CN112299717A - Photochromic jun porcelain glaze and preparation method thereof - Google Patents
Photochromic jun porcelain glaze and preparation method thereof Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
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Abstract
The invention provides photochromic jun porcelain glaze, which comprises the following components in parts by weight: 40-45 parts of potash feldspar, 15-21 parts of calcite, 25-28 parts of the traditional Chinese medicine, 4-6 parts of calcium phosphate, 2-5 parts of kaolin, 5-13 parts of spodumene, 22-30 parts of borax, 2-4 parts of zinc oxide, 0.5-1.5 parts of ferric oxide and 3-5 parts of silicon oxide; the firing process is strictly controlled, the firing temperature is accurately controlled, and the fired glaze has fewer pores on the surface, strong jade texture and difficult damage through compounding of the components, so that the yield of the Jun porcelain is improved.
Description
Technical Field
The invention belongs to the field of jun porcelain manufacturing, and particularly relates to photochromic jun porcelain glaze and a preparation method thereof.
Background
Jun porcelain is famous for the world with unique furnace transmutation art, starts from Tang, is contained in Song, is one of five famous porcelain in Song Dynasty, is used by royal, and is vegetatively reputable as gold valuable Jun is worthless, and is not as good as Jun porcelain; since 2000, Jun porcelain is rich in the massive historical culture base and the substantial kiln change of ghost workers, and is ascended in an important international place for many times in the name of national ceremony, so that the development of Jun porcelain artwork is unprecedented and prosperous; however, the traditional display art Jun porcelain is complex in manufacturing process, high in cost and classical in style, so that the Jun porcelain is mostly an ornament or collected;
the opalescence state and the transmutation phenomenon of the jun glaze are two appearance characteristics forming the artistic beauty of the jun porcelain, the opalescence state refers to the azure half-opalescence state of the jun glaze which is beautiful like green agate or opal, not only the jun glaze generates a series of blue colors from light to deep, but also endows the glaze with the advantages of the storage luster and elegant texture, reduces the flamboyance and the floating light caused by the vitrification of the glaze surface, and has the transmutation phenomenon that the jun glaze is melted and flows at high temperature, and the opacification and the coloring color are changed in a complex and staggered way, the glaze color becomes gorgeous and colorful, purple, red, blue and white are mutually hidden, the feeling of beauty that nature changes instantly and forever is given, the secret of 'kiln change' is in the glaze firing mechanism, the components of the Jun porcelain glaze are complex, in the glaze firing process, slight changes of the temperature and atmosphere in the kiln can cause different chemical reactions, and the color of the Jun porcelain can be changed.
Under the condition of strictly controlling glaze firing temperature and atmosphere, the colorant in the glaze plays a role in determining color generation, the most commonly used colorant is oxides such as copper oxide, iron oxide and the like, the glaze color of the fired jun porcelain is fixed, the glaze is beautiful, but the requirement of people for pursuing higher levels of jun porcelain art cannot be met, so that the research on novel functionalized jun porcelain glaze is forced to be in the forefront, at present, the research on the functionalized glaze is mainly focused on the aspect of color-changing glaze, the color-changing glaze is prepared by adding the color-changing glaze into the jun porcelain glaze, the jun porcelain glaze can show different color effects under different light sources, but photochromic powder is poor in high-temperature stability and cannot stably exist, and the yield of the currently fired photochromic glaze is low, so that great waste is caused.
Disclosure of Invention
Aiming at the problems, the invention provides photochromic jun porcelain glaze and a preparation method thereof, which are mainly realized in the following way;
photochromic Jun porcelain glaze comprises the following components in parts by weight: 40-45 parts of potash feldspar, 15-21 parts of calcite, 25-28 parts of the traditional Chinese medicine, 4-6 parts of calcium phosphate, 2-5 parts of kaolin, 5-13 parts of spodumene, 22-30 parts of borax, 2-4 parts of zinc oxide, 0.5-1.5 parts of ferric oxide and 3-5 parts of silicon oxide.
The photochromic Jun porcelain glaze comprises the following components in parts by weight: 42 parts of potash feldspar, 18 parts of calcite, 27 parts of the traditional Chinese medicine, 5 parts of calcium phosphate, 3 parts of kaolin, 9 parts of spodumene, 26 parts of borax, 3.5 parts of zinc oxide, 1 part of ferric oxide and 4 parts of silicon oxide.
The preparation method of the photochromic Jun porcelain glaze comprises the following steps:
1) weighing quantitative zinc oxide, iron oxide and silicon oxide according to a proportion, and preparing the zinc oxide, the iron oxide and the silicon oxide into a photochromic compound;
2) weighing quantitative potash feldspar, calcite, the traditional Chinese medicine, calcium phosphate, kaolin, spodumene, borax and a photochromic compound according to a proportion, mixing to obtain mixed powder, adding the mixed powder into a ball milling tank containing alumina ball milling balls and distilled water, fixing the ball milling tank on a high-speed vibration ball mill, rotating and ball milling, and controlling slurry to be 400-mesh and 450-mesh to prepare glaze slurry;
3) uniformly dipping the glaze slip on the blank body in a glaze dipping mode;
4) and firing and molding the glazed green body.
In the preparation method of the photochromic jun enamel, the preparation method of the photochromic compound in the step 1) is as follows:
weighing quantitative zinc oxide, iron oxide and silicon oxide according to a proportion, uniformly mixing the weighed zinc oxide, iron oxide and silicon oxide, grinding for 40-50min by using a ball mill, and calcining for 45-55min at the high temperature of 1250-.
In the preparation method of the photochromic jun enamel, the firing and forming in the step 4) are divided into three stages:
(1) a preheating stage: uniformly heating the furnace temperature from a normal temperature state to 500 ℃ within 5 hours, and keeping the temperature for 1.5 hours;
(2) a temperature rising stage: the furnace temperature is uniformly raised to 1225-1250 ℃ within 2-3 hours, and the temperature is kept for 12-13 hours;
(3) and (3) a cooling stage: naturally cooling to 200-300 ℃, and then taking out of the kiln.
The invention has the beneficial technical effects that: the invention takes potash feldspar, calcite and the traditional Chinese medicine as main materials, and adds calcium phosphate, kaolin, spodumene and borax as additives to be used as basic materials of glaze; the potassium feldspar is mainly used for improving the content of alumina in glaze ingredients, reducing the melting temperature and increasing the content of alkali so as to reduce the consumption of the alkali, and in addition, the process of changing the potassium feldspar into the vitreous glaze after melting is slower, the crystallization capacity is small, and crystal precipitation in the glass forming process can be preventedThe kaolin for destroying the product mainly improves the melting temperature of the glaze, and has the auxiliary effect of improving the suspension property of the glaze so that glaze water is not easy to precipitate; the refractive index of the glaze can be increased in the glaze by calcite, so that the glossiness is improved, and the light transmittance of the glaze can be improved; the medicine is a natural glaze stone, and has chemical composition and potash feldspar (K)2O·Al2O3·6SiO2) Approximately, the porcelain glaze plays a role of basic glaze in Jun porcelain glaze; calcium phosphate is mainly used as a binder; the spodumene has good thermal shock resistance and fluxing property, can reduce the sintering temperature of the product, shorten the sintering time, and can improve the strength, ductility, corrosion resistance and thermal shock resistance of the product; the borax can improve the compressive strength, the wear resistance and the chemical resistance of the porcelain, the adaptability of the blank glaze is improved due to the control of the thermal expansion coefficient, and meanwhile, the melting temperature can also be reduced, the devitrification is prevented, and the product is smoother and more perfect;
the photochromic compound prepared by adding quantitative zinc oxide, iron oxide and silicon oxide powder into the basic glaze, and through strictly controlling the firing process, the firing temperature is accurately controlled, so that the fired jun porcelain glaze is red on the whole, and can be blue under the irradiation of light, thereby having the photochromic function, and the fired glaze has fewer surface pores through the compounding among the components, has strong jade texture, is not easy to damage, and improves the yield of the jun porcelain.
DETAILED DESCRIPTION OF EMBODIMENT (S) OF INVENTION
The technical solution of the present invention will be described clearly and completely with reference to the following embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments; all other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
Photochromic Jun porcelain glaze comprises the following components in parts by weight: 40-45 parts of potash feldspar, 15-21 parts of calcite, 25-28 parts of the traditional Chinese medicine, 4-6 parts of calcium phosphate, 2-5 parts of kaolin, 5-13 parts of spodumene, 22-30 parts of borax, 2-4 parts of zinc oxide, 0.5-1.5 parts of ferric oxide and 3-5 parts of silicon oxide.
The preparation method of the photochromic Jun porcelain glaze comprises the following steps:
1) weighing quantitative zinc oxide, iron oxide and silicon oxide according to a proportion, and preparing the zinc oxide, the iron oxide and the silicon oxide into a photochromic compound;
2) weighing quantitative potash feldspar, calcite, the traditional Chinese medicine, calcium phosphate, kaolin, spodumene, borax and a photochromic compound according to a proportion, mixing to obtain mixed powder, adding the mixed powder into a ball milling tank containing alumina ball milling balls and distilled water, fixing the ball milling tank on a high-speed vibration ball mill, rotating and ball milling, and controlling slurry to be 400-mesh and 450-mesh to prepare glaze slurry;
3) uniformly dipping the glaze slip on the blank body in a glaze dipping mode;
4) and firing and molding the glazed green body.
In the preparation method of the photochromic jun enamel, the preparation method of the photochromic compound in the step 1) is as follows:
weighing quantitative zinc oxide, iron oxide and silicon oxide according to a proportion, uniformly mixing the weighed zinc oxide, iron oxide and silicon oxide, grinding for 40-50min by using a ball mill, and calcining for 45-55min at the high temperature of 1250-.
In the preparation method of the photochromic jun enamel, the firing and forming in the step 4) are divided into three stages:
(1) a preheating stage: uniformly heating the furnace temperature from a normal temperature state to 500 ℃ within 5 hours, and keeping the temperature for 1.5 hours;
(2) a temperature rising stage: the furnace temperature is uniformly raised to 1225-1250 ℃ within 2-3 hours, and the temperature is kept for 12-13 hours;
(3) and (3) a cooling stage: naturally cooling to 200-300 ℃, and then taking out of the kiln.
The invention takes potash feldspar, calcite and the traditional Chinese medicine as main materials, and adds calcium phosphate, kaolin, spodumene and borax as additives to be used as basic materials of glaze; the potassium feldspar is mainly used for improving the content of alumina in glaze ingredients, reducing the melting temperature and increasing the content of alkali so as to reduce the consumption of the alkali, in addition, the process of changing the potassium feldspar into a vitreous glaze after melting is slower, the crystallization capacity is small, the phenomenon that the kaolin product is damaged due to crystal precipitation in the glass forming process is prevented, the melting temperature of the glaze is mainly improved, the suspension property of the glaze is improved, and glaze water is not easy to precipitate; the refractive index of the glaze can be increased in the glaze by calcite, so that the glossiness is improved, and the light transmittance of the glaze can be improved; the natural glaze stone has a chemical composition similar to that of potassium feldspar (K2O. Al2O 3. 6SiO 2), and plays a role of basic glaze in Jun porcelain glaze; calcium phosphate is mainly used as a binder; the spodumene has good thermal shock resistance and fluxing property, can reduce the sintering temperature of the product, shorten the sintering time, and can improve the strength, ductility, corrosion resistance and thermal shock resistance of the product; the borax can improve the compressive strength, the wear resistance and the chemical resistance of the porcelain, the adaptability of the blank glaze is improved due to the control of the thermal expansion coefficient, and meanwhile, the melting temperature can also be reduced, the devitrification is prevented, and the product is smoother and more perfect;
the photochromic compound prepared by adding quantitative zinc oxide, iron oxide and silicon oxide powder into the basic glaze, and through strictly controlling the firing process, the firing temperature is accurately controlled, so that the fired jun porcelain glaze is red on the whole, and can be blue under the irradiation of light, thereby having the photochromic function, and the fired glaze has fewer surface pores through the compounding among the components, has strong jade texture, is not easy to damage, and improves the yield of the jun porcelain.
Example 2
Photochromic Jun porcelain glaze comprises the following components in parts by weight: 42 parts of potash feldspar, 18 parts of calcite, 27 parts of the traditional Chinese medicine, 5 parts of calcium phosphate, 3 parts of kaolin, 9 parts of spodumene, 26 parts of borax, 3.5 parts of zinc oxide, 1 part of ferric oxide and 4 parts of silicon oxide.
The preparation method of the photochromic Jun porcelain glaze comprises the following steps:
1) weighing quantitative zinc oxide, iron oxide and silicon oxide according to a proportion, and preparing the zinc oxide, the iron oxide and the silicon oxide into a photochromic compound;
2) weighing quantitative potash feldspar, calcite, the traditional Chinese medicine, calcium phosphate, kaolin, spodumene, borax and a photochromic compound according to a proportion, mixing to obtain mixed powder, adding the mixed powder into a ball milling tank containing alumina ball milling balls and distilled water, fixing the ball milling tank on a high-speed vibration ball mill, rotating and ball milling, and controlling slurry to be 400-mesh and 450-mesh to prepare glaze slurry;
3) uniformly dipping the glaze slip on the blank body in a glaze dipping mode;
4) and firing and molding the glazed green body.
In the preparation method of the photochromic jun enamel, the preparation method of the photochromic compound in the step 1) is as follows:
weighing quantitative zinc oxide, iron oxide and silicon oxide according to a proportion, uniformly mixing the weighed zinc oxide, iron oxide and silicon oxide, grinding for 40-50min by using a ball mill, and calcining for 45-55min at the high temperature of 1250-.
In the preparation method of the photochromic jun enamel, the firing and forming in the step 4) are divided into three stages:
(1) a preheating stage: uniformly heating the furnace temperature from a normal temperature state to 500 ℃ within 5 hours, and keeping the temperature for 1.5 hours;
(2) a temperature rising stage: the furnace temperature is uniformly raised to 1225-1250 ℃ within 2-3 hours, and the temperature is kept for 12-13 hours;
(3) and (3) a cooling stage: naturally cooling to 200-300 ℃, and then taking out of the kiln.
Through strict control of firing process parameters and accurate control of firing temperature, the fired jun porcelain glaze is red on the whole, can be blue under light irradiation, has a photochromic function, has fewer pores on the surface of the fired glaze through compounding of all components, has strong jade texture, is not easy to damage, and improves the yield of jun porcelain.
Example 3
Photochromic Jun porcelain glaze comprises the following components in parts by weight: 45 parts of potash feldspar, 20 parts of calcite, 25 parts of the traditional Chinese medicine, 6 parts of calcium phosphate, 4 parts of kaolin, 11 parts of spodumene, 23 parts of borax, 2.5 parts of zinc oxide, 1.2 parts of ferric oxide and 3.5 parts of silicon oxide.
The preparation method of the photochromic Jun porcelain glaze comprises the following steps:
1) weighing quantitative zinc oxide, iron oxide and silicon oxide according to a proportion, and preparing the zinc oxide, the iron oxide and the silicon oxide into a photochromic compound;
2) weighing quantitative potash feldspar, calcite, the traditional Chinese medicine, calcium phosphate, kaolin, spodumene, borax and a photochromic compound according to a proportion, mixing to obtain mixed powder, adding the mixed powder into a ball milling tank containing alumina ball milling balls and distilled water, fixing the ball milling tank on a high-speed vibration ball mill, rotating and ball milling, and controlling slurry to be 400-mesh and 450-mesh to prepare glaze slurry;
3) uniformly dipping the glaze slip on the blank body in a glaze dipping mode;
4) and firing and molding the glazed green body.
In the preparation method of the photochromic jun enamel, the preparation method of the photochromic compound in the step 1) is as follows:
weighing quantitative zinc oxide, iron oxide and silicon oxide according to a proportion, uniformly mixing the weighed zinc oxide, iron oxide and silicon oxide, grinding for 40-50min by using a ball mill, and calcining for 45-55min at the high temperature of 1250-.
In the preparation method of the photochromic jun enamel, the firing and forming in the step 4) are divided into three stages:
(1) a preheating stage: uniformly heating the furnace temperature from a normal temperature state to 500 ℃ within 5 hours, and keeping the temperature for 1.5 hours;
(2) a temperature rising stage: the furnace temperature is uniformly raised to 1225-1250 ℃ within 2-3 hours, and the temperature is kept for 12-13 hours;
(3) and (3) a cooling stage: naturally cooling to 200-300 ℃, and then taking out of the kiln.
Through strict control of firing process parameters and accurate control of firing temperature, the fired jun porcelain glaze is red on the whole, can be blue under light irradiation, has a photochromic function, has fewer pores on the surface of the fired glaze through compounding of all components, has strong jade texture, is not easy to damage, and improves the yield of jun porcelain.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like that fall within the spirit and principle of the present invention are intended to be included therein.
Claims (5)
1. A photochromic jun porcelain glaze is characterized in that: the glaze comprises the following components in parts by weight: 40-45 parts of potash feldspar, 15-21 parts of calcite, 25-28 parts of the traditional Chinese medicine, 4-6 parts of calcium phosphate, 2-5 parts of kaolin, 5-13 parts of spodumene, 22-30 parts of borax, 2-4 parts of zinc oxide, 0.5-1.5 parts of ferric oxide and 3-5 parts of silicon oxide.
2. Photochromic Jun porcelain glaze according to claim 1, wherein: the glaze comprises the following components in parts by weight: 42 parts of potash feldspar, 18 parts of calcite, 27 parts of the traditional Chinese medicine, 5 parts of calcium phosphate, 3 parts of kaolin, 9 parts of spodumene, 26 parts of borax, 3.5 parts of zinc oxide, 1 part of ferric oxide and 4 parts of silicon oxide.
3. A preparation method of photochromic Jun porcelain glaze is characterized by comprising the following steps: the preparation method of the photochromic jun porcelain glaze comprises the photochromic jun porcelain glaze of any one of claims 1 to 2;
the preparation method of the photochromic Jun porcelain glaze comprises the following steps:
1) weighing quantitative zinc oxide, iron oxide and silicon oxide according to a proportion, and preparing the zinc oxide, the iron oxide and the silicon oxide into a photochromic compound;
2) weighing quantitative potash feldspar, calcite, the traditional Chinese medicine, calcium phosphate, kaolin, spodumene, borax and a photochromic compound according to a proportion, mixing to obtain mixed powder, adding the mixed powder into a ball milling tank containing alumina ball milling balls and distilled water, fixing the ball milling tank on a high-speed vibration ball mill, rotating and ball milling, and controlling slurry to be 400-mesh and 450-mesh to prepare glaze slurry;
3) uniformly dipping the glaze slip on the blank body in a glaze dipping mode;
4) and firing and molding the glazed green body.
4. The method for preparing photochromic Jun porcelain glaze according to claim 3, wherein the method comprises the following steps: the preparation method of the photochromic compound comprises the following steps:
weighing quantitative zinc oxide, iron oxide and silicon oxide according to a proportion, uniformly mixing the weighed zinc oxide, iron oxide and silicon oxide, grinding for 40-50min by using a ball mill, and calcining for 45-55min at the high temperature of 1250-.
5. The method for preparing photochromic Jun porcelain glaze according to claim 3, wherein the method comprises the following steps: the firing and forming in the step 4) are divided into three stages:
a preheating stage: uniformly heating the furnace temperature from a normal temperature state to 500 ℃ within 5 hours, and keeping the temperature for 1.5 hours;
a temperature rising stage: the furnace temperature is uniformly raised to 1225-1250 ℃ within 2-3 hours, and the temperature is kept for 12-13 hours;
and (3) a cooling stage: naturally cooling to 200-300 ℃, and then taking out of the kiln.
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| 王邓等: ""不同烧成窑炉对变色钧瓷呈色与显微结构的影响"", 《硅酸盐通报》 * |
| 苑金生: ""稀土元素的发色特性及其在陶瓷色釉料中的应用"", 《陶瓷》 * |
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| 陆小荣: ""变色结晶釉的研制"", 《江苏陶瓷》 * |
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