CN112094566A - Water-based epoxy orange-peel paint and production method thereof - Google Patents

Water-based epoxy orange-peel paint and production method thereof Download PDF

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Publication number
CN112094566A
CN112094566A CN202010860590.0A CN202010860590A CN112094566A CN 112094566 A CN112094566 A CN 112094566A CN 202010860590 A CN202010860590 A CN 202010860590A CN 112094566 A CN112094566 A CN 112094566A
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CN
China
Prior art keywords
component
water
parts
dispersing
based epoxy
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202010860590.0A
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Chinese (zh)
Inventor
施生珺
丁艳美
魏祥勋
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Shanghai Hanzhong Coatings Co ltd
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Shanghai Hanzhong Coatings Co ltd
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Priority to CN202010860590.0A priority Critical patent/CN112094566A/en
Publication of CN112094566A publication Critical patent/CN112094566A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D163/00Coating compositions based on epoxy resins; Coating compositions based on derivatives of epoxy resins
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/14Paints containing biocides, e.g. fungicides, insecticides or pesticides
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/28Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes for wrinkle, crackle, orange-peel, or similar decorative effects
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/60Additives non-macromolecular
    • C09D7/61Additives non-macromolecular inorganic
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/65Additives macromolecular
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/18Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/20Oxides; Hydroxides
    • C08K3/22Oxides; Hydroxides of metals
    • C08K2003/2237Oxides; Hydroxides of metals of titanium
    • C08K2003/2241Titanium dioxide
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/30Sulfur-, selenium- or tellurium-containing compounds
    • C08K2003/3045Sulfates

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Plant Pathology (AREA)
  • Paints Or Removers (AREA)

Abstract

The invention provides a water-based epoxy orange-peel paint and a production method thereof. The waterborne epoxy interior wall coating provided by the invention comprises waterborne epoxy resin and a waterborne epoxy curing agent, and has the characteristics of health, ecology, environmental protection and no smell; the paint film after use is flat and soft, has good leveling property, high hardness, good adhesive force and wear resistance, has the characteristics of moisture resistance, mildew resistance, bacteria resistance and good organic matter volatile matter free property, is suitable for places requiring purification and registration comparison, such as food factories, pharmaceutical factories, electronic factories, cosmetic factories, paper mills and the like, and is coated on walls or ceilings, and can also be used in schools, markets, public places and the like.

Description

Water-based epoxy orange-peel paint and production method thereof
Technical Field
The invention relates to the technical field of coatings, in particular to a water-based epoxy orange-peel paint and a production method thereof.
Background
The interior wall paint also called as interior wall paint comprises liquid paint and powder paint, and because the interior paint contains volatile organic solvent components, volatile organic compounds, free formaldehyde, soluble heavy metals such as lead, cadmium, chromium, mercury and the like, and harmful substances such as benzene, toluene, xylene and the like are mainly generated in the construction and use processes, the quality of the interior air can be reduced, and the health of human bodies can be possibly influenced.
The water-based epoxy coating is a coating using water as a solvent or a dispersion medium. The ecological environment-friendly tea has the advantages of healthy ecology, environmental protection and no smell, and is more and more popular with people.
Disclosure of Invention
Aiming at the problems pointed out in the background technology, the invention provides the water-based epoxy orange-peel paint and the production method thereof, and the water-based epoxy orange-peel paint has the characteristics of good leveling property, high hardness, good adhesive force and wear resistance.
The technical scheme of the invention is realized as follows:
a water-based epoxy orange-peel paint and a production method thereof are characterized in that: the composition is prepared by mixing a component A and a component B, wherein the component A is prepared from the following raw materials in parts by mass:
90-95 parts of water-based epoxy resin;
8-13 parts of a diluent;
90-100 parts of color paste;
the component B comprises the following raw materials in parts by mass:
180 portions of water and 190 portions of water;
0.1-0.2 part of defoaming agent;
1-2 parts of a dispersant;
5-7 parts of wax powder;
5-8 parts of powder;
90-100 parts of barium sulfate;
90-100 parts of bentonite;
1-2 parts of a wetting agent;
180 portions of water-based epoxy curing agent and 230 portions.
The invention is further configured to: the powder mesh number is between 800 meshes and 1200 meshes.
A production method of a water-based epoxy orange-peel paint comprises the following operation steps:
1) mixing the component A:
s1, adding the diluent into the waterborne epoxy resin, and dispersing at a medium speed for 15 minutes;
s2, adding the color paste into the diluted epoxy resin, and dispersing at medium speed for 20 minutes;
2) and B, mixing the components:
s3, adding water into the container, opening the dispersing machine, adding the dispersing agent, and dispersing at medium speed;
s4, adding the defoaming agent, and dispersing at a medium speed;
s5, adjusting the speed of a dispersing machine to a high speed, then sequentially adding the wax powder, the barium sulfate and the bentonite, and dispersing for 40 minutes at a high speed;
s6, adjusting the speed of the dispersing machine to be a medium speed, and adding the wetting agent;
s7, adding a water-based epoxy curing agent, and dispersing at a medium speed for 15 minutes;
and S8, sampling and testing, mixing the component A and the component B, adding water according to the proportion of 10-15% of the mixed mass of the components A and B to adjust the viscosity, then brushing, and observing the apparent effect.
The invention is further configured to: when sampling and testing, if shrinkage cavity, adding wetting agent in the mixture of the component A and the component B; if the bubbles are more, the mixture of the component A and the component B is supplemented with the defoaming agent, the addition amount of the wetting agent and the defoaming agent is controlled each time, and then the mixture is dispersed for 5 minutes at medium speed.
The invention is further configured to: the wetting agent and the defoaming agent are added repeatedly until the mixture of the component A and the component B is coated with paint without shrinkage cavity and with little bubbles.
In conclusion, the beneficial effects of the invention are as follows: the waterborne epoxy interior wall coating provided by the invention comprises waterborne epoxy resin and a waterborne epoxy curing agent, and has the characteristics of health, ecology, environmental protection and no smell; the paint film after use is flat and soft, has good leveling property, high hardness, good adhesive force and wear resistance, has the characteristics of moisture resistance, mildew resistance, bacteria resistance and good organic matter volatile matter free property, is suitable for places requiring purification and registration comparison, such as food factories, pharmaceutical factories, electronic factories, cosmetic factories, paper mills and the like, and is coated on walls or ceilings, and can also be used in schools, markets, public places and the like.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The first embodiment is as follows:
a water-based epoxy orange-peel paint and a production method thereof are characterized in that: the composition is prepared by mixing a component A and a component B, wherein the component A is prepared from the following raw materials in parts by mass:
94.5 parts of waterborne epoxy resin;
10.5 parts of a diluent;
95 parts of color paste;
the component B comprises the following raw materials in parts by mass:
185.5 parts of water;
0.2 part of defoaming agent;
1.5 parts of a dispersing agent;
6 parts of wax powder;
6 parts of powder;
100 parts of barium sulfate;
100 parts of bentonite;
2 parts of a wetting agent;
200 parts of a water-based epoxy curing agent.
The invention is further configured to: the powder mesh number is between 800 meshes and 1200 meshes.
A production method of a water-based epoxy orange-peel paint comprises the following operation steps:
1) mixing the component A:
s1, adding the diluent into the waterborne epoxy resin, and dispersing at a medium speed for 15 minutes;
s2, adding the color paste into the diluted epoxy resin, and dispersing at medium speed for 20 minutes;
2) and B, mixing the components:
s3, adding water into the container, opening the dispersing machine, adding the dispersing agent, and dispersing at medium speed;
s4, adding the defoaming agent, and dispersing at a medium speed;
s5, adjusting the speed of a dispersing machine to a high speed, then sequentially adding the wax powder, the barium sulfate and the bentonite, and dispersing for 40 minutes at a high speed;
s6, adjusting the speed of the dispersing machine to be a medium speed, and adding the wetting agent;
s7, adding a water-based epoxy curing agent, and dispersing at a medium speed for 15 minutes;
and S8, sampling and testing, mixing the component A and the component B, adding water according to the proportion of 10-15% of the mixed mass of the components A and B to adjust the viscosity, then brushing, and observing the apparent effect.
The invention is further configured to: when sampling and testing, if shrinkage cavity, adding wetting agent in the mixture of the component A and the component B; if the bubbles are more, the mixture of the component A and the component B is supplemented with the defoaming agent, the addition amount of the wetting agent and the defoaming agent is controlled each time, and then the mixture is dispersed for 5 minutes at medium speed.
The invention is further configured to: the wetting agent and the defoaming agent are added repeatedly until the mixture of the component A and the component B is coated with paint without shrinkage cavity and with little bubbles.
The second embodiment is as follows:
a water-based epoxy orange-peel paint and a production method thereof are characterized in that: the composition is prepared by mixing a component A and a component B, wherein the component A is prepared from the following raw materials in parts by mass:
94.5 parts of waterborne epoxy resin;
10.5 parts of a diluent;
95 parts of color paste;
the component B comprises the following raw materials in parts by mass:
180 parts of water;
0.2 part of defoaming agent;
1.5 parts of a dispersing agent;
6 parts of wax powder;
6 parts of powder;
90.5 parts of barium sulfate;
100 parts of bentonite;
2 parts of a wetting agent;
215 parts of a water-based epoxy curing agent.
The rest is the same as the first embodiment.
By adopting the technical scheme, the waterborne epoxy interior wall coating provided by the invention comprises waterborne epoxy resin and a waterborne epoxy curing agent, and has the characteristics of health, ecology, environmental protection and no smell; the paint film after use is flat and soft, has good leveling property, high hardness, good adhesive force and wear resistance, has the characteristics of moisture resistance, mildew resistance, bacteria resistance and good organic matter volatile matter free property, is suitable for places requiring purification and registration comparison, such as food factories, pharmaceutical factories, electronic factories, cosmetic factories, paper mills and the like, and is coated on walls or ceilings, and can also be used in schools, markets, public places and the like.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like that fall within the spirit and principle of the present invention are intended to be included therein.

Claims (5)

1. A water-based epoxy orange-peel paint and a production method thereof are characterized in that: the composition is prepared by mixing a component A and a component B, wherein the component A is prepared from the following raw materials in parts by mass:
90-95 parts of water-based epoxy resin;
8-13 parts of a diluent;
90-100 parts of color paste;
the component B comprises the following raw materials in parts by mass:
180 portions of water and 190 portions of water;
0.1-0.2 part of defoaming agent;
1-2 parts of a dispersant;
5-7 parts of wax powder;
5-8 parts of powder;
90-100 parts of barium sulfate;
90-100 parts of bentonite;
1-2 parts of a wetting agent;
180 portions of water-based epoxy curing agent and 230 portions.
2. The waterborne epoxy orange peel coating of claim 1, wherein: the powder mesh number is between 800 meshes and 1200 meshes.
3. The production method of the water-based epoxy orange-peel paint according to claim 1, characterized by comprising the following operation steps:
1) mixing the component A:
s1, adding the diluent into the waterborne epoxy resin, and dispersing at a medium speed for 15 minutes;
s2, adding the color paste into the diluted epoxy resin, and dispersing at medium speed for 20 minutes;
2) and B, mixing the components:
s3, adding water into the container, opening the dispersing machine, adding the dispersing agent, and dispersing at medium speed;
s4, adding the defoaming agent, and dispersing at a medium speed;
s5, adjusting the speed of a dispersing machine to a high speed, then sequentially adding the wax powder, the barium sulfate and the bentonite, and dispersing for 40 minutes at a high speed;
s6, adjusting the speed of the dispersing machine to be a medium speed, and adding the wetting agent;
s7, adding a water-based epoxy curing agent, and dispersing at a medium speed for 15 minutes;
and S8, sampling and testing, mixing the component A and the component B, adding water according to the proportion of 10-15% of the mixed mass of the components A and B to adjust the viscosity, then brushing, and observing the apparent effect.
4. The method for producing the water-based epoxy orange-peel paint according to claim 3, characterized in that: when sampling and testing, if shrinkage cavity, adding wetting agent in the mixture of the component A and the component B; if the bubbles are more, the mixture of the component A and the component B is supplemented with the defoaming agent, the addition amount of the wetting agent and the defoaming agent is controlled each time, and then the mixture is dispersed for 5 minutes at medium speed.
5. The water-based epoxy orange-peel paint and the production method thereof according to claim 4, characterized in that: the wetting agent and the defoaming agent are added repeatedly until the mixture of the component A and the component B is coated with paint without shrinkage cavity and with little bubbles.
CN202010860590.0A 2020-08-25 2020-08-25 Water-based epoxy orange-peel paint and production method thereof Pending CN112094566A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202010860590.0A CN112094566A (en) 2020-08-25 2020-08-25 Water-based epoxy orange-peel paint and production method thereof

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Application Number Priority Date Filing Date Title
CN202010860590.0A CN112094566A (en) 2020-08-25 2020-08-25 Water-based epoxy orange-peel paint and production method thereof

Publications (1)

Publication Number Publication Date
CN112094566A true CN112094566A (en) 2020-12-18

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CN202010860590.0A Pending CN112094566A (en) 2020-08-25 2020-08-25 Water-based epoxy orange-peel paint and production method thereof

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103013286A (en) * 2013-01-14 2013-04-03 上海维度化工科技有限公司 Water-based epoxy inner wall paint and preparation method thereof
CN108795236A (en) * 2018-06-15 2018-11-13 河北晨阳工贸集团有限公司 A kind of superpower anti-corrosion function aqueous double-component epoxy orange-peel paint and preparation method thereof convenient for application
CN109337515A (en) * 2018-10-08 2019-02-15 辽宁大学 A kind of high-strength waterborne polyurethane modified epoxy orange-peel paint and its preparation method and application
CN109749579A (en) * 2018-12-19 2019-05-14 枣庄学院 A kind of environment-friendly and energy-efficient aqueous epoxy floor coating and preparation method thereof
CN109777264A (en) * 2019-02-25 2019-05-21 河北晨阳工贸集团有限公司 A kind of thick coated type water-base epoxy orange-peel paint and preparation method thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103013286A (en) * 2013-01-14 2013-04-03 上海维度化工科技有限公司 Water-based epoxy inner wall paint and preparation method thereof
CN108795236A (en) * 2018-06-15 2018-11-13 河北晨阳工贸集团有限公司 A kind of superpower anti-corrosion function aqueous double-component epoxy orange-peel paint and preparation method thereof convenient for application
CN109337515A (en) * 2018-10-08 2019-02-15 辽宁大学 A kind of high-strength waterborne polyurethane modified epoxy orange-peel paint and its preparation method and application
CN109749579A (en) * 2018-12-19 2019-05-14 枣庄学院 A kind of environment-friendly and energy-efficient aqueous epoxy floor coating and preparation method thereof
CN109777264A (en) * 2019-02-25 2019-05-21 河北晨阳工贸集团有限公司 A kind of thick coated type water-base epoxy orange-peel paint and preparation method thereof

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Application publication date: 20201218

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