CN112089667A - Plant decocted shampoo and preparation method thereof - Google Patents

Plant decocted shampoo and preparation method thereof Download PDF

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CN112089667A
CN112089667A CN202010910105.6A CN202010910105A CN112089667A CN 112089667 A CN112089667 A CN 112089667A CN 202010910105 A CN202010910105 A CN 202010910105A CN 112089667 A CN112089667 A CN 112089667A
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parts
extract
shampoo
mixture
plant
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张仁飞
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9794Liliopsida [monocotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9755Gymnosperms [Coniferophyta]
    • A61K8/9761Cupressaceae [Cypress family], e.g. juniper or cypress
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/006Antidandruff preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/008Preparations for oily hair
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/02Preparations for cleaning the hair
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/12Preparations containing hair conditioners
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/85Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine

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  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
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  • Botany (AREA)
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  • Mycology (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Dermatology (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses a plant boiled shampoo and a preparation method thereof, wherein the active ingredients of the plant boiled shampoo are prepared from the following raw materials in parts by mass: 3-6 parts of saponin, 10-15 parts of polygonum multiflorum, 3-8 parts of soapberry, 1-5 parts of tea seed, 1-5 parts of pepper, 1-5 parts of old ginger, 1-5 parts of black bean, 0.1-1 part of garlic, 1-5 parts of sophora flavescens, 1-5 parts of mulberry fruit, 0.1-1 part of cortex dictamni, 1-5 parts of glossy privet fruit, 0.1-1 part of folium artemisiae argyi, 0.1-1 part of lateral bur leaf, 0.05-0.5 part of hot pepper, 0.1-1 part of climbing rock old ginger, 0.1-1 part of rhizoma polygonati and 0.05-0.5 part of almond. The invention prepares the traditional Chinese medicine extract by boiling and fermenting a plurality of plants such as Chinese honeylocust fruit, fleece-flower root, soapberry and the like, and a plurality of fresh plants such as mulberry fruit, glossy privet fruit, lateral bur leaf and the like, and the traditional Chinese medicine extract is prepared into the shampoo and hair conditioner, which can clean hair and scalp, remove dandruff, balance the grease secretion of the scalp, promote the blood circulation of the head and has special effect on the health of the scalp and hair.

Description

Plant decocted shampoo and preparation method thereof
Technical Field
The invention relates to the technical field of shampoo preparation, and particularly relates to a plant decocted shampoo and a preparation method thereof.
Background
At present, the texture, color and character of hair are mostly changed by pure chemical products in hair-beautifying and hair-protecting products, so that the aims of hair health and beauty are expected to be fulfilled. However, the hair care products prepared by using pure chemical preparations in large quantities have the defects of damaging hair quality, treating symptoms and not treating root causes, and the effects are poor, so that the damage to the hair is serious after long-term use.
The existing chemical shampoo has poor effect on improving hair texture, treating alopecia and removing dandruff, and can cause more serious damage to hair after long-term use. Especially, seborrheic alopecia and the like which exist at present seriously affect the improvement of living standard and the pursuit of aesthetic quality.
In conclusion, the existing hair washing and protecting products can not improve the hair quality fundamentally, and the development of a plant boiled shampoo is urgently needed.
Disclosure of Invention
Therefore, the invention provides a plant decocted shampoo and a preparation method thereof.
In order to achieve the above purpose, the invention provides the following technical scheme:
a plant decocted shampoo is characterized in that active ingredients of the shampoo are prepared from the following raw materials in parts by weight: 3-6 parts of saponin, 10-15 parts of polygonum multiflorum, 3-8 parts of soapberry, 1-5 parts of tea seed, 1-5 parts of pepper, 1-5 parts of old ginger, 1-5 parts of black bean, 0.1-1 part of garlic, 1-5 parts of sophora flavescens, 1-5 parts of mulberry fruit, 0.1-1 part of cortex dictamni, 1-5 parts of glossy privet fruit, 0.1-1 part of folium artemisiae argyi, 0.1-1 part of lateral bur leaf, 0.05-0.5 part of hot pepper, 0.1-1 part of climbing rock old ginger, 0.1-1 part of rhizoma polygonati and 0.05-0.5 part of almond.
Preferably, the active ingredients of the plant decocted shampoo are prepared from the following raw materials in parts by weight: 4-5 parts of saponin, 11-14 parts of polygonum multiflorum, 4-7 parts of soapberry, 2-4 parts of tea seed, 2-4 parts of pepper, 2-4 parts of old ginger, 2-4 parts of black bean, 0.2-0.8 part of garlic, 2-4 parts of bitter ginseng root, 2-4 parts of mulberry fruit, 0.2-0.8 part of cortex dictamni, 2-4 parts of glossy privet fruit, 0.2-0.8 part of folium artemisiae argyi, 0.2-0.8 part of lateral bur leaf, 0.1-0.4 part of hot pepper, 0.2-0.8 part of climbing rock old ginger, 0.12-0.8 part of rhizoma polygonati and 0.1-0.4 part of almond.
The invention also provides a preparation method of the plant decocted shampoo, which comprises the following steps:
1) weighing the traditional Chinese medicine raw materials according to the proportion of claim 1 or 2 for later use;
2) soaking the Chinese honeylocust fruits, the polygonum multiflorum, the soapberry fruits and the tea seeds in the step 1) in lime water for 1-3 days, removing the lime water, adding cold water and the pepper into the Chinese honeylocust fruits, the polygonum multiflorum, the soapberry fruits and the tea seeds, heating at 60 ℃, simultaneously adding brown sugar to form a mixture, and fermenting the mixture for 3-6 months under the conditions that the temperature is 25 ℃ and the humidity is 45-60% to obtain a first mixture;
3) boiling the black beans in the step 1) until the skins crack, then adding old ginger and garlic, boiling for 10min, adding mature vinegar, and standing in the shade for 3-6 months to obtain a second mixture;
4) soaking the sophora flavescens roots, the mulberries and the cortex dictamni in the wine in the step 1) for not less than 90 days to obtain a third mixture;
5) soaking the glossy privet fruit, the folium artemisiae argyi, the cacumen biotae, the hot pepper, the peruvian ginger, the rhizoma polygonati and the almond in the rice washing water in the step 1) for 2 to 3 months to obtain a fourth mixture;
6) and removing dregs in the first mixture, the second mixture, the third mixture and the fourth mixture respectively to obtain a first extract, a second extract, a third extract and a fourth extract, and mixing the first extract, the second extract, the third extract and the fourth extract to obtain the plant decocting shampoo.
Preferably, in the plant decocted shampoo, the mass ratio of the first extract to the second extract to the third extract to the fourth extract is 7:0.2:1: 1.8.
Preferably, in the step 2), the brown sugar is added in an amount of 0.1-0.5% by mass.
Preferably, in the step 3, the volume fraction of the mature vinegar added is 10-25%.
Preferably, in the fermentation process, 3% of lactic acid bacteria liquid is inoculated, the lactic acid bacteria liquid is lactobacillus bulgaricus and streptococcus thermophilus according to the ratio of 1:1, and is inoculated into the emulsion and cultured at the constant temperature of 40 ℃ for 15 hours to obtain the lactic acid bacteria liquid.
Preferably, in the step 4, the adding amount of the wine is 20-30 times of the mass of the sophora flavescens root, the mulberry and the cortex dictamni.
The hair care agent taking the plant decocted shampoo as an active component also belongs to the protection scope of the invention.
In the invention, the Chinese honeylocust fruit is warm in nature, pungent and salty in taste. Has little toxicity. It enters lung and large intestine meridians. Inducing resuscitation, eliminating phlegm, resolving hard mass, relieving swelling, moistening dryness and relaxing bowels.
He shou Wu is bitter, sweet, astringent and slightly warm. It enters liver and kidney meridians. The efficacy of the polygonum multiflorum is as follows: tonify essence and blood, check malaria, remove toxicity, moisten intestines to relieve constipation. Radix Polygoni Multiflori is used for dizziness, dim eyesight, early white beard and hair, persistent malaria, superficial infection, scrofula, constipation due to intestinal dryness.
Sapindus mukorossi, cool in nature, bitter and slightly pungent in taste. Has little toxicity. They enter heart and lung meridians. Clearing lung-heat, eliminating phlegm, relieving sore throat, promoting qi circulation, and killing parasites. Belonging to the category of heat-clearing herbs.
Zanthoxylum, pungent and hot. Has little toxicity. It enters spleen, stomach and kidney meridians. The Chinese prickly ash has the following effects: warm middle energizer to alleviate pain, dry dampness and kill parasites. The pricklyash peel is used for treating abdominal psychroalgia, cold-dampness diarrhea, abdominal pain due to parasitic infestation, eczema and pruritus.
Old ginger, slightly warm, pungent taste, entering meridians: spleen, lung, stomach. The functions are mainly used for relieving exterior syndrome and dispelling cold, warming middle energizer and arresting vomiting, and reducing phlegm and relieving cough. Can be used for treating common cold due to wind-cold, emesis due to stomach cold, and cough due to cold phlegm.
Black soya bean, sweet in taste, slightly cold in nature, neutral in nature, enters spleen and kidney meridians. Tonify kidney, nourish yin, invigorate spleen, remove dampness, remove heat and toxic materials.
Garlic is warm in nature and pungent in flavor, and passes through spleen, lung and stomach. The efficacy is as follows: warming middle energizer to promote digestion, warming spleen and stomach, removing food retention and removing toxic substance, and killing parasites.
Ku Shen root, bitter and cold. It enters heart, liver, stomach, large intestine and bladder meridians. Clearing away heat, removing dampness, expelling pathogenic wind, killing parasites, and promoting urination. The main treatment of the sophora flavescens is as follows: can be used for treating damp-heat in lower-jiao, leukorrhagia, pudendal pruritus, skin pruritus, scabies, tinea, and pain due to heat stranguria.
Mulberry fruit, sweet and cold. It enters heart, liver and kidney meridians. Nourish yin and enrich blood, moisten intestine and promote fluid production. Can be used for treating yin deficiency and blood deficiency, yin deficiency and thirst, fluid deficiency and thirst, giddiness and tinnitus, and constipation due to intestinal dryness.
Bai Xian Pi is cold and bitter. It enters spleen and stomach meridians. Clear heat and remove toxicity, dispel wind and dry dampness. Can be used for treating damp-heat sore, eczema, scabies, skin pruritus, damp-heat jaundice, and rheumatism.
Glossy privet fruit, sweet, bitter and cool. It enters liver and kidney meridians. Tonify liver and kidney, improve vision, clear deficiency heat. Can be used for treating dizziness, premature gray hair, blurred vision, and fever due to yin deficiency.
Folium Artemisiae Argyi, bitter and pungent, warm. It enters liver, spleen and kidney meridians. The efficacy of the folium artemisiae argyi is as follows: warm meridians to stop bleeding, dispel cold to alleviate pain. Folium Artemisiae Argyi is used for hematemesis, epistaxis, metrorrhagia, metrostaxis, lower blood, abdominal psychroalgia, and abdominal pain during menstruation.
Ce Bai Ye is bitter, astringent and slightly cold. It enters lung, liver and large intestine meridians. Efficacy of cacumen biotae: cool blood to stop bleeding, dispel phlegm to arrest cough. Cacumen biotae is used for internal and external bleeding, cough and profuse sputum.
Hot pepper, hot in nature, pungent in flavor, entering the heart and spleen, has the effects of warming the middle-jiao to dispel cold, stimulating appetite and helping digestion, and is suitable for: cold type stomach ache, inappetence, dysentery, rheumarthritis, traumatic blood stasis and swelling, bugantia, anemia, scurvy disease, and gingival hemorrhage.
Zingiber reptans, also called as drynaria rhizome, centipede, etc., is slightly bitter in taste and warm in nature. Has effects in tonifying deficiency, relaxing muscles and tendons, and promoting blood circulation. Can be used for treating infantile malnutrition, kidney deficiency, tinnitus, traumatic injury, and fracture. It can be drunk after soaking in wine, but is not suitable for people with yin deficiency and internal heat.
Huang Jing is neutral in nature and sweet in flavor, and enters spleen, lung and kidney. The functional indications are as follows: tonify qi and yin, invigorate spleen, moisten lung and tonify kidney. Can be used for treating weakness of spleen and stomach, asthenia, xerostomia, anorexia, lung deficiency, cough, essence and blood deficiency, and internal heat diabetes.
Apricot kernel, bitter and slightly warm. Has little toxicity. It enters lung and large intestine meridians. The almond has the following effects: relieve cough and dyspnea, moisten intestines to relieve constipation. Semen Armeniacae amarum can be used for treating cough, asthma, and constipation due to intestinal dryness.
The invention relates to a hair washing lotion which is prepared by decocting Chinese medicinal herbs such as Chinese honeylocust fruit, tuber fleeceflower root, soapberry fruit, tea seed, old ginger, garlic, lightyellow sophora root, mulberry, cortex dictamni, glossy privet fruit, Chinese mugwort leaf, cacumen biotae, hot pepper, climbing rock ginger, common cnidium fruit, cassia seed, medcinal evodia fruit, chinaberry fruit and the like produced in local mountainous areas, is convenient to obtain materials and prepare, is economical and effective, can remove greasy sweat, refresh hair, relieve itching, treat sore and remove scabies, has good effect, and becomes a Zhang's family ancestral technique by decocting shampoo with the Chinese medicinal herbs.
The plant boiled shampoo is further added with medicinal materials such as white mulberry root-bark, eclipta alba, medlar, black sesame, black rice, black bean, hot pepper, rhizoma polygonati, almond, brown sugar, aloe and the like, and the raw materials transported after the boiling processing in Xingwen county are prepared into plant source spring plant boiled hair washing hair protoplasm products which are sold on the market, so the plant boiled shampoo has good effects of removing dandruff, removing grease, protecting and nourishing hair, and is certain by consumers.
The invention has the following advantages:
the invention prepares the plant boiled shampoo by boiling and fermenting a plurality of plants such as Chinese honeylocust fruit, fleece-flower root, soapberry and the like, and the plant boiled shampoo is prepared by boiling a plurality of fresh plants such as mulberry fruit, glossy privet fruit, lateral bur leaf and the like.
In the fermentation process, lactic acid bacteria are added to obtain the shampoo which has better nutritive value, promotes the microcirculation of scalp, regulates oil and has good effect of reducing dandruff.
Detailed Description
The present invention is described in terms of particular embodiments, other advantages and features of the invention will become apparent to those skilled in the art from the following disclosure, and it is to be understood that the described embodiments are merely exemplary of the invention and that it is not intended to limit the invention to the particular embodiments disclosed. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1 preparation of a herbal decocted shampoo of the invention
The invention relates to a preparation method of a plant boiled shampoo, which comprises the following steps:
1) weighing 300g of Chinese honeylocust fruit, 1000g of polygonum multiflorum, 300g of soapberry, 100g of tea seed, 100g of pepper, 100g of old ginger, 100g of black bean, 10g of garlic, 100g of sophora flavescens, 100g of mulberry, 10g of cortex dictamni, 100g of glossy privet fruit, 10g of folium artemisiae argyi, 10g of lateral bur leaf, 5g of hot pepper, 10g of climbing rock old ginger, 10g of rhizoma polygonati and 5g of almond according to a proportion for later use;
2) soaking the Chinese honeylocust fruits, the tuber fleeceflower roots, the soapberries and the tea seeds in the step 1) in 1% by mass of lime water for 1-3 days, removing the lime water, adding cold water and the pepper into the Chinese honeylocust fruits, the tuber fleeceflower roots, the soapberries and the tea seeds, heating at 60 ℃, simultaneously adding 0.1-0.5% by mass of brown sugar to form a mixture, and fermenting the mixture at 25 ℃ and 45-60% of humidity for 3-6 months to obtain a first mixture; wherein, in the fermentation process, 3 percent of lactic acid bacteria liquid is also inoculated, the lactic acid bacteria liquid is lactobacillus bulgaricus and streptococcus thermophilus according to the ratio of 1:1, and the lactic acid bacteria liquid is obtained by inoculating the lactic acid bacteria liquid into the emulsion and culturing at the constant temperature of 40 ℃ for 15 hours.
3) Boiling the black beans in the step 1) until the skins crack, then adding old ginger and garlic, boiling for 10min, adding mature vinegar with the volume fraction of 10-25%, and standing in a shade for 3-6 months to obtain a second mixture;
4) soaking the sophora flavescens roots, the mulberries and the cortex dictamni in the step 1) in 45-degree wine of 20-30 times for 3-5 days to obtain a third mixture;
5) soaking the glossy privet fruit, the folium artemisiae argyi, the cacumen biotae, the hot pepper, the peruvian ginger, the rhizoma polygonati and the almond in the rice washing water in the step 1) for 2 to 3 months to obtain a fourth mixture;
6) removing residues from the first mixture, the second mixture, the third mixture and the fourth mixture to obtain a first extract, a second extract, a third extract and a fourth extract, and mixing the first extract, the second extract, the third extract and the fourth extract to obtain the plant decocting shampoo. Wherein, in the plant decocted shampoo, the mass ratio of the first extract to the second extract to the third extract to the fourth extract is 7:0.2:1: 1.8.
Example 2 preparation of the plant boiled shampoo of the invention
The invention relates to a preparation method of a plant boiled shampoo, which comprises the following steps:
1) weighing 400g of Chinese honeylocust fruit, 1200g of polygonum multiflorum, 500g of soapberry, 250g of tea seed, 250g of pepper, 250g of old ginger, 250g of black bean, 50g of garlic, 250g of sophora flavescens, 250g of mulberry, 50g of cortex dictamni, 250g of glossy privet fruit, 50g of folium artemisiae argyi, 50g of lateral bur leaf, 25g of hot pepper, 50g of climbing rock old ginger, 50g of rhizoma polygonati and 25g of almond according to a proportion for later use;
2) soaking the Chinese honeylocust fruits, the tuber fleeceflower roots, the soapberries and the tea seeds in the step 1) in 1% by mass of lime water for 1-3 days, removing the lime water, adding cold water and the pepper into the Chinese honeylocust fruits, the tuber fleeceflower roots, the soapberries and the tea seeds, heating at 60 ℃, simultaneously adding 0.1-0.5% by mass of brown sugar to form a mixture, and fermenting the mixture at 25 ℃ and 45-60% of humidity for 3-6 months to obtain a first mixture; wherein, in the fermentation process, 3 percent of lactic acid bacteria liquid is also inoculated, the lactic acid bacteria liquid is lactobacillus bulgaricus and streptococcus thermophilus according to the ratio of 1:1, and the lactic acid bacteria liquid is obtained by inoculating the lactic acid bacteria liquid into the emulsion and culturing at the constant temperature of 40 ℃ for 15 hours.
3) Boiling the black beans in the step 1) until the skins crack, then adding old ginger and garlic, boiling for 10min, adding mature vinegar with the volume fraction of 10-25%, and standing in a shade for 3-6 months to obtain a second mixture;
4) soaking the sophora flavescens roots, the mulberries and the cortex dictamni in the step 1) in 45-degree wine of 20-30 times for 3-5 days to obtain a third mixture;
5) soaking the glossy privet fruit, the folium artemisiae argyi, the cacumen biotae, the hot pepper, the peruvian ginger, the rhizoma polygonati and the almond in the rice washing water in the step 1) for 2 to 3 months to obtain a fourth mixture;
6) removing residues from the first mixture, the second mixture, the third mixture and the fourth mixture to obtain a first extract, a second extract, a third extract and a fourth extract, and mixing the first extract, the second extract, the third extract and the fourth extract to obtain the plant decocting shampoo. Wherein, in the plant decocted shampoo, the mass ratio of the first extract to the second extract to the third extract to the fourth extract is 7:0.2:1: 1.8.
Example 3 preparation of the herbal decocted shampoo of the invention
The invention relates to a preparation method of a plant boiled shampoo, which comprises the following steps:
1) weighing 600g of Chinese honeylocust fruit, 1500g of polygonum multiflorum, 800g of soapberry, 500g of tea seed, 500g of pepper, 500g of old ginger, 500g of black bean, 100g of garlic, 500g of sophora flavescens, 500g of mulberry, 100g of cortex dictamni, 500g of glossy privet fruit, 100g of folium artemisiae argyi, 100g of lateral bur leaf, 50g of hot pepper, 100g of climbing rock old ginger, 100g of rhizoma polygonati and 50g of almond according to a proportion for later use;
2) soaking the Chinese honeylocust fruits, the tuber fleeceflower roots, the soapberries and the tea seeds in the step 1) in 1% by mass of lime water for 1-3 days, removing the lime water, adding cold water and the pepper into the Chinese honeylocust fruits, the tuber fleeceflower roots, the soapberries and the tea seeds, heating at 60 ℃, simultaneously adding 0.1-0.5% by mass of brown sugar to form a mixture, and fermenting the mixture at 25 ℃ and 45-60% of humidity for 3-6 months to obtain a first mixture; wherein, in the fermentation process, 3 percent of lactic acid bacteria liquid is also inoculated, the lactic acid bacteria liquid is lactobacillus bulgaricus and streptococcus thermophilus according to the ratio of 1:1, and the lactic acid bacteria liquid is obtained by inoculating the lactic acid bacteria liquid into the emulsion and culturing at the constant temperature of 40 ℃ for 15 hours.
3) Boiling the black beans in the step 1) until the skins crack, then adding old ginger and garlic, boiling for 10min, adding mature vinegar with the volume fraction of 10-25%, and standing in a shade for 3-6 months to obtain a second mixture;
4) soaking the sophora flavescens roots, the mulberries and the cortex dictamni in the step 1) in 45-degree wine of 20-30 times for 3-5 days to obtain a third mixture;
5) soaking the glossy privet fruit, the folium artemisiae argyi, the cacumen biotae, the hot pepper, the peruvian ginger, the rhizoma polygonati and the almond in the rice washing water in the step 1) for 2 to 3 months to obtain a fourth mixture;
6) removing residues from the first mixture, the second mixture, the third mixture and the fourth mixture to obtain a first extract, a second extract, a third extract and a fourth extract, and mixing the first extract, the second extract, the third extract and the fourth extract to obtain the plant decocting shampoo. Wherein, in the plant decocted shampoo, the mass ratio of the first extract to the second extract to the third extract to the fourth extract is 7:0.2:1: 1.8.
Example 5 clinical trial of the plant-boiled shampoo of the present invention
Purpose of the experiment: the seborrhoeic hair quality population is selected, a grouping test is designed, and the plant boiled shampoo and the reference substance of the embodiment 1, the embodiment 2 and the embodiment 3 of the invention are respectively used for the same time and times.
The experimental process comprises the following steps: selecting 150 persons with age of 20-40 years, wherein the experimental group comprises 100 persons, the control group comprises 50 persons, and the control group comprises commercially available shampoo prepared by chemical method.
Evaluation criteria:
oil control effect: the reduction of scalp oil secretion is effective, and the effective classification is good and general. Scalp oil was unchanged and was not effective.
Dandruff treatment effect: dandruff reduction is effective, which is classified as good and general. Dandruff was unchanged and ineffective.
Comfort level: the detergent is fresh and cool after being washed, is effective in softening and is effectively classified into good and general. It is not felt and is not effective.
The test results are shown in tables 2 to 7.
TABLE 1 Hair conditioner prepared with the herbal extracts prepared in example 1 as active ingredients
TABLE 1
Figure BDA0002662949910000091
TABLE 2 control shampoo use effect
TABLE 2
Figure BDA0002662949910000092
TABLE 3 Hair conditioner prepared with the herbal extracts prepared in example 2 as active ingredients
TABLE 3
Figure BDA0002662949910000093
TABLE 4 control shampoo use effect
TABLE 4
Figure BDA0002662949910000101
TABLE 5 Hair conditioner prepared with the herbal extracts prepared in example 3 as active ingredients
TABLE 5
Figure BDA0002662949910000102
TABLE 6 shampoo use effect of control group
TABLE 6
Figure BDA0002662949910000103
As shown in the results of tables 1 to 6, the hair care agent of the present invention, which uses the herbal extracts of example 1, example 2, or example 3 as the active ingredient, has an effective rate of more than 80% in both oil control and anti-dandruff.
Example 6 report of quality test of herbal boiled shampoo of the invention
1. The results of the microbial tests performed on the plant boiled hair shampoo hair washing puree prepared in example 1 of the present invention according to the technical standards for cosmetic safety are shown in the following table 7:
TABLE 7
Figure BDA0002662949910000111
2. The results of the microbiological examination of the plant boiled hair shampoo hair washing puree prepared in example 1 of the present invention according to the technical standards for cosmetic safety are shown in the following table 8:
TABLE 8
Figure BDA0002662949910000112
As can be seen from the test data in tables 7 and 8, the plant-boiled shampoo prepared in example 1 of the present invention has satisfactory results of both the microbiological test and the hygienic chemical test.
Although the invention has been described in detail above with reference to a general description and specific examples, it will be apparent to one skilled in the art that modifications or improvements may be made thereto based on the invention. Accordingly, such modifications and improvements are intended to be within the scope of the invention as claimed.

Claims (9)

1. The plant decocted shampoo is characterized in that active ingredients of the shampoo are prepared from the following raw materials in parts by mass: 3-6 parts of saponin, 10-15 parts of polygonum multiflorum, 3-8 parts of soapberry, 1-5 parts of tea seed, 1-5 parts of pepper, 1-5 parts of old ginger, 1-5 parts of black bean, 0.1-1 part of garlic, 1-5 parts of sophora flavescens, 1-5 parts of mulberry fruit, 0.1-1 part of cortex dictamni, 1-5 parts of glossy privet fruit, 0.1-1 part of folium artemisiae argyi, 0.1-1 part of lateral bur leaf, 0.05-0.5 part of hot pepper, 0.1-1 part of climbing rock old ginger, 0.1-1 part of rhizoma polygonati and 0.05-0.5 part of almond.
2. The plant-decocted shampoo of claim 1, wherein,
the active ingredients of the plant boiled shampoo are prepared from the following raw materials in parts by mass: 4-5 parts of saponin, 11-14 parts of polygonum multiflorum, 4-7 parts of soapberry, 2-4 parts of tea seed, 2-4 parts of pepper, 2-4 parts of old ginger, 2-4 parts of black bean, 0.2-0.8 part of garlic, 2-4 parts of bitter ginseng root, 2-4 parts of mulberry fruit, 0.2-0.8 part of cortex dictamni, 2-4 parts of glossy privet fruit, 0.2-0.8 part of folium artemisiae argyi, 0.2-0.8 part of lateral bur leaf, 0.1-0.4 part of hot pepper, 0.2-0.8 part of climbing rock old ginger, 0.12-0.8 part of rhizoma polygonati and 0.1-0.4 part of almond.
3. A preparation method of a plant decocted shampoo comprises the following steps:
1) weighing the traditional Chinese medicine raw materials according to the proportion of claim 1 or 2 for later use;
2) soaking the Chinese honeylocust fruits, the polygonum multiflorum, the soapberry fruits and the tea seeds in the step 1) in lime water for 1-3 days, removing the lime water, adding cold water and the pepper into the Chinese honeylocust fruits, the polygonum multiflorum, the soapberry fruits and the tea seeds, heating at 60 ℃, simultaneously adding brown sugar to form a mixture, and fermenting the mixture for 3-6 months under the conditions that the temperature is 25 ℃ and the humidity is 45-60% to obtain a first mixture;
3) boiling the black beans in the step 1) until the skins crack, then adding old ginger and garlic, boiling for 10min, adding mature vinegar, and standing in the shade for 3-6 months to obtain a second mixture;
4) soaking the sophora flavescens roots, the mulberries and the cortex dictamni in the wine in the step 1) for not less than 90 days to obtain a third mixture;
5) soaking the glossy privet fruit, the folium artemisiae argyi, the cacumen biotae, the hot pepper, the peruvian ginger, the rhizoma polygonati and the almond in the rice washing water in the step 1) for 2 to 3 months to obtain a fourth mixture;
6) and removing dregs in the first mixture, the second mixture, the third mixture and the fourth mixture respectively to obtain a first extract, a second extract, a third extract and a fourth extract, and mixing the first extract, the second extract, the third extract and the fourth extract to obtain the plant decocting shampoo.
4. The method of claim 3,
in the plant decocted shampoo, the mass ratio of the first extract to the second extract to the third extract to the fourth extract is 7:0.2:1: 1.8.
5. The method of claim 3,
in the step 2), the brown sugar is added in an amount of 0.1-0.5% by mass.
6. The method of claim 3,
in the step 3), the volume fraction of the mature vinegar is 10-25%.
7. The method of claim 3,
in the step 4), the adding amount of the wine is 20-30 times of the mass of the sophora flavescens root, the mulberry and the cortex dictamni.
8. The method of claim 3,
in the fermentation process, 3% of lactic acid bacteria liquid is inoculated, the lactic acid bacteria liquid is lactobacillus bulgaricus and streptococcus thermophilus according to the ratio of 1:1, and the lactic acid bacteria liquid is obtained by inoculating the lactic acid bacteria liquid into emulsion and culturing at the constant temperature of 40 ℃ for 15 hours.
9. A hair care agent comprising the plant-boiled shampoo of claim 1 or 2 as an active ingredient.
CN202010910105.6A 2020-09-02 2020-09-02 Plant decocted shampoo and preparation method thereof Pending CN112089667A (en)

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CN114191535A (en) * 2021-12-30 2022-03-18 汪太琴 Medicament for whitening and blackening hair and preparation method thereof
CN116286544A (en) * 2023-04-14 2023-06-23 山东向日葵生物工程有限公司 Application of lactobacillus delbrueckii subspecies bulgaricus SF-L-18 in preparation of hair loss prevention and hair quality improvement fermented product

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Application publication date: 20201218