CN112251087A - Glazing oil and preparation method thereof - Google Patents
Glazing oil and preparation method thereof Download PDFInfo
- Publication number
- CN112251087A CN112251087A CN202011243996.0A CN202011243996A CN112251087A CN 112251087 A CN112251087 A CN 112251087A CN 202011243996 A CN202011243996 A CN 202011243996A CN 112251087 A CN112251087 A CN 112251087A
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- China
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- parts
- portions
- reaction kettle
- glazing
- oil
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D125/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring; Coating compositions based on derivatives of such polymers
- C09D125/02—Homopolymers or copolymers of hydrocarbons
- C09D125/04—Homopolymers or copolymers of styrene
- C09D125/08—Copolymers of styrene
- C09D125/14—Copolymers of styrene with unsaturated esters
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Lubricants (AREA)
Abstract
The application discloses glazing oil and a preparation method thereof, wherein raw materials comprise toluene, dimethylbenzene, styrene, methyl methacrylate, acrylic acid, butyl acrylate, an initiator and 206 resin. The lustering oil has high luster, good durability and excellent lubricating and color developing performance.
Description
Technical Field
The invention relates to the technical field of laminating adhesives, in particular to glazing oil and a preparation method thereof.
Background
Glazing is an important means of finishing after printing, and is a process or technology which mainly forms a thin and uniform transparent bright layer on the surface of a printed matter by coating (or spraying and printing) a layer of transparent coating on the surface of the printed matter and performing leveling, drying, calendering and curing to enhance the surface smoothness of a carrier and protect the finishing function of printed pictures and texts. The glazing can not only enhance the surface brightness and protect the printing graphics, but also does not influence the recycling of the paper. Therefore, the method is widely applied to surface processing of printed products such as packaging cartons, books, picture books, posters and the like. The existing glazing oil has poor color development performance on color and influences the appearance.
Disclosure of Invention
The invention aims to provide glazing oil and a preparation method thereof, which are used for overcoming the defects in the prior art.
In order to achieve the purpose, the invention provides the following technical scheme:
the embodiment of the application discloses glazing oil, which consists of the following raw materials in parts by weight: 670 portions of toluene 675, 670 portions of xylene 675, 955 portions of styrene 960, 90 to 100 portions of methyl methacrylate, 50 to 70 portions of acrylic acid, 100 portions of butyl acrylate 110 portions, 25 to 30 portions of initiator and 10 to 15 portions of 206 resin.
Preferably, in the gloss oil and the preparation method thereof, the gloss oil is prepared from the following raw materials in parts by weight: 671.1 parts of toluene, 671.1 parts of xylene, 958 parts of styrene, 95 parts of methyl methacrylate, 60 parts of acrylic acid, 105 parts of butyl acrylate, 27.6 parts of an initiator and 12.2 parts of 206 resin.
Preferably, in the gloss oil and the preparation method thereof, the initiator is benzoyl peroxide.
A preparation method of glazing oil comprises the following specific steps: respectively pumping the metered methylbenzene and dimethylbenzene into a reaction kettle by using a pneumatic diaphragm pump, pumping the metered styrene, methyl methacrylate, acrylic acid, butyl acrylate, benzoyl peroxide and 206 resin into a dripping tank by using the pneumatic diaphragm pump, uniformly dripping the materials in the dripping tank into the reaction kettle within 3-4h, preserving heat after dripping is finished, and cooling to room temperature after heat preservation to obtain the glazing oil.
Preferably, in the above method for preparing gloss oil, when the dropping tank drops the materials into the reaction kettle, the temperature of the reaction kettle is controlled at 100-150 ℃.
Preferably, in the above method for preparing gloss oil, the holding time is 3 h.
Preferably, in the above method for preparing gloss oil, the cooling is performed by filling circulating water into the reaction kettle.
Compared with the prior art, the invention has the advantages that: the glazing oil has high glossiness, good durability and excellent lubricating and color developing performance.
Detailed Description
The invention is further illustrated by the following examples: the invention will be better understood from the following examples. However, those skilled in the art will readily appreciate that the specific material ratios, process conditions and results thereof described in the examples are illustrative only and should not be taken as limiting the invention as detailed in the claims.
671.1 parts of toluene and 671.1 parts of xylene are respectively pumped into a reaction kettle by a pneumatic diaphragm pump, 958 parts of styrene, 95 parts of methyl methacrylate, 60 parts of acrylic acid, 105 parts of butyl acrylate, 27.6 parts of benzoyl peroxide and 12.2 parts of 206 resin which are metered are respectively pumped into a dropping tank by the pneumatic diaphragm pump, materials in the dropping tank are evenly dropped into the reaction kettle within 3 to 4 hours to start polymerization exothermic reaction, the reaction temperature is controlled at 150 ℃ and controlled by a circulating water cooling mode, the temperature is kept for 3 hours after the dropping is finished, the mixture is cooled to room temperature after the temperature is kept, a small amount of white viscous transparent liquid is taken from a discharge port of the reaction kettle, the viscosity is detected, the required material can be discharged, and the raw materials in the corresponding proportion are added into the reaction kettle according to the detection and analysis results to adjust until the requirements are met, the polishing oil can be obtained.
In conclusion, the glazing oil has high glossiness, good durability and excellent lubricating and color developing performance.
It should be noted that, in order to avoid obscuring the present invention with unnecessary details, only the structures and/or processing steps closely related to the scheme according to the present invention are shown in the embodiments, and other details not closely related to the present invention are omitted.
Finally, it should also be noted that the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
Claims (7)
1. The glazing oil is characterized in that: the glazing oil is prepared from the following raw materials in parts by weight: 670 portions of toluene 675, 670 portions of xylene 675, 955 portions of styrene 960, 90 to 100 portions of methyl methacrylate, 50 to 70 portions of acrylic acid, 100 portions of butyl acrylate 110 portions, 25 to 30 portions of initiator and 10 to 15 portions of 206 resin.
2. The gloss oil according to claim 1, wherein: the glazing oil is prepared from the following raw materials in parts by weight: 671.1 parts of toluene, 671.1 parts of xylene, 958 parts of styrene, 95 parts of methyl methacrylate, 60 parts of acrylic acid, 105 parts of butyl acrylate, 27.6 parts of an initiator and 12.2 parts of 206 resin.
3. The gloss oil according to claim 1, wherein: the initiator is benzoyl peroxide.
4. A method of preparing a varnish according to any one of claims 1 to 3, wherein: the preparation method comprises the following specific steps: respectively pumping the metered methylbenzene and dimethylbenzene into a reaction kettle by using a pneumatic diaphragm pump, pumping the metered styrene, methyl methacrylate, acrylic acid, butyl acrylate, benzoyl peroxide and 206 resin into a dripping tank by using the pneumatic diaphragm pump, uniformly dripping the materials in the dripping tank into the reaction kettle within 3-4h, preserving heat after dripping is finished, and cooling to room temperature after heat preservation to obtain the glazing oil.
5. The method for preparing gloss oil according to claim 4, wherein: when the dropwise adding tank is used for dropwise adding materials into the reaction kettle, the temperature of the reaction kettle is controlled to be 100-150 ℃.
6. The method for preparing gloss oil according to claim 4, wherein: the heat preservation time is 3 h.
7. The method for preparing gloss oil according to claim 4, wherein: the cooling mode is a mode of filling circulating water into the reaction kettle.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011243996.0A CN112251087A (en) | 2020-11-09 | 2020-11-09 | Glazing oil and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011243996.0A CN112251087A (en) | 2020-11-09 | 2020-11-09 | Glazing oil and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN112251087A true CN112251087A (en) | 2021-01-22 |
Family
ID=74266745
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202011243996.0A Pending CN112251087A (en) | 2020-11-09 | 2020-11-09 | Glazing oil and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN112251087A (en) |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0457856A (en) * | 1990-06-27 | 1992-02-25 | Mitsubishi Rayon Co Ltd | Coating composition for glazing paper |
| CN101974275A (en) * | 2010-10-29 | 2011-02-16 | 苏州凯康化工科技有限公司 | Alcohol-soluble vacuum-forming oil and preparation method thereof |
| CN102219875A (en) * | 2010-01-22 | 2011-10-19 | 北京高盟新材料股份有限公司 | Alcohol-soluble resin composition, alcohol-soluble glazing agent and preparation method thereof |
| CN109485783A (en) * | 2018-10-23 | 2019-03-19 | 杭州方周科技有限公司 | A kind of high gloss gloss oil is with water soluble acrylic resin and preparation method thereof |
| CN111138595A (en) * | 2019-12-25 | 2020-05-12 | 广东银洋环保新材料有限公司 | Water-based glazing oil emulsion with heat resistance, preparation method thereof and water-based glazing oil |
-
2020
- 2020-11-09 CN CN202011243996.0A patent/CN112251087A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0457856A (en) * | 1990-06-27 | 1992-02-25 | Mitsubishi Rayon Co Ltd | Coating composition for glazing paper |
| CN102219875A (en) * | 2010-01-22 | 2011-10-19 | 北京高盟新材料股份有限公司 | Alcohol-soluble resin composition, alcohol-soluble glazing agent and preparation method thereof |
| CN101974275A (en) * | 2010-10-29 | 2011-02-16 | 苏州凯康化工科技有限公司 | Alcohol-soluble vacuum-forming oil and preparation method thereof |
| CN109485783A (en) * | 2018-10-23 | 2019-03-19 | 杭州方周科技有限公司 | A kind of high gloss gloss oil is with water soluble acrylic resin and preparation method thereof |
| CN111138595A (en) * | 2019-12-25 | 2020-05-12 | 广东银洋环保新材料有限公司 | Water-based glazing oil emulsion with heat resistance, preparation method thereof and water-based glazing oil |
Non-Patent Citations (3)
| Title |
|---|
| HF0546339: "206树脂", 《百度文库》 * |
| 周玉松等: "《现代胶印机的使用与调节》", 30 April 2009, 中国轻工业出版社 * |
| 李高宁等: "醇溶型热塑性哑光涂料的研制", 《精细石油化工》 * |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20210122 |
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| RJ01 | Rejection of invention patent application after publication |