CN108970813A - A kind of fluidization coarse flotation equipment and method for floating - Google Patents

A kind of fluidization coarse flotation equipment and method for floating Download PDF

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Publication number
CN108970813A
CN108970813A CN201811246340.7A CN201811246340A CN108970813A CN 108970813 A CN108970813 A CN 108970813A CN 201811246340 A CN201811246340 A CN 201811246340A CN 108970813 A CN108970813 A CN 108970813A
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bubble
flotation
cylinder
inlet
fluidization
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CN108970813B (en
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孙伟
卫召
韩海生
王若林
胡岳华
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Central South University
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Central South University
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B03SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
    • B03DFLOTATION; DIFFERENTIAL SEDIMENTATION
    • B03D1/00Flotation
    • B03D1/14Flotation machines

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  • Engineering & Computer Science (AREA)
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  • Manufacture And Refinement Of Metals (AREA)

Abstract

The invention discloses a kind of fluidization coarse flotation equipment, comprising: flotation cylinder, top are equipped with overflow launder and charging gear;Bubble generator is arranged on the flotation cylinder;Bubble distributer is arranged in the flotation column body and is connected with the bubble generator, the bubble that bubble generator generates is uniformly distributed in flotation column body;It further include being connected to flotation cylinder lower end inlet to form the liquid feed device for rising liquid stream in flotation column body, the bubble distributer is located at the top of the inlet, is equipped with turbulence plate between the inlet and bubble distributer in the flotation column body.The present invention forms the solution-air compound flowing stateization interference bed of bubble and ascending current by the combined use of bubble distributer and turbulence plate in cylinder, realize to grade 150 μm of -1000 μm or so coarse granule mineral flotation recovery.

Description

A kind of fluidization coarse flotation equipment and method for floating
Technical field
The invention belongs to mining equiment flotation technology field more particularly to a kind of fluidization coarse flotation equipment and flotation sides Method.
Background technique
In mineral manufacture field, flotation is the recycling most common method of valuable mineral.And flotation is for the grain of selected mineral Spend it is more demanding, material size usually require that the specific gravity of 74 μm or less grades 60%~90% or so, the material size upper limit Usually at 100~150 μm, and the particle relatively thick for 150 μm or more granularities, flotation recovery effect are poor, therefore thick Particle usually requires to return to material size of the ball mill fine grinding to reach flotation.And for grade at 150 μm~1000 μm or so Ore, regrind be easy to cause ore cross crush, lead to the unnecessary increase of thin mud amount, at the same increase again ore grinding at This.The grade of valuable mineral is usually lower with respect to fine fraction ore in coarse granule ore, and grinding operation is all carried out to it and is caused A degree of energy dissipation.Therefore, in the process flow of " ore grinding-flotation ", to grade on 150 μm~1000 μm left sides Right ore carries out throwing tail in advance and has important practical significance.
Coarse granule is ineffective using traditional floatation equipment recycling.Coarse granule ore liberation degree of minerals is poor, ore The exposure of surface valuable mineral is relatively low, poor with the function and effect of collecting agent, causes the hydrophobicity on ore particles surface inadequate, It is smaller with the sticking probability of bubble;Coarse granule weight is relatively large, floats and needs the bubble of more volume and intensity, general gas Bubble is formed by buoyancy and is not enough to bring coarse granule into froth bed;Coarse granule specific surface area is relatively small, the adhesion strength with bubble It is relatively poor, adhesion time needed for cannot keep flotation and intensity, it is easy to fall off from bubble.Therefore, coarse granule mineral Often sink to entering tailing in floatation process, causes the loss of valuable mineral.And for sorting coarse grained interference bed Sorting machine, separating effect depend on the partial size and density of mineral, since the grade of valuable mineral in coarse granule is usually lower, divides It is thin to dissipate disseminated grain size, causes the specific gravity of same particle size ore particles almost without difference, therefore hindered bed separator is to coarse granule In valuable mineral recognition capability it is poor, equally will cause the loss of valuable mineral.Therefore, single traditional floatation equipment and again Optional equipment all cannot achieve the high efficiente callback to coarse granule target minreal.
Summary of the invention
The application aims to solve at least one of the technical problems existing in the prior art.For this purpose, an object of the present invention It is to provide a kind of fluidization coarse flotation equipment and method for floating, the flotation recovery to coarse granule target minreal may be implemented, And coarse granule gangue mineral is subjected to throwing tail, realize the pretreatment of ore.
In order to solve the above technical problems, the present invention adopts the following technical scheme:
A kind of fluidization coarse flotation equipment, comprising:
Flotation cylinder, top are equipped with overflow launder and charging gear;
Bubble generator is arranged on the flotation cylinder;
Bubble distributer is arranged in the flotation column body and is connected with the bubble generator;
Flotation cylinder lower end is equipped with inlet, and the bubble distributer is located at the top of the inlet, described floating It selects and is equipped with turbulence plate in cylinder between the inlet and bubble distributer.
Further, the bubble generator includes the collapsible tube, trunnion and diffuser being sequentially connected to, the diffuser Output end docked with efferent duct, the input end of the collapsible tube is docked with closed gas-liquid mixed room, the gas-liquid mixed room Be equipped with pressed gas air inlet pipe and fluid injection pipe, be equipped with helical blade in the efferent duct, the efferent duct with it is described The bubble import of bubble distributer is docked.
Further, the bubble generator is arranged circumferentially along flotation cylinder, and the bubble distributer includes concentric At least two annular gas distribution pipes that are horizontally disposed and being connected by connecting tube are evenly equipped with outlet on each annular gas distribution pipe Hole is located at outermost annular gas distribution pipe and is equipped with and each one-to-one bubble import of bubble generator.
Further, the axis of the fluid injection pipe is overlapped with the axis of the trunnion, the fluid injection pipe and institute It states air inlet pipe to arrange in angle, the size of the angle is 40-45 °.
Further, the cone angle of the collapsible tube is 30-35 °, and the cone angle of the diffuser is 35-40 °, the contraction The longitudinal length ratio of pipe, trunnion and diffuser is 1:4:2.
Further, the spout of the fluid injection pipe is the conical nozzle that cone angle is 15-20 °.
Further, tripper is equipped in the feeding inlet at the top of flotation cylinder.
Further, the turbulence plate is in the taper of falling water chestnut, is evenly equipped with the perforation that feed flow stream passes through on the turbulence plate, described The cone bottom of turbulence plate is directly connected to flotation cylinder bottom gape, and the ore discharge valve automatically controlled is equipped at the gape.
Further, the inlet is evenly arranged along flotation cylinder peripheral wall.
Further, the flotation column is arranged with annular inlet tube in vitro, the annular inlet tube be equipped with it is each described Inlet correspond connection liquid outlet, it is described annular inlet tube be equipped with the total mouth of feed liquor, the axis of the total mouth of feed liquor with The axis of the annular inlet tube is tangent.
A kind of method for floating using above-mentioned fluidization coarse flotation equipment, includes the following steps:
S1: liquid feed device is opened, pressurised stream enters flotation column body from flotation cylinder lower end inlet, through turbulence plate Afterwards, uniform ascending current is formed in flotation column body;
S2: air enters bubble generator through bubble generator air inlet after air compressor compresses, and foaming agent is through cream It is added in the water flow pressurizeed by the second force (forcing) pump after changing device emulsification, and enters in microvesicle generators through bubble generator water inlet, A large amount of micro air bubbles that bubble generator generates are passed through bubble distributer, and bubble is dispersed in flotation cylinder by bubble distributer Interior, bubble and ascending current form stable gas-liquid compound flowing stateization interference bed in flotation column body;
S3: ore pulp and floating agent are sized mixing after agitator sufficiently acts on and are divided by charging gear from flotation cylinder top warp Enter in flotation column body after the dispersion of mine device and slowly decline along the entire section of flotation cylinder, interferes bed in gas-liquid compound flowing stateization Ore particle and bubble and ascending current act in layer, and the vertical lift of buoyancy and ascending current of the final purpose mineral through bubble is continuous Rise and then overflow cylinder and enter overflow launder as concentrate, and gangue mineral sinks in cylinder and finally from gape discharge at For tailing.
Compared with prior art, it is had the beneficial effect that brought by the present invention
1. passing through the comprehensive function of bubble and ascending current, the solution-air that bubble and ascending current are formd in cylinder is multiple It closes fluidization and interferes bed, given full play to the dense medium grading principle of interference bed and the advantage of floating principle, realized to grain Flotation recovery of the grade in 150 μm~1000 μm or so coarse granule mineral.
2. ascending current increases mineral grain in the climbing power of vertical direction, target minreal averag density is greatly reduced, Valuable mineral is compensated for because of particle the is relatively thick defect weaker with bubble adhesive force, target minreal is allowed to increase with bubble Into concentrate, and gangue mineral sinks due to not by bubble buoyancy into tailing, to realize that the flotation to coarse granule mineral is returned It receives.
3. grade of the tailing containing target minreal obtained by the equipment is extremely low, can be direct in the beneficiation flowsheet of " ore grinding-flotation " Throwing tail is carried out as true tailings, gangue mineral is removed from process in time, reduces the load of ball mill, is reduced floating Flow processing amount is selected, energy consumption is significantly reduced.
4. the equipment has the oxide ores such as the sulphide ores such as copper-sulphide ores, molybdenite and scheelite, cassiterite, cerussite Good separating effect.
Detailed description of the invention
Fig. 1 is the structural diagram of the present invention;
Fig. 2 is annular inlet tube schematic diagram in the present invention;
Fig. 3 is turbulence plate schematic diagram of the present invention;
Fig. 4 is bubble generator schematic diagram of the present invention;
Fig. 5 is that schematic diagram is applied in combination in bubble generator of the present invention and bubble distributer;
Fig. 6 is specific implementation process equipment connection schematic diagram of the invention.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other Embodiment shall fall within the protection scope of the present invention.
Referring to Fig. 1-Fig. 6, a kind of fluidization coarse flotation equipment, including flotation cylinder 1, bubble generator 14 and bubble Distributor 15,1 bottom of flotation cylinder be bracket 7, the top of flotation cylinder 1 be equipped with overflow launder 2 and with flotation cylinder feeding inlet 3 The charging gear of docking, overflow launder 2 are equipped with overflow port 6.Bubble generator 14 is mounted on the outer wall of flotation cylinder 1, bubble Distributor 15 is horizontally set in flotation cylinder 1 and is connected with bubble generator 14, the bubble that bubble generator is generated It is uniformly distributed in flotation cylinder 1.1 lower end of flotation cylinder be equipped with inlet 11, bubble distributer 15 be located in the liquid inlet 11 it is upper Side is equipped with turbulence plate 12 being located in the liquid inlet between 11 and bubble distributer 15 in flotation cylinder 1, the liquid entered from inlet 11 Body forms in flotation column body after turbulence plate 12 and rises liquid stream.
The present embodiment rises liquid stream by being formed inside flotation cylinder 1, by the comprehensive function of bubble and ascending current, The solution-air compound flowing stateization interference bed that bubble and ascending current are formd in cylinder, has given full play to the weight of interference bed The advantage of Jie's grading principle and floating principle realizes the flotation recovery to coarse granule mineral.Ascending current increases mineral grain In the climbing power of vertical direction, target minreal averag density is greatly reduced, compensates for valuable mineral due to particle is relatively thick and bubble The weaker defect of adhesive force, allows target minreal to ascend into concentrate with bubble, and gangue mineral is not because by bubble floating Power and sink into tailing, to realize to the flotation recoveries of coarse granule mineral.
To improve the stability for rising liquid stream, inlet 11 is evenly arranged along 1 peripheral wall of flotation cylinder, 1 housing of flotation cylinder Equipped with annular inlet tube 10, annular inlet tube 10, which is equipped with, corresponds the liquid outlet being connected to each inlet 10 by branch pipe, Annular inlet tube 10 is equipped with the total mouth 9 of feed liquor, and the axis of the total mouth 9 of feed liquor and the axis of annular inlet tube 10 are tangent, the total mouth 9 of feed liquor It is connected to by tube body with liquid feed device.
It should be noted that in practical applications, bubble generator 14 includes tube body 19, and tube body 19 is by the receipts that are sequentially connected to The draw, trunnion and diffuser composition, the output end of diffuser are docked with efferent duct, the input end of collapsible tube and closed gas-liquid Mixing chamber docking, gas-liquid mixed room are equipped with pressed gas air inlet pipe 22 and fluid injection pipe 21, are equipped with spiral in efferent duct Blade 29, efferent duct are docked with the bubble import of bubble distributer 15.The bubble generator of above structure combines high pressure solution gas The method that deposition method and Venturi tube jet stream are formed at two kinds of microvesicles of bubble, the bubble size of formation are stablized in 0.1-0.3mm.It needs Illustrate, in actual design, bubble generator 14 is arranged circumferentially along flotation cylinder 1, and bubble distributer 15 includes same The heart is horizontally disposed and passes through at least two that connecting tube 151 is connected annular gas distribution pipes 152, uniformly distributed on each annular gas distribution pipe 152 There is venthole (not shown), is located at outermost annular gas distribution pipe 152 and is equipped with and each bubble generator 14 one-to-one correspondence Bubble import.
Specifically, this implementation, using two annular gas distribution pipes 152, the diameter ratio of two annular gas distribution pipes 152 is 1:2, even Adapter tube 151 is evenly arranged in the annular space between two annular gas distribution pipes, sets that there are four air inlets on outermost layer annular gas distribution pipe 152 Mouthful, to being connected to a bubble distributer on each air inlet.Pressurised stream enters from the fluid injection pipe of bubble generator, adds It presses air to enter from the air inlet pipe of bubble generator, forms a large amount of micro-bubbles at diffuser, bubble is entered by air inlet Shape gas distribution pipe, and sprayed by the venthole on shape gas distribution pipe, the rising bubble for being evenly distributed stable is formed in flotation column body.
It preferably, is further bubble disintegration, the axis of fluid injection pipe 21 is overlapped with the axis of trunnion, fluid injection pipe 21 arrange with air inlet pipe 22 in angle, and the size of angle is 40-45 °, and the cone angle of collapsible tube is 30-35 °, and the cone angle of diffuser is 35-40 °, the longitudinal length ratio of collapsible tube, trunnion and diffuser is 1:4:2, and the spout of fluid injection pipe 21 is that cone angle is 15-20 ° of conical nozzle, by above-mentioned setting, bubble size can be refined further.
As a kind of preferred embodiment of fluidization coarse flotation equipment of the present invention, the fan that turbulence plate 12 is obliquely installed by three pieces Shape plate head and the tail are mutually spliced, and shape is in the taper of falling water chestnut, and fanning strip tilt angle angle with horizontal plane is 30~35 °, turbulence plate The perforation 13 that feed flow stream passes through is evenly equipped on 12, perforate 13 axis it is parallel with the axis of flotation cylinder 1, the cone of turbulence plate 12 Bottom is equipped with and is connected to outlet 8 with flotation cylinder bottom gape, is equipped with the ore discharge valve 18 automatically controlled at gape.Flotation cylinder 1 In be equipped with sensor 17 for detecting composite interference bed density in cylinder, at the top of flotation cylinder 1 by bracket 4 be equipped with The controller 5 that sensor 17 communicates to connect, controller 5 carry out ore discharge operation according to the density domination ore discharge valve 18 of interference bed, When density reaches a certain level, controller opens ore discharge valve 18 and tailing is discharged.
Working principle of the present invention is as follows: when fluidization coarse flotation equipment works, pressurised stream and forced air point Do not enter mixed foaming in bubble generator from fluid injection pipe 21 and air inlet pipe 22, is formed in efferent duct output end a large amount of small Bubble, bubble enter bubble distributer 15 by air inlet, are sprayed by the venthole on bubble distributer 15, and full of entire The cross section of cylinder forms the stable micro air bubble that is evenly distributed in cylinder.Water flow driven by pressure through the total mouth 9 of feed liquor into Enter and enter cylinder bottom along each inlet 11 after annular inlet tube 10, then from 13 vertical up-spray of perforation on turbulence plate 12 Out, stable ascending current is formed in cylinder, and is full of the cross section of entire cylinder.The small gas that bubble distributer 15 generates The ascending current that bubble and turbulence plate 12 are formed, which exists simultaneously in cylinder and forms collaboration, rises situation, is fed by rationally adjusting The air pressure of air and the hydraulic pressure of water flow can form stable gas-liquid compound flowing stateization interference bed, at this in cylinder In gas-liquid compound flowing stateization interference bed, the coarse granule containing target minreal is by the buoyancy and ascending current simultaneously by bubble Vertical lift, thus particle can adhere to bubble and constantly rise and enter overflow launder 2 becomes concentrate, and gangue mineral does not have bubble Adherency, final subsidence become tailing through the discharge of gape 8.
A kind of method of fluidization coarse flotation equipment flotation, water flow 23 is after the pressurization of the first force (forcing) pump 24, through feed liquor Total mouth 9 enters in flotation cylinder 1 through annular inlet tube 10, and, cylinder in shape spouting through the perforation 13 on turbulence plate 12 At ascending current.Air 29 enters bubble generator 14 after the compression of air compressor 28, through air inlet pipe 22, and water flow 23 is by the The pressurization of two force (forcing) pumps 25, foaming agent 27 is added in the water flow pressurizeed by the second force (forcing) pump 25 after the emulsification of emulsifier 26, through fluid Injection pipe 21 enters bubble generator 14, and bubble generator 14 generates a large amount of micro air bubbles and is passed through bubble distributer 15, bubble Bubble is dispersed in cylinder by distributor 15.Bubble and ascending current form stable gas-liquid compound flowing state in cylinder Change interference bed.Ore pulp 30 is delivered in mixing cirtern 32 through the first delivery pump 31, is added pH regulator 33 into mixing cirtern 32, is stirred Rear ore pulp to be mixed to enter in mixing cirtern 32, addition collecting agent 35 stirs, it is delivered in feed barrel 37 after sizing mixing through the second delivery pump 36, Feed barrel 37 is fixed on cylinder top, and the ore pulp in feed barrel 37 is entered in feeding inlet 3 by pipeline 39, by mine distributor 16 Enter in cylinder after (mine distributor is preferably umbrella shape mine distributor) dispersion and slowly declines along the entire section of cylinder, it is compound in gas-liquid Fluidization interferes ore particle and bubble and ascending current in bed to act on, buoyancy and ascending current of the final purpose mineral through bubble Vertical lift, which constantly rises and then overflows cylinder, enters overflow launder as concentrate, and gangue mineral sinks in cylinder and finally from Gape discharge becomes tailing.Obtained concentrate can be further processed recycling, and tailing can be directly as most finality Mine is discharged from the process flow of " ore grinding-flotation ", realizes the throwing tail of gangue mineral.
Below with reference to specific application examples, the present invention is further illustrated.
Application examples 1
Test material is certain copper-sulphide ores.Ore enters cyclone classification after ball mill ore grinding, obtain granularity 150~ The ore pulp of 1000 μm or so partial sizes gives mine raw material, copper grade 0.52% as experiment, and 600 μm or less grade accountings are 85% Left and right.It is 8.0 that ore pulp, which is added pH regulator and adjusts pH values of pulp, and the stirring of collecting agent butyl xanthate is then added and sizes mixing, terpenic oil is added Foaming agent is passed through sufficiently size mixing after, feed fluidization coarse flotation equipment from feeding inlet and carry out flotation, overflow product is as coarse-fine Mine, and underflow becomes tailing through gape discharge, the tailing is directly as true tailings.Collecting agent is with respect to the additional amount of raw ore 200g/t, foaming agent 30g/t, pH regulator are sodium carbonate, and flotation temperature is 25 DEG C.Test obtains rough concentrate Cu grade 1.29%, the rate of recovery 92.78%, tailing Cu grade 0.06%, yield 62.60%, the copper loss for throwing portion, which is lost, is only 7.22% (such as table 1).
The fluidization coarse flotation equipment test result of 1 certain copper-sulphide ores of table
Application examples 2
Test material is certain molybdenite.Ore enters cyclone classification after ball mill ore grinding, obtain granularity 150~ The ore pulp of 1000 μm or so partial sizes gives mine raw material as experiment, and molybdenum grade is 0.17%, and 600 μm or less grade accountings are 90% Left and right.It is 8.0 that ore pulp, which is added pH regulator and adjusts pH values of pulp, and collecting agent butyl xanthate is then added and black powder stirring is sized mixing, is added Terpenic oil foaming agent is passed through sufficiently size mixing after, feed fluidization coarse flotation equipment from feeding inlet and carry out flotation, overflow product is For rough concentrate, and underflow becomes tailing through gape discharge, and the tailing is directly as true tailings.Collecting agent adds with respect to raw ore Entering amount butyl xanthate is 150g/t, and black powder 50g/t, foaming agent 20g/t, pH regulator is sodium carbonate, and flotation temperature is 25 DEG C. Test obtains rough concentrate Mo grade 0.373%, the rate of recovery 94.21%, tailing Mo grade 0.017%, yield 57.40%, throwing The molybdenum loss of portion is only 5.79% (such as table 2).
The fluidization coarse flotation equipment test result of 2 certain molybdenite of table
Application examples 3
Test material is certain scheelite.Ore enters cyclone classification after ball mill ore grinding, obtain granularity 150~ The ore pulp of 1000 μm or so partial sizes gives mine raw material, WO as experiment3Grade is 0.41%, and 600 μm or less grade accountings are 78% or so.It is 9.5 that ore pulp, which is added pH regulator and adjusts pH values of pulp, and the stirring of complex collecting agent is then added and sizes mixing, pine is added Alcohol oil foaming agent is passed through sufficiently size mixing after, feed fluidization coarse flotation equipment from feeding inlet and carry out flotation, overflow product is Rough concentrate, and underflow becomes tailing through gape discharge, the tailing is directly as true tailings.Addition of the collecting agent with respect to raw ore Amount plumbi nitras is 600g/t, and benzyl hydroximic acid 500g/t, foaming agent 40g/t, pH regulator is sodium carbonate, and flotation temperature is 25℃.Test obtains rough concentrate WO3Grade 0.86%, the rate of recovery 87.02%, tailing WO3Grade 0.091%, yield are 58.50%, throw the WO of portion3Loss is only 12.98% (such as table 3).
The fluidization coarse flotation equipment test result of 3 certain scheelite of table
Application examples 4
Test material is certain cassiterite mine.Ore enters cyclone classification after ball mill ore grinding, obtain granularity 150~ The ore pulp of 1000 μm or so partial sizes gives mine raw material, SnO as experiment2Grade is 0.332%, and 600 μm or less grade accountings are 75% or so.It is 8.5 that ore pulp, which is added pH regulator and adjusts pH values of pulp, and the stirring of complex collecting agent is then added and sizes mixing, pine is added Alcohol oil foaming agent is passed through sufficiently size mixing after, feed fluidization coarse flotation equipment from feeding inlet and carry out flotation, overflow product is Rough concentrate, and underflow becomes tailing through gape discharge, the tailing is directly as true tailings.Addition of the collecting agent with respect to raw ore Amount plumbi nitras is 400g/t, and benzyl hydroximic acid 400g/t, foaming agent 50g/t, pH regulator is sodium carbonate, and flotation temperature is 25℃.Test obtains rough concentrate SnO2Grade 0.78%, the rate of recovery 86.10%, tailing SnO2Grade 0.073%, yield are 63.30%, throw the SnO of portion2Loss is only 13.90% (such as table 4).
The fluidization coarse flotation equipment test result of 4 certain cassiterite of table
Application examples 5
Test material is certain cerussite.Ore enters cyclone classification after ball mill ore grinding, obtain granularity 150~ The ore pulp of 1000 μm or so partial sizes gives mine raw material as experiment, and Pb grade is 4.36%, and 600 μm or less grade accountings are 91% Left and right.It is 8.0 that ore pulp, which is added pH regulator and adjusts pH values of pulp, and collecting agent stirring is then added and sizes mixing, terpenic oil foaming agent is added It passes through after sufficiently sizing mixing, feeds fluidization coarse flotation equipment from feeding inlet and carry out flotation, overflow product is rough concentrate, and bottom Flowing through gape discharge becomes tailing, and the tailing is directly as true tailings.Collecting agent is with respect to the additional amount vulcanized sodium of raw ore 4000g/t, butyl xanthate 300g/t, foaming agent 20g/t, pH regulator are sodium carbonate, and flotation temperature is 25 DEG C.Test obtains Rough concentrate Pb grade 7.72%, the rate of recovery 90.60%, tailing Pb grade 0.84%, yield 48.80% throw the lead of portion Loss is only 9.40% (such as table 5).
The fluidization coarse flotation equipment test result of 5 certain cerussite of table
Above-described embodiment is only to clearly demonstrate examples made by the present invention, rather than the restriction to embodiment.For For those of ordinary skill in the art, other various forms of variations or change can also be made on the basis of the above description It is dynamic.Here without can not be also exhaustive to all embodiments.And the obvious variation or change thus amplified out It is dynamic to be still in the protection scope of this invention.

Claims (10)

1. a kind of fluidization coarse flotation equipment, comprising:
Flotation cylinder, top are equipped with overflow launder and charging gear;
Bubble generator is arranged on the flotation cylinder;
Bubble distributer is arranged in the flotation column body and is connected with the bubble generator;
It is characterized by: flotation cylinder lower end is equipped with inlet, the bubble distributer is located at the top of the inlet, Turbulence plate is equipped in the flotation column body between the inlet and bubble distributer.
2. fluidization coarse flotation equipment according to claim 1, it is characterised in that:
The bubble generator includes the collapsible tube, trunnion and diffuser being sequentially connected to, the output end of the diffuser with it is defeated Outlet pipe docking, the input end of the collapsible tube are docked with closed gas-liquid mixed room, and the gas-liquid mixed room is equipped with pressure gas Body air inlet pipe and fluid injection pipe, the efferent duct is interior to be equipped with helical blade, the efferent duct and the bubble distributer Bubble import docking.
3. fluidization coarse flotation equipment according to claim 2, it is characterised in that: the bubble generator is along flotation column Body is arranged circumferentially, and the bubble distributer includes at least two annulars that are horizontally disposed with one heart and being connected by connecting tube Gas distribution pipe is evenly equipped with venthole on each annular gas distribution pipe, is located at outermost annular gas distribution pipe and is equipped with and each gas Steep the one-to-one bubble import of generator.
4. fluidization coarse flotation equipment according to claim 2, it is characterised in that: the axis of the fluid injection pipe with The axis of the trunnion is overlapped, and the fluid injection pipe and the air inlet pipe are arranged in angle, and the size of the angle is 40- 45°。
5. fluidization coarse flotation equipment according to claim 2, it is characterised in that: the cone angle of the collapsible tube is 30- 35 °, the cone angle of the diffuser is 35-40 °, and the longitudinal length ratio of the collapsible tube, trunnion and diffuser is 1:4:2, The spout of the fluid injection pipe is the conical nozzle that cone angle is 15-20 °.
6. fluidization coarse flotation equipment according to claim 1, it is characterised in that: in the feeding inlet at the top of flotation cylinder Equipped with tripper.
7. fluidization coarse flotation equipment according to claim 1-6, it is characterised in that: the turbulence plate is in Water chestnut taper, is evenly equipped with the perforation that feed flow stream passes through on the turbulence plate, the cone bottom of the turbulence plate directly with flotation cylinder bottom Gape is connected to, and the ore discharge valve automatically controlled is equipped at the gape.
8. fluidization coarse flotation equipment according to claim 7, it is characterised in that: the inlet is along flotation cylinder week Wall is evenly arranged.
9. fluidization coarse flotation equipment according to claim 7, it is characterised in that: the flotation column is arranged with ring in vitro Shape inlet tube, the annular inlet tube, which is equipped with, corresponds the liquid outlet being connected to, the annular feed liquor with each inlet Pipe is equipped with the total mouth of feed liquor, and the axis of the total mouth of feed liquor and the axis of the annular inlet tube are tangent.
10. a kind of method for floating using the described in any item fluidization coarse flotation equipment of claim 1-9, feature exist In including the following steps:
S1: opening liquid feed device, and pressurised stream enters flotation column body from flotation cylinder lower end inlet, after turbulence plate, Uniform ascending current is formed in flotation column body;
S2: air enters bubble generator through bubble generator air inlet after air compressor compresses, and foaming agent is through emulsifier It is added after emulsification in the water flow pressurizeed by force (forcing) pump, and enters in bubble generator through bubble generator water inlet, bubble occurs A large amount of micro air bubbles that device generates are passed through bubble distributer, and bubble is dispersed in flotation column body by bubble distributer, bubble Stable gas-liquid compound flowing stateization interference bed is formed in flotation column body with ascending current;
S3: ore pulp and floating agent are sized mixing after agitator sufficiently acts on and pass through charging gear at the top of flotation cylinder through mine distributor Enter in flotation column body after dispersion and slowly decline along the entire section of flotation cylinder, in gas-liquid compound flowing stateization interference bed Ore particle and bubble and ascending current act on, and the vertical lift of buoyancy and ascending current of the final purpose mineral through bubble constantly rises And then overflow cylinder and enter overflow launder as concentrate, and gangue mineral sinks in cylinder and finally becomes tail from gape discharge Mine.
CN201811246340.7A 2018-10-24 2018-10-24 Fluidized coarse grain flotation equipment and flotation method Active CN108970813B (en)

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CN201811246340.7A CN108970813B (en) 2018-10-24 2018-10-24 Fluidized coarse grain flotation equipment and flotation method

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Application Number Priority Date Filing Date Title
CN201811246340.7A CN108970813B (en) 2018-10-24 2018-10-24 Fluidized coarse grain flotation equipment and flotation method

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Cited By (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109453902A (en) * 2018-12-29 2019-03-12 江苏大丰新安德矿业有限公司 A kind of floating magnetic separation column device and combined type bubble generator
CN110586340A (en) * 2019-09-30 2019-12-20 郑州大学 Coarse particle mineral hydraulic flotation equipment and method based on orifice plate hydraulic cavitation bubble formation
CN110813519A (en) * 2019-11-25 2020-02-21 郑州大学 Method for protecting crystalline graphite flakes by improving mineral separation process of graphite ore
CN110882829A (en) * 2019-12-11 2020-03-17 郑州大学 Coarse particle tailing discarding sorting system based on hydraulic flotation technology
CN110882850A (en) * 2019-12-11 2020-03-17 郑州大学 Mineral separation system and mineral separation method for protecting graphite flakes
WO2020181758A1 (en) * 2019-03-14 2020-09-17 中国矿业大学 Wide-size-fraction flotation system and process
CN111974746A (en) * 2020-08-21 2020-11-24 中国石油大学(华东) Device for cleaning filler by flotation bubbles and cleaning method
CN112391864A (en) * 2020-11-13 2021-02-23 郑州磊展科技造纸机械有限公司 Flotation deinking machine for removing printing ink in waste paper pulp by utilizing air flotation principle
CN112474025A (en) * 2020-11-16 2021-03-12 福州大学 Calcite acid triggering-hydraulic flotation method
CN112474034A (en) * 2020-11-16 2021-03-12 福州大学 Magnesite acid triggering-fluidization separation method
CN113198619A (en) * 2021-05-18 2021-08-03 中南大学 Coarse particle flotation equipment and method adopting rotational flow and damping coupled fluidization
CN113578532A (en) * 2021-07-25 2021-11-02 张雪峰 Ore flotation equipment with adjustable
CN114733651A (en) * 2022-05-06 2022-07-12 江苏泓顺硅基半导体科技有限公司 Continuous flotation machine for producing high-purity quartz sand in semiconductor field
CN114950741A (en) * 2022-04-27 2022-08-30 江苏泓顺硅基半导体科技有限公司 Method for removing feldspar in quartz sand by flotation

Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5431286A (en) * 1994-01-06 1995-07-11 Inco Limited Recirculating column flotation apparatus
CN201399385Y (en) * 2009-03-11 2010-02-10 湖南省电力粉煤灰开发有限公司 Dedicated flotation column for fly ash
US20100193408A1 (en) * 2007-02-26 2010-08-05 Newcastle Innovation Limited Method and apparatus for flotation in a fluidized bed
CN101844104A (en) * 2010-04-15 2010-09-29 河南理工大学 Hydraulic classifier
CN103464057A (en) * 2013-09-06 2013-12-25 天津聚贤达科技有限公司 Novel gas distributor
CN103657839A (en) * 2013-12-09 2014-03-26 中国矿业大学 Gas-liquid-solid three-phase fluidized bed sorting machine and sorting method thereof
CN104632216A (en) * 2015-01-16 2015-05-20 中国矿业大学 Rotary jet self-priming type short-range strengthening foam production device for dust suppression of coal mining machine
CN105689155A (en) * 2016-04-08 2016-06-22 中国矿业大学 Multi-product flotation column separation equipment and method
CN209020582U (en) * 2018-10-24 2019-06-25 中南大学 A kind of fluidization coarse flotation equipment

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5431286A (en) * 1994-01-06 1995-07-11 Inco Limited Recirculating column flotation apparatus
US20100193408A1 (en) * 2007-02-26 2010-08-05 Newcastle Innovation Limited Method and apparatus for flotation in a fluidized bed
CN201399385Y (en) * 2009-03-11 2010-02-10 湖南省电力粉煤灰开发有限公司 Dedicated flotation column for fly ash
CN101844104A (en) * 2010-04-15 2010-09-29 河南理工大学 Hydraulic classifier
CN103464057A (en) * 2013-09-06 2013-12-25 天津聚贤达科技有限公司 Novel gas distributor
CN103657839A (en) * 2013-12-09 2014-03-26 中国矿业大学 Gas-liquid-solid three-phase fluidized bed sorting machine and sorting method thereof
CN104632216A (en) * 2015-01-16 2015-05-20 中国矿业大学 Rotary jet self-priming type short-range strengthening foam production device for dust suppression of coal mining machine
CN105689155A (en) * 2016-04-08 2016-06-22 中国矿业大学 Multi-product flotation column separation equipment and method
CN209020582U (en) * 2018-10-24 2019-06-25 中南大学 A kind of fluidization coarse flotation equipment

Cited By (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109453902A (en) * 2018-12-29 2019-03-12 江苏大丰新安德矿业有限公司 A kind of floating magnetic separation column device and combined type bubble generator
CN109453902B (en) * 2018-12-29 2023-11-07 江苏大丰新安德矿业有限公司 Floating magnetic separation column device and combined bubble generator
WO2020181758A1 (en) * 2019-03-14 2020-09-17 中国矿业大学 Wide-size-fraction flotation system and process
CN110586340A (en) * 2019-09-30 2019-12-20 郑州大学 Coarse particle mineral hydraulic flotation equipment and method based on orifice plate hydraulic cavitation bubble formation
CN110586340B (en) * 2019-09-30 2021-11-02 郑州大学 Coarse particle mineral hydraulic flotation equipment and method based on orifice plate hydraulic cavitation bubble formation
CN110813519A (en) * 2019-11-25 2020-02-21 郑州大学 Method for protecting crystalline graphite flakes by improving mineral separation process of graphite ore
CN110882829A (en) * 2019-12-11 2020-03-17 郑州大学 Coarse particle tailing discarding sorting system based on hydraulic flotation technology
CN110882850A (en) * 2019-12-11 2020-03-17 郑州大学 Mineral separation system and mineral separation method for protecting graphite flakes
CN111974746B (en) * 2020-08-21 2021-09-24 中国石油大学(华东) Device for cleaning filler by flotation bubbles and cleaning method
CN111974746A (en) * 2020-08-21 2020-11-24 中国石油大学(华东) Device for cleaning filler by flotation bubbles and cleaning method
CN112391864A (en) * 2020-11-13 2021-02-23 郑州磊展科技造纸机械有限公司 Flotation deinking machine for removing printing ink in waste paper pulp by utilizing air flotation principle
CN112474025A (en) * 2020-11-16 2021-03-12 福州大学 Calcite acid triggering-hydraulic flotation method
CN112474034A (en) * 2020-11-16 2021-03-12 福州大学 Magnesite acid triggering-fluidization separation method
CN113198619A (en) * 2021-05-18 2021-08-03 中南大学 Coarse particle flotation equipment and method adopting rotational flow and damping coupled fluidization
CN113198619B (en) * 2021-05-18 2022-02-11 中南大学 Coarse particle flotation equipment and method adopting rotational flow and damping coupled fluidization
CN113578532A (en) * 2021-07-25 2021-11-02 张雪峰 Ore flotation equipment with adjustable
CN113578532B (en) * 2021-07-25 2022-12-27 平利县篮泰重晶石工贸有限公司 Ore flotation equipment with adjustable
CN114950741A (en) * 2022-04-27 2022-08-30 江苏泓顺硅基半导体科技有限公司 Method for removing feldspar in quartz sand by flotation
CN114733651A (en) * 2022-05-06 2022-07-12 江苏泓顺硅基半导体科技有限公司 Continuous flotation machine for producing high-purity quartz sand in semiconductor field

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