CN112266237A - Water-based inorganic nano-polymer luminous ceramic material and preparation method thereof - Google Patents
Water-based inorganic nano-polymer luminous ceramic material and preparation method thereof Download PDFInfo
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- CN112266237A CN112266237A CN202011215410.XA CN202011215410A CN112266237A CN 112266237 A CN112266237 A CN 112266237A CN 202011215410 A CN202011215410 A CN 202011215410A CN 112266237 A CN112266237 A CN 112266237A
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- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/14—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silica
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- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
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- C04B2235/602—Making the green bodies or pre-forms by moulding
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Abstract
The invention discloses a water-based inorganic nano-polymer luminous ceramic material and a preparation method thereof. In the invention, one electronic weighing scale is taken, 60-70 parts of ethyl orthosilicate, 15-25 parts of silicon dioxide dispersion liquid, 10-30 parts of absolute ethyl alcohol, 1-5 parts of anhydrous acetic acid, 5-15 parts of distilled water, 1-3 parts of thickening agent and 2-5 parts of wetting agent are weighed, 20-30 parts of energy storage luminescent material are used for weighing the raw materials in the step S1 to obtain required weight, the raw materials are mixed and loaded into a charging barrel of a ball mill, and then water is added to open a switch of the ball mill for ball milling; the luminous ceramic material produced by adopting the formula has the advantages of long service life, no toxicity, no harm, no radioactive elements, long luminous time, super-strong hydrophobicity, self-cleaning, no adhesion, corrosion resistance, high temperature resistance, weather resistance, no aging, freezing resistance and the like, effectively improves the decorative effect, and prolongs the service life of the material; the invention is mainly applied to luminous signs in buildings, decorations, advertisements, traffic signs, artificial landscapes, markets and special occasions, and can also be used for low-degree emergency lighting.
Description
Technical Field
The invention belongs to the technical field of ceramic material preparation, and particularly relates to a water-based inorganic nano-polymer luminous ceramic material and a preparation method thereof.
Background
The ceramic material is an inorganic non-metallic material prepared by forming and high-temperature sintering natural or synthetic compounds. It has the advantages of high melting point, high hardness, high wear resistance, oxidation resistance, etc. The ceramic can be used as a structural material and a cutter material, and can also be used as a functional material because the ceramic also has certain special properties.
However, the traditional luminescent coating of the traditional ceramic material mostly contains organic volatile matters such as benzene, formaldehyde, ethylene glycol monobutyl ether and the like; the traditional luminous coating is easy to generate static electricity, is easy to be sticky again at high temperature, is easy to adsorb dust in the air, and causes low luminous efficiency; the traditional luminescent coating is easy to age, and the traditional luminescent coating has short luminescent time.
Disclosure of Invention
The invention aims to: in order to solve the problems, an aqueous inorganic nano-polymer luminous ceramic material and a preparation method thereof are provided.
The technical scheme adopted by the invention is as follows: an aqueous inorganic nano-polymer luminous ceramic material and a preparation method thereof are disclosed, wherein the aqueous inorganic nano-polymer luminous ceramic material and the preparation method thereof need to use: 60-70 parts of ethyl orthosilicate, 15-25 parts of silicon dioxide dispersion liquid, 10-30 parts of absolute ethyl alcohol, 1-5 parts of anhydrous acetic acid, 5-15 parts of distilled water, 1-3 parts of thickening agent, 2-5 parts of wetting agent, 20-30 parts of energy storage luminescent material, one ball mill, one wet magnetic separator, one plunger pump, one filter press, one gypsum mold, one hydraulic press, one vacuum pugging machine, one comb kiln and one electronic metering scale.
In a preferred embodiment, the water-based inorganic nano-polymer luminous ceramic material and the preparation method thereof comprise the following steps:
s1, taking one electronic weighing scale, weighing 60-70 parts of ethyl orthosilicate, 15-25 parts of silicon dioxide dispersion liquid, 10-30 parts of absolute ethyl alcohol, 1-5 parts of absolute acetic acid, 5-15 parts of distilled water, 1-3 parts of thickening agent, 2-5 parts of wetting agent and 20-30 parts of energy storage luminescent material;
s2, weighing the raw materials in the step S1 to obtain required weight, mixing and loading the raw materials into a charging barrel of a ball mill, and then adding water to open a switch of the ball mill for ball milling;
s3, in step S2, after the ball milling is finished, coarse particles and tail sand are removed by a sieve after the ground paste after the ball milling is detected to reach the fineness requirement;
s4, screening in the step S3, taking the mixture out of the wet magnetic separator, and removing iron impurities by using the wet magnetic separator;
s5, pumping the sieved and de-ironed slurry into a filter press by a plunger pump, and squeezing out excessive water by the filter press;
s6, taking the vacuum pug mill, and performing vacuum treatment on the mud segment again in the vacuum pug mill;
s7, using a gypsum board manufacturing die, after the die is manufactured, placing the refined pug into an extrusion model, and extruding blanks in various shapes under the action of a hydraulic press;
s8, putting the ligand prepared in the step S7 into the comb kiln, and starting to fire the ceramic material;
s9, after the firing process is finished, the grade of the fired or decorated product is judged by sorting in a sorting workshop;
and S10, designing a proper carton size and a corresponding partition plate according to the requirements of customers, so that the products are correspondingly protected in the transportation process and then packaged and stored.
In a preferred embodiment, in the step S2, the ball milling is assisted by the alumina ball, and the glaze-containing part is assisted by the high alumina ball.
In a preferred embodiment, in the ball milling process in step S2, a part of the ingredients is generally placed and ball milled for a period of time, and then the rest of the ingredients are added and ball milled together, and the total ball milling time varies from tens of hours to thirty hours.
In a preferred embodiment, in the step S3, the size of the screen cloth is that the blank is generally between 160 and 180 meshes; the glaze-containing part is generally between 200 and 250 meshes.
In a preferred embodiment, in step S4, after the iron removal is finished, the sieving and iron removal operations are performed again for a total of two times.
In a preferred embodiment, in the step S6, the hardness and the vacuum degree of the mud segment are both made to meet the requirements required by the production process by refining, so that the plasticity and the density of the mud segment are further improved, the composition is more uniform, and the drying strength of the formed blank is increased.
In a preferred embodiment, in step S8, the temperature of the comb kiln can be adjusted, the kiln can be turned off every day, and the residual temperature in the kiln can be fully used in the product drying process, so that the method is energy-saving and environment-friendly, and consumes relatively little energy.
In summary, due to the adoption of the technical scheme, the invention has the beneficial effects that:
1. according to the invention, the luminous ceramic material produced by adopting the improved formula has the advantages of long service life, no toxicity, no harm, no radioactive elements, long luminous time, super-strong hydrophobicity, self-cleaning, no adhesion, corrosion resistance, high temperature resistance, weather resistance, no aging, freezing resistance and the like, the decoration effect is effectively improved, and the service life of the material is prolonged; the invention is mainly applied to luminous signs in buildings, decorations, advertisements, traffic signs, artificial landscapes, markets and special occasions, and can also be used for low-degree emergency lighting.
2. In the invention, the processes of sieving and refining are added in the preparation process, impurities in the preparation process are screened, and the purity of the ceramic material is improved, so that the product precision of the ceramic material is improved.
Detailed Description
In order to make the objects, technical solutions and advantages of the embodiments of the present invention clearer, the technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are some embodiments of the present invention, but not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The first embodiment is as follows:
the water-based inorganic nano-polymer luminous ceramic material and the preparation method thereof need to use: 60-70 parts of ethyl orthosilicate, 15-25 parts of silicon dioxide dispersion liquid, 10-30 parts of absolute ethyl alcohol, 1-5 parts of anhydrous acetic acid, 5-15 parts of distilled water, 1-3 parts of thickening agent, 2-5 parts of wetting agent, 20-30 parts of energy storage luminescent material, one ball mill, one wet magnetic separator, one plunger pump, one filter press, one gypsum mold, one hydraulic press, one vacuum pugging machine, one comb kiln and one electronic metering scale. The water-based inorganic nano-polymer luminous ceramic material and the preparation method thereof comprise the following steps:
s1, taking one electronic weighing scale, weighing 60-70 parts of ethyl orthosilicate, 15-25 parts of silicon dioxide dispersion liquid, 10-30 parts of absolute ethyl alcohol, 1-5 parts of anhydrous acetic acid, 5-15 parts of distilled water, 1-3 parts of thickening agent, 2-5 parts of wetting agent and 20 parts of energy storage luminescent material;
s2, weighing the raw materials in the step S1 by required weight, mixing and loading the raw materials into a charging barrel of a ball mill, then adding water to open a switch of the ball mill for ball milling, carrying out auxiliary ball milling on aluminum ball stones during ball milling in the step S2, carrying out auxiliary ball milling on glaze-containing parts by using high-alumina ball stones, generally placing part of ingredients for ball milling for a period of time in the ball milling process in the step S2, then adding the rest ingredients for ball milling together, wherein the total ball milling time is different from more than ten hours to more than thirty hours according to the difference of the ingredients;
s3, in step S2, after the ball milling is finished, coarse particles and tail sand are removed by a sieve after the slurry after the ball milling is detected to meet the fineness requirement, and in step S3, the specification of the sieve cloth is that the blank is generally between 160 and 180 meshes; the glaze-containing part is generally between 200 and 250 meshes;
s4, taking the wet magnetic separator after the sieving in the step S3, removing iron impurities by using the wet magnetic separator, and carrying out sieving and iron removal again after the iron removal in the step S4 for twice in total;
s5, pumping the sieved and de-ironed slurry into a filter press by a plunger pump, and squeezing out excessive water by the filter press;
s6, taking a vacuum pug mill, performing vacuum treatment on the mud segment again by using the vacuum pug mill, and refining in the step S6 to ensure that the hardness and the vacuum degree of the mud segment meet the requirements required by the production process, so that the plasticity and the density of the mud segment are further improved, the composition is more uniform, and the drying strength of the formed blank body is increased;
s7, using a gypsum board manufacturing die, after the die is manufactured, placing the refined pug into an extrusion model, and extruding blanks in various shapes under the action of a hydraulic press;
s8, placing the ligand manufactured in the step S7 into a comb-type kiln, and starting to fire ceramic materials, wherein in the step S8, the temperature of the comb-type kiln can be adjusted, the kiln can be closed every day, and the residual temperature in the kiln can be fully used in the product drying link, so that the energy is saved, the environment is protected, and the relative energy consumption is low;
s9, after the firing process is finished, the grade of the fired or decorated product is judged by sorting in a sorting workshop;
and S10, designing a proper carton size and a corresponding partition plate according to the requirements of customers, so that the products are correspondingly protected in the transportation process and then packaged and stored.
Example two:
the water-based inorganic nano-polymer luminous ceramic material and the preparation method thereof need to use: 60-70 parts of ethyl orthosilicate, 15-25 parts of silicon dioxide dispersion liquid, 10-30 parts of absolute ethyl alcohol, 1-5 parts of anhydrous acetic acid, 5-15 parts of distilled water, 1-3 parts of thickening agent, 2-5 parts of wetting agent, 20-30 parts of energy storage luminescent material, one ball mill, one wet magnetic separator, one plunger pump, one filter press, one gypsum mold, one hydraulic press, one vacuum pugging machine, one comb kiln and one electronic metering scale. The water-based inorganic nano-polymer luminous ceramic material and the preparation method thereof comprise the following steps:
s1, taking one electronic weighing scale, weighing 60-70 parts of ethyl orthosilicate, 15-25 parts of silicon dioxide dispersion liquid, 10-30 parts of absolute ethyl alcohol, 1-5 parts of anhydrous acetic acid, 5-15 parts of distilled water, 1-3 parts of thickening agent, 2-5 parts of wetting agent and 25 parts of energy storage luminescent material;
s2, weighing the raw materials in the step S1 by required weight, mixing and loading the raw materials into a charging barrel of a ball mill, then adding water to open a switch of the ball mill for ball milling, carrying out auxiliary ball milling on aluminum ball stones during ball milling in the step S2, carrying out auxiliary ball milling on glaze-containing parts by using high-alumina ball stones, generally placing part of ingredients for ball milling for a period of time in the ball milling process in the step S2, then adding the rest ingredients for ball milling together, wherein the total ball milling time is different from more than ten hours to more than thirty hours according to the difference of the ingredients;
s3, in step S2, after the ball milling is finished, coarse particles and tail sand are removed by a sieve after the slurry after the ball milling is detected to meet the fineness requirement, and in step S3, the specification of the sieve cloth is that the blank is generally between 160 and 180 meshes; the glaze-containing part is generally between 200 and 250 meshes;
s4, taking the wet magnetic separator after the sieving in the step S3, removing iron impurities by using the wet magnetic separator, and carrying out sieving and iron removal again after the iron removal in the step S4 for twice in total;
s5, pumping the sieved and de-ironed slurry into a filter press by a plunger pump, and squeezing out excessive water by the filter press;
s6, taking a vacuum pug mill, performing vacuum treatment on the mud segment again by using the vacuum pug mill, and refining in the step S6 to ensure that the hardness and the vacuum degree of the mud segment meet the requirements required by the production process, so that the plasticity and the density of the mud segment are further improved, the composition is more uniform, and the drying strength of the formed blank body is increased;
s7, using a gypsum board manufacturing die, after the die is manufactured, placing the refined pug into an extrusion model, and extruding blanks in various shapes under the action of a hydraulic press;
s8, placing the ligand manufactured in the step S7 into a comb-type kiln, and starting to fire ceramic materials, wherein in the step S8, the temperature of the comb-type kiln can be adjusted, the kiln can be closed every day, and the residual temperature in the kiln can be fully used in the product drying link, so that the energy is saved, the environment is protected, and the relative energy consumption is low;
s9, after the firing process is finished, the grade of the fired or decorated product is judged by sorting in a sorting workshop;
and S10, designing a proper carton size and a corresponding partition plate according to the requirements of customers, so that the products are correspondingly protected in the transportation process and then packaged and stored.
Example three:
the water-based inorganic nano-polymer luminous ceramic material and the preparation method thereof need to use: 60-70 parts of ethyl orthosilicate, 15-25 parts of silicon dioxide dispersion liquid, 10-30 parts of absolute ethyl alcohol, 1-5 parts of anhydrous acetic acid, 5-15 parts of distilled water, 1-3 parts of thickening agent, 2-5 parts of wetting agent, 20-30 parts of energy storage luminescent material, one ball mill, one wet magnetic separator, one plunger pump, one filter press, one gypsum mold, one hydraulic press, one vacuum pugging machine, one comb kiln and one electronic metering scale. The water-based inorganic nano-polymer luminous ceramic material and the preparation method thereof comprise the following steps:
s1, taking one electronic weighing scale, weighing 60-70 parts of ethyl orthosilicate, 15-25 parts of silicon dioxide dispersion liquid, 10-30 parts of absolute ethyl alcohol, 1-5 parts of absolute acetic acid, 5-15 parts of distilled water, 1-3 parts of thickening agent, 2-5 parts of wetting agent and 30 parts of energy storage luminescent material;
s2, weighing the raw materials in the step S1 by required weight, mixing and loading the raw materials into a charging barrel of a ball mill, then adding water to open a switch of the ball mill for ball milling, carrying out auxiliary ball milling on aluminum ball stones during ball milling in the step S2, carrying out auxiliary ball milling on glaze-containing parts by using high-alumina ball stones, generally placing part of ingredients for ball milling for a period of time in the ball milling process in the step S2, then adding the rest ingredients for ball milling together, wherein the total ball milling time is different from more than ten hours to more than thirty hours according to the difference of the ingredients;
s3, in step S2, after the ball milling is finished, coarse particles and tail sand are removed by a sieve after the slurry after the ball milling is detected to meet the fineness requirement, and in step S3, the specification of the sieve cloth is that the blank is generally between 160 and 180 meshes; the glaze-containing part is generally between 200 and 250 meshes;
s4, taking the wet magnetic separator after the sieving in the step S3, removing iron impurities by using the wet magnetic separator, and carrying out sieving and iron removal again after the iron removal in the step S4 for twice in total;
s5, pumping the sieved and de-ironed slurry into a filter press by a plunger pump, and squeezing out excessive water by the filter press;
s6, taking a vacuum pug mill, performing vacuum treatment on the mud segment again by using the vacuum pug mill, and refining in the step S6 to ensure that the hardness and the vacuum degree of the mud segment meet the requirements required by the production process, so that the plasticity and the density of the mud segment are further improved, the composition is more uniform, and the drying strength of the formed blank body is increased;
s7, using a gypsum board manufacturing die, after the die is manufactured, placing the refined pug into an extrusion model, and extruding blanks in various shapes under the action of a hydraulic press;
s8, placing the ligand manufactured in the step S7 into a comb-type kiln, and starting to fire ceramic materials, wherein in the step S8, the temperature of the comb-type kiln can be adjusted, the kiln can be closed every day, and the residual temperature in the kiln can be fully used in the product drying link, so that the energy is saved, the environment is protected, and the relative energy consumption is low;
s9, after the firing process is finished, the grade of the fired or decorated product is judged by sorting in a sorting workshop;
and S10, designing a proper carton size and a corresponding partition plate according to the requirements of customers, so that the products are correspondingly protected in the transportation process and then packaged and stored.
It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Moreover, the terms "comprises," "comprising," or 014, and any other variations thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus. Without further limitation, an element defined by the phrase "comprising an … …" does not exclude the presence of other identical elements in a process, method, article, or apparatus that comprises the element.
The above examples are only intended to illustrate the technical solution of the present invention, but not to limit it; although the present invention has been described in detail with reference to the foregoing embodiments, it will be understood by those of ordinary skill in the art that: the technical solutions described in the foregoing embodiments may still be modified, or some technical features may be equivalently replaced; and such modifications or substitutions do not depart from the spirit and scope of the corresponding technical solutions of the embodiments of the present invention.
Claims (8)
1. A water-based inorganic nanometer high-molecular luminous ceramic material and a preparation method thereof are characterized in that: the water-based inorganic nano-polymer luminous ceramic material and the preparation method thereof need to use the following components in preparation: 60-70 parts of ethyl orthosilicate, 15-25 parts of silicon dioxide dispersion liquid, 10-30 parts of absolute ethyl alcohol, 1-5 parts of anhydrous acetic acid, 5-15 parts of distilled water, 1-3 parts of thickening agent, 2-5 parts of wetting agent, 20-30 parts of energy storage luminescent material, one ball mill, one wet magnetic separator, one plunger pump, one filter press, one gypsum mold, one hydraulic press, one vacuum pugging machine, one comb kiln and one electronic metering scale.
2. The aqueous inorganic nano-polymer luminous ceramic material and the preparation method thereof as claimed in claim 1, wherein the preparation method comprises the following steps: the water-based inorganic nano-polymer luminous ceramic material and the preparation method thereof comprise the following steps:
s1, taking one electronic weighing scale, weighing 60-70 parts of ethyl orthosilicate, 15-25 parts of silicon dioxide dispersion liquid, 10-30 parts of absolute ethyl alcohol, 1-5 parts of absolute acetic acid, 5-15 parts of distilled water, 1-3 parts of thickening agent, 2-5 parts of wetting agent and 20-30 parts of energy storage luminescent material;
s2, weighing the raw materials in the step S1 to obtain required weight, mixing and loading the raw materials into a charging barrel of a ball mill, and then adding water to open a switch of the ball mill for ball milling;
s3, in step S2, after the ball milling is finished, coarse particles and tail sand are removed by a sieve after the ground paste after the ball milling is detected to reach the fineness requirement;
s4, screening in the step S3, taking the mixture out of the wet magnetic separator, and removing iron impurities by using the wet magnetic separator;
s5, pumping the sieved and de-ironed slurry into a filter press by a plunger pump, and squeezing out excessive water by the filter press;
s6, taking the vacuum pug mill, and performing vacuum treatment on the mud segment again in the vacuum pug mill;
s7, using a gypsum board manufacturing die, after the die is manufactured, placing the refined pug into an extrusion model, and extruding blanks in various shapes under the action of a hydraulic press;
s8, putting the ligand prepared in the step S7 into the comb kiln, and starting to fire the ceramic material;
s9, after the firing process is finished, the grade of the fired or decorated product is judged by sorting in a sorting workshop;
and S10, designing a proper carton size and a corresponding partition plate according to the requirements of customers, so that the products are correspondingly protected in the transportation process and then packaged and stored.
3. The aqueous inorganic nano-polymer luminous ceramic material and the preparation method thereof as claimed in claim 1, wherein the preparation method comprises the following steps: and in the step S2, auxiliary ball milling is carried out on the aluminum ball stone during ball milling, and auxiliary ball milling is carried out on the part containing the glaze by using the high-alumina ball stone.
4. The aqueous inorganic nano-polymer luminous ceramic material and the preparation method thereof as claimed in claim 1, wherein the preparation method comprises the following steps: in the ball milling process in the step S2, part of the ingredients are generally placed first to be ball milled for a period of time, and then the rest ingredients are added to be ball milled together, and the total ball milling time is different from dozens of hours to more than thirty hours according to the difference of the ingredients.
5. The aqueous inorganic nano-polymer luminous ceramic material and the preparation method thereof as claimed in claim 1, wherein the preparation method comprises the following steps: in the step S3, the size of the screen cloth is that the blank is generally between 160 and 180 meshes; the glaze-containing part is generally between 200 and 250 meshes.
6. The aqueous inorganic nano-polymer luminous ceramic material and the preparation method thereof as claimed in claim 1, wherein the preparation method comprises the following steps: in step S4, after the iron removal is finished, the sieving and iron removal operations are performed again for two times in total.
7. The aqueous inorganic nano-polymer luminous ceramic material and the preparation method thereof as claimed in claim 1, wherein the preparation method comprises the following steps: in the step S6, the hardness and the vacuum degree of the mud segment are both made to meet the requirements required by the production process by refining, so that the plasticity and the density of the mud segment are further improved, the composition is more uniform, and the drying strength of the formed blank body is increased.
8. The aqueous inorganic nano-polymer luminous ceramic material and the preparation method thereof as claimed in claim 1, wherein the preparation method comprises the following steps: in the step S8, the temperature of the comb kiln can be adjusted, the kiln can be closed every day, the residual temperature in the kiln can be fully used in the product drying link, and the comb kiln is energy-saving, environment-friendly and relatively low in energy consumption.
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| CN114279223A (en) * | 2021-11-25 | 2022-04-05 | 江苏华航新材料科技集团有限公司 | Ceramic hanging piece for producing cement preheater inner barrel and production process thereof |
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| 陈照峰: "《无机非金属材料学 第2版》", 29 February 2016, 西北工业大学出版社 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112979276A (en) * | 2021-03-26 | 2021-06-18 | 福建省德化新吉利工艺有限公司 | High-hardness domestic ceramic and production process thereof |
| CN114279223A (en) * | 2021-11-25 | 2022-04-05 | 江苏华航新材料科技集团有限公司 | Ceramic hanging piece for producing cement preheater inner barrel and production process thereof |
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