CN112237863A - Device for preparing graphene dispersion slurry - Google Patents

Device for preparing graphene dispersion slurry Download PDF

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Publication number
CN112237863A
CN112237863A CN202011081379.5A CN202011081379A CN112237863A CN 112237863 A CN112237863 A CN 112237863A CN 202011081379 A CN202011081379 A CN 202011081379A CN 112237863 A CN112237863 A CN 112237863A
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CN
China
Prior art keywords
fixedly connected
transmission rod
rod
plate
graphene dispersion
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202011081379.5A
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Chinese (zh)
Inventor
刘振禹
马有明
亓秀昌
吕振国
陈韶华
刘进
赵娟
李传龙
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
SHANDONG HUAGUAN SMART CARD CO Ltd
Original Assignee
SHANDONG HUAGUAN SMART CARD CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by SHANDONG HUAGUAN SMART CARD CO Ltd filed Critical SHANDONG HUAGUAN SMART CARD CO Ltd
Priority to CN202011081379.5A priority Critical patent/CN112237863A/en
Publication of CN112237863A publication Critical patent/CN112237863A/en
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/90Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with paddles or arms 
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/85Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with two or more stirrers on separate shafts
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00Other mixers; Mixing plants; Combinations of mixers
    • B01F33/70Mixers specially adapted for working at sub- or super-atmospheric pressure, e.g. combined with de-foaming
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/40Mounting or supporting mixing devices or receptacles; Clamping or holding arrangements therefor
    • B01F35/41Mounting or supporting stirrer shafts or stirrer units on receptacles
    • B01F35/413Mounting or supporting stirrer shafts or stirrer units on receptacles by means of clamps or clamping arrangements for fixing attached stirrers or independent stirrer units
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/90Heating or cooling systems
    • B01F35/92Heating or cooling systems for heating the outside of the receptacle, e.g. heated jackets or burners
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/90Heating or cooling systems
    • B01F2035/99Heating

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Mixers Of The Rotary Stirring Type (AREA)

Abstract

The invention discloses a device for preparing graphene dispersion slurry, which belongs to the field of graphene preparation and comprises a bottom plate, wherein a supporting plate is fixedly connected to the left side of the top of the bottom plate, a sliding rail is fixedly connected to the right side of the supporting plate, a sliding block is connected to the sliding rail in a sliding manner, a connecting plate is fixedly connected to the right side of the sliding block, a stirring barrel is arranged at the top of the bottom plate, a driving cover is fixedly connected to the top of the connecting plate, a first transmission rod and a second transmission rod are respectively and rotatably connected to the top of the inner wall of the driving cover from right to left, a sealing cover is fixedly connected to the bottom of the connecting plate, and the bottom ends of the first transmission rod and the second transmission rod. The first transmission rod, the second transmission rod and the transmission gear are arranged, so that the first transmission rod and the second transmission rod can rotate relatively while rotating, raw materials in the stirring barrel can be mixed more fully, and the preparation efficiency can be improved.

Description

Device for preparing graphene dispersion slurry
Technical Field
The invention relates to the field of graphene preparation, in particular to a device for preparing graphene dispersion slurry.
Background
Graphene is a polymer made of carbon atoms in sp2The hybrid tracks form a hexagonal honeycomb lattice two-dimensional carbon nanomaterial. The graphene has excellent optical, electrical and mechanical properties, has important application prospects in the aspects of materials science, micro-nano processing, energy, biomedicine, drug delivery and the like, and is considered to be a revolutionary material in the future.
Most current preparation facilities are at the in-process that uses, and holistic treatment effeciency is low, and current some preparation equipment all processes the processing to graphite alkene material under normal atmospheric temperature and pressure, and machining efficiency is lower, and is inconvenient simultaneously to take out and put into the raw materials.
Disclosure of Invention
1. Technical problem to be solved
The invention aims to provide a device for preparing graphene dispersion slurry, which can effectively improve the treatment efficiency and processing quality of graphene and is convenient for taking out and putting in materials.
2. Technical scheme
In order to solve the problems, the invention adopts the following technical scheme:
a device for preparing graphene dispersion slurry comprises a bottom plate, wherein a supporting plate is fixedly connected to the left side of the top of the bottom plate, a sliding rail is fixedly connected to the right side of the supporting plate, a sliding block is connected to the sliding rail in a sliding mode, a connecting plate is fixedly connected to the right side of the sliding block, a stirring barrel is arranged at the top of the bottom plate, a driving cover is fixedly connected to the top of the connecting plate, a first driving rod and a second driving rod are respectively and rotatably connected to the top of the inner wall of the driving cover from right to left, a sealing cover is fixedly connected to the bottom of the connecting plate, the bottom ends of the first driving rod and the second driving rod sequentially penetrate through the connecting plate and the sealing cover and extend to the outside of the sealing cover, the top end of the first driving rod penetrates through the driving cover and extends to the outside of the driving cover, a driving motor is fixedly connected, the surfaces of the first transmission rod and the second transmission rod are fixedly connected with transmission gears, and the two transmission gears are meshed with each other.
Preferably, the surfaces of the first transmission rod and the second transmission rod are fixedly connected with stirring rods, and the top of the right side of the stirring barrel is communicated with a vacuumizing pipe.
Preferably, the top of the bottom plate is provided with a mounting groove, and an electric heating wire is fixedly connected between two sides of the inner wall of the mounting groove.
Preferably, the fixed slot has all been seted up on backup pad and the slider, the quantity of fixed slot is two, the inside of fixed slot is provided with the locating lever, the left end fixedly connected with stopper of locating lever, the right side fixedly connected with spring of the inner wall bottom of locating lever, the top fixedly connected with kelly of spring, the top of kelly runs through the locating lever and extends to the outside of locating lever.
Preferably, the front side and the rear side at the top of the bottom plate are fixedly connected with fixing blocks, fixing screws penetrate through the fixing blocks, one ends of the fixing screws are rotatably connected with clamping plates, and the other ends of the fixing screws are fixedly connected with hand wheels.
Preferably, the right side of the top of the connecting plate is fixedly connected with a handle.
3. Advantageous effects
(1) According to the invention, the top of the inner wall of the driving cover is respectively connected with the first transmission rod and the second transmission rod in a rotating manner from right to left, the bottom of the connecting plate is fixedly connected with the sealing cover, the bottom ends of the first transmission rod and the second transmission rod sequentially penetrate through the connecting plate and the sealing cover and extend to the outside of the sealing cover, the surfaces of the first transmission rod and the second transmission rod are respectively fixedly connected with the transmission gear, and the two transmission gears are mutually meshed, so that the first transmission rod and the second transmission rod can rotate relatively while rotating, thus raw materials in the stirring barrel can be more fully mixed, and meanwhile, the preparation efficiency can be improved.
(2) According to the invention, the mounting groove is formed in the top of the bottom plate, the electric heating wires are fixedly connected between the two sides of the inner wall of the mounting groove, and the stirring barrel can be heated after the electric heating wires are powered on, so that the temperature of materials in the stirring barrel is raised, and the processing and preparation efficiency is higher.
(3) According to the invention, the front side and the rear side of the top of the bottom plate are fixedly connected with the fixed blocks, the fixed blocks are penetrated by the fixed screws, one ends of the fixed screws are rotatably connected with the clamping plates, the other ends of the fixed screws are fixedly connected with the hand wheels, and after the stirring barrel is placed on the bottom plate, the hand wheels are rotated to drive the fixed screws to rotate, so that the two clamping plates are pushed towards the middle, the stirring barrel is further clamped and fixed, and the material is prevented from being spilled due to the shaking of the stirring barrel in the preparation process.
Drawings
Fig. 1 is a schematic structural diagram of an apparatus for preparing a graphene dispersion paste according to a preferred embodiment of the present invention;
FIG. 2 is a right side view of the structure of the base plate shown in FIG. 1;
fig. 3 is a partially enlarged view of a portion a shown in fig. 1.
Reference numerals: 1. a base plate; 2. a support plate; 3. a slide rail; 4. a slider; 5. a connecting plate; 6. a stirring barrel; 7. a drive cap; 8. a first drive lever; 9. a second transmission rod; 10. a sealing cover; 11. a drive motor; 12. a stirring rod; 13. vacuumizing a tube; 14. mounting grooves; 15. an electric heating wire; 16. fixing grooves; 17. positioning a rod; 18. a limiting block; 19. a spring; 20. a clamping rod; 21. a fixed block; 22. fixing the screw rod; 23. a splint; 24. a hand wheel; 25. a grip; 26. a transmission gear.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Referring to fig. 1-3, an embodiment of the present invention is shown: a device for preparing graphene dispersion slurry comprises a bottom plate 1, a supporting plate 2 is fixedly connected to the left side of the top of the bottom plate 1, a sliding rail 3 is fixedly connected to the right side of the supporting plate 2, a sliding block 4 is connected to the sliding rail 3 in a sliding manner, a connecting plate 5 is fixedly connected to the right side of the sliding block 4, a stirring barrel 6 is arranged at the top of the bottom plate 1, a driving cover 7 is fixedly connected to the top of the connecting plate 5, a first transmission rod 8 and a second transmission rod 9 are respectively and rotatably connected to the top of the inner wall of the driving cover 7 from right to left, a sealing cover 10 is fixedly connected to the bottom of the connecting plate 5, the bottom ends of the first transmission rod 8 and the second transmission rod 9 sequentially penetrate through the connecting plate 5 and the sealing cover 10 and extend to the outside of the sealing cover 10, the top end of the first transmission rod 8 penetrates, the output end of the driving motor 11 is fixedly connected with the top end of the first transmission rod 8, the surfaces of the first transmission rod 8 and the second transmission rod 9 are both fixedly connected with a transmission gear 26, and the two transmission gears 26 are meshed with each other.
The surface of the first transmission rod 8 and the surface of the second transmission rod 9 are fixedly connected with stirring rods 12, the top on the right side of the stirring barrel 6 is communicated with a vacuumizing tube 13, and after the stirring barrel 6 is covered by a sealing cover 10 through the vacuumizing tube 13, the inside of the stirring barrel 6 is pumped into a near vacuum state, so that the preparation efficiency can be effectively improved.
Mounting groove 14 has been seted up at the top of bottom plate 1, fixedly connected with electric heating wire 15 between the both sides of 14 inner walls of mounting groove, and electric heating wire 15 is connected with external power source, can heat agitator 6 after electric heating wire 15 circular telegram, makes the inside material of agitator 6 intensifies, makes processing preparation efficiency higher.
Fixed slots 16 have been all seted up on backup pad 2 and slider 4, the quantity of fixed slot 16 is two, the inside of fixed slot 16 is provided with locating lever 17, locating lever 17's left end fixedly connected with stopper 18, the right side fixedly connected with spring 19 of the inner wall bottom of locating lever 17, spring 19's top fixedly connected with kelly 20, the top of kelly 20 runs through locating lever 17 and extends to locating lever 17's outside, when needing the position of adjusting slider 4, take locating lever 17 outside out, press kelly 20 downwards, make locating lever 17 can pass through fixed slot 16, it fixes to insert locating lever 17 in fixed slot 16 again after moving slider 4 to the target position.
The equal fixedly connected with fixed block 21 in front side and the rear side at bottom plate 1 top, it has set screw 22 to run through on the fixed block 21, set screw 22's one end is rotated and is connected with splint 23, set screw 22's other end fixedly connected with hand wheel 24, put upper plate 1 back with agitator 6, rotate hand wheel 24, drive set screw 22 and rotate, thereby impel two splint 23 to the centre, further press from both sides tight fixedly with agitator 6, prevent to rock at the in-process agitator 6 of preparation and lead to the material to spill.
A handle 25 is fixedly connected to the right side of the top of the connecting plate 5, and the connecting plate 5 can be lifted up by the handle 25, so that the sealing cover 10 can be taken out of the stirring barrel 6.
The working principle is as follows: when in use, firstly, the prepared raw materials are put into the stirring barrel 6, then the stirring barrel 6 is put on the bottom plate 1, the hand wheel 24 is rotated to drive the fixing screw 22 to rotate, thereby the two clamping plates 23 are pushed towards the middle, the stirring barrel 6 is further clamped and fixed, the materials are prevented from spilling out caused by the shaking of the stirring barrel 6 in the preparation process, then the positioning rod 17 is drawn out, the connecting plate 5 is pressed downwards, the sealing cover 10 covers the stirring barrel 6, the positioning rod 17 is drawn out outwards, the clamping rod 20 is pressed downwards, the positioning rod 17 can pass through the fixing groove 16, the positioning rod 17 is inserted into the fixing groove 16 again after the sliding block 4 is moved to the target position, then the vacuum tube 13 can be used for covering the stirring barrel 6 on the sealing cover 10, the inside of the stirring barrel 6 is drawn to be in a near vacuum state, the preparation efficiency can be effectively improved, and the driving motor 11 is further started, driving motor 11 drives first transfer line 8 and rotates, further drive gear 26 rotates, thereby drive second transfer line 9 and rotate, further drive stirring rod 12 and rotate, stir raw and other materials, can heat agitator 6 after electric heating wire 15 circular telegram, make the inside material of agitator 6 intensification, it is higher to make processing preparation efficiency, after the preparation finishes, take out locating lever 17 the back and upwards lift up connecting plate 5 through handle 25, take out agitator 6 after loosening splint 23.
It should be understood by those skilled in the art that the above embodiments are only for illustrating the present invention and are not to be used as a limitation of the present invention, and that changes and modifications to the above embodiments are within the scope of the claims of the present invention as long as they are within the spirit and scope of the present invention.

Claims (6)

1. An apparatus for preparing graphene dispersion slurry, comprising a base plate (1), characterized in that: the stirring device is characterized in that a supporting plate (2) is fixedly connected to the left side of the top of the bottom plate (1), a sliding rail (3) is fixedly connected to the right side of the supporting plate (2), a sliding block (4) is connected to the sliding rail (3) in a sliding manner, a connecting plate (5) is fixedly connected to the right side of the sliding block (4), a stirring barrel (6) is arranged at the top of the bottom plate (1), a driving cover (7) is fixedly connected to the top of the connecting plate (5), a first transmission rod (8) and a second transmission rod (9) are respectively connected to the top of the inner wall of the driving cover (7) in a rotating manner from right to left, a sealing cover (10) is fixedly connected to the bottom of the connecting plate (5), the bottom of the first transmission rod (8) and the bottom of the second transmission rod (9) sequentially penetrate through the connecting plate (5) and the sealing cover (10) and extend to the outside of the sealing cover (10, the right side at drive lid (7) top is through support fixedly connected with driving motor (11), the output of driving motor (11) and the top fixed connection of first transfer line (8), equal fixed connection drive gear (26), two in the surface of first transfer line (8) and second transfer line (9) drive gear (26) intermeshing.
2. The device for preparing graphene dispersion paste according to claim 1, wherein the surfaces of the first transmission rod (8) and the second transmission rod (9) are fixedly connected with a stirring rod (12), and the top of the right side of the stirring barrel (6) is communicated with an evacuation tube (13).
3. The device for preparing graphene dispersion paste according to claim 1, wherein a mounting groove (14) is formed at the top of the bottom plate (1), and an electric heating wire (15) is fixedly connected between two sides of the inner wall of the mounting groove (14).
4. The device for preparing graphene dispersion paste according to claim 1, wherein fixing grooves (16) are formed in the supporting plate (2) and the sliding block (4), the number of the fixing grooves (16) is two, a positioning rod (17) is arranged inside each fixing groove (16), a limiting block (18) is fixedly connected to the left end of each positioning rod (17), a spring (19) is fixedly connected to the right side of the bottom of the inner wall of each positioning rod (17), a clamping rod (20) is fixedly connected to the top end of each spring (19), and the top end of each clamping rod (20) penetrates through each positioning rod (17) and extends to the outside of each positioning rod (17).
5. The device for preparing graphene dispersion slurry according to claim 1, wherein the front side and the rear side of the top of the bottom plate (1) are fixedly connected with fixing blocks (21), fixing screws (22) penetrate through the fixing blocks (21), one ends of the fixing screws (22) are rotatably connected with clamping plates (23), and the other ends of the fixing screws (22) are fixedly connected with hand wheels (24).
6. The apparatus for preparing graphene dispersion paste according to claim 1, wherein a handle (25) is fixedly connected to the right side of the top of the connection plate (5).
CN202011081379.5A 2020-09-29 2020-09-29 Device for preparing graphene dispersion slurry Pending CN112237863A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202011081379.5A CN112237863A (en) 2020-09-29 2020-09-29 Device for preparing graphene dispersion slurry

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202011081379.5A CN112237863A (en) 2020-09-29 2020-09-29 Device for preparing graphene dispersion slurry

Publications (1)

Publication Number Publication Date
CN112237863A true CN112237863A (en) 2021-01-19

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113332878A (en) * 2021-05-21 2021-09-03 浙江兰树化妆品有限公司 Vacuum nanometer high-speed dispersion machine
CN114225747A (en) * 2021-12-17 2022-03-25 南通强生新材料科技股份有限公司 Improved generation dressing trough with regulatory function

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1588619A2 (en) * 2004-04-23 2005-10-26 FMC Technologies, Inc. Mixing apparatus
CN108501237A (en) * 2018-04-03 2018-09-07 王圆圆 A kind of elastic polymer material raw material processing equipment
CN207970754U (en) * 2018-01-02 2018-10-16 绍兴君泰纺织科技有限公司 A kind of blender producing corrosion-resistant textile dyestuff
CN210278897U (en) * 2019-06-03 2020-04-10 广州市博诺通化工技术服务有限公司 High-speed dispersion machine convenient to centre gripping
CN210303288U (en) * 2019-06-20 2020-04-14 精创(广州)石墨烯新材料科技有限公司 Efficient and energy-saving graphene slurry preparation system
CN210410494U (en) * 2019-06-20 2020-04-28 枣阳四海道普化工有限公司 Double-shaft dispersion machine

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1588619A2 (en) * 2004-04-23 2005-10-26 FMC Technologies, Inc. Mixing apparatus
CN207970754U (en) * 2018-01-02 2018-10-16 绍兴君泰纺织科技有限公司 A kind of blender producing corrosion-resistant textile dyestuff
CN108501237A (en) * 2018-04-03 2018-09-07 王圆圆 A kind of elastic polymer material raw material processing equipment
CN210278897U (en) * 2019-06-03 2020-04-10 广州市博诺通化工技术服务有限公司 High-speed dispersion machine convenient to centre gripping
CN210303288U (en) * 2019-06-20 2020-04-14 精创(广州)石墨烯新材料科技有限公司 Efficient and energy-saving graphene slurry preparation system
CN210410494U (en) * 2019-06-20 2020-04-28 枣阳四海道普化工有限公司 Double-shaft dispersion machine

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113332878A (en) * 2021-05-21 2021-09-03 浙江兰树化妆品有限公司 Vacuum nanometer high-speed dispersion machine
CN114225747A (en) * 2021-12-17 2022-03-25 南通强生新材料科技股份有限公司 Improved generation dressing trough with regulatory function

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Application publication date: 20210119

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