CN112295519A - A hydrothermal reaction cauldron inner bag for panel steam-curing treatment - Google Patents
A hydrothermal reaction cauldron inner bag for panel steam-curing treatment Download PDFInfo
- Publication number
- CN112295519A CN112295519A CN202011121441.9A CN202011121441A CN112295519A CN 112295519 A CN112295519 A CN 112295519A CN 202011121441 A CN202011121441 A CN 202011121441A CN 112295519 A CN112295519 A CN 112295519A
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- China
- Prior art keywords
- reaction kettle
- hydrothermal reaction
- liner
- plate
- curing treatment
- Prior art date
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Links
- 238000001027 hydrothermal synthesis Methods 0.000 title claims abstract description 38
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 27
- 238000005192 partition Methods 0.000 claims abstract description 19
- 238000006243 chemical reaction Methods 0.000 claims abstract description 15
- 238000012545 processing Methods 0.000 claims description 3
- 230000008878 coupling Effects 0.000 claims description 2
- 238000010168 coupling process Methods 0.000 claims description 2
- 238000005859 coupling reaction Methods 0.000 claims description 2
- 239000007788 liquid Substances 0.000 description 6
- 238000000034 method Methods 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- 239000000463 material Substances 0.000 description 3
- 238000011160 research Methods 0.000 description 3
- 238000002791 soaking Methods 0.000 description 3
- 229910052918 calcium silicate Inorganic materials 0.000 description 2
- 239000000378 calcium silicate Substances 0.000 description 2
- OYACROKNLOSFPA-UHFFFAOYSA-N calcium;dioxido(oxo)silane Chemical compound [Ca+2].[O-][Si]([O-])=O OYACROKNLOSFPA-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 229920001343 polytetrafluoroethylene Polymers 0.000 description 2
- 239000004810 polytetrafluoroethylene Substances 0.000 description 2
- 238000007789 sealing Methods 0.000 description 2
- 229910001220 stainless steel Inorganic materials 0.000 description 2
- 239000010935 stainless steel Substances 0.000 description 2
- -1 Polytetrafluoroethylene Polymers 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000004568 cement Substances 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
Images
Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/24—Stationary reactors without moving elements inside
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Devices For Post-Treatments, Processing, Supply, Discharge, And Other Processes (AREA)
Abstract
The invention discloses a hydrothermal reaction kettle liner for steam curing treatment of plates, which comprises a liner cover and a liner body, wherein the liner cover is connected with the liner body to form a reaction kettle inner cavity, the upper end of the liner body is provided with a table body, the table body is positioned in the inner cavity of the reaction kettle, the table body is provided with a water storage tank, the upper end of the table body is provided with a partition plate, the partition plate is positioned above the water storage tank and comprises a rectangular part and an arc part, the rectangular part and the arc part are integrally formed, and the rectangular part is provided with uniformly distributed holes. The problem of reation kettle steam curing when handling panel, panel takes place to warp and bubble water is solved, this simple structure has increased the efficiency of steam curing panel.
Description
Technical Field
The invention relates to the field of experimental instruments, in particular to a hydrothermal reaction kettle inner container for steam curing treatment of plates.
Background
The hydrothermal reaction kettle is a high-temperature-resistant, high-pressure-resistant, corrosion-resistant and high-purity reaction vessel, and is widely applied to scientific research experiments in the fields of new materials, energy, environmental engineering and the like. The hydrothermal reaction kettle is a common small reactor for scientific research in teaching and scientific research units and chemical laboratories of colleges and universities. The hydrothermal reaction kettle usually comprises a shell and an inner container, wherein the shell is generally formed by finely processing high-quality nonmagnetic stainless steel, and the inner container can be respectively made of primary Polytetrafluoroethylene (PTFE) capable of resisting the temperature of 220 ℃ and para-polyphenol (PPL) capable of resisting the temperature of 280 ℃. The inner container bearing is arranged inside the reaction kettle, the stainless steel kettle body and the top cover are screwed down to seal the inner container during use, and the inner container can be ejected upwards through the bottom cover of the reaction kettle when being taken out. The inner container of the existing hydrothermal reaction kettle comprises a container body and a container cover, and the inner container is integrally cylindrical and is suitable for containing liquid or solid-liquid amorphous samples.
At present, the formed plates such as calcium silicate plates in laboratories contain higher moisture, the mechanical strength is lower before the plates are subjected to hydrothermal reaction at high temperature and high pressure, and when the laboratory carries out hydrothermal hardening reaction of the plates such as the calcium silicate plates and fiber cement plates, the plates placed by using the existing inner containers have certain defects: 1. steam condensate water generated after the hydrothermal reaction is finished is deposited at the bottom of the inner container of the reaction kettle, so that the plate is soaked in water; 2. in order to increase the contact area between the plate and the steam, the plate is vertically or obliquely placed in the inner container of the reaction kettle, so that the plate is easily stressed unevenly, and deformation is caused.
Disclosure of Invention
Aiming at the technical problems in the prior art, the invention aims to: a hydrothermal reaction kettle inner container for plate steam curing treatment is additionally provided with a structure capable of placing a partition plate, and is used for placing plates for steam curing treatment and preventing the plates from deforming and soaking water.
In order to achieve the purpose, the invention adopts the following technical scheme:
the utility model provides a hydrothermal reaction kettle inner bag for panel evaporates foster processing, includes the courage lid and courage body, courage lid and courage body coupling form the reation kettle inner chamber, the upper end of the courage body is equipped with the stage body, the stage body is located reation kettle's inner chamber, the stage body is equipped with the aqua storage tank, the baffle is installed to the upper end of stage body, the baffle is located the top of aqua storage tank.
Preferably, the baffle includes rectangle portion and arc portion, rectangle portion and arc portion integrated into one piece, rectangle portion is equipped with evenly distributed's hole.
Preferably, the upper end of the table body is provided with a sliding chute and a supporting surface, and two ends of the rectangular part are connected with the sliding chute; the arc-shaped part is tightly attached to the supporting surface.
Preferably, the distance between the central axes of the adjacent 2 holes is 20-30 mm, and the diameter of each hole is 30 mm.
Preferably, the stage body is provided with two inclined planes, and the two inclined planes are symmetrically arranged relative to the central axis of the stage body.
Preferably, the partition is horizontally disposed.
Preferably, the upper end of the liner body is provided with an annular groove, the liner cover comprises a cover body and a cover opening, the cover body and the cover opening are integrally formed, and the cover opening is embedded into the annular groove.
Preferably, the chute is located above the annular groove.
Compared with the prior art, the invention has the following advantages and beneficial effects:
1. the invention relates to a hydrothermal reaction kettle liner for steam curing of plates, which adopts a partition plate to support rectangular plates for steam curing, a water storage tank is arranged below the partition plate and used for collecting steam condensate water after the hydrothermal reaction is finished, and the plates horizontally placed on the partition plate can not deform and soak water.
2. The hydrothermal reaction kettle liner for the steam curing treatment of the plate is provided with the holes in the rectangular part, and the holes increase the contact area between the plate and steam during high-temperature steam curing reaction, so that the steam curing efficiency of the plate is improved.
3. The inner container of the hydrothermal reaction kettle for the steam curing treatment of the plate is additionally provided with the inclined surface, the inclined surface is used for accelerating the collection of steam condensate water after the hydrothermal reaction is finished, and the plate is prevented from soaking water in the steam curing process.
4. The inner container of the hydrothermal reaction kettle for the steam curing treatment of the plate is inverted for use, has the reaction effect of the conventional hydrothermal reaction kettle, and can be filled with liquid or solid-liquid amorphous samples.
Drawings
FIG. 1 is a sectional view of the inner container of a hydrothermal reaction kettle for steam-curing a plate material
FIG. 2 is a schematic view of the inner container of a hydrothermal reaction kettle for steam curing treatment of plates
FIG. 3 is a plan view of a table body in the inner container of a hydrothermal reaction kettle for steam-curing plate material
FIG. 4 is a schematic diagram of a partition board in the inner container of a hydrothermal reaction kettle for steam-curing treatment of plates
Wherein, 1 is the courage lid, 101 is the lid, 102 is the flap, 2 is the courage body, 3 is the annular groove, 4 is the stage body, 401 is the inclined plane, 402 is the holding surface, 5 is the spout, 6 is the aqua storage tank, 7 is the baffle, 701 is the rectangle portion, 702 is the arc portion, 703 is the hole.
Detailed Description
The following describes the object of the present invention in further detail with reference to the drawings and specific examples, which are not repeated herein, but the embodiments of the present invention are not limited to the following examples.
As shown in fig. 1 to 4, a hydrothermal reaction kettle liner for steam-curing treatment of plates comprises a liner cover 1 and a liner body 2, wherein the liner cover 1 is connected with the liner body 2 to form a reaction kettle inner cavity, a table body 4 is arranged at the upper end of the liner body 2, the table body 4 is positioned in the inner cavity of the reaction kettle, the table body 4 is provided with a water storage tank 6, and the water storage tank 6 is used for collecting steam condensate water after the hydrothermal reaction is finished to avoid soaking plates in water. A partition plate 7 is installed at the upper end of the table body 4, the partition plate 7 is located above the water storage tank 6, a plate is placed at the upper end of the partition plate 7 and used for a hydrothermal reaction test, and the partition plate 7 evenly bears the pressure of the plate, so that the plate is evenly stressed and is not prone to deformation. The partition plate 7 comprises a rectangular portion 701 and an arc-shaped portion 702, the rectangular portion 701 and the arc-shaped portion 702 are integrally formed, holes 703 are uniformly distributed in the rectangular portion 701, the holes 703 increase the contact area of the plate and water vapor, and the steam curing efficiency of the plate is improved. The distance between the central axes of the adjacent holes 703 is 20-30 mm, the diameter of each hole 703 is 30mm, the contact area between the plate and water vapor is increased, and the compression strength of the partition plate 7 is met.
The upper end of the table body 4 is provided with a sliding chute 5 and a supporting surface 402, and two ends of the rectangular part 701 are connected with the sliding chute 5; arc portion 702 pastes tightly with holding surface 402 mutually, and when baffle 7 embedded spout 5 was in, the holding surface 402 of stage body 4 was used for supporting baffle 7, spout 5 fixed baffle 7, and baffle 7 is difficult for making a round trip to slide, has improved baffle 7's stability, and another function of spout 5 is used for receiving the comdenstion water that the lateral wall of reation kettle inner chamber flowed in, and the comdenstion water of spout 5 flows into aqua storage tank 6.
The baffle 7 is horizontally arranged, the upper end of the sample plate for placing the baffle 7 is stressed uniformly, and the plate is not easy to deform when being heated in the hydrothermal reaction process.
The upper end of the liner body 2 is provided with an annular groove 3, the liner cover 1 comprises a cover body 101 and a cover opening 102, the cover body 101 and the cover opening 102 are integrally formed, the cover opening 102 is embedded into the annular groove 3, the annular groove 3 is hermetically connected with the cover opening 102, a sealing ring is mounted at the joint of the liner cover 1 and the liner body 2, and the sealing performance of the reaction kettle is improved. The chute 5 is located above the annular groove 3, ensuring that the partition 7 can be installed in the chute 5.
The liner cover 1 and the liner body 2 are used in an inverted mode, the partition plate 7 is taken out, the test effect of a conventional hydrothermal reaction kettle is achieved, liquid or solid-liquid amorphous samples can be filled, and the liner of the reaction kettle has multiple using methods at the same time, so that different requirements of hydrothermal reaction tests are met.
The above-mentioned embodiments are preferred embodiments of the present invention, and the present invention is not limited thereto, and any other modifications or equivalent substitutions that do not depart from the technical spirit of the present invention are included in the scope of the present invention.
Claims (8)
1. The utility model provides a hydrothermal reaction kettle inner bag for panel evaporates foster processing, includes courage lid and courage body, and courage lid forms the reation kettle inner chamber with courage body coupling, its characterized in that: the upper end of the container body is provided with a table body, the table body is positioned in the inner cavity of the reaction kettle, the table body is provided with a water storage tank, the upper end of the table body is provided with a partition plate, and the partition plate is positioned above the water storage tank.
2. The hydrothermal reaction kettle liner for the steam curing treatment of the plate as claimed in claim 1, is characterized in that: the baffle includes rectangle portion and arc portion, rectangle portion and arc portion integrated into one piece, rectangle portion is equipped with evenly distributed's hole.
3. The hydrothermal reaction kettle liner for the steam curing treatment of the plate as claimed in claim 2, is characterized in that: the upper end of the table body is provided with a sliding chute and a supporting surface, and the two ends of the rectangular part are connected with the sliding chute; the arc-shaped part is tightly attached to the supporting surface.
4. The hydrothermal reaction kettle liner for the steam curing treatment of the plate as claimed in claim 2, is characterized in that: the distance between the central axes of the adjacent 2 holes is 20-30 mm, and the diameter of each hole is 30 mm.
5. The hydrothermal reaction kettle liner for the steam curing treatment of the plate as claimed in claim 3, is characterized in that: the stage body is equipped with two inclined planes, two inclined planes are relative the axis symmetry setting of stage body.
6. The hydrothermal reaction kettle liner for the steam curing treatment of the plate as claimed in claim 3, is characterized in that: the partition plate is horizontally arranged.
7. The hydrothermal reaction kettle liner for the steam curing treatment of the plate as claimed in claim 1, is characterized in that: the upper end of the liner body is provided with an annular groove, the liner cover comprises a cover body and a cover opening, the cover body and the cover opening are integrally formed, and the cover opening is embedded into the annular groove.
8. The hydrothermal reaction kettle liner for the steam curing treatment of the plate as claimed in claim 3, is characterized in that: the chute is located above the annular groove.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011121441.9A CN112295519A (en) | 2020-10-20 | 2020-10-20 | A hydrothermal reaction cauldron inner bag for panel steam-curing treatment |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011121441.9A CN112295519A (en) | 2020-10-20 | 2020-10-20 | A hydrothermal reaction cauldron inner bag for panel steam-curing treatment |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN112295519A true CN112295519A (en) | 2021-02-02 |
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ID=74328451
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202011121441.9A Pending CN112295519A (en) | 2020-10-20 | 2020-10-20 | A hydrothermal reaction cauldron inner bag for panel steam-curing treatment |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN112295519A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113813877A (en) * | 2021-10-26 | 2021-12-21 | 遵义师范学院 | A reation kettle for preparing black phosphorus |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2836912Y (en) * | 2005-11-18 | 2006-11-15 | 广西师范大学 | High-pressure reaction kettle |
| CN104437297A (en) * | 2014-11-06 | 2015-03-25 | 上海远怀化工科技有限公司 | Hydrothermal synthesis reaction kettle inner container |
| CN104892026A (en) * | 2015-05-14 | 2015-09-09 | 甘昌成 | Concrete closed hydrothermal synthesis hardening process |
| CN207105223U (en) * | 2017-08-28 | 2018-03-16 | 滁州职业技术学院 | A kind of cement electric pole aids in steam curing device |
| CN209451810U (en) * | 2018-12-26 | 2019-10-01 | 吕梁学院 | A kind of hydrothermal reaction kettle |
| CN111702935A (en) * | 2020-05-28 | 2020-09-25 | 郑州市雷德水泥制品有限公司 | Cement wire pole evaporates foster pond |
| CN213913697U (en) * | 2020-10-20 | 2021-08-10 | 华南理工大学 | A hydrothermal reaction cauldron inner bag for panel steam-curing treatment |
-
2020
- 2020-10-20 CN CN202011121441.9A patent/CN112295519A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2836912Y (en) * | 2005-11-18 | 2006-11-15 | 广西师范大学 | High-pressure reaction kettle |
| CN104437297A (en) * | 2014-11-06 | 2015-03-25 | 上海远怀化工科技有限公司 | Hydrothermal synthesis reaction kettle inner container |
| CN104892026A (en) * | 2015-05-14 | 2015-09-09 | 甘昌成 | Concrete closed hydrothermal synthesis hardening process |
| CN207105223U (en) * | 2017-08-28 | 2018-03-16 | 滁州职业技术学院 | A kind of cement electric pole aids in steam curing device |
| CN209451810U (en) * | 2018-12-26 | 2019-10-01 | 吕梁学院 | A kind of hydrothermal reaction kettle |
| CN111702935A (en) * | 2020-05-28 | 2020-09-25 | 郑州市雷德水泥制品有限公司 | Cement wire pole evaporates foster pond |
| CN213913697U (en) * | 2020-10-20 | 2021-08-10 | 华南理工大学 | A hydrothermal reaction cauldron inner bag for panel steam-curing treatment |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113813877A (en) * | 2021-10-26 | 2021-12-21 | 遵义师范学院 | A reation kettle for preparing black phosphorus |
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