CN112046121A - Novel glass laminating process - Google Patents

Novel glass laminating process Download PDF

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Publication number
CN112046121A
CN112046121A CN202010974053.9A CN202010974053A CN112046121A CN 112046121 A CN112046121 A CN 112046121A CN 202010974053 A CN202010974053 A CN 202010974053A CN 112046121 A CN112046121 A CN 112046121A
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Prior art keywords
glass
heating
temperature
vacuum bag
vacuum
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Pending
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CN202010974053.9A
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Chinese (zh)
Inventor
廖仲明
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Guangzhou Mr Glass Industry Co ltd
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Guangzhou Mr Glass Industry Co ltd
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Priority to CN202010974053.9A priority Critical patent/CN112046121A/en
Publication of CN112046121A publication Critical patent/CN112046121A/en
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B37/00Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding
    • B32B37/10Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding characterised by the pressing technique, e.g. using action of vacuum or fluid pressure
    • B32B37/1018Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding characterised by the pressing technique, e.g. using action of vacuum or fluid pressure using only vacuum
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B17/00Layered products essentially comprising sheet glass, or glass, slag, or like fibres
    • B32B17/06Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B37/00Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding
    • B32B37/12Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding characterised by using adhesives
    • B32B37/1207Heat-activated adhesive
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B37/00Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding
    • B32B37/12Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding characterised by using adhesives
    • B32B37/1284Application of adhesive

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  • Physics & Mathematics (AREA)
  • Fluid Mechanics (AREA)
  • Joining Of Glass To Other Materials (AREA)

Abstract

The invention relates to the technical field of glass doubling processing, and particularly discloses a novel glass doubling process. The process is very simple, a large-scale high-temperature laminating furnace and a high-pressure kettle which are required by the traditional process are completely omitted, the processing cost is greatly reduced, the time and the labor are saved, the space is saved, the safety is improved, and the laminating processing can be realized in any place except a factory and in other places.

Description

Novel glass laminating process
Technical Field
The invention relates to the technical field of glass deep processing, in particular to a novel glass laminating process.
Background
Glass is a common building material, almost all buildings have glass, but the glass has a great defect, is easy to break and hurt people. The laminated glass overcomes the weakness of common glass, broken laminated glass fragments can still be adhered to the laminated film, and the surface of the glass can still be smooth and complete, so that personal injury is avoided to a great extent. Laminated glass has excellent performance and has attracted more and more attention. In countries such as europe and the united states, laminated glass has been used in most buildings because of its good safety and strong safety. In our country, laminated glass has also begun to enter our lives as economic and social progress has been made. Except that the security performance is good, doubling glass still has fine syllable-dividing effect, is difficult to accumulate the oil smoke, and these advantages all play an important role in daily life.
The mainstream laminated glass production process mainly comprises two types (dry method and wet method): the first method is a film method (commonly called dry method), the films are different, the high-pressure kettle is a PVB film, and the laminating furnace is an EVA film; the second is a grouting method (commonly called wet method), which refers to a production process of laminated glass, wherein two pieces of glass are surrounded by edge strips, and then liquid glue is filled into a gap between the two pieces of glass along a reserved glue filling opening and then the liquid glue is cured. The laminating process for glass processing can be applied in a large scale, and the quality improvement effect is mainly achieved by a dry laminating process, namely a laminating process of a film.
The PVB film method is to clamp the PVB film between two or more pieces of glass. Cutting and cutting the film (PVB is clamped between two or more pieces of glass) — "preheating and prepressing (the semi-finished product after laminating is preheated and prepressed to remove the air between the glass and the film) —" placing in a high-pressure autoclave, and pressing and laminating under the condition of high temperature and high pressure in the high-pressure autoclave to obtain the laminated glass.
The EVA film method is characterized in that high-temperature vacuumizing is performed, an EVA film is used for assisting in the middle of two or more pieces of glass, the whole glass is placed into a high-temperature laminating furnace for heating, bubbles are completely pumped away after high-temperature melting, the laminated glass equipment adopts a vacuum heating principle, after the glass is placed into a vacuum bag, the glass air in the vacuum bag is emptied by a vacuumizing system, so that a vacuum state is achieved, the situation that the bubbles cannot be generated between the glass is ensured, the glass is pressed by vacuum pressure, the film is melted under the high-temperature state, and the two pieces of glass are firmly bonded together.
1. The PVB film method needs the following equipment cost:
(1) adopts an autoclave with 380V
(2) The production equipment specifically comprises: constant temperature and humidity sheet-combining chamber, preheating and prepressing roller press, air compressor and glass autoclave
(3) The investment is large, about 80-150 ten thousand.
(4) Manual work: about 5-7 people.
(5) Power consumption amount: the power consumption is large, about hundreds of kilowatts.
(6) The processing time is long: the one-pot time is about 5-7 hours.
(7) The occupied area is large.
(8) The production cost is high, and the production cost is high,
(9) can not be processed and produced in site in different places.
2. The EVA film method needs the following equipment cost:
the production equipment specifically comprises:
(1) 380V is adopted in the high-temperature laminating furnace
(2) Doubling furnace (with heating pipe, blower), vacuum machine and vacuum bag
(3) The investment is little, about 10-30 ten thousand.
(4) Manual work: about 2-3 people.
(5) Power consumption amount: the power consumption is slightly less, 25-50 kilowatts.
(6) Processing time: the one-furnace time is about 95 to 120 minutes.
(7) The occupied area is slightly smaller than that of the autoclave.
(8) The production cost is lower than that of a PVB film method.
(9) Can not be processed and produced in site in different places.
The laminating process of the film needs a large autoclave or heating equipment, has high cost, large power consumption, long consumed time and low productivity, and simultaneously needs a specially designed workshop space for processing due to huge equipment and large used space. Under the condition, the glass laminating process which is novel, simple, high in efficiency, low in energy consumption, uniform in heating and only needs a 220V power supply is urgently needed by the existing laminating process.
Disclosure of Invention
The invention aims to provide a glass laminating process with uniform heating, which aims to solve the problems of large equipment and special sites required in the background technology, omits high equipment cost, saves high electric quantity loss, is simple and easy, has uniform heating, only needs a processing process of a 220V power supply, does not need the requirements of fixed sites and large special equipment workshop space, and can be processed and produced at any place and even on site.
In order to achieve the purpose, the invention provides the following technical scheme:
a novel glass doubling process is characterized in that a doubling processing process which comprises the steps of vacuumizing a vacuum bag and arranging a heating device in the vacuum bag for heating and vacuumizing is adopted.
The processing technology comprises the following steps:
s1, preparing a vacuum bag, putting a heating device of the vacuum bag, two pieces of glass, an EVA (or PVC) film clamped between the two pieces of glass, and 2 pieces of temperature-resistant exhaust nets;
s2, the following preparation is made:
a heating device is flatly laid on the lower vacuum bag, a temperature-resistant exhaust net is flatly laid on the heating device, and a glass sheet I, an EVA (ethylene vinyl acetate) film and a glass sheet II are sequentially stacked on the upper surface of the temperature-resistant net in a flatwise manner; covering a temperature-resistant exhaust net on the second glass sheet, closing the upper vacuum bag, pressing a sealing strip of the vacuum bag, and simultaneously inserting a vacuum pump to be connected with an exhaust port of the vacuum bag;
s3, connecting the heating device with the power supply, connecting the vacuum pump with the power supply, realizing side vacuum in the vacuum bag and heating the contact glass and the film by the heating device in the bag, realizing the film bonding between the two pieces of glass, and realizing the laminating process.
The heating device is a plane heating sheet, and the heating temperature is only 150 ℃ at most.
One kind of heating device adopts the heating device that graphite alkene heating film generates heat.
In the step S3, firstly, a vacuum pump performs cold pumping for 5 minutes at normal temperature, air in the silica gel bag is evacuated, and when the vacuum value reaches 1x10-1 Pa, the heating device is heated to 80-90 ℃ and the holding time is 20-30 minutes; then continuously heating to the surface temperature of the glass of 110-130 ℃ and keeping the time for 45-60 minutes; and then stopping heating, taking out the glass when the temperature of the glass is reduced to below 60 ℃, and vacuumizing the glass by a vacuum pump until the processed laminated glass is taken out.
The vacuum bag is a silica gel vacuum bag, and the temperature resistance requirement reaches 250 ℃.
The vacuum bag sealing strip be equipped with all around and open or compress tightly the trench of matching, realize that two silica gel vacuum bags open or sticis and close, when opening, put into heating device, the glass and the film that need process, cover and close well, sticis the trench, during the evacuation, realize leak protection gas, the corner edge of vacuum bag on be equipped with air pump hole or power pin hole, the centre is equipped with the heating region.
The air pump or the power supply lead hole is arranged on the periphery of the heating area of the vacuum bag.
The heating device for heating the graphene heating film is switched on 220v alternating current to work, the heating film with heating power of 1200W per square is adopted, the heating temperature is detected by adopting a thermal resistor, and the set temperature value is controlled by using a temperature controller, so that the heating temperature is controlled.
Compared with the prior art, the invention has the beneficial effects that:
1. the process is very simple, a high-cost rubber clamping furnace or a high-pressure kettle is completely saved, and the processing cost is greatly reduced.
2. High-power-consumption equipment is omitted, electric quantity loss is greatly reduced, the heating surface is directly heated with the glass, processing time is prolonged, electric quantity is saved, processing cost is further saved, and safety is improved by adopting 220V voltage;
3. the silica gel bag and the heating equipment in the silica gel bag are heating devices which adopt the graphene heating film to generate heat, the heating devices can realize a flaky flexible structure, are convenient to carry, are not limited by special processing space places, can be processed on site even, and are very convenient and practical.
4. The heating device adopting the graphene heating film to generate heat can realize a flaky soft structure, after vacuumizing, the heating film can be tightly attached to the glass surface to be directly heated, the heating effect and quality are improved, heating is uniform, in addition, the heating film can also be deformed along with the shape of glass to be tightly attached to the glass surface to be heated, and the laminating process of the special-shaped glass can be simply realized.
5. The periphery of the glass is provided with a temperature-resistant exhaust net, so that exhaust is effectively realized, effective vacuumizing is realized, effective bubble discharge is achieved, and the quality of glue among the glass is effectively guaranteed.
Drawings
FIG. 1 is a schematic view of the structure of the apparatus used in the process of the present invention;
FIG. 2 is a schematic view of a disassembled arrangement of a part of the equipment used in the process of the present invention;
fig. 3 is a schematic side view of the groove structure of the part a of the silicone vacuum bag in fig. 2.
Detailed Description
The technical solution of the present invention will be described in further detail with reference to specific embodiments.
Example 1 doubling of two sheets of sheet glass
Referring to the attached drawings, fig. 1-3, a novel glass laminating process is characterized in that a laminating processing process is adopted, wherein a vacuum pumping bag 1 is adopted, and a heating device 2 is arranged in the vacuum bag 1 for heating and vacuum pumping.
The processing technology comprises the following steps:
s1, preparing a vacuum bag 1, placing a heating device 2 of the vacuum bag 1, two pieces of glass, an EVA (or PVC) film 5 sandwiched between the two pieces of glass, and 2 pieces of temperature-resistant exhaust nets 4;
s2, the following preparation is made:
a heating device 2 is flatly laid on the lower vacuum bag, a temperature-resistant exhaust net 4 is flatly laid on the heating device, and a first glass sheet 31, an EVA (ethylene vinyl acetate) film 5 and a second glass sheet 32 are sequentially stacked on the upper surface of the temperature-resistant net; covering a temperature-resistant exhaust net 4 on the second glass sheet, closing the upper layer vacuum pumping bag, pressing a sealing strip of the vacuum pumping bag, and simultaneously inserting a vacuum pump to be connected with an exhaust port of the vacuum bag;
s3, the heating device 2 is connected with the power supply 6, the vacuum pump 7 is connected with the power supply 6, the vacuum bag is vacuumized, the heating device in the bag directly heats the contact glass and the film, the adhesion of the film between the two pieces of glass is realized, and the laminating process is realized.
The heating device is a plane heating sheet, and the heating temperature is only 150 ℃ at most.
One kind of heating device adopts the heating device that graphite alkene heating film generates heat.
In the step S3, firstly, a vacuum pump performs cold pumping for 5 minutes at normal temperature, air in the silica gel bag is evacuated, and when the vacuum value reaches 1x10-1 Pa, the heating device is heated to 80-90 ℃ and the holding time is 20-30 minutes; then continuously heating to the surface temperature of the glass of 110-130 ℃ and keeping the time for 45-60 minutes; and then stopping heating, taking out the glass when the temperature of the glass is reduced to below 60 ℃, and vacuumizing the glass by a vacuum pump until the processed laminated glass is taken out.
The vacuum bag is a silica gel vacuum bag, and the temperature resistance requirement reaches 250 ℃.
The sealing strip of vacuum bag be equipped with all around and open or compress tightly the trench of matching, realize that two silica gel vacuum bags open or sticis and close, when opening, put into heating device, the glass and the film that need process, cover and close well, sticis the trench, leak protection gas during evacuation simultaneously, the corner edge of vacuum bag on be equipped with air pump hole or power pin hole, the centre is equipped with the heating region.
The air pump or the power supply lead hole is arranged on the periphery of the heating area of the vacuum bag, so that the vacuum pumping is effectively realized, and the vacuum pumping cannot be influenced by the heating device. The periphery of the glass is provided with the temperature-resistant exhaust net, so that exhaust is effectively realized, effective vacuumizing is realized, effective bubble discharge is realized, and the quality of glue among the glass is effectively ensured.
The heating device for heating the graphene heating film works when being switched on with 220v alternating current, the heating power per square is 120W, the heating temperature is detected by adopting a thermal resistor, and the temperature controller 8 is used for setting a temperature value so as to realize the control of the heating temperature. The temperature control principle belongs to the prior art. Heating temperature is controlled below 150 degrees, and the EVA or PVB glue realizes bonding glass at 105 degrees, and the silica gel vacuum bag is not influenced by the temperature, and glass is not influenced yet, and the welding that meets heat is only the film, and in addition, in the heating process, the aspiration pump is in controlling the vacuum always, produces the negative pressure, realizes gluing the bubble in and discharges, realizes gluing simultaneously and glass's good bonding, in the silica gel vacuum bag, the heat is concentrated, and the loss is little.
Example 2 double-sided processing of two flat, identical profiles or curved surfaces
The processing sequence and the temperature of the device are consistent with those of the embodiment 1, when the device is vacuumized, the heating device which generates heat by the graphene heating film is adopted, the flaky flexible structure can be realized, after the device is vacuumized, the heating film can be directly heated by clinging to a glass surface of an abnormal or curved surface, and the processing of the glass interlayer adhesive of the abnormal or curved surface is realized.
By adopting the processing technology of the invention, the following cost is achieved according to calculation:
the investment is minimum, about 1-5 ten thousand.
Production equipment: vacuum pump, vacuum bag and heating film
Manual work: about 2-3 people.
Power consumption amount: the power consumption is very low, 6-10 kilowatts.
Processing time: the time is about 50-75 minutes.
Compared with the processing equipment cost of the background art, the processing cost is greatly reduced, the time and the labor are saved, the space is saved, and the rubber clamping processing can be realized in any place.
The processing technology of the invention can be realized as follows:
1. the process is very simple, a high-cost rubber clamping furnace or a high-pressure kettle is completely saved, and the processing cost is greatly reduced.
2. High-power-consumption equipment is omitted, electric quantity loss is greatly reduced, the heating surface is directly heated with the glass, processing time is prolonged, electric quantity is saved, processing cost is further saved, and safety is improved by adopting 220V voltage;
3. the silica gel bag and the heating equipment in the silica gel bag adopt the heating device which generates heat by the graphene heating film, the heating device can realize a flaky flexible structure, is convenient to carry, is not limited by special processing space places, and is very convenient and practical.
4. The heating device adopting the graphene heating film to generate heat can realize a flaky soft structure, after vacuumizing, the heating film can be tightly attached to the glass surface to be directly heated, the heating effect and quality are improved, heating is uniform, in addition, the heating film can also be deformed along with the shape of glass to be tightly attached to the glass surface to be heated, and the laminating process of the special-shaped glass can be simply realized.
While the preferred embodiments of the present invention have been described in detail, the present invention is not limited to the above embodiments, and various changes can be made without departing from the spirit of the present invention within the knowledge of those skilled in the art.

Claims (9)

1. A novel glass doubling process is characterized in that a doubling processing process which comprises the steps of vacuumizing a vacuum bag and arranging a heating device in the vacuum bag for heating and vacuumizing is adopted.
2. The novel glass-laminating process according to claim 1, wherein the process comprises the following steps:
s1, preparing a vacuum bag, putting a heating device of the vacuum bag, two pieces of glass, an EVA (or PVC) film clamped between the two pieces of glass, and 2 pieces of temperature-resistant exhaust nets;
s2, the following preparation is made:
a heating device is flatly laid on the lower vacuum bag, a temperature-resistant exhaust net is flatly laid on the heating device, and a glass sheet I, an EVA (ethylene vinyl acetate) film and a glass sheet II are sequentially stacked on the upper surface of the temperature-resistant net in a flatwise manner; covering a temperature-resistant exhaust net on the second glass sheet, closing the upper vacuum bag, pressing a sealing strip of the vacuum bag, and simultaneously inserting a vacuum pump to be connected with an exhaust port of the vacuum bag;
s3, connecting the heating device with the power supply, connecting the vacuum pump with the power supply, realizing side vacuum in the vacuum bag and heating the contact glass and the film by the heating device in the bag, realizing the film bonding between the two pieces of glass, and realizing the laminating process.
3. The novel glass laminating process according to claim 2, characterized in that: the heating device is a plane heating sheet, and the heating temperature is only 150 ℃ at most.
4. The novel glass laminating process according to claim 3, characterized in that: one kind of heating device adopts the heating device that graphite alkene heating film generates heat.
5. The novel glass laminating process according to claim 4, characterized in that: in the step S3, firstly, a vacuum pump performs cold pumping for 5 minutes at normal temperature, air in the silica gel bag is evacuated, and when the vacuum value reaches 1x10-1 Pa, the heating device is heated to 80-90 ℃ and the holding time is 20-30 minutes; then continuously heating to the surface temperature of the glass of 110-130 ℃ and keeping the time for 45-60 minutes; and then stopping heating, taking out the glass when the temperature of the glass is reduced to below 60 ℃, and vacuumizing the glass by a vacuum pump until the processed laminated glass is taken out.
6. The novel glass laminating process according to claim 5, characterized in that: the vacuum bag is a silica gel vacuum bag, and the temperature resistance requirement reaches 250 ℃.
7. The novel glass laminating process according to claim 6, characterized in that: the vacuum bag sealing strip be equipped with all around and open or compress tightly the trench of matching, realize that two silica gel vacuum bags open or sticis and close, realize leak protection gas when realizing the evacuation simultaneously, the corner edge of vacuum bag on be equipped with air pump hole or power pin hole, the centre is equipped with the heating region.
8. The novel glassing process according to claim 7, wherein said air pump or power feed-through holes are provided around the periphery of the heating zone of the vacuum bag.
9. The novel glass laminating process according to claim 4, wherein the heating device for heating the graphene heating film is operated by switching on 220v alternating current, the heating film has a heating power of 1200W per square, and the heating film is controlled by detecting the heating temperature by using a thermal resistor and controlling the set temperature value by using a temperature controller.
CN202010974053.9A 2020-09-16 2020-09-16 Novel glass laminating process Pending CN112046121A (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112659714A (en) * 2020-12-31 2021-04-16 天津南玻节能玻璃有限公司 Laminated glass processing device
CN113666119A (en) * 2021-08-05 2021-11-19 巢湖市伟业玻璃有限公司 Laminated glass bubble removing device and method
CN113665216A (en) * 2021-08-05 2021-11-19 巢湖市伟业玻璃有限公司 Laminated glass bubble removing device
CN113844126A (en) * 2021-09-27 2021-12-28 秦皇岛玻璃工业研究设计院有限公司 Manufacturing method of bulletproof glass for vehicle and bulletproof glass
CN114393907A (en) * 2022-01-20 2022-04-26 漳州市瑞隆达工贸有限公司 Dry laminating process for laminated glass

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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112659714A (en) * 2020-12-31 2021-04-16 天津南玻节能玻璃有限公司 Laminated glass processing device
CN113666119A (en) * 2021-08-05 2021-11-19 巢湖市伟业玻璃有限公司 Laminated glass bubble removing device and method
CN113665216A (en) * 2021-08-05 2021-11-19 巢湖市伟业玻璃有限公司 Laminated glass bubble removing device
CN113844126A (en) * 2021-09-27 2021-12-28 秦皇岛玻璃工业研究设计院有限公司 Manufacturing method of bulletproof glass for vehicle and bulletproof glass
CN113844126B (en) * 2021-09-27 2023-03-07 秦皇岛玻璃工业研究设计院有限公司 Manufacturing method of bulletproof glass for vehicle and bulletproof glass
CN114393907A (en) * 2022-01-20 2022-04-26 漳州市瑞隆达工贸有限公司 Dry laminating process for laminated glass
CN114393907B (en) * 2022-01-20 2024-02-13 漳州市瑞隆达工贸有限公司 Dry method laminating process for laminated glass

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