CN111974746B - Device for cleaning filler by flotation bubbles and cleaning method - Google Patents

Device for cleaning filler by flotation bubbles and cleaning method Download PDF

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Publication number
CN111974746B
CN111974746B CN202010850187.XA CN202010850187A CN111974746B CN 111974746 B CN111974746 B CN 111974746B CN 202010850187 A CN202010850187 A CN 202010850187A CN 111974746 B CN111974746 B CN 111974746B
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cleaning
filler
bubble
pipe
overflow
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CN111974746A (en
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李强
曹昊
李安萌
郭林飞
邱擎柱
许伟伟
王振波
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China University of Petroleum East China
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China University of Petroleum East China
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B08CLEANING
    • B08BCLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
    • B08B3/00Cleaning by methods involving the use or presence of liquid or steam
    • B08B3/04Cleaning involving contact with liquid
    • B08B3/10Cleaning involving contact with liquid with additional treatment of the liquid or of the object being cleaned, e.g. by heat, by electricity or by vibration
    • B08B3/12Cleaning involving contact with liquid with additional treatment of the liquid or of the object being cleaned, e.g. by heat, by electricity or by vibration by sonic or ultrasonic vibrations
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B08CLEANING
    • B08BCLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
    • B08B3/00Cleaning by methods involving the use or presence of liquid or steam
    • B08B3/04Cleaning involving contact with liquid
    • B08B3/048Overflow-type cleaning, e.g. tanks in which the liquid flows over the tank in which the articles are placed
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B08CLEANING
    • B08BCLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
    • B08B3/00Cleaning by methods involving the use or presence of liquid or steam
    • B08B3/04Cleaning involving contact with liquid
    • B08B3/10Cleaning involving contact with liquid with additional treatment of the liquid or of the object being cleaned, e.g. by heat, by electricity or by vibration
    • B08B3/102Cleaning involving contact with liquid with additional treatment of the liquid or of the object being cleaned, e.g. by heat, by electricity or by vibration with means for agitating the liquid
    • B08B3/104Cleaning involving contact with liquid with additional treatment of the liquid or of the object being cleaned, e.g. by heat, by electricity or by vibration with means for agitating the liquid using propellers

Abstract

The invention discloses a device and a method for cleaning a filler by flotation bubbles, wherein the device for cleaning the filler by flotation bubbles comprises a cylinder, an overflow structure, a bubble generation structure, an ultrasonic structure and a stirring and shearing structure, wherein the bubble generation structure mainly comprises a bubble nozzle, a gas-liquid cavity, a gas-liquid guide pipe and the like, the bubble nozzle comprises a reducing pipe, a throat pipe, a diffusion pipe and a mixing pipe, the channels of the bubble nozzle are connected to form a Venturi tube-shaped flow channel, and micro gas columns are sucked from a micropore channel by generating negative pressure and sheared to form bubbles; and refining bubbles by combining an ultrasonic structure and a stirring and shearing structure to form micro bubbles, so that oil slurry on the surface of the filler is desorbed and is discharged into an overflow structure through floating of the bubbles, and the filler is cleaned. Compared with other filler backwashing methods, the device disclosed by the invention has the advantages that less cleaning liquid is used for cleaning, the cleaning speed is higher, the cleaning effect is better, and less waste liquid is generated.

Description

Device for cleaning filler by flotation bubbles and cleaning method
Technical Field
The invention relates to the field of filler cleaning of electrostatic separation devices, and mainly relates to a device and a method for cleaning a filler by flotation bubbles.
Background
The catalytic cracking slurry oil is a byproduct of a catalytic cracking device, and is generally sold as waste oil at low price or burnt as fuel, so that not only can a furnace mouth generate corrosion and coking, but also great waste of resources is caused. The main component of the catalytic oil slurry is polycyclic aromatic hydrocarbon, and high-quality petroleum coke, carbon black, rubber softening oil and the like can be produced by deep processing. However, the oil slurry contains high catalyst particles, which brings difficulty to the comprehensive utilization of the oil slurry. Therefore, the catalyst particles in the slurry oil need to be treated to meet the requirements of different products on the catalyst particles.
As the particle size of solid-phase particles in the FCC slurry is in the range of 0-80 μm, the proportion of particles with the particle size of less than 20 μm is relatively heavy. Compared with a settling method, a filtering method, a cyclone separation method and the like, the electrostatic separation method has the advantages that micron-sized catalyst particles are removed more obviously when catalytic oil slurry is treated, and the pressure drop is small. The electrostatic separation is to generate a non-uniform high-voltage electric field by a high-voltage power supply, catalyst particles are polarized by the electric field to generate non-uniform coulomb force, and then the catalyst particles move directionally to realize the removal of the particles. In order to enhance the local electric field strength, it is necessary to incorporate glass fillers in the electrostatic separator. After being polarized, the catalyst particles are adsorbed at the contact point position of the filler, when the catalyst particles adsorbed by the filler reach saturation, a back washing measure is adopted for cleaning, and the operation of the next period is carried out again. The backwashing aims to clean the glass bead filler, the conventional method is mostly a mode of directly performing liquid or gas-liquid mixed backwashing on an electrostatic separator, complete cleaning and cleanness of the glass filler are difficult to ensure, the consumption of backwashing liquid is high, and high backwashing pressure needs to be ensured. And the conventional back washing mode also generates a large amount of waste liquid, so that the recycling of the cleaned oil slurry is difficult to realize.
Disclosure of Invention
Based on the defects of the prior art, the invention designs a device for cleaning the filler by flotation bubbles, which utilizes an air flotation method and adopts ultrasonic cavitation and shearing action to refine the bubbles, thereby realizing removal of slurry mixed with a catalyst on the surface of the glass filler and effectively reducing the dosage of a cleaning solution.
In order to achieve the above purpose, the scheme of the invention is as follows: the utility model provides a device of flotation bubble washing filler which characterized in that, includes barrel, overflow structure, bubble generation structure, supersound structure and stirring shear structure.
The top of the cylinder body is provided with an overflow mechanism, the overflow mechanism is used for collecting floating foam floating oil and comprises a cover plate, an overflow groove, an overflow weir and a floating oil outlet; the cover plate is used for controlling the overflow of floating oil foam and is provided with a filler inlet and a stirring rod hole; the filler inlet is used for feeding filler to be cleaned; the overflow groove is annularly arranged on the outer side of the cylinder body, and the bottom of the overflow groove is lower than the opening of the cylinder body; the side edge of the overflow groove is provided with a floating oil outlet which is used for collecting the oil slurry of the washed mixed catalyst particles;
the bubble generation structure is used for generating continuous and stable micro bubbles and comprises a bubble nozzle, an air cavity, a liquid cavity, an air inlet guide pipe, a compressed air tank, an air compressor, a liquid inlet guide pipe and a pump; the bubble nozzle comprises a reducing pipe, a throat pipe, a diffusion pipe and a mixing pipe, the bubble nozzle is the most main part for generating bubbles, the size of the bubbles and the cleaning speed are influenced by the design of the bubble nozzle, and the integrated design of a bubble generating structure and a cleaning liquid inlet pipeline is carried out in the invention, so that micro bubbles with adjustable bubble sizes can be continuously generated under the condition of ensuring that the total volume of the cylinder body is basically unchanged; the insides of the reducing pipe, the throat pipe and the diffusion pipe form a Venturi-shaped flow passage, and the flow passages are respectively a reducing flow passage, a throat flow passage and an expanding flow passage; the throat part is provided with air inlet micropores, and the diameter of each micropore is controlled to be less than 1 mm; the air inlet micropores are used for sucking air into the throat flow passage; when liquid flows in the flow channel, negative pressure is generated at the throat position, air is sucked out of the micropores to form a micro air column, and the micro air column is changed into tiny bubbles to be mixed with water under the shearing action of liquid flow; the mixing tube is provided with a gas-liquid mixing chamber and a micropore diffusion sheet, the micropore diffusion sheet is provided with micropores capable of controlling the diameters of the bubbles, and the micropore diffusion sheet can be replaced according to different requirements of the diameters of the bubbles.
In the embodiment of the invention, the taper angle of the tapered flow channel is 18-23 degrees, and the taper angle of the expanded flow channel is 11-16 degrees; in other embodiments, the adjustment can be made according to the bubble generation.
The reducing pipe part of the bubble nozzle is arranged in a liquid cavity at the bottom of the cylinder, the throat part of the bubble nozzle is arranged in an air cavity at the bottom of the cylinder, and the diffusion pipe and the mixing pipe of the bubble nozzle are arranged at the inner side of the bottom of the cylinder; the connection interfaces of the three parts of the reducing pipe, the throat pipe and the diffusion pipe are sealed, and the flow passages of the three parts are communicated;
the bottom of the cylinder body is in a funnel shape and is provided with a filler outlet, an air cavity and a liquid cavity; the bottom of the glass filler to be cleaned is designed into a funnel shape to facilitate discharging the cleaned glass filler; the air cavity is connected with the compressed air tank through an air inlet conduit and is used for discharging air into the air inlet micropores; the liquid cavity is connected with a pump through a liquid inlet conduit and is used for discharging water or other cleaning liquid into the reducing flow channel.
In the embodiment of the invention, the bubble nozzles are perpendicular to the conical surface of the cylinder bottom when being installed, and the multiple groups of bubble nozzles are annularly arranged on the conical surface; in other embodiments, the bubble jet nozzle may be angled with respect to the conical surface, or arranged in other configurations.
The ultrasonic structure comprises an ultrasonic controller and an ultrasonic probe, wherein the ultrasonic controller is arranged on the outer side wall of the cylinder body and used for controlling the generation and stop of an ultrasonic force field and controlling the energy; the ultrasonic probes are uniformly arranged on the inner side wall of the cylinder body; the ultrasonic structure is used for destroying an oil film on the surface of the glass filler, thinning bubbles and enhancing the bubble cleaning effect;
the upper part of the cylinder body is provided with a stirring and shearing structure, and the shearing structure comprises a lifting rod, a connecting rod, a motor, a stirring rod and a shearing blade; the lifter passes through the connecting rod control motor and moves in vertical direction to realize shearing blade's upper and lower application, guarantee basically that all positions of barrel inside can receive the effect that the blade stirred and sheared. The shearing blades are arranged in parallel and fixed on the stirring rod.
In addition, the invention also provides a method for cleaning the filler by flotation bubbles, which comprises the following steps: before cleaning, opening an ultrasonic controller, and adjusting parameters such as frequency, sound intensity and the like to be optimal, 1) pouring the filler to be cleaned into the cylinder through a filler inlet; 2) simultaneously starting a pump switch and a switch of an air inlet pipeline, and then starting a motor; 3) collecting the cleaned catalytic slurry oil through a floating oil outlet; 4) when the floating oil discharge port does not produce catalytic slurry oil any more, the pump, the air inlet guide pipe and the motor are turned off, and the cleaned filler is discharged through the bottom filler outlet; 5) and (4) closing the filler outlet, and repeating the steps 1) to 4) to carry out the next group of cleaning work.
Compared with the prior art, the invention has the beneficial effects that:
1. the invention introduces the air floatation method into the field of cleaning the filler for the electrostatic separator for the first time, adopts a Venturi tube-shaped flow passage to carry out gas-liquid mixing, combines the effects of ultrasonic cavitation and stirring shearing, carries out refining treatment on micro bubbles, and can realize the removal of oil slurry mixed with catalyst particles attached to the surface of the filler;
2. the ultrasonic wave has a certain cleaning effect on the filler while playing a role of micronizing bubbles, so that the device disclosed by the invention has a better cleaning effect on the filler;
3. according to the invention, the filler is cleaned by a flotation bubble method, so that the using amount of cleaning liquid or cleaning water can be effectively reduced, and meanwhile, the amount of waste liquid can be reduced; accelerating the falling of the substances attached to the surface of the filler under the dual actions of stirring and ultrasound; the size of the generated bubbles can be adjusted by replacing the microporous diffusion sheet of the nozzle so as to control the cleaning effect and the cleaning speed of the filler.
Drawings
FIG. 1 is a front sectional view of the structure of the flotation bubble cleaning and filling device of the invention;
FIG. 2 is a top view of the apparatus of FIG. 1 from direction A;
FIG. 3 is a top view of the cover plate of the present invention;
FIG. 4 is a front view of the structure of the bubble jet nozzle;
FIG. 5 is a bottom layout view of the bubble jet nozzle
In the figure: 1. a cover plate; 2. an overflow weir; 3. an overflow trough; 4. a stirring rod; 5. a barrel; 6. an ultrasonic controller; 7. an ultrasonic probe; 8. a liquid cavity; 9. a pump; 10. a liquid inlet conduit; 11. a bubble nozzle; 12. a filler outlet; 13. an air cavity; 14. an air intake duct; 15. an air compression tank; 16. an air compressor; 17. a floating oil outlet; 18. a motor; 19. a connecting rod; 20. a lifting rod; 21. shearing the blade; 22. an overflow structure; 23. a filler inlet; 24. a stir bar port; 25. a reducer; 26. air inlet micropores; 27. a throat; 28. a diffuser tube; 29. a mixing tube; 30. a gas-liquid mixing chamber; 31. a microporous diffuser plate; 32. a tapered flow channel; 33. a throat flow passage; 34. and expanding the flow channel.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
As shown in fig. 1-3, fig. 1 is a front sectional view of the flotation bubble cleaning and filling device of the invention, fig. 2 is a top view of the device shown in fig. 1 from the direction of a, and fig. 3 is a top view of a cover plate of the invention; the device for cleaning the filler by flotation bubbles is characterized by comprising a cylinder body 5, an overflow structure 22, a bubble generation structure, an ultrasonic structure and a stirring and shearing structure.
An overflow structure 22 is arranged on the outer periphery of the top of the cylinder 5, is used for collecting floating foam floating oil and comprises a cover plate 1, an overflow groove 3, an overflow weir 2 and a floating oil outlet 17; the cover plate 1 and the overflow weir 2 are used for sealing the upper part of the overflow groove 3 and controlling the overflow of floating oil foam, and the cover plate 1 is provided with a filler inlet 23 and a stirring rod hole 24; the filler inlet 23 is used for feeding filler to be cleaned; the overflow groove 3 is annularly arranged on the outer side of the cylinder body, and the bottom of the overflow groove 3 is lower than the opening of the cylinder body 5; the side edge of the overflow groove 3 is provided with a floating oil outlet 17, and the floating oil outlet 17 is used for collecting the oil slurry of the cleaned mixed catalyst particles.
FIG. 4 is a front view of the structure of the bubble jet nozzle in the present invention, as shown in FIG. 4; the bubble generation structure is used for generating continuous and stable micro bubbles and comprises a bubble nozzle 11, an air cavity 13, a liquid cavity 8, an air inlet conduit 14, a compressed air tank 15, an air compressor 16, a liquid inlet conduit 10 and a pump 9; the bubble jet 11 comprises a reducer 25, a throat 27, a diffuser 28 and a mixing tube 29; the insides of the reducing pipe 25, the throat pipe 27 and the diffusion pipe 28 form a Venturi-shaped flow passage, and the flow passages are respectively a reducing flow passage 25, a throat flow passage 33 and an expanding flow passage 34; the throat part is provided with air inlet micropores 26, the diameter of each micropore is controlled to be less than 1mm, and the air inlet micropores 26 are communicated with the air cavity 13 and the throat flow passage 33 and are used for sucking air into the throat flow passage 33; when liquid flows in the flow channel, negative pressure is generated at the position of the throat flow channel 33, air is sucked from the micropores to form a micro air column, and the micro air column is changed into micro bubbles to be mixed with the liquid under the shearing action of liquid flow; the mixing pipe 29 is communicated with the diffusion pipe 28, a gas-liquid mixing chamber 30 and a micropore diffusion sheet 31 are arranged in the mixing pipe, and the micropore diffusion sheet 31 is provided with micropores with adjustable bubble diameters and can be replaced according to different required bubble diameters.
The reducing pipe 25 of the bubble nozzle is arranged in the liquid cavity 8 at the bottom of the cylinder 5, the throat pipe 27 of the bubble nozzle is arranged in the air cavity 13 at the bottom of the cylinder 5, and the diffusion pipe 28 and the mixing pipe 29 of the bubble nozzle are arranged at the inner side of the bottom of the cylinder 5; the connection interfaces of the three parts of the reducing pipe 25, the throat pipe 27 and the diffusion pipe 28 are sealed, and the flow passages of the three parts are communicated;
referring to fig. 1, the bottom of the cylinder 5 is funnel-shaped, the inner space of the bottom wall of the funnel-shaped cylinder is divided into two layers, the two layers comprise an air cavity 13 and a liquid cavity 8 from inside to outside, and the bottom end of the cylinder 5 is further provided with a filler outlet 12; the bottom of the glass filler to be cleaned is designed into a funnel shape to facilitate discharging the cleaned glass filler; the air cavity 13 is used for discharging air into the air inlet micropores 26 and is connected with the compressed air tank 15 through the air inlet conduit 14; the liquid cavity is connected to a pump 9 via a feed line 10 for discharging water or other cleaning liquid into the tapering flow channel 32.
The ultrasonic structure comprises an ultrasonic controller 6 and an ultrasonic probe 7, wherein the ultrasonic controller is arranged on the outer side wall of the cylinder body and used for controlling the generation and stop of an ultrasonic force field and controlling the energy; the ultrasonic probes 7 are uniformly arranged on the inner side wall of the cylinder body; the ultrasonic structure is used for destroying an oil film on the surface of the glass filler, thinning bubbles and enhancing the bubble cleaning effect;
FIG. 5 is a view showing the arrangement of the bubble jet nozzle installed on the bottom of the cylinder in the present invention; the installation direction of the bubble nozzles 11 is vertical to the conical surface of the cylinder bottom, and the bubble nozzles 11 are four groups of rings and are arranged on the conical surface at equal intervals; in the inside-out sequence, the distances among the bubble nozzles in each circle are 45 degrees, 30 degrees, 26 degrees and 23 degrees, and the bubbles are uniformly distributed in the initial state of entering the cylinder 5 through the design of different distances and angles of the annularly distributed bubble nozzles on different rings.
As shown in fig. 2, fig. 2 is a top view of the apparatus shown in fig. 1 from direction a, i.e., a top view of the cylinder with the cover plate removed; the upper part of the cylinder 5 is provided with a stirring and shearing structure, and the shearing structure comprises a lifting rod 20, a connecting rod 19, a motor 18, a stirring rod 4 and a shearing blade 21; the lifting rod 20 controls the motor 18 to move in the vertical direction through the connecting rod 19, so that the up-and-down movement of the shearing blade 21 is realized; in the cleaning process, all the positions in the cylinder body can basically be subjected to stirring and shearing actions by adjusting the periodic lifting of the lifting rod 20; the shearing blades 21 are arranged in parallel and fixed on the stirring rod 4; the cover plate is provided with a stirring rod hole 24 for the stirring rod 20 to pass through.
The invention provides a method for cleaning a filler by flotation bubbles, which comprises the following steps: before cleaning begins, the ultrasonic controller 6 is opened, and parameters such as frequency, sound intensity and the like are adjusted to be optimal, 1) filling materials to be cleaned are poured into the barrel 5 through the filling material inlet 21; 2) simultaneously turning on the switch of the pump 9 and the switch of the air inlet pipeline 14, and then turning on the motor 18; 3) collecting the cleaned catalytic slurry oil through a floating oil outlet 17; 4) when the floating oil outlet 17 does not produce catalytic slurry oil any more, the pump 9, the air inlet guide pipe 14 and the motor 18 are closed, and the cleaned filler is discharged through the bottom filler outlet 12; 5) and (4) closing the filler outlet 12, and repeating the steps 1) to 4) to perform the next group of cleaning work.
Although the embodiments of the present invention have been described with reference to the accompanying drawings, it is not intended to limit the scope of the invention, and it should be understood by those skilled in the art that various modifications and changes in equivalent structure or equivalent flow, or direct or indirect application to other related fields without creative efforts based on the technical solutions of the present invention may be made within the scope of the present invention.

Claims (7)

1. An apparatus for flotation bubble cleaning of packing, comprising: the device comprises a cylinder body, an overflow structure, a bubble generation structure and an ultrasonic structure;
the top of the cylinder body is provided with an overflow structure, and the overflow structure is used for discharging floating oil at the top of the cylinder body; the bubble generating structure is arranged at the bottom of the cylinder body; the ultrasonic structure is arranged on the side wall of the cylinder body; the bubble generating structure is used for simultaneously generating micro bubbles when cleaning liquid is injected;
the bubble generating structure comprises a bubble nozzle, an air cavity, a liquid cavity, an air inlet guide pipe, a compressed air tank, an air compressor, a liquid inlet guide pipe and a pump;
the internal space of the bottom wall of the cylinder body is divided into two layers, the two layers comprise an air cavity and a liquid cavity from inside to outside, the bubble nozzle is arranged on the bottom wall of the cylinder body and extends into the cylinder body and is communicated with an air cavity and the liquid cavity, the air cavity is communicated with a compressed air tank and an air compressor through an air inlet guide pipe, and the liquid cavity is communicated with a pump through a liquid inlet guide pipe;
the bubble nozzle comprises a reducing pipe, a throat pipe, a diffusion pipe and a mixing pipe; the passages in the reducing pipe, the throat pipe and the diffusion pipe penetrate through to form a flow passage in the shape of a Venturi pipe; the throat pipe is provided with a plurality of rows of micro air inlets; the mixing tube is communicated with the diffusion tube, a mixing chamber and a microporous diffusion sheet are arranged in the mixing tube, and the microporous diffusion sheet can be replaced according to the required bubble size;
the reducing pipe is arranged in the liquid cavity at the bottom of the cylinder and is used for communicating the bubble nozzle with the liquid cavity; the throat pipe is arranged in the air cavity at the bottom of the cylinder and is used for communicating the bubble nozzle with the air cavity;
the stirring and shearing mechanism comprises a lifting rod, a connecting rod, a motor, a stirring rod and shearing blades; the lifting rod controls the motor to move in the vertical direction through the connecting rod; the shearing blades are arranged in parallel; the motor drives the blades to rotate through the stirring rod, and the stirring rod extends into the cylinder body through the stirring hole in the cover plate.
2. The apparatus for cleaning packing by flotation bubbles according to claim 1, wherein the overflow structure comprises a cover plate, an overflow weir, an overflow trough and a floating oil outlet, the overflow trough is arranged outside the cylinder in a circular shape, the overflow weir is arranged at the outer ring of the overflow trough, and the cover plate and the overflow weir close the upper part of the overflow trough; the side edge of the overflow groove is provided with a floating oil outlet, and the cover plate is provided with a filler inlet.
3. An apparatus for flotation bubble cleaning packing as claimed in claim 1 further characterized in that said micro air inlet holes are less than 1mm in diameter; the contraction flow channel of the reducing pipe is 18-23 degrees, and the expansion flow channel of the diffusion pipe is 11-16 degrees.
4. A device for flotation bubble cleaning packing according to any one of claims 1 to 3, wherein the bottom of the cylinder is funnel-shaped and is provided with a packing outlet; the filler outlet is openable.
5. An apparatus for flotation bubble cleaning packing as claimed in claim 1 wherein the bubble jet is mounted to the bottom of the tank at an angle perpendicular to the bottom wall of the tank or at an angle inclined to the conical surface of the bottom wall of the tank.
6. An apparatus for flotation bubble cleaning packing according to any one of claims 1 to 3, wherein the ultrasonic structure includes an ultrasonic controller and an ultrasonic probe, which are respectively mounted on the outside and inside of the cylinder.
7. A method for cleaning flotation bubble cleaning filler, which adopts the device for cleaning flotation bubble cleaning filler disclosed by any one of claims 1-6, and comprises the following steps:
starting an ultrasonic controller before cleaning, and 1) pouring the filler to be cleaned into the cylinder through a filler inlet; 2) simultaneously turning on a pump switch and a switch of the air inlet guide pipe, and then turning on a motor; 3) collecting the cleaned catalytic slurry oil through a floating oil outlet; 4) when the floating oil discharge port does not produce catalytic slurry oil any more, the pump, the air inlet guide pipe and the motor are turned off, and the cleaned filler is discharged through the bottom filler outlet; 5) and (4) closing the filler outlet, and repeating the steps 1) to 4) to carry out the next group of cleaning work.
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