CN112244269A - A heat irreversible meat jelly prepared from curdlan and gellan gum and its preparation method - Google Patents
A heat irreversible meat jelly prepared from curdlan and gellan gum and its preparation method Download PDFInfo
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- CN112244269A CN112244269A CN202011055420.1A CN202011055420A CN112244269A CN 112244269 A CN112244269 A CN 112244269A CN 202011055420 A CN202011055420 A CN 202011055420A CN 112244269 A CN112244269 A CN 112244269A
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- Prior art keywords
- gellan gum
- curdlan
- meat
- fermentation
- heat irreversible
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- 229920002148 Gellan gum Polymers 0.000 title claims abstract description 64
- 239000000216 gellan gum Substances 0.000 title claims abstract description 64
- 235000010492 gellan gum Nutrition 0.000 title claims abstract description 64
- 235000013372 meat Nutrition 0.000 title claims abstract description 43
- 239000001879 Curdlan Substances 0.000 title claims abstract description 39
- 229920002558 Curdlan Polymers 0.000 title claims abstract description 39
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 title claims abstract description 39
- 235000019316 curdlan Nutrition 0.000 title claims abstract description 39
- 229940078035 curdlan Drugs 0.000 title claims abstract description 39
- 235000015110 jellies Nutrition 0.000 title claims abstract description 28
- 239000008274 jelly Substances 0.000 title claims abstract description 28
- 230000002427 irreversible effect Effects 0.000 title claims abstract description 19
- 238000002360 preparation method Methods 0.000 title abstract description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 22
- 238000003756 stirring Methods 0.000 claims abstract description 19
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 claims abstract description 16
- 239000001110 calcium chloride Substances 0.000 claims abstract description 16
- 229910001628 calcium chloride Inorganic materials 0.000 claims abstract description 16
- 235000013882 gravy Nutrition 0.000 claims abstract description 15
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims abstract description 14
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 claims abstract description 12
- 239000000920 calcium hydroxide Substances 0.000 claims abstract description 12
- 229910001861 calcium hydroxide Inorganic materials 0.000 claims abstract description 12
- 230000001954 sterilising effect Effects 0.000 claims abstract description 9
- 239000000243 solution Substances 0.000 claims abstract description 7
- 239000002253 acid Substances 0.000 claims abstract description 5
- 239000007864 aqueous solution Substances 0.000 claims abstract description 5
- 235000013622 meat product Nutrition 0.000 claims abstract description 5
- 230000007935 neutral effect Effects 0.000 claims abstract description 5
- 239000002245 particle Substances 0.000 claims abstract description 5
- 238000007872 degassing Methods 0.000 claims abstract description 3
- 238000000855 fermentation Methods 0.000 claims description 41
- 230000004151 fermentation Effects 0.000 claims description 41
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 33
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 24
- 239000007788 liquid Substances 0.000 claims description 20
- 235000002639 sodium chloride Nutrition 0.000 claims description 20
- 238000000034 method Methods 0.000 claims description 18
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 16
- -1 alkaline earth metal salt Chemical class 0.000 claims description 16
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 claims description 14
- 239000000835 fiber Substances 0.000 claims description 12
- 238000000926 separation method Methods 0.000 claims description 12
- 235000015165 citric acid Nutrition 0.000 claims description 11
- 238000010438 heat treatment Methods 0.000 claims description 10
- 239000000047 product Substances 0.000 claims description 10
- 239000000463 material Substances 0.000 claims description 9
- 239000001888 Peptone Substances 0.000 claims description 8
- 108010080698 Peptones Proteins 0.000 claims description 8
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 8
- 229930006000 Sucrose Natural products 0.000 claims description 8
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims description 8
- 229910052783 alkali metal Inorganic materials 0.000 claims description 8
- 229910052784 alkaline earth metal Inorganic materials 0.000 claims description 8
- 229910000019 calcium carbonate Inorganic materials 0.000 claims description 8
- 239000012153 distilled water Substances 0.000 claims description 8
- 239000001963 growth medium Substances 0.000 claims description 8
- 239000002609 medium Substances 0.000 claims description 8
- 235000019319 peptone Nutrition 0.000 claims description 8
- 239000000843 powder Substances 0.000 claims description 8
- 239000005720 sucrose Substances 0.000 claims description 8
- 229910052943 magnesium sulfate Inorganic materials 0.000 claims description 7
- 235000019341 magnesium sulphate Nutrition 0.000 claims description 7
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims description 6
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 claims description 6
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 claims description 6
- OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Chemical compound [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 claims description 6
- 239000012043 crude product Substances 0.000 claims description 6
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 claims description 6
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 claims description 4
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 claims description 4
- 229910052921 ammonium sulfate Inorganic materials 0.000 claims description 4
- 235000011130 ammonium sulphate Nutrition 0.000 claims description 4
- 230000001580 bacterial effect Effects 0.000 claims description 4
- 229940041514 candida albicans extract Drugs 0.000 claims description 4
- 238000001035 drying Methods 0.000 claims description 4
- 230000003311 flocculating effect Effects 0.000 claims description 4
- ZXEKIIBDNHEJCQ-UHFFFAOYSA-N isobutanol Chemical compound CC(C)CO ZXEKIIBDNHEJCQ-UHFFFAOYSA-N 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 4
- 229910000402 monopotassium phosphate Inorganic materials 0.000 claims description 4
- 235000019796 monopotassium phosphate Nutrition 0.000 claims description 4
- PJNZPQUBCPKICU-UHFFFAOYSA-N phosphoric acid;potassium Chemical compound [K].OP(O)(O)=O PJNZPQUBCPKICU-UHFFFAOYSA-N 0.000 claims description 4
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 claims description 4
- 238000005086 pumping Methods 0.000 claims description 4
- 238000012216 screening Methods 0.000 claims description 4
- 239000011780 sodium chloride Substances 0.000 claims description 4
- 238000004659 sterilization and disinfection Methods 0.000 claims description 4
- 238000005406 washing Methods 0.000 claims description 4
- 239000012138 yeast extract Substances 0.000 claims description 4
- 239000002054 inoculum Substances 0.000 claims description 3
- 239000004310 lactic acid Substances 0.000 claims description 3
- 235000014655 lactic acid Nutrition 0.000 claims description 3
- 229910001629 magnesium chloride Inorganic materials 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 claims description 3
- 239000001103 potassium chloride Substances 0.000 claims description 3
- 235000011164 potassium chloride Nutrition 0.000 claims description 3
- OTYBMLCTZGSZBG-UHFFFAOYSA-L potassium sulfate Chemical compound [K+].[K+].[O-]S([O-])(=O)=O OTYBMLCTZGSZBG-UHFFFAOYSA-L 0.000 claims description 3
- 229910052939 potassium sulfate Inorganic materials 0.000 claims description 3
- 235000011151 potassium sulphates Nutrition 0.000 claims description 3
- BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 claims description 2
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 2
- BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 claims description 2
- 239000001630 malic acid Substances 0.000 claims description 2
- 235000011090 malic acid Nutrition 0.000 claims description 2
- 229910052938 sodium sulfate Inorganic materials 0.000 claims description 2
- 235000011152 sodium sulphate Nutrition 0.000 claims description 2
- 238000005303 weighing Methods 0.000 claims description 2
- 238000002844 melting Methods 0.000 abstract description 7
- 230000008018 melting Effects 0.000 abstract description 7
- 239000000499 gel Substances 0.000 description 24
- 239000006185 dispersion Substances 0.000 description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 239000012670 alkaline solution Substances 0.000 description 2
- 229910001424 calcium ion Inorganic materials 0.000 description 2
- 150000001768 cations Chemical class 0.000 description 2
- 239000000084 colloidal system Substances 0.000 description 2
- 235000019659 mouth feeling Nutrition 0.000 description 2
- 238000004806 packaging method and process Methods 0.000 description 2
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 description 1
- 125000002252 acyl group Chemical group 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 239000001506 calcium phosphate Substances 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 235000013373 food additive Nutrition 0.000 description 1
- 239000002778 food additive Substances 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
- 238000011081 inoculation Methods 0.000 description 1
- 230000000813 microbial effect Effects 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 230000002441 reversible effect Effects 0.000 description 1
- 238000010008 shearing Methods 0.000 description 1
- 235000011121 sodium hydroxide Nutrition 0.000 description 1
- 239000001488 sodium phosphate Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 description 1
- 229940078499 tricalcium phosphate Drugs 0.000 description 1
- 229910000391 tricalcium phosphate Inorganic materials 0.000 description 1
- 235000019731 tricalcium phosphate Nutrition 0.000 description 1
- RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 description 1
- 229910000406 trisodium phosphate Inorganic materials 0.000 description 1
- 235000019801 trisodium phosphate Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/20—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents
- A23L29/269—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents of microbial origin, e.g. xanthan or dextran
- A23L29/272—Gellan
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L13/00—Meat products; Meat meal; Preparation or treatment thereof
- A23L13/06—Meat products; Meat meal; Preparation or treatment thereof with gravy or sauce
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L13/00—Meat products; Meat meal; Preparation or treatment thereof
- A23L13/40—Meat products; Meat meal; Preparation or treatment thereof containing additives
- A23L13/42—Additives other than enzymes or microorganisms in meat products or meat meals
- A23L13/422—Addition of natural plant hydrocolloids, e.g. gums of cellulose derivatives or of microbial fermentation gums
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L13/00—Meat products; Meat meal; Preparation or treatment thereof
- A23L13/40—Meat products; Meat meal; Preparation or treatment thereof containing additives
- A23L13/42—Additives other than enzymes or microorganisms in meat products or meat meals
- A23L13/432—Addition of inorganic compounds, e.g. minerals; oligo-elements
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L21/00—Marmalades, jams, jellies or the like; Products from apiculture; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/015—Inorganic compounds
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/20—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents
- A23L29/269—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents of microbial origin, e.g. xanthan or dextran
- A23L29/271—Curdlan; beta-1-3 glucan; Polysaccharides produced by agrobacterium or alcaligenes
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Dispersion Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Jellies, Jams, And Syrups (AREA)
Abstract
The invention relates to a heat irreversible meat jelly made of curdlan and gellan gum and a preparation method thereof, wherein (1) calcium hydroxide and calcium chloride are weighed and dissolved by a small amount of water; putting curdlan and gellan gum into the meat juice, and stirring to fully disperse the curdlan and gellan gum in the meat juice; after properly stirring, adding the prepared calcium hydroxide and calcium chloride aqueous solution, and stirring until the solution is fine and smooth and has no particles; (2) adding edible acid, and adjusting pH to neutral; (3) placing into a mould and degassing to make the whole gravy system have no bubbles; (4) pouring the prepared meat juice into the meat product, sterilizing and storing. The meat jelly is irreversible meat jelly, can not be melted when being heated, still has the mouth feel of melting in the mouth, and gives real mouth feel of the meat jelly.
Description
Technical Field
The invention relates to a heat irreversible meat jelly made of curdlan and gellan gum and a preparation method thereof, belonging to the field of food additives.
Background
Curdlan (also known as curdlan) is a fermented polysaccharide substance discovered in 1966 by microbial fermentation by doctor osaka, japan, then. This material is known as Curdlan (Curdlan) because of its ability to set upon heating (Curdle character). It has the following characteristics:
1. solubility: curdlan is soluble in aqueous alkaline solutions but not in water. Although the curdlan can not be dissolved in water, the curdlan is easily dispersed in cold water and is stirred at a high speed to form a more uniform water dispersion. The curdlan can be completely dissolved in alkaline solution systems with pH above 12 such as sodium hydroxide, trisodium phosphate, tricalcium phosphate, etc.
2. Gel property: the water dispersion of curdlan can form a thermally irreversible colloid after being heated to a temperature of 80 ℃ or higher. Colloids formed from curdlan can be classified into low-order gels and high-order gels according to their properties. Low gel (thermal reversibility) the aqueous dispersion of curdlan is heated to about 55-65 deg.C and then cooled to below about 40 deg.C to form the thermal reversible low gel. When the low gel is heated to about 60 deg.C, it returns to its original state. While when the low-position gel is heated to more than 80 ℃, the thermally irreversible high-position gel can be formed. After the low gel is stirred and crushed, the low gel and the high gel can still be formed by heating. Also, low gels at comparable gel concentrations have weaker gel strength than higher gels. High-order gel (thermal irreversibility) when the aqueous dispersion of curdlan is heated to above about 80 ℃, a strong thermally irreversible high-order gel is formed. The high gel cannot return to the original shape once it is crushed.
Gellan gum, in the presence of cations, forms a hard brittle gel when cooled after heating. The hardness is directly proportional to the gellan gum concentration and at lower divalent cation concentrations yields maximum gel low acyl gellan gum hardness. The gellan gum can form gel with the general dosage of 0.05 percent, and the dosage is usually 0.1 to 0.3 percent. The gel is rich in juice, has good flavor release property, and has mouth feel of melting in the mouth.
Disclosure of Invention
The meat jelly made of curdlan and gellan gum is a heat irreversible meat jelly which is not melted by heating, but still keeps the mouth feel of melting in the mouth, and gives people a real mouth feel of the meat jelly. The meat jelly prepared by the method is different from meat jelly prepared by independently using gellan gum, the damage rate of the meat jelly can be improved while the mouth feeling of melting in the mouth but not melting by heating is kept, the integrity of the meat jelly is kept in the processes of production, packaging and transportation, and the pressure resistance and the falling resistance are obviously improved.
The technical scheme of the invention is as follows:
a method for preparing heat irreversible meat jelly by curdlan and gellan gum comprises the following steps:
(1) weighing calcium hydroxide and calcium chloride, and dissolving with a small amount of water; putting curdlan and gellan gum into the meat juice, and stirring to fully disperse the curdlan and gellan gum in the meat juice; after properly stirring, adding the prepared calcium hydroxide and calcium chloride aqueous solution, and stirring until the solution is fine and smooth and has no particles;
(2) adding edible acid, and adjusting pH to neutral;
(3) placing into a mould and degassing to make the whole gravy system have no bubbles;
(4) pouring the prepared meat juice into the meat product, sterilizing and storing.
Wherein the addition amount of the calcium hydroxide is 0.01-0.2% of the mass of the whole gravy system, and the addition amount of the calcium chloride is 0.01-0.5% of the mass of the whole gravy system.
The addition amount of curdlan is 0.1-5% of the mass of the whole gravy system, and the addition amount of gellan gum is 0.05-0.5% of the mass of the whole gravy system.
The edible acid is citric acid, malic acid, and lactic acid.
The sterilization temperature is 85-150 ℃, and the sterilization time is 20-100 minutes.
Further, the gellan gum is prepared by the following preparation method:
(1) inoculating the mixed bacterial liquid into a culture medium of an incubator according to the inoculum size of 10% for culture under the conditions of 25-30 ℃, pH value of 7.3 and 24 hours to obtain a fermentation mother liquid, and then: transferring the fermentation medium into a fermentation tank for culture according to the volume ratio of 1: 10, wherein the culture conditions are that the temperature is 25-30 ℃, the pH value is 7.3, and the time is 72 hours, so as to obtain fermentation liquor;
(2) heating the fermentation liquor to 50-90 ℃, adding water-soluble alkaline earth metal salt accounting for 3-5% of the volume of the fermentation liquor into the fermentation liquor, adjusting the pH value to 8.5-10.5, flocculating the fermentation liquor, and then carrying out solid-liquid separation to obtain a partially deacylated gellan gum crude product; the alkaline earth metal salt comprises one or more of calcium chloride, magnesium chloride, calcium sulfate and magnesium sulfate;
(3) adding the crude gellan gum product into lower alcohol with the volume 0.4-0.6 times of the initial volume of the fermentation liquid, adjusting the pH value to 4.0-5.0, stirring and washing, and performing solid-liquid separation to obtain gellan gum fiber; the lower alcohol comprises one or more of ethanol, isopropanol, n-propanol, n-butanol and isobutanol;
(4) adding 75-95% alcohol by volume into the obtained gellan gum fibers until the materials are in a fiber separation state, pumping the materials into a dehydrator to remove alcohol and water, drying for 2-5 hours by a dryer, and crushing and screening to obtain gellan gum powder;
(5) uniformly mixing the obtained gellan gum powder with alkali metal salt accounting for 5-10% of the final finished product to obtain a gellan gum finished product; the alkali metal salt comprises one or more of potassium chloride, sodium chloride, potassium sulfate and sodium sulfate.
Wherein, the components of the culture medium of the incubator comprise: 25g of sucrose, 4.5g of peptone, 3.6g of ammonium sulfate, 2.8g of yeast extract, 3.3g of citric acid, 1.6g of calcium carbonate and 1000ml of distilled water. The components of the fermentation medium comprise: 37g of sucrose, 6.4g of peptone, 2.3g of potassium dihydrogen phosphate, 2.4g of citric acid, 1.8g of calcium carbonate, 0.6g of magnesium sulfate and 1000ml of distilled water.
The meat jelly prepared by the method is different from meat jelly prepared by independently using gellan gum, the damage rate of the meat jelly can be improved while the mouth feeling of melting in the mouth but not melting by heating is kept, the integrity of the meat jelly is kept in the processes of production, packaging and transportation, and the pressure resistance and the falling resistance are obviously improved.
The method related by the invention is also different from the conventional method that curdlan is subjected to high-speed shearing or acid-base neutralization, a method that calcium ions bridge gel is adopted, and the curdlan can react with the calcium ions to form heat irreversible gel with gellan gum at the same time, so that the curdlan and the gellan gum have good compatibility.
The meat jelly can be made into different shapes or colors for beautifying, and brings a new experience in the process of hot eating such as chafing dish.
Detailed Description
The invention will now be illustrated in further detail by the following examples.
Example 1
1. 0.02 g of calcium hydroxide and 0.1 g of calcium chloride are weighed out and dissolved in a small amount of water.
2. 2 g of curdlan and 0.3 g of gellan gum are put into 97.7 g of gravy, and are stirred to be fully dispersed in the gravy; adding the prepared calcium hydroxide and calcium chloride aqueous solution after proper stirring, and stirring until the solution is fine and smooth and has no particles (if the solution is not uniformly stirred and is easy to layer, a stirrer can be properly used for stirring to prevent layering).
3. Citric acid was added in an appropriate amount to adjust the pH to about neutral.
4. And (4) placing the meat into a mould to degas so that the whole meat juice system has no bubbles.
5. Pouring the prepared meat juice into the meat product, sterilizing at 125 deg.C for 20 min, and storing.
The gellan gum is prepared by the following preparation method:
(1) inoculating the mixed bacterial liquid into a culture medium of a culture device according to the inoculation amount of 10% for culture under the conditions of 30 ℃ of temperature, 7.3 of pH value and 24 hours of time to obtain a fermentation mother liquid, and then: transferring the fermentation medium into a fermentation tank according to the volume ratio of 1: 10 for culture under the conditions of 30 ℃ of temperature, 7.3 of pH value and 72 hours to obtain fermentation liquor;
wherein, the components of the culture medium of the incubator comprise: 25g of sucrose, 4.5g of peptone, 3.6g of ammonium sulfate, 2.8g of yeast extract, 3.3g of citric acid, 1.6g of calcium carbonate and 1000ml of distilled water. The components of the fermentation medium comprise: 37g of sucrose, 6.4g of peptone, 2.3g of potassium dihydrogen phosphate, 2.4g of citric acid, 1.8g of calcium carbonate, 0.6g of magnesium sulfate and 1000ml of distilled water.
(2) Heating the fermentation liquor to 75 ℃, adding water-soluble alkaline earth metal salt accounting for 5% of the volume of the fermentation liquor into the fermentation liquor, adjusting the pH value to 9, flocculating the fermentation liquor, and then carrying out solid-liquid separation to obtain a crude product of partially deacylated gellan gum; the alkaline earth metal salt comprises one or more of calcium chloride, magnesium chloride, calcium sulfate and magnesium sulfate;
(3) adding the crude product of the gellan gum into lower alcohol with the volume 0.45 times of the initial volume of the fermentation liquid, adjusting the pH value to 4.0, stirring and washing, and performing solid-liquid separation to obtain gellan gum fiber; the lower alcohol comprises isopropanol;
(4) adding 95 vol% alcohol into the obtained gellan gum fiber until the material is in a fiber separation state, pumping the material into a dehydrator to remove alcohol and water, drying for 2 hours by a dryer, and crushing and screening to obtain gellan gum powder;
(5) uniformly mixing the obtained gellan gum powder with alkali metal salt accounting for 8% of the final finished product in mass to obtain a gellan gum finished product; the alkali metal salt comprises a combination of sodium chloride and potassium sulfate.
Example 2
1. 0.03 g of calcium hydroxide and 0.1 g of calcium chloride are weighed out and dissolved in a small amount of water.
2. 2.5 g of curdlan and 0.2 g of gellan gum are put into 97.3 g of gravy, and are stirred to be fully dispersed in the gravy; adding the prepared calcium hydroxide and calcium chloride aqueous solution after proper stirring, and stirring until the solution is fine and smooth and has no particles (if the solution is not uniformly stirred and is easy to layer, a stirrer can be properly used for stirring to prevent layering).
3. Adding proper amount of lactic acid, and adjusting pH to about neutral.
4. And (4) placing the meat into a mould to degas so that the whole meat juice system has no bubbles.
5. Pouring the prepared meat juice into the meat product, sterilizing at 115 ℃ for 30 minutes and storing.
The gellan gum used in example 2 was prepared by the following method:
(1) inoculating the mixed bacterial liquid into a culture medium of a culture device according to the inoculum size of 10% for culture under the culture conditions of 28 ℃ of temperature, 7.3 of pH value and 24 hours to obtain a fermentation mother liquid, and then: transferring the fermentation medium into a fermentation tank according to the volume ratio of 1: 10 for culture under the conditions of 28 ℃ and pH value of 7.3 for 72 hours to obtain fermentation liquor; wherein, the components of the culture medium of the incubator comprise: 25g of sucrose, 4.5g of peptone, 3.6g of ammonium sulfate, 2.8g of yeast extract, 3.3g of citric acid, 1.6g of calcium carbonate and 1000ml of distilled water. The components of the fermentation medium comprise: 37g of sucrose, 6.4g of peptone, 2.3g of potassium dihydrogen phosphate, 2.4g of citric acid, 1.8g of calcium carbonate, 0.6g of magnesium sulfate and 1000ml of distilled water.
(2) Heating the fermentation liquor to 85 ℃, adding water-soluble alkaline earth metal salt accounting for 4% of the volume of the fermentation liquor into the fermentation liquor, adjusting the pH value to 9.5, flocculating the fermentation liquor, and then carrying out solid-liquid separation to obtain a crude product of partially deacylated gellan gum; the alkaline earth metal salt is calcium chloride;
(3) adding the crude product of the gellan gum into lower alcohol with the volume 0.5 times of the initial volume of the fermentation liquid, adjusting the pH value to 4.0, stirring and washing, and performing solid-liquid separation to obtain gellan gum fiber; the lower alcohol is ethanol;
(4) adding 75% alcohol by volume into the obtained gellan gum fiber until the material is in a fiber separation state, pumping the material into a dehydrator to remove alcohol and water, drying for 3 hours by a dryer, and crushing and screening to obtain gellan gum powder;
(5) uniformly mixing the obtained gellan gum powder with alkali metal salt accounting for 8.5% of the final finished product mass to obtain a gellan gum finished product; the alkali metal salt includes potassium chloride and sodium chloride.
Claims (9)
1. A method for preparing heat irreversible meat jelly by curdlan and gellan gum is characterized by comprising the following steps:
(1) weighing calcium hydroxide and calcium chloride, and dissolving with a small amount of water; putting curdlan and gellan gum into the meat juice, and stirring to fully disperse the curdlan and gellan gum in the meat juice; after properly stirring, adding the prepared calcium hydroxide and calcium chloride aqueous solution, and stirring until the solution is fine and smooth and has no particles;
(2) adding edible acid, and adjusting pH to neutral;
(3) placing into a mould and degassing to make the whole gravy system have no bubbles;
(4) pouring the prepared meat juice into the meat product, sterilizing and storing.
2. The method for preparing the heat irreversible meat jelly by curdlan and gellan gum according to claim 1, wherein the addition amount of calcium hydroxide is 0.01 to 0.2% by mass of the whole gravy system, and the addition amount of calcium chloride is 0.01 to 0.5% by mass of the whole gravy system.
3. The method for preparing the heat irreversible meat jelly by using curdlan and gellan gum as claimed in claim 1, wherein the addition amount of curdlan is 0.1-5% of the mass of the whole gravy system, and the addition amount of gellan gum is 0.05-0.5% of the mass of the whole gravy system.
4. The method for preparing the heat irreversible meat jelly of curdlan and gellan gum according to claim 1, wherein the edible acid is citric acid, malic acid, lactic acid.
5. The method for preparing the heat irreversible meat jelly by using the curdlan and the gellan gum as claimed in claim 1, wherein the sterilization temperature is 85-150 ℃ and the sterilization time is 20-100 minutes.
6. The method for preparing the heat irreversible meat jelly by curdlan and gellan gum according to claim 1, wherein the gellan gum is prepared by the following method:
(1) inoculating the mixed bacterial liquid into a culture medium of an incubator according to the inoculum size of 10% for culture under the conditions of 25-30 ℃, pH value of 7.3 and 24 hours to obtain a fermentation mother liquid, and then: transferring the fermentation medium into a fermentation tank for culture according to the volume ratio of 1: 10, wherein the culture conditions are that the temperature is 25-30 ℃, the pH value is 7.3, and the time is 72 hours, so as to obtain fermentation liquor;
(2) heating the fermentation liquor to 50-90 ℃, adding water-soluble alkaline earth metal salt accounting for 3-5% of the volume of the fermentation liquor into the fermentation liquor, adjusting the pH value to 8.5-10.5, flocculating the fermentation liquor, and then carrying out solid-liquid separation to obtain a partially deacylated gellan gum crude product; the alkaline earth metal salt comprises one or more of calcium chloride, magnesium chloride, calcium sulfate and magnesium sulfate;
(3) adding the crude gellan gum product into lower alcohol with the volume 0.4-0.6 times of the initial volume of the fermentation liquid, adjusting the pH value to 4.0-5.0, stirring and washing, and performing solid-liquid separation to obtain gellan gum fiber; the lower alcohol comprises one or more of ethanol, isopropanol, n-propanol, n-butanol and isobutanol;
(4) adding 75-95% alcohol by volume into the obtained gellan gum fibers until the materials are in a fiber separation state, pumping the materials into a dehydrator to remove alcohol and water, drying for 2-5 hours by a dryer, and crushing and screening to obtain gellan gum powder;
(5) uniformly mixing the obtained gellan gum powder with alkali metal salt accounting for 5-10% of the final finished product to obtain a gellan gum finished product; the alkali metal salt comprises one or more of potassium chloride, sodium chloride, potassium sulfate and sodium sulfate.
7. The method as claimed in claim 6, wherein the culture medium of the incubator comprises: 25g of sucrose, 4.5g of peptone, 3.6g of ammonium sulfate, 2.8g of yeast extract, 3.3g of citric acid, 1.6g of calcium carbonate and 1000ml of distilled water.
8. The method for preparing the heat irreversible meat jelly of curdlan and gellan gum according to claim 6, wherein the components of the fermentation medium comprise: 37g of sucrose, 6.4g of peptone, 2.3g of potassium dihydrogen phosphate, 2.4g of citric acid, 1.8g of calcium carbonate, 0.6g of magnesium sulfate and 1000ml of distilled water.
9. A heat irreversible meat jelly made of curdlan and gellan gum, characterized by being obtained by the production method of any one of claims 1 to 8.
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CN113273688A (en) * | 2021-05-23 | 2021-08-20 | 上海统益生物科技有限公司 | Vegetarian boneless chicken feet and preparation method thereof |
CN113712191A (en) * | 2021-09-07 | 2021-11-30 | 上海交通大学 | Preparation method of instant high-simulation-factor tripe |
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