CN112342100A - Formula and preparation method of high-efficiency antibacterial low-irritation handmade soap - Google Patents
Formula and preparation method of high-efficiency antibacterial low-irritation handmade soap Download PDFInfo
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- CN112342100A CN112342100A CN202011007307.6A CN202011007307A CN112342100A CN 112342100 A CN112342100 A CN 112342100A CN 202011007307 A CN202011007307 A CN 202011007307A CN 112342100 A CN112342100 A CN 112342100A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D10/00—Compositions of detergents, not provided for by one single preceding group
- C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/14—Preparations for removing make-up
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/29—Sulfates of polyoxyalkylene ethers
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/662—Carbohydrates or derivatives
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Chemical & Material Sciences (AREA)
- Dermatology (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses a formula of a high-efficiency antibacterial low-irritation handmade soap, which is characterized by comprising the following components in parts by weight: the environment-friendly and environment-friendly type environment-friendly cleaning agent comprises 100-140 parts of sorbitol, 40-60 parts of propylene glycol, 40-60 parts of sodium laureth sulfate, 80-120 parts of cocamidopropyl dimethylamine caprolactone, 50-100 parts of glycerol, 130-190 parts of stearic acid and 40-70 parts of lauric acid; 32-37 parts of sodium hydroxide, 100-125 parts of water and 18-23 parts of sodium citrate; 40-60 parts of alkyl glycoside and 150-180 parts of sucrose; 1-2 parts of a sax. The advantages are that: experiments show that the handmade soap prepared by the formula has broad-spectrum antibacterial activity, the antibacterial rate of escherichia coli, staphylococcus aureus and candida albicans reaches 99.99%, and the handmade soap has high-efficiency antibacterial activity, can keep skin moisture, and reduces degreasing power and irritation to skin.
Description
Technical Field
The invention relates to the technical field of daily washing and caring, in particular to a formula of a high-efficiency antibacterial low-irritation handmade soap and a manufacturing method thereof.
Background
Bacteria are one of the major groups of organisms, and the most abundant of all organisms. On the one hand, humans utilize bacteria, and on the other hand, bacteria are also the causative agents of many diseases. In particular Escherichia coli, Staphylococcus aureus, and Candida albicans. Meanwhile, the commercially available bacteriostatic handmade soap basically contains a large amount of anionic surfactants, has high degreasing power and high skin irritation, and bacteriostatic components in the soap easily cause bacteria to generate drug resistance and easily remain on the surface of the skin to cause irritation to the skin, so that various inflammatory reactions are caused. Based on the above, there is a need to develop a formula of handmade soap, which has high antibacterial activity, can keep skin moisture, and reduce degreasing power and irritation to skin.
Disclosure of Invention
The invention aims to overcome the technical defects and provides a formula and a preparation method of the high-efficiency bacteriostatic low-irritation handmade soap, which is simple to prepare, high in practicability, high in efficiency and bacteriostatic effect, small in irritation to skin and good in using effect.
In order to solve the technical problems, the technical scheme provided by the invention is as follows: the formula of the high-efficiency antibacterial low-irritation handmade soap comprises 100-140 parts of sorbitol, 40-60 parts of propylene glycol, 40-60 parts of sodium laureth sulfate, 80-120 parts of cocamidopropyl dimethylamine caprolactone, 50-100 parts of glycerol, 130-190 parts of stearic acid and 40-70 parts of lauric acid; 32-37 parts of sodium hydroxide, 100-125 parts of water and 18-23 parts of sodium citrate; 40-60 parts of alkyl glycoside and 150-180 parts of sucrose; 1-2 parts of a sax.
Further, 120 parts of sorbitol, 50 parts of propylene glycol, 50 parts of sodium laureth sulfate, 100 parts of cocamidopropyl dimethylamine caprolactone, 80 parts of glycerol, 160 parts of stearic acid and 60 parts of lauric acid; 34.5 parts of sodium hydroxide, 110.5 parts of water and 20 parts of sodium citrate; 50 parts of alkyl glycoside and 165 parts of cane sugar; 1.5 portions of the saili.
Further, the manufacturing method of the handmade soap comprises the following steps:
s1: adding sodium hydroxide into the first container and adding water for dissolving, and adding sodium citrate into the second container and adding water for dissolving;
s2, sequentially adding sorbitol, propylene glycol, sodium laureth sulfate, cocamidopropyl dimethylamine lactone, glycerol, stearic acid and lauric acid into a stirring kettle, and stirring for dissolving;
s3, adding the dissolved sodium hydroxide in the first container and the dissolved sodium citrate in the second container into a stirring kettle in sequence for saponification;
s4, after saponification, adding alkyl glycoside and sucrose into a stirring kettle;
s5: when the temperature of the reaction kettle is reduced to 70 ℃, adding the saleratus, stirring for 10min, discharging the soap liquid, and cooling and forming.
Further, the rotation speed of the step S2 is 25R/minThe temperature was 70 ℃.
Further, the rotation speed of the step S3 is 35R/minThe temperature was 70 ℃.
Further, the step S4 is executed at a rotation speed of 40R/minAnd the temperature is 90 ℃.
Compared with the prior art, the invention has the advantages that: experiments show that the handmade soap prepared by the formula has broad-spectrum antibacterial activity, the antibacterial rate of escherichia coli, staphylococcus aureus and candida albicans reaches 99.99%, and the handmade soap has high-efficiency antibacterial activity, can keep skin moisture, and reduces degreasing power and irritation to skin.
Detailed Description
The following further illustrates embodiments of the present invention.
The formula of the high-efficiency antibacterial low-irritation handmade soap is characterized in that: the environment-friendly and environment-friendly type environment-friendly cleaning agent comprises 100-140 parts of sorbitol, 40-60 parts of propylene glycol, 40-60 parts of sodium laureth sulfate, 80-120 parts of cocamidopropyl dimethylamine caprolactone, 50-100 parts of glycerol, 130-190 parts of stearic acid and 40-70 parts of lauric acid; 32-37 parts of sodium hydroxide, 100-125 parts of water and 18-23 parts of sodium citrate; 40-60 parts of alkyl glycoside and 150-180 parts of sucrose; 1-2 parts of a sax.
120 parts of sorbitol, 50 parts of propylene glycol, 50 parts of sodium laureth sulfate, 100 parts of cocamidopropyl dimethylamine caprolactone, 80 parts of glycerol, 160 parts of stearic acid and 60 parts of lauric acid; 34.5 parts of sodium hydroxide, 110.5 parts of water and 20 parts of sodium citrate; 50 parts of alkyl glycoside and 165 parts of cane sugar; 1.5 portions of the saili.
The manufacturing method of the handmade soap comprises the following steps:
s1: adding sodium hydroxide into the first container and adding water for dissolving, and adding sodium citrate into the second container and adding water for dissolving;
s2 adding sorbitol, propylene glycol, sodium laureth sulfate, cocamidopropyl dimethylamine lactone, glycerol, stearic acid, and lauric acid into a stirring kettle in sequence, stirring and dissolving at 25 deg.CR/minThe temperature was 70 ℃. (ii) a
S3, adding the dissolved sodium hydroxide in the first container and the dissolved sodium citrate in the second container into a stirring kettle in sequence for saponification, wherein the rotating speed is 35R/minThe temperature was 70 ℃. (ii) a
S4, after saponification, adding the alkyl glycoside and the cane sugar into a stirring kettle at the rotating speed of 40 DEGR/minAnd the temperature is 90 ℃. (ii) a
S5: when the temperature of the reaction kettle is reduced to 70 ℃, adding the saleratus, stirring for 10min, discharging the soap liquid, and cooling and forming.
The cleaning of the skin is a vital step for skin care, the formula of the handmade soap is added with cocamidopropyl dimethylamine ethyl lactone (CAB-35), belongs to an amphoteric surfactant, and is compounded with a sodium fatty acid anionic surfactant, so that the irritation of the anionic surfactant is reduced, and the CAB-35 has certain bactericidal property. The formula of the handmade soap is added with sodium citrate as a complexing agent, an antioxidant, a plasticizer and a detergent, and is compounded with a nonionic surfactant alkyl glycoside (APG). According to the principle of similarity and intermiscibility, the nonionic surfactant has a good cleaning effect on color cosmetics and the like, and the APG can reduce the irritation of the anionic surfactant and improve the skin feeling; the handmade soap is added with the bacteriostatic agent which is sexually times, has the main component of the chlorhexidine undecylenate, and is the bacteriostatic agent with high biocompatibility, easy degradation, low harm to the environment and bacterial drug resistance close to zero probability. According to the standards of QB/T2850-2007 'antibacterial bacteriostatic detergent' and GB/T19877.3-2005 'special soap', the detection result in an authoritative institution shows that the bacteriostatic rate of escherichia coli, staphylococcus aureus and candida albicans reaches 99.99%, and the detergent has a high-efficiency broad-spectrum bacteriostatic effect.
The first embodiment is as follows: 100 parts of sorbitol, 40 parts of propylene glycol, 40 parts of sodium laureth sulfate, 80 parts of cocamidopropyl dimethylamine caprolactone, 50 parts of glycerol, 130 parts of stearic acid and 40 parts of lauric acid; 32 parts of sodium hydroxide, 100 parts of water and 18 parts of sodium citrate; 40 parts of alkyl glycoside and 150 parts of sucrose; 1 part of the compound preparation.
Example two: 140 parts of sorbitol, 60 parts of propylene glycol, 60 parts of sodium laureth sulfate, 120 parts of cocamidopropyl dimethylamine caprolactone, 100 parts of glycerol, 190 parts of stearic acid and 70 parts of lauric acid; 37 parts of sodium hydroxide, 125 parts of water and 23 parts of sodium citrate; 60 parts of alkyl glycoside and 180 parts of sucrose; 2 portions of the saili.
Example three: 120 parts of sorbitol, 50 parts of propylene glycol, 50 parts of sodium laureth sulfate, 100 parts of cocamidopropyl dimethylamine caprolactone, 80 parts of glycerol, 160 parts of stearic acid and 60 parts of lauric acid; 34.5 parts of sodium hydroxide, 110.5 parts of water and 20 parts of sodium citrate; 50 parts of alkyl glycoside and 165 parts of cane sugar; 1.5 portions of the saili.
The invention and its embodiments have been described above, without this being limitative. In conclusion, those skilled in the art should appreciate that they can readily use the disclosed conception and specific embodiments as a basis for designing or modifying other structures for carrying out the same purposes of the present invention without departing from the spirit and scope of the invention as defined by the appended claims.
Claims (6)
1. The formula of the high-efficiency antibacterial low-irritation handmade soap is characterized in that: the environment-friendly and environment-friendly type environment-friendly cleaning agent comprises 100-140 parts of sorbitol, 40-60 parts of propylene glycol, 40-60 parts of sodium laureth sulfate, 80-120 parts of cocamidopropyl dimethylamine caprolactone, 50-100 parts of glycerol, 130-190 parts of stearic acid and 40-70 parts of lauric acid; 32-37 parts of sodium hydroxide, 100-125 parts of water and 18-23 parts of sodium citrate; 40-60 parts of alkyl glycoside and 150-180 parts of sucrose; 1-2 parts of a sax.
2. The formula of the high-efficiency bacteriostatic low-irritation handmade soap according to claim 1, which is characterized in that: 120 parts of sorbitol, 50 parts of propylene glycol, 50 parts of sodium laureth sulfate, 100 parts of cocamidopropyl dimethylamine caprolactone, 80 parts of glycerol, 160 parts of stearic acid and 60 parts of lauric acid; 34.5 parts of sodium hydroxide, 110.5 parts of water and 20 parts of sodium citrate; 50 parts of alkyl glycoside and 165 parts of cane sugar; 1.5 portions of the saili.
3. A method for preparing high-efficiency bacteriostatic low-irritation handmade soap is characterized by comprising the following steps: the manufacturing method of the handmade soap comprises the following steps:
s1: adding sodium hydroxide into the first container and adding water for dissolving, and adding sodium citrate into the second container and adding water for dissolving;
s2, sequentially adding sorbitol, propylene glycol, sodium laureth sulfate, cocamidopropyl dimethylamine lactone, glycerol, stearic acid and lauric acid into a stirring kettle, and stirring for dissolving;
s3, adding the dissolved sodium hydroxide in the first container and the dissolved sodium citrate in the second container into a stirring kettle in sequence for saponification;
s4, after saponification, adding alkyl glycoside and sucrose into a stirring kettle;
s5: when the temperature of the reaction kettle is reduced to 70 ℃, adding the saleratus, stirring for 10min, discharging the soap liquid, and cooling and forming.
4. The method for preparing the high-efficiency antibacterial low-irritation handmade soap according to claim 3, which is characterized in that: the rotating speed of the step S2 is 25R/minThe temperature was 70 ℃.
5. The method for preparing the high-efficiency antibacterial low-irritation handmade soap according to claim 3, which is characterized in that: the rotating speed of the step S3 is 35R/minThe temperature was 70 ℃.
6. The method for preparing the high-efficiency antibacterial low-irritation handmade soap according to claim 3, which is characterized in that: step S4 speed 40R/minAnd the temperature is 90 ℃.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011007307.6A CN112342100A (en) | 2020-09-23 | 2020-09-23 | Formula and preparation method of high-efficiency antibacterial low-irritation handmade soap |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011007307.6A CN112342100A (en) | 2020-09-23 | 2020-09-23 | Formula and preparation method of high-efficiency antibacterial low-irritation handmade soap |
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| CN112342100A true CN112342100A (en) | 2021-02-09 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN202011007307.6A Pending CN112342100A (en) | 2020-09-23 | 2020-09-23 | Formula and preparation method of high-efficiency antibacterial low-irritation handmade soap |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114736748A (en) * | 2022-04-20 | 2022-07-12 | 成都花荟缘文化发展有限公司 | Composition, antibacterial hibiscus handmade soap and preparation method thereof |
| CN114836275A (en) * | 2022-04-18 | 2022-08-02 | 重庆菩璞生物科技有限公司 | Antibacterial gold fragrant willow handmade soap and preparation process thereof |
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| CN106883959A (en) * | 2017-02-24 | 2017-06-23 | 浙江如美日化有限公司 | A kind of Chinese torreya essential oil soap |
| WO2017137818A1 (en) * | 2016-02-12 | 2017-08-17 | Salicylates & Chemicals | Synthesis and application of an antimicrobial active |
| CN109401869A (en) * | 2018-11-09 | 2019-03-01 | 广州宏度精细化工有限公司 | Liquid cleansing composition and its preparation method and application |
| CN110846161A (en) * | 2019-11-28 | 2020-02-28 | 上海绿瑞生物科技有限公司 | Soap-based composition for personal washing care |
-
2020
- 2020-09-23 CN CN202011007307.6A patent/CN112342100A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2017137818A1 (en) * | 2016-02-12 | 2017-08-17 | Salicylates & Chemicals | Synthesis and application of an antimicrobial active |
| CN106883959A (en) * | 2017-02-24 | 2017-06-23 | 浙江如美日化有限公司 | A kind of Chinese torreya essential oil soap |
| CN109401869A (en) * | 2018-11-09 | 2019-03-01 | 广州宏度精细化工有限公司 | Liquid cleansing composition and its preparation method and application |
| CN110846161A (en) * | 2019-11-28 | 2020-02-28 | 上海绿瑞生物科技有限公司 | Soap-based composition for personal washing care |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114836275A (en) * | 2022-04-18 | 2022-08-02 | 重庆菩璞生物科技有限公司 | Antibacterial gold fragrant willow handmade soap and preparation process thereof |
| CN114736748A (en) * | 2022-04-20 | 2022-07-12 | 成都花荟缘文化发展有限公司 | Composition, antibacterial hibiscus handmade soap and preparation method thereof |
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Application publication date: 20210209 |