of carbon black, 1% of adhesion promoter, 0.05% of stabilizer, 2% of photoinitiator and 0.5% of promoter.
4. The low odor, low irritation mascara for eyelash attachment use according to claim 1, wherein said stabilizer is sulfur dioxide.
5. The low odor, low irritation mascara for eyelash attachment use according to claim 1, wherein said photoinitiator is phenyl bis (2, 4, 6 trimethylformyl) phosphine oxide.
6. The low-odor, low-irritation black mascara for eyelash attachment use according to claim 1, wherein said accelerator is a crown ether compound.
7. A preparation method of black eyelash glue for eyelash sticking with low odor and low irritation is characterized by comprising the following steps:
1: selecting a proper amount of @ -cyanoacrylate ethyl and methoxyl groups, and fully mixing in a reaction kettle;
2: selecting a proper amount of polymethyl methacrylate and carbon black, baking at the temperature of 80 ℃ for 12-24 hours, and drying the moisture content of the product;
3: physically mixing the dried polymethyl methacrylate and the carbon black;
4: adding the fully mixed powder into a reaction kettle and a sizing material for constant-temperature reaction;
5: adding other additives during the reaction;
6: until the powder is completely dissolved in the sizing material, ending;
7: the obtained black low-odor and low-irritation eyelash jelly.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910756621.5A CN112386523A (en) | 2019-08-16 | 2019-08-16 | Low-odor low-irritation black eyelash beautifying gel for eyelash adhesion |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910756621.5A CN112386523A (en) | 2019-08-16 | 2019-08-16 | Low-odor low-irritation black eyelash beautifying gel for eyelash adhesion |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN112386523A true CN112386523A (en) | 2021-02-23 |
Family
ID=74601931
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910756621.5A Pending CN112386523A (en) | 2019-08-16 | 2019-08-16 | Low-odor low-irritation black eyelash beautifying gel for eyelash adhesion |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN112386523A (en) |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20130068242A1 (en) * | 2008-08-12 | 2013-03-21 | Cry Baby Culture, LLC | Semi-Permanent Mascara and Method of Applying |
| CN103251525A (en) * | 2013-05-10 | 2013-08-21 | 上海创馨化妆品有限公司 | Grafting liquid for making up eyelashes and using method thereof |
| CN104927680A (en) * | 2014-03-17 | 2015-09-23 | 宁波百仕高联合工业有限公司 | Fast-curing instant glue and preparation method thereof |
| CN108137752A (en) * | 2015-07-31 | 2018-06-08 | 艾弗尼卡技术有限公司 | Rapid photocuring cyanoacrylate compositions |
| CN111278938A (en) * | 2017-10-27 | 2020-06-12 | 汉高知识产权控股有限责任公司 | Toughened low odor/low blooming cyanoacrylate compositions |
-
2019
- 2019-08-16 CN CN201910756621.5A patent/CN112386523A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20130068242A1 (en) * | 2008-08-12 | 2013-03-21 | Cry Baby Culture, LLC | Semi-Permanent Mascara and Method of Applying |
| CN103251525A (en) * | 2013-05-10 | 2013-08-21 | 上海创馨化妆品有限公司 | Grafting liquid for making up eyelashes and using method thereof |
| CN104927680A (en) * | 2014-03-17 | 2015-09-23 | 宁波百仕高联合工业有限公司 | Fast-curing instant glue and preparation method thereof |
| CN108137752A (en) * | 2015-07-31 | 2018-06-08 | 艾弗尼卡技术有限公司 | Rapid photocuring cyanoacrylate compositions |
| CN111278938A (en) * | 2017-10-27 | 2020-06-12 | 汉高知识产权控股有限责任公司 | Toughened low odor/low blooming cyanoacrylate compositions |
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| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| CB02 | Change of applicant information | ||
| CB02 | Change of applicant information |
Address after: Room 502, Building 2, No. 459, Xiecao Road, Xiegang Town, Dongguan City, Guangdong 523000 Applicant after: Dongguan Xinli New Material Technology Co.,Ltd. Address before: No.38, Changtang No.1 Industrial Zone, Changtang community, Dongguan, Guangdong 523779 Applicant before: Dongguan instant adhesive technology Co.,Ltd. |
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| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20210223 |