CN112129486B - Liquid CO at different pressures and temperatures 2 Phase-change jet impact power experimental method - Google Patents
Liquid CO at different pressures and temperatures 2 Phase-change jet impact power experimental method Download PDFInfo
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- CN112129486B CN112129486B CN202010996835.2A CN202010996835A CN112129486B CN 112129486 B CN112129486 B CN 112129486B CN 202010996835 A CN202010996835 A CN 202010996835A CN 112129486 B CN112129486 B CN 112129486B
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Abstract
The invention discloses liquid CO under different pressures and temperatures 2 The phase-change jet impact power experiment method comprises the following steps: s1, preparing a liquid carbon dioxide phase change jet impact dynamics experiment system; s2, establishing an experimental scheme; s3, preparing an experiment; s4,Preparing high-pressure liquid carbon dioxide; s5, forming liquid CO 2 Jetting, and carrying out jet form, speed and pressure data testing; s6, adjusting CO 2 Repeating S4-S5 under the conditions of initial pressure and temperature of the constant temperature and humidity box body, and carrying out liquid CO under different initial pressures and different temperatures 2 Phase change jet shape, speed and pressure variation parameter experiment, analyzing jet shape, jet speed and fluid pressure along with time, CO 2 Initial pressure, constant temperature and humidity box. The device is used for researching the jet flow form, speed and pressure change rule influence in the carbon dioxide phase change jet flow process under different initial pressures and temperatures without the aid of a dynamic and static load loading device and a coal rock sample, and the development of the technical basic theory and the application technology is promoted.
Description
Technical Field
The invention belongs to the technical field of carbon dioxide phase change cracking of coal rock mass, and particularly relates to liquid CO under different initial pressures and temperatures 2 Phase-change jet impact power experimental method.
Background
The liquid carbon dioxide phase change fracturing technology is used as an effective coal rock fracturing technology and is widely applied to rock mass fracturing and fracturing permeability increase of low-permeability coal rock reservoirs. The technical principle is as follows: the carbon dioxide is pressurized, liquefied and stored in a sealed container, and a high-pressure gas jet is generated to act on a target coal rock mass by adopting an instant heating or instant pressure relief mode, so that the coal rock mass generates structural damage and destruction under the action of the high-pressure gas. At present, the technology has made great progress in the aspects of field application, technical equipment and the like, but a dynamic and static load loading device and a coal rock sample are also needed for a liquid carbon dioxide phase change jet flow simulation experiment, and the research on impact dynamics parameters, influence factors and influence rules of the impact dynamics parameters, such as fluid form, jet flow pressure, striking target body pressure and the like in the carbon dioxide phase change jet flow process is in a primary stage, so that the development of the basic theory and application technology of the technology is influenced to a certain extent.
Disclosure of Invention
The invention aims to provide liquid CO 2 The experimental method of the phase change jet impact dynamics is used for researching the jet shape, speed and pressure change rule influence in the carbon dioxide phase change jet process under different initial pressures and temperatures without the aid of a dynamic and static load loading device and a coal rock sample, and promotes the development of the technical basic theory and the application technology.
Therefore, the technical scheme adopted by the invention is as follows: liquid CO under different pressures and temperatures 2 The phase-change jet impact power experiment method comprises the following steps:
s1, preparing a liquid carbon dioxide phase change jet impact dynamics experiment system;
the liquid carbon dioxide phase change jet impact dynamics experiment system comprises a carbon dioxide pressurization liquefaction system, a liquid carbon dioxide phase change jet and monitoring system thereof, and a remote control and data acquisition system;
the carbon dioxide pressurizing and liquefying system is used for liquefying and pressurizing carbon dioxide to form high-pressure liquid carbon dioxide capable of carrying out phase change jet, and comprises an air compressor, a carbon dioxide steel cylinder, a carbon dioxide liquefying pump, a low-pressure carbon dioxide storage tank, a liquid carbon dioxide pressurizing pump and a high-pressure liquid carbon dioxide storage tank, wherein the air compressor is used for generating compressed air, and can be used for driving the carbon dioxide liquefying pump to pressurize the carbon dioxide in the carbon dioxide steel cylinder and store the carbon dioxide in the low-pressure carbon dioxide storage tank through valve control, and can also be used for driving the liquid carbon dioxide pressurizing pump to pressurize the liquid carbon dioxide in the low-pressure carbon dioxide storage tank to an experimental preset pressure and store the liquid carbon dioxide in the high-pressure liquid carbon dioxide storage tank for later use;
the liquid carbon dioxide phase-change jet and monitoring system thereof comprises a constant-temperature and constant-humidity box body, and a liquid carbon dioxide phase-change jet device, a liquid carbon dioxide phase-change jet impact stress testing device, a liquid carbon dioxide phase-change jet fluid form testing device and a box body environment testing device which are arranged in the constant-temperature and constant-humidity box body;
the liquid carbon dioxide phase change jet device comprises a pressure sensor, a temperature sensor, a pneumatic valve and a jet nozzle, wherein the jet nozzle is connected with a high-pressure liquid carbon dioxide outlet of a carbon dioxide pressurization liquefaction system positioned outside the constant-temperature and constant-humidity box body through an air pressure pipe and is used for realizing instant release of high-pressure liquid carbon dioxide by combining with the pneumatic valve, a liquid carbon dioxide phase change jet is formed by the jet nozzle, and the pressure sensor and the temperature sensor are used for monitoring fluid pressure and temperature change parameters at the jet nozzle in real time;
the liquid carbon dioxide phase change jet impact stress testing device comprises a guide rail, an impact stress sensor, a rotation angle sensor and a laser ranging sensor, wherein the impact stress sensor and the laser ranging sensor are rotatably and adjustably mounted on a rotating seat through the same sensor support, the sensor support is slidably and adjustably mounted on the guide rail through the rotating seat, the impact stress sensor is used for testing the liquid carbon dioxide phase change jet impact stress, the laser ranging sensor is used for measuring the distance from the impact stress sensor to a jet nozzle, and the rotation angle sensor is mounted at the bottom of the sensor support and used for testing the angle between the impact stress sensor and the jet nozzle;
the liquid carbon dioxide phase change jet fluid form testing device comprises a high-speed camera, an infrared camera and a particle image speed field tester, wherein the high-speed camera, the infrared camera and the particle image speed field tester are respectively arranged on a guide rail by a mounting bracket in a sliding and adjusting manner;
the box body environment testing device comprises a temperature and humidity sensor and is used for testing the change rule of the environmental temperature and the humidity in the constant temperature box body;
the remote control and data acquisition system comprises a computer, a control system and a data acquisition system and is used for acquiring, displaying and storing various data and test results in the liquid carbon dioxide phase-change jet impact dynamics experiment process;
s2, establishing an experimental scheme;
considering CO in a high-pressure liquid carbon dioxide storage tank 2 Initial pressure, ambient temperature parameters vs. liquid CO 2 The phase change jet flow shape, speed and pressure change rule influence the establishment of an experimental scheme;
s3, preparing an experiment;
connecting related pipelines of the carbon dioxide pressurizing and liquefying system, and checking the air tightness of the pipelines; checking whether the air compressor, the carbon dioxide gas liquefaction pump and the liquid carbon dioxide booster pump can work normally or not; adjusting the positions of a high-speed camera, an infrared camera and a particle image velocity field tester, and detecting whether the high-speed camera, the infrared camera and the particle image velocity field tester can work normally;
s4, preparing high-pressure liquid carbon dioxide;
closing a No. 5 valve at the bottom of the low-pressure carbon dioxide storage tank, opening an air compressor, a carbon dioxide steel cylinder, a carbon dioxide gas liquefaction pump, 1#, 2#, 3#, and 4# valves at the low-pressure carbon dioxide storage tank, starting a power supply of the air compressor, pressurizing and filling carbon dioxide in the carbon dioxide steel cylinder to the low-pressure carbon dioxide storage tank until the pressure in the low-pressure carbon dioxide storage tank reaches a set pressure, closing the carbon dioxide gas liquefaction pump, 3#, and 7# valves at the high-pressure liquid carbon dioxide storage tank, opening the low-pressure carbon dioxide storage tank, 5#, and 6# valves at the liquid carbon dioxide booster pump, re-pressurizing liquid carbon dioxide in the low-pressure carbon dioxide storage tank, filling the liquid carbon dioxide into the high-pressure liquid carbon dioxide storage tank until the set pressure is reached 2 Initial pressure, closing the 6# valve and opening the 8# valve;
s5, forming liquid CO 2 Jetting, and carrying out jet form, speed and pressure data testing;
adjusting the initial pressure and the temperature of the constant-temperature and constant-humidity box body according to experimental conditions, and closing a power supply of the constant-temperature and constant-humidity box body after the conditions are met;
starting a pressure sensor, a temperature sensor, a high-speed camera, an infrared camera, a particle image speed field tester and a temperature and humidity sensor;
the remote control pneumatic valve is opened by a remote control and data acquisition system, and high-pressure liquid CO is stored in the high-pressure liquid carbon dioxide storage tank 2 Instantaneous release of liquid CO from the jet nozzle 2 Phase change jetting;
the liquid CO is obtained by testing the pressure sensor and the temperature sensor 2 The liquid CO is obtained by testing the change rule of the fluid pressure and temperature in the jet nozzle along with time in the phase change jet process by a high-speed camera and an infrared camera 2 The liquid CO is obtained by testing the change rule of the fluid form with time in the phase change jet process by a particle image velocity field tester 2 In the phase change jet process, parameters of fluid velocity field, jet size, core area length and jet angle are tested by a temperature and humidity sensor to obtain liquid CO 2 The change rule of the environmental temperature and the humidity in the phase change jet process;
s6, adjusting CO 2 Repeating S4-S5 under the conditions of initial pressure and temperature of the constant temperature and humidity box body, and carrying out liquid CO under different initial pressures and different temperatures 2 Phase change jet shape, speed and pressure variation parameter experiment, analyzing jet shape, jet speed and fluid pressure along with time, CO 2 Initial pressure, constant temperature and humidity box.
Preferably, the maximum pressure of the compressed air generated by the air compressor is 0.8MPa, the input-output pressure ratio of the carbon dioxide gas liquefaction pump is 1:10, and the compressed air is used for pressurizing the carbon dioxide in the carbon dioxide steel cylinder to 8MPa at maximum; the input-output pressure ratio of the liquid carbon dioxide booster pump is 1:100, the liquid carbon dioxide booster pump is used for boosting the liquid carbon dioxide in the low-pressure carbon dioxide storage tank to 80MPa at maximum, and the experimental preset pressure is 8-60 MPa.
Preferably, a gas-water separator is arranged on a pipeline between the carbon dioxide steel cylinder and the carbon dioxide gas liquefaction pump, the carbon dioxide pressurization liquefaction system is integrally installed in the same box body, and the bottom of the box body and the bottom of the constant-temperature and constant-humidity box body are provided with rollers; the system integration level is high, and the system is convenient to move.
Preferably, the high-speed camera and the infrared camera share the same mounting bracket, so that the structure is simplified.
Further preferably, the temperature and humidity sensor is arranged at the top of the constant temperature and humidity box body.
The invention has the beneficial effects that:
(1) the liquid carbon dioxide phase-change jet and a monitoring system thereof are used as the core part of the experimental system and mainly used for creating a constant-temperature and constant-humidity environment, generating the liquid carbon dioxide phase-change jet, and testing parameters such as temperature, humidity, fluid form, flow field velocity distribution, jet impact pressure and the like of a jet process;
the constant temperature and humidity box body can ensure that the environmental temperature and humidity of the liquid carbon dioxide phase change jet flow are constant before experimental test, and reduce experimental errors caused by the change of the environmental temperature and humidity; the box body environment testing device can monitor the environmental temperature and humidity change in the liquid carbon dioxide phase change jet flow process in real time, and provides data support for later-stage related theoretical research; the liquid carbon dioxide phase change jet impact stress testing device can be used for researching the stress change rule of a carbon dioxide phase change jet hitting target body under the conditions of different distances and different angles, and errors caused by artificial testing angles and artificial testing distances are avoided; the liquid carbon dioxide phase-change jet fluid form testing device can monitor the fluid form change characteristics and the flow field speed distribution characteristics research in the liquid carbon dioxide phase-change jet process in real time.
(2) The traditional experimental system directly takes place and monitors in the air, but because the impact dynamics parameters such as carbon dioxide phase change jet fluid form, pressure and the like are greatly influenced by temperature, humidity and the like, the environmental temperature and humidity in each experimental research can not be guaranteed to be constant. The liquid carbon dioxide phase change jet experiment is carried out in the constant temperature and humidity box body, and is combined with the pressure sensor and the temperature sensor which are arranged in the jet nozzle, so that the fluid pressure and the temperature change parameters at the jet nozzle can be monitored in real time, the stable experimental state can be ensured, and the accuracy and the consistency of the experimental analysis result can be ensured.
(3) The traditional experimental system can not carry out the research on the stress change rule of the carbon dioxide phase change jet hitting target body under the conditions of different distances and different angles, and the research has important influence on the determination of the size of the carbon dioxide phase change fracturing drill hole, the outlet angle of the fracturing device and the like; the experimental device adopts the liquid carbon dioxide phase change jet impact stress testing device, can be used for researching the stress change rule of the carbon dioxide phase change jet hitting target body under the conditions of different distances and different angles, avoids errors caused by artificial testing angles and artificial testing distances, and has an important effect on determining the carbon dioxide phase change fracturing drilling hole size, the fracturing device outlet angle and the like.
(4) The research on impact dynamics parameters, influence factors and influence rules of the impact dynamics parameters such as jet flow form, speed and pressure change in the carbon dioxide phase change jet flow process can be carried out without the aid of a dynamic and static load loading device and a coal rock sample, and the research has important significance for promoting the development of technical basic theory and application technology.
Drawings
FIG. 1 is a liquid carbon dioxide phase change jet impact dynamics experimental system used in the present invention.
Fig. 2 is a schematic structural diagram of a carbon dioxide pressurized liquefaction system.
FIG. 3 is a schematic diagram of the composition of a liquid carbon dioxide phase change jet and its monitoring system.
Fig. 4 is a schematic structural diagram of a liquid carbon dioxide phase change jet and a monitoring system thereof.
FIG. 5 is a flow chart of the experimental procedures of the present invention.
Detailed Description
The invention will be further illustrated by the following examples in conjunction with the accompanying drawings:
as shown in fig. 1, the liquid carbon dioxide phase change jet impact dynamics experiment system used in the present invention mainly comprises a carbon dioxide pressurization liquefaction system 100, a liquid carbon dioxide phase change jet and monitoring system 200 thereof, and a remote control and data acquisition system 300.
The carbon dioxide pressurization liquefaction system 100 is used for liquefying and pressurizing carbon dioxide to form high-pressure liquid carbon dioxide capable of performing phase change jet. As shown in fig. 2, the carbon dioxide pressurized liquefaction system 100 preferably adopts a two-stage pressurized liquefaction system, and mainly comprises an air compressor 1, a carbon dioxide steel cylinder 2, a carbon dioxide gas liquefaction pump 3, a low-pressure carbon dioxide storage tank 4, a liquid carbon dioxide booster pump 5, a high-pressure liquid carbon dioxide storage tank 6, and a plurality of pipelines.
The air compressor 1 is used for generating compressed air, is switched through valve control, can be used for driving the carbon dioxide gas liquefaction pump 3 to pressurize the carbon dioxide in the carbon dioxide steel cylinder 2, and stores the carbon dioxide into the low-pressure carbon dioxide storage tank 4, and can be used for driving the liquid carbon dioxide booster pump 5 to pressurize the liquid carbon dioxide in the low-pressure carbon dioxide storage tank 4 to the experiment preset pressure, and stores the carbon dioxide into the high-pressure liquid carbon dioxide storage tank 6 for later use.
The maximum pressure of compressed air generated by the air compressor 1 is 0.8MPa, the input-output pressure ratio of the carbon dioxide gas liquefaction pump 3 is 1:10, and the maximum pressure boosting device is used for boosting the carbon dioxide in the carbon dioxide steel cylinder 2 to 8 MPa; the input-output pressure ratio of the liquid carbon dioxide booster pump 5 is 1:100, the liquid carbon dioxide booster pump is used for boosting the liquid carbon dioxide in the low-pressure carbon dioxide storage tank 4 to 80MPa at maximum, and the experimental preset pressure is 8-60 MPa.
Preferably, a gas-water separator 7 is disposed on a pipeline between the carbon dioxide cylinder 2 and the carbon dioxide gas liquefaction pump 3, and the carbon dioxide pressurization liquefaction system 100 is integrally installed in the same box, and the bottom of the box is provided with rollers for facilitating moving.
The carbon dioxide pressurization liquefaction system 100 adopts the carbon dioxide gas liquefaction pump 3 and the liquid carbon dioxide booster pump 5 to form a high-low pressure double-pump pressurization liquefaction system for carbon dioxide liquefaction pressurization, the carbon dioxide in the carbon dioxide steel cylinder 2 is pressurized by the carbon dioxide gas liquefaction pump 3, and the liquefied carbon dioxide is pressurized again by the liquid carbon dioxide booster pump 5, so that the carbon dioxide pressurization efficiency is improved, and the defects of low pressurization efficiency and large carbon dioxide loss in the single-pump pressurization process are avoided.
The specific implementation of the carbon dioxide pressurization liquefaction system 100 for preparing high-pressure liquid carbon dioxide is as follows: closing a 5# valve at the bottom of the low-pressure carbon dioxide storage tank 4, opening 1#, 2#, 3#, and 4# valves at the air compressor 1, the carbon dioxide steel cylinder 2, the carbon dioxide liquefaction pump 3, and the low-pressure carbon dioxide storage tank 4, starting a power supply of the air compressor 1, pressurizing and filling carbon dioxide in the carbon dioxide steel cylinder 2 to the low-pressure carbon dioxide storage tank 4 until the carbon dioxide in the low-pressure carbon dioxide storage tank 4 is filledWhen the pressure reaches the set pressure, the valves 3# and 7# at the carbon dioxide gas liquefaction pump 3 and the high-pressure liquid carbon dioxide storage tank 6 are closed, the valves 5# and 6# at the low-pressure carbon dioxide storage tank 4 and the liquid carbon dioxide booster pump 5 are opened, the liquid carbon dioxide in the low-pressure carbon dioxide storage tank 4 is pressurized again and filled into the high-pressure liquid carbon dioxide storage tank 6 until the set pressure reaches the set CO 2 Initial pressure, close valve # 6, open valve # 8.
As shown in fig. 3, the liquid carbon dioxide phase-change jet and monitoring system 200 includes a constant temperature and humidity box 13, and a liquid carbon dioxide phase-change jet device 400, a liquid carbon dioxide phase-change jet impact stress testing device 500, a liquid carbon dioxide phase-change jet fluid form testing device 600, and a box environment testing device 700 disposed in the constant temperature and humidity box 13.
The constant temperature and humidity box body 13 is mainly used for keeping the ambient temperature and humidity of the liquid carbon dioxide phase-change jet constant, is not influenced by external weather, and provides favorable conditions for the experiment system to test the impact kinetic parameters of the liquid carbon dioxide phase-change jet under different conditions such as initial pressure of carbon dioxide, ambient temperature/humidity and the like. The bottom of the constant temperature and humidity box body 13 is preferably provided with rollers for convenient movement. Before the experiment begins, the temperature and the humidity of the constant temperature and humidity box body 13 are adjusted, and the power supply of the constant temperature and humidity box body 13 is closed after the conditions are met.
Referring to fig. 3 and 4, the liquid carbon dioxide phase change jet device 400 mainly comprises a pressure sensor 14, a temperature sensor 15, a pneumatic valve 16 and a jet nozzle 17. The jet nozzle 17 is connected with a high-pressure liquid carbon dioxide outlet of the carbon dioxide pressurizing and liquefying system 100 which is positioned outside the constant-temperature and constant-humidity box body 13 through an air pressure pipe 11, and is combined with a pneumatic valve 16 to realize the instant release of the high-pressure liquid carbon dioxide, and the jet nozzle 17 forms liquid carbon dioxide phase change jet. The pressure sensor 14 and the temperature sensor 15 are installed in the jet nozzle 17 and used for monitoring the fluid pressure and temperature change parameters at the jet nozzle 17 in real time. The working process is as follows: the pneumatic valve 16 is remotely controlled by the remote control and data acquisition system 300 to release high-pressure liquid carbon dioxide instantly, the liquid carbon dioxide phase change jet is formed by the jet nozzle 17, and the pressure sensor 14 and the temperature sensor 15 can monitor the pressure and temperature change parameters in the jet nozzle 17 in real time. The liquid carbon dioxide phase change jet device 400 mainly functions to form a liquid carbon dioxide phase change jet and monitor the change law of fluid pressure and temperature at the jet nozzle.
The liquid carbon dioxide phase change jet impact stress testing device 500 mainly comprises a guide rail 18, an impact stress sensor 19, a rotating seat 20, a rotating angle sensor 21, a laser ranging sensor 22 and a sensor support 23. The impact stress sensor 19 and the laser distance measuring sensor 22 are rotatably and adjustably mounted on the rotating base 20 through the same sensor bracket 23, and the sensor bracket 23 is slidably and adjustably mounted on the guide rail 18 through the rotating base 20. The impact stress sensor 19 is used for testing the impact stress of liquid carbon dioxide phase change jet flow, the laser ranging sensor 22 is used for measuring the distance from the impact stress sensor 19 to the jet flow nozzle 17, and the rotating angle sensor 21 is installed at the bottom of the sensor support 23 and used for testing the angle between the impact stress sensor 19 and the jet flow nozzle 17. The sensor bracket 23 is fastened to the rotary base 20 through a bolt after being adjusted to a proper angle in a rotating manner, and the rotary base 20 is fastened to the guide rail 18 through a bolt after sliding to a proper position, so that the adjustable installation of rotating and sliding is realized.
The liquid carbon dioxide phase change jet impact stress testing device 500 can monitor the liquid carbon dioxide phase change jet impact stress at different distances and different angles, and provides support for researching influence factors and change rules of the liquid carbon dioxide phase change jet impact stress at a later stage.
The liquid carbon dioxide phase change jet fluid form testing device 600 mainly comprises a high-speed camera 25, an infrared camera 24 and a particle image speed field tester 10. The high-speed camera 25, the infrared camera 24 and the particle image velocity field tester 10 are slidably and adjustably mounted on the guide rail 18 by the mounting bracket 12, respectively. The high speed camera 25 and the infrared camera 24 preferably share the same mounting bracket 12. The mounting bracket 12 is bolted to the rail 18 after being slid into place, thereby achieving a slide adjustment mounting. The high-speed camera 25 mainly tests the fluid form change rule in the liquid carbon dioxide phase change jet process to obtain fluid flow video data; the infrared camera 24 is mainly used for obtaining the fluid form characteristics of the liquid carbon dioxide phase-change jet process by monitoring the temperature change; the particle image velocity field tester 10 adopts an imaging technology and an image analysis technology to obtain various instantaneous parameters of a full flow field, and can measure parameters such as a liquid carbon dioxide phase change jet flow fluid velocity field, jet flow size, core area length, jet flow angle and the like.
The box environment testing device 700 mainly comprises a humidity sensor and a second temperature sensor, and is used for testing the ambient temperature and humidity change rule in the constant temperature box 13 and providing basic parameters for the theoretical research of liquid carbon dioxide phase change jet impact dynamics. Preferably, the humidity sensor and the second temperature sensor are integrated temperature and humidity sensor 9, and the temperature and humidity sensor 9 is arranged on the top of the constant temperature and humidity box body 13.
The remote control and data acquisition system 300 includes a computer, a control system and a data acquisition system for acquiring, displaying and storing various data and test results during the liquid carbon dioxide phase change jet impact dynamics experiment. Each sensor is connected with the remote control and data acquisition system 300 by a data acquisition line 8. Preferably, the pneumatic valve 16 is electrically connected to a remote control and data acquisition system 300 for remote control.
The main functions of the remote control and data acquisition system 300 include: remotely controlling liquid CO under different pressures and temperatures 2 Closing and opening a pneumatic valve in a phase-change jet impact power experiment method; collecting, displaying and storing liquid CO under different pressure and temperature 2 Data of a pressure sensor and a temperature sensor in the phase change jet impact power experiment method; collecting, displaying and storing data of a second temperature sensor and a humidity sensor in the box body environment testing device; collecting, displaying and storing liquid CO at different pressures and temperatures 2 Data of a laser distance measuring sensor, a rotation angle sensor and an impact stress sensor in the phase change jet impact power experiment method; collecting, displaying and storing liquid CO at different pressures and temperatures 2 High-speed shooting in phase-change jet impact power experiment methodCamera, infrared camera, and particle image velocity field tester.
As shown in FIG. 5, a liquid CO at different pressures and temperatures 2 The phase change jet impact power experiment method comprises the following steps:
s1, preparing the liquid carbon dioxide phase change jet impact dynamics experiment system.
S2, establishing an experimental scheme;
considering CO in the high pressure liquid carbon dioxide storage tank 6 2 Initial pressure, ambient temperature parameters vs. liquid CO 2 The phase change jet shape, speed and pressure change rule influence the formulation of an experimental scheme. The experimental protocol can be referred to the following table:
s3, preparing an experiment;
connecting related pipelines of the carbon dioxide pressurizing and liquefying system 100, and checking the air tightness of the pipelines; checking whether the air compressor 1, the carbon dioxide gas liquefaction pump 3 and the liquid carbon dioxide booster pump 5 can work normally or not; and adjusting the positions of the high-speed camera 25, the infrared camera 24 and the particle image velocity field tester 10, and detecting whether the particle image velocity field tester can work normally.
S4, preparing high-pressure liquid carbon dioxide;
closing a No. 5 valve at the bottom of a low-pressure carbon dioxide storage tank 4, opening an air compressor 1, a carbon dioxide steel cylinder 2, a carbon dioxide gas liquefaction pump 3, 1#, 2#, 3#, and 4# valves at the position of the low-pressure carbon dioxide storage tank 4, starting a power supply of the air compressor 1, pressurizing and filling carbon dioxide in the carbon dioxide steel cylinder 2 to the low-pressure carbon dioxide storage tank 4 until the pressure in the low-pressure carbon dioxide storage tank 4 reaches a set pressure (such as 8MPa), closing the carbon dioxide gas liquefaction pump 3, the 3#, and 7# valves at the position of a high-pressure liquid carbon dioxide storage tank 6, opening the low-pressure carbon dioxide storage tank 4, the 5#, and the 6# valves at the position of a liquid carbon dioxide booster pump 5, re-pressurizing the liquid carbon dioxide in the low-pressure carbon dioxide storage tank 4, filling the liquid carbon dioxide into the high-pressure liquid carbon dioxide storage tank 6 until the set pressure is reached 2 InitialAnd (4) pressure, closing the 6# valve and opening the 8# valve.
S5, forming liquid CO 2 Jetting, and carrying out jet form, speed and pressure data testing;
the method comprises the following steps: (1) adjusting the initial pressure and the temperature of the constant temperature and humidity box body 13 according to experimental conditions, and closing the power supply of the constant temperature and humidity box body 13 after the conditions are met;
(2) starting a pressure sensor 14, a temperature sensor 15, a high-speed camera 25, an infrared camera 24, a particle image speed field tester 10 and a temperature and humidity sensor 9;
(3) the remote control pneumatic valve 16 is opened by the remote control and data acquisition system 300, and the high-pressure liquid CO in the high-pressure liquid carbon dioxide storage tank 6 2 Instantaneous release of liquid CO from the jet nozzle 17 2 Phase change jetting;
(4) the liquid CO is obtained by testing the pressure sensor 14 and the temperature sensor 15 2 The liquid pressure and temperature in the jet nozzle 17 change with time in the phase change jet process, and the liquid CO is obtained by testing the high-speed camera 25 and the infrared camera 24 2 The liquid CO is obtained by testing the change rule of the fluid form with time in the phase change jet process by a particle image velocity field tester 12 2 In the phase change jet process, parameters of a fluid velocity field, jet size, core area length and jet angle are tested by a temperature and humidity sensor 9 to obtain liquid CO 2 And the change rule of the ambient temperature and the humidity in the phase change jet flow process.
S6, adjusting CO 2 Repeating the steps of S4-S5 according to the initial pressure and the temperature of the constant temperature and humidity box body 13, and carrying out liquid CO under different initial pressures and different temperatures 2 Phase change jet shape, speed and pressure variation parameter experiment, analyzing jet shape, jet speed and fluid pressure along with time, CO 2 Initial pressure, constant temperature and humidity box 13.
Claims (5)
1. Liquid CO under different pressures and temperatures 2 The phase-change jet impact power experimental method is characterized by comprising the following steps of:
s1, preparing a liquid carbon dioxide phase change jet impact dynamics experiment system;
the liquid carbon dioxide phase change jet impact dynamics experiment system comprises a carbon dioxide pressurization liquefaction system (100), a liquid carbon dioxide phase change jet and monitoring system (200) thereof and a remote control and data acquisition system (300);
the carbon dioxide pressurization liquefaction system (100) is used for liquefying and pressurizing carbon dioxide to form high-pressure liquid carbon dioxide capable of carrying out phase change jet, and comprises an air compressor (1), a carbon dioxide steel cylinder (2), a carbon dioxide gas liquefaction pump (3), a low-pressure carbon dioxide storage tank (4), a liquid carbon dioxide booster pump (5) and a high-pressure liquid carbon dioxide storage tank (6), wherein the air compressor (1) is used for generating compressed air, the valve control can be used for driving the carbon dioxide gas liquefaction pump (3) to pressurize the carbon dioxide in the carbon dioxide steel cylinder (2), the liquid carbon dioxide is stored in a low-pressure carbon dioxide storage tank (4), and can be used for driving a liquid carbon dioxide booster pump (5) to boost the liquid carbon dioxide in the low-pressure carbon dioxide storage tank (4) to an experimental preset pressure, and the liquid carbon dioxide is stored in a high-pressure liquid carbon dioxide storage tank (6) for later use;
the liquid carbon dioxide phase-change jet and monitoring system (200) comprises a constant-temperature and constant-humidity box body (13), and a liquid carbon dioxide phase-change jet device (400), a liquid carbon dioxide phase-change jet impact stress testing device (500), a liquid carbon dioxide phase-change jet fluid form testing device (600) and a box body environment testing device (700) which are arranged in the constant-temperature and constant-humidity box body (13);
the liquid carbon dioxide phase change jet device (400) comprises a pressure sensor (14), a temperature sensor (15), a pneumatic valve (16) and a jet nozzle (17), wherein the jet nozzle (17) is connected with a high-pressure liquid carbon dioxide outlet of a carbon dioxide pressurization liquefaction system (100) outside a constant-temperature and constant-humidity box body (13) through an air pressure pipe (11), and is combined with a remote control pneumatic valve (16) to realize instant release of the high-pressure liquid carbon dioxide, a liquid carbon dioxide phase change jet is formed by the jet nozzle (17), and the pressure sensor (14) and the temperature sensor (15) are used for monitoring fluid pressure and temperature change parameters at the jet nozzle (17) in real time;
the liquid carbon dioxide phase change jet flow impact stress testing device (500) comprises a guide rail (18), an impact stress sensor (19), a rotation angle sensor (21) and a laser ranging sensor (22), the impact stress sensor (19) and the laser distance measuring sensor (22) are rotatably and adjustably arranged on the rotating seat (20) through the same sensor bracket (23), the sensor holder (23) is mounted on the guide rail (18) in a sliding and adjustable manner by means of a rotary base (20), the impact stress sensor (19) is used for testing the impact stress of the liquid carbon dioxide phase-change jet flow, the laser ranging sensor (22) is used for measuring the distance from the impact stress sensor (19) to the jet flow nozzle (17), the rotation angle sensor (21) is arranged at the bottom of the sensor bracket (23) and used for testing the angle between the impact stress sensor (19) and the jet flow nozzle (17);
the liquid carbon dioxide phase change jet fluid form testing device (600) comprises a high-speed camera (25), an infrared camera (24) and a particle image speed field tester (10), wherein the high-speed camera (25), the infrared camera (24) and the particle image speed field tester (10) are respectively installed on a guide rail (18) by an installation support (12) in a sliding and adjustable manner;
the box body environment testing device (700) comprises a temperature and humidity sensor (9) which is used for testing the change rule of the environmental temperature and the humidity in the constant temperature and humidity box body (13);
the remote control and data acquisition system (300) comprises a computer, a control system and a data acquisition system, and is used for acquiring, displaying and storing various data and test results in the liquid carbon dioxide phase-change jet impact dynamics experiment process;
s2, establishing an experimental scheme;
considering CO in the high-pressure liquid carbon dioxide storage tank (6) 2 Initial pressure, ambient temperature parameters vs. liquid CO 2 The phase change jet flow shape, speed and pressure change rule influence the establishment of an experimental scheme;
s3, preparing an experiment;
connecting related pipelines of the carbon dioxide pressurization liquefaction system (100) and checking the air tightness of the pipelines; checking whether the air compressor (1), the carbon dioxide gas liquefaction pump (3) and the liquid carbon dioxide booster pump (5) can work normally or not; adjusting the positions of a high-speed camera (25), an infrared camera (24) and a particle image velocity field tester (10), and detecting whether the high-speed camera, the infrared camera and the particle image velocity field tester can work normally;
s4, preparing high-pressure liquid carbon dioxide;
closing a No. 5 valve at the bottom of a low-pressure carbon dioxide storage tank (4), opening an air compressor (1), a carbon dioxide steel cylinder (2), a carbon dioxide gas liquefaction pump (3) and No. 1, No. 2, No. 3 and No. 4 valves at the position of the low-pressure carbon dioxide storage tank (4), starting a power supply of the air compressor (1), pressurizing and filling carbon dioxide in the carbon dioxide steel cylinder (2) into the low-pressure carbon dioxide storage tank (4) until the pressure in the low-pressure carbon dioxide storage tank (4) reaches a set pressure, closing the carbon dioxide gas liquefaction pump (3), No. 3 and No. 7 valves at the position of a high-pressure liquid carbon dioxide storage tank (6), opening the low-pressure carbon dioxide storage tank (4) and No. 5 and No. 6 valves at the position of a liquid carbon dioxide pressurizing pump (5), re-pressurizing liquid carbon dioxide in the low-pressure carbon dioxide storage tank (4) and filling into the high-pressure liquid carbon dioxide storage tank (6), until the set CO is reached 2 Initial pressure, closing the 6# valve and opening the 8# valve;
s5, forming liquid CO 2 Jetting, and carrying out jet form, speed and pressure data testing;
adjusting the initial pressure and the temperature of the constant temperature and humidity box body (13) according to experimental conditions, and closing the power supply of the constant temperature and humidity box body (13) after the conditions are met;
starting a pressure sensor (14), a temperature sensor (15), a high-speed camera (25), an infrared camera (24), a particle image speed field tester (10) and a temperature and humidity sensor (9);
the remote control pneumatic valve (16) is opened by the remote control and data acquisition system (300), and high-pressure liquid CO is stored in the high-pressure liquid carbon dioxide storage tank (6) 2 Instantaneous release of liquid CO from the jet nozzle (17) 2 Phase change jet flow;
the liquid CO is obtained by testing the pressure sensor (14) and the temperature sensor (15) 2 The liquid pressure and temperature in the jet nozzle (17) change with time in the phase change jet process, and the liquid CO is obtained by testing the high-speed camera (25) and the infrared camera (24) 2 The liquid CO is obtained by testing the change rule of the fluid form with time in the phase change jet flow process by a particle image velocity field tester (12) 2 Fluid in phase change jet processParameters of a speed field, jet flow size, core area length and jet flow angle are tested by a temperature and humidity sensor (9) to obtain liquid CO 2 The change rule of the environmental temperature and the humidity in the phase change jet process;
s6, adjusting CO 2 The initial pressure and the temperature of the constant temperature and humidity box body (13) are repeated from S4 to S5, and liquid CO is carried out under the conditions of different initial pressures and different temperatures 2 Phase change jet shape, speed and pressure variation parameter experiment, analyzing the CO and the CO of the jet shape, the jet speed and the fluid pressure along with the time 2 The initial pressure and the constant temperature and humidity box body (13).
2. The liquid CO2 phase change jet impact dynamic experimental method under different pressures and temperatures according to claim 1, wherein: the maximum pressure of compressed air generated by the air compressor (1) is 0.8MPa, the input-output pressure ratio of the carbon dioxide gas liquefaction pump (3) is 1:10, and the maximum pressure of carbon dioxide in the carbon dioxide steel cylinder (2) is increased to 8 MPa; the input-output pressure ratio of the liquid carbon dioxide booster pump (5) is 1:100, the liquid carbon dioxide booster pump is used for boosting the liquid carbon dioxide in the low-pressure carbon dioxide storage tank (4) to 80MPa at maximum, and the experimental preset pressure is 8-60 MPa.
3. The liquid CO2 phase change jet impact dynamic experimental method under different pressures and temperatures according to claim 2, wherein: a gas-water separator (7) is arranged on a pipeline between the carbon dioxide steel cylinder (2) and the carbon dioxide gas liquefaction pump (3), the carbon dioxide pressurization liquefaction system (100) is integrally installed in the same box body, and the bottom of the box body and the bottom of the constant-temperature constant-humidity box body (13) are provided with rollers.
4. The liquid CO2 phase change jet impact dynamic experimental method under different pressures and temperatures according to claim 1, wherein: the high-speed camera (25) and the infrared camera (24) share the same mounting bracket (12).
5. The liquid CO2 phase change jet impact dynamic experimental method under different pressures and temperatures according to claim 1, wherein: the temperature and humidity sensor (9) is arranged at the top of the constant temperature and humidity box body (13).
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