CN111962288A - Silver ion anti-discoloration silk pantyhose and production process thereof - Google Patents

Silver ion anti-discoloration silk pantyhose and production process thereof Download PDF

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Publication number
CN111962288A
CN111962288A CN202010710799.9A CN202010710799A CN111962288A CN 111962288 A CN111962288 A CN 111962288A CN 202010710799 A CN202010710799 A CN 202010710799A CN 111962288 A CN111962288 A CN 111962288A
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Prior art keywords
parts
silver ion
pantyhose
silk
aes
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陶然
李金品
苏海革
李德凤
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Zhejiang Yongchun Technology Co ltd
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Zhejiang Yongchun Technology Co ltd
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Priority to CN202010710799.9A priority Critical patent/CN111962288A/en
Publication of CN111962288A publication Critical patent/CN111962288A/en
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    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • A—HUMAN NECESSITIES
    • A41—WEARING APPAREL
    • A41B—SHIRTS; UNDERWEAR; BABY LINEN; HANDKERCHIEFS
    • A41B11/00—Hosiery; Panti-hose
    • A41B11/14—Panti-hose; Body-stockings
    • A—HUMAN NECESSITIES
    • A41—WEARING APPAREL
    • A41B—SHIRTS; UNDERWEAR; BABY LINEN; HANDKERCHIEFS
    • A41B17/00—Selection of special materials for underwear
    • D—TEXTILES; PAPER
    • D02—YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
    • D02G—CRIMPING OR CURLING FIBRES, FILAMENTS, THREADS, OR YARNS; YARNS OR THREADS
    • D02G3/00—Yarns or threads, e.g. fancy yarns; Processes or apparatus for the production thereof, not otherwise provided for
    • D02G3/02—Yarns or threads characterised by the material or by the materials from which they are made
    • D02G3/04—Blended or other yarns or threads containing components made from different materials
    • D02G3/045—Blended or other yarns or threads containing components made from different materials all components being made from artificial or synthetic material
    • D—TEXTILES; PAPER
    • D02—YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
    • D02G—CRIMPING OR CURLING FIBRES, FILAMENTS, THREADS, OR YARNS; YARNS OR THREADS
    • D02G3/00—Yarns or threads, e.g. fancy yarns; Processes or apparatus for the production thereof, not otherwise provided for
    • D02G3/22—Yarns or threads characterised by constructional features, e.g. blending, filament/fibre
    • D02G3/34—Yarns or threads having slubs, knops, spirals, loops, tufts, or other irregular or decorative effects, i.e. effect yarns
    • D—TEXTILES; PAPER
    • D03—WEAVING
    • D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
    • D03D15/00—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B15/00—Removing liquids, gases or vapours from textile materials in association with treatment of the materials by liquids, gases or vapours
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B3/00—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating
    • D06B3/04—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating of yarns, threads or filaments
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B3/00—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating
    • D06B3/30—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating of articles, e.g. stockings
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/77—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
    • D06M11/79—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof with silicon dioxide, silicic acids or their salts
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    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
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    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/005—Compositions containing perfumes; Compositions containing deodorants
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    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
    • D06M13/188—Monocarboxylic acids; Anhydrides, halides or salts thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
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    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
    • D06M13/207—Substituted carboxylic acids, e.g. by hydroxy or keto groups; Anhydrides, halides or salts thereof
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    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
    • A—HUMAN NECESSITIES
    • A41—WEARING APPAREL
    • A41B—SHIRTS; UNDERWEAR; BABY LINEN; HANDKERCHIEFS
    • A41B2400/00—Functions or special features of shirts, underwear, baby linen or handkerchiefs not provided for in other groups of this subclass
    • A41B2400/34—Functions or special features of shirts, underwear, baby linen or handkerchiefs not provided for in other groups of this subclass antimicrobial or antibacterial
    • A—HUMAN NECESSITIES
    • A41—WEARING APPAREL
    • A41B—SHIRTS; UNDERWEAR; BABY LINEN; HANDKERCHIEFS
    • A41B2500/00—Materials for shirts, underwear, baby linen or handkerchiefs not provided for in other groups of this subclass
    • A41B2500/20—Woven
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    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
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    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/16—Synthetic fibres, other than mineral fibres
    • D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M2101/32—Polyesters
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    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/16—Synthetic fibres, other than mineral fibres
    • D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M2101/34—Polyamides
    • D—TEXTILES; PAPER
    • D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2331/00—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products
    • D10B2331/02—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products polyamides
    • D—TEXTILES; PAPER
    • D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2331/00—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products
    • D10B2331/04—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products polyesters, e.g. polyethylene terephthalate [PET]

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Materials Engineering (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention discloses silver ion anti-fading silk pantyhose which comprise the following components in parts by weight: 30-40 parts of polyester yarn, 30-40 parts of nylon yarn, 60-80 parts of nylon yarn, 10-20 parts of silver ion solution, 10-12 parts of 3-hydroxybenzoic acid, 6-10 parts of plant saponin, 6-8 parts of fatty acid salt amphoteric antistatic agent, 8-10 parts of muscovite powder, 1-3 parts of antibacterial agent, 5-9 parts of anti-fading auxiliary agent and 6-8 parts of anti-mosquito emulsion. The invention has the technical effects of strong antibacterial performance, good deodorization effect, crack prevention, no silk scattering and mosquito removal effect.

Description

Silver ion anti-discoloration silk pantyhose and production process thereof
Technical Field
The invention relates to the technical field of silk pantyhose formula and technology, in particular to silver ion anti-fading silk pantyhose and a production technology thereof.
Background
The silk stockings are the second layer of skin of women and are also a necessity in modern female life, most of the silk stockings on the market at present are third-generation silk stockings, and are generally woven in vertical and horizontal directions by nylon and high-quality stretch yarns. Although the elasticity is good, the hand feeling is soft, the silk stockings are damaged and taken off occasionally in the use process due to the thin texture, and even the whole stocking ring is taken off after continuous use, so that the wearing comfort and the aesthetic property are greatly influenced. The existing pure nylon silk stockings are wear-resistant and high in elasticity and are deeply favored by consumers, but the nylon silk stockings generate static electricity when being rubbed with clothes, so that discomfort is easily caused, and meanwhile, the nylon silk does not absorb sweat, so that bacteria are easily remained in the silk stockings to cause skin inflammation; for many years, the sock is mainly used for keeping warm and protecting feet, and after people wear the sock for a long time, a large amount of bacteria can be bred in the sock, so that beriberi and foot odor are caused, and people with abundant feet sweat are particularly so that the life of people is inconvenient. In recent years, socks with antibacterial function are more and more concerned by people, some manufacturers use natural bamboo carbon fibers, castor fibers or chitin fibers to manufacture socks, and although the socks have certain antibacterial property, the socks also have some defects, namely, the production cost is high, the abrasion resistance of the socks is poor, and the socks are easy to wrinkle and break after being washed for many times. Some manufacturers coat the silica gel layer on the surface of the silk stockings, so that the silk stockings have an antibacterial effect, but lose the original air permeability and flexibility of the silk stockings and have poor wearing comfort; people wear the fabric in summer, especially women wear the fabric very cool, and the skin exposed outside is easy to be bitten by mosquitoes, which brings troubles to the life of people. Most women go out and are not sprayed because of the poor taste of floral water, so that the skin is bitten at many places.
Therefore, the silver ion anti-discoloration silk pantyhose and the production process thereof have the advantages of strong antibacterial performance, good deodorization effect, crack prevention, no silk scattering and mosquito removal effect.
Disclosure of Invention
The invention aims to provide silver ion anti-fading silk pantyhose and a production process thereof, so as to solve the problems in the background technology.
In order to realize the purpose, the invention provides the following technical scheme: silver ion anti-fading silk pantyhose comprise the following components in parts by weight: 30-40 parts of polyester yarn, 30-40 parts of nylon yarn, 60-80 parts of nylon yarn, 10-20 parts of silver ion solution, 10-12 parts of 3-hydroxybenzoic acid, 6-10 parts of plant saponin, 6-8 parts of fatty acid salt amphoteric antistatic agent, 8-10 parts of muscovite powder, 1-3 parts of antibacterial agent, 5-9 parts of anti-fading auxiliary agent and 6-8 parts of anti-mosquito emulsion.
Preferably, the anti-decoloration auxiliary agent is prepared by mixing AES, starch transaminase, dimethyl phenyl acetate, AES mate thickener, polyethylene glycol, ramination, sodium octadecyl benzene sulfonate, sodium oleate, cation agglomerate and water.
Preferably, the anti-fading auxiliary agent comprises the following components in parts by weight: the modified anion exchange resin comprises, by weight, 15-20 parts of AES, 6-10 parts of starch transaminase, 6-10 parts of dimethyl phenyl acetate, 3-5 parts of AES mate thickener, 20-30 parts of polyethylene glycol, 3-5 parts of Ramipron, 8-12 parts of sodium octadecyl benzene sulfonate, 2-3 parts of sodium oleate, 1-2 parts of cation agglomerate and 40-60 parts of water.
Preferably, the method comprises the steps of fully and uniformly mixing AES, starch transaminase, dimethyl phenyl acetate and AES mate thickener, adding polyethylene glycol, ramination, sodium oleate and cation agglomerate, adding water, fully stirring and dissolving by using a stirrer, and finally adding sodium octadecyl benzene sulfonate for thickening.
Preferably, the mosquito-proof emulsion is prepared by mixing methyl salicylate, argy wormwood leaf oil, eucalyptus citriodora oil, amomum villosum leaf oil, base oil and a volatile auxiliary agent.
Preferably, the mosquito-proof emulsion comprises the following components in parts by weight: 6-10 parts of methyl salicylate, 8-10 parts of argyi leaf oil, 6-8 parts of eucalyptus citriodora oil, 12-14 parts of amomum villosum leaf oil, 4-8 parts of base oil and 2-6 parts of volatile auxiliary agents.
Preferably, the antimicrobial agent is prepared by mixing an organic metal compound, licorice, mint and water.
Preferably, the antibacterial agent comprises the following components in parts by weight: 6-10 parts of organic metal compound, 10-12 parts of liquorice, 6-8 parts of mint and 20-30 parts of water.
Preferably, the organometallic compound is an organocopper compound, an organozinc compound or an organomercury compound.
A preparation process of silver ion anti-discoloration silk pantyhose specifically comprises the following steps:
the method comprises the following steps: soaking polyester yarns, nylon yarns and nylon yarns in a silver ion solution for 1-2 days, drying by using an air heater, melting the polyester yarns, the nylon yarns and the nylon yarns, and then mutually bonding to prepare the reticular anti-drop core-spun yarns;
step two: cutting the prepared short fibers, uniformly mixing, carrying out coarse carding and fine carding by a carding machine, and then carrying out drawing and fine carding;
step three: taking one chemical fiber filament as a core filament, twisting the other chemical fiber filament to form a coating yarn of the chemical fiber filament, preparing a composite yarn, and finally performing warp and weft weaving on the composite yarn;
step four: weaving a waist of trousers, weaving a left leg, weaving a right leg and weaving a crotch part, wherein the left leg comprises an upper trousers body and a lower sock cylinder, and the right leg comprises an upper trousers body and a lower sock cylinder to prepare a semi-finished silk pantyhose;
step five: immersing the semi-finished silk pantyhose again in the silver ion solution for 2-3 h, then uniformly mixing 3-hydroxybenzoic acid, plant saponin, a fatty acid salt amphoteric antistatic agent, muscovite powder and an antibacterial agent, adding the mixture into the silver ion solution, controlling the temperature to be 20-30 ℃, and immersing for 1-2 h;
step six: spraying an anti-mosquito emulsion and a silver ion solution on the surface of the semi-finished silk stockings at the temperature of 30-40 ℃, and performing air drying treatment to obtain dry blanks;
step seven: controlling the temperature at 80-90 ℃ and the pH value at 7-9, fixing the finished dried blank, dyeing, and adding an anti-decoloration auxiliary agent in the dyeing process to obtain a silk pantyhose blank;
step eight: and (3) washing the dyed semi-finished silk pantyhose for 20-30 min, and heating, drying and shaping by adopting steam at 220-280 ℃ to obtain the finished silk pantyhose.
Compared with the prior art, the invention has the beneficial effects that:
1. silver ions are positive cations formed by silver atoms losing one or more electrons, such as Ag +, Ag2+, Ag3+ and the like; the antibacterial and antibacterial pantyhose can inhibit the reproduction of fungi to prevent and treat tinea pedis and smelly feet by preparing the pantyhose from silver-plated fibers; when a trace amount of silver ions reach the cell membrane of the microorganism, the silver ions are charged with negative charges and are firmly adsorbed by coulomb attraction, penetrate through the cell wall to enter the cell and react with SH groups to solidify proteins, destroy the activity of cell synthetase, and the cell loses division and proliferation capacity to die.
2. In the production process, the polyester yarns, the nylon yarns and the nylon yarns are soaked in the silver ion solution for 1-2 days, then are dried by using an air heater, are melted and then are bonded with each other to prepare the netted anti-dropping core-spun yarns, and are combined with the fatty acid salt amphoteric antistatic agent, so that static electricity generated among the polyester yarns, the nylon yarns and the nylon yarns is reduced, and the technical effect of better anti-cracking and non-loosing yarns is realized.
3. The mosquito-proof emulsion is prepared by emulsifying mosquito-proof liquid consisting of methyl salicylate, argyi leaf oil, eucalyptus citriodora oil, amomum villosum leaf oil, base oil and a volatile auxiliary agent. The prepared mosquito-proof silk stockings can effectively protect the leg skin of cool women wearing in summer and prevent mosquito bites.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
Silver ion anti-fading silk pantyhose comprise the following components in parts by weight: 30 parts of polyester yarn, 30 parts of nylon yarn, 60 parts of nylon yarn, 10 parts of silver ion solution, 10 parts of 3-hydroxybenzoic acid, 6 parts of plant saponin, 6 parts of fatty acid salt amphoteric antistatic agent, 8 parts of muscovite powder, 1 part of antibacterial agent, 5 parts of anti-fading auxiliary agent and 6 parts of anti-mosquito emulsion.
In this embodiment, the anti-decoloring auxiliary agent is prepared by mixing AES, starch transaminase, dimethyl phenyl acetate, an AES partner thickener, polyethylene glycol, ramination, sodium octadecyl benzene sulfonate, sodium oleate, a cationic agglomerate, and water.
In this embodiment, the anti-discoloration auxiliary comprises the following components in parts by weight: AES15 parts, 6 parts of starch transaminase, 6 parts of dimethyl phenyl acetate, 3 parts of AES mate thickener, 20 parts of polyethylene glycol, 3 parts of Ramipron, 8 parts of sodium octadecyl benzene sulfonate, 2 parts of sodium oleate, 1 part of cation agglomerate and 40 parts of water.
In the embodiment, AES, starch transaminase, dimethylacetophenone and an AES mate thickener are fully and uniformly mixed, then polyethylene glycol, ramination, sodium oleate and cation agglomerates are added, water is added, a stirrer is used for fully stirring and dissolving, and finally sodium octadecylbenzene sulfonate is added for thickening.
In the embodiment, the mosquito-proof emulsion is prepared by mixing methyl salicylate, argy wormwood leaf oil, eucalyptus citriodora oil, amomum villosum leaf oil, base oil and a volatile auxiliary agent.
In the embodiment, the mosquito-proof emulsion comprises the following components in parts by weight: 6 parts of methyl salicylate, 8 parts of argyi leaf oil, 6 parts of lemon eucalyptus oil, 12 parts of villous amomum leaf oil, 4 parts of base oil and 2 parts of volatile auxiliary agent.
In this embodiment, the antimicrobial agent is formed by mixing an organic metal compound, licorice, mint and water.
In the embodiment, the antibacterial agent comprises the following components in parts by weight: 6 parts of organic metal compound, 10 parts of liquorice, 6 parts of mint and 20 parts of water.
In this embodiment, the organometallic compound is an organic copper compound, an organic zinc compound, or an organic mercury compound.
Example 2
Silver ion anti-fading silk pantyhose comprise the following components in parts by weight: 40 parts of polyester yarn, 40 parts of nylon yarn, 80 parts of nylon yarn, 20 parts of silver ion solution, 12 parts of 3-hydroxybenzoic acid, 10 parts of plant saponin, 8 parts of fatty acid salt amphoteric antistatic agent, 10 parts of muscovite powder, 3 parts of antibacterial agent, 9 parts of anti-fading auxiliary agent and 8 parts of anti-mosquito emulsion.
In this embodiment, the anti-decoloring auxiliary agent is prepared by mixing AES, starch transaminase, dimethyl phenyl acetate, an AES partner thickener, polyethylene glycol, ramination, sodium octadecyl benzene sulfonate, sodium oleate, a cationic agglomerate, and water.
In this embodiment, the anti-discoloration auxiliary comprises the following components in parts by weight: 120 parts of AES, 10 parts of starch transaminase, 10 parts of dimethyl phenyl acetate, 5 parts of AES mate thickener, 30 parts of polyethylene glycol, 5 parts of Ramipron, 12 parts of sodium octadecyl benzene sulfonate, 3 parts of sodium oleate, 2 parts of cation agglomerate and 60 parts of water.
In the embodiment, AES, starch transaminase, dimethylacetophenone and an AES mate thickener are fully and uniformly mixed, then polyethylene glycol, ramination, sodium oleate and cation agglomerates are added, water is added, a stirrer is used for fully stirring and dissolving, and finally sodium octadecylbenzene sulfonate is added for thickening.
In the embodiment, the mosquito-proof emulsion is prepared by mixing methyl salicylate, argy wormwood leaf oil, eucalyptus citriodora oil, amomum villosum leaf oil, base oil and a volatile auxiliary agent.
In the embodiment, the mosquito-proof emulsion comprises the following components in parts by weight: 10 parts of methyl salicylate, 10 parts of argyi leaf oil, 8 parts of lemon eucalyptus oil, 14 parts of villous amomum leaf oil, 8 parts of base oil and 6 parts of volatile auxiliary agent.
In this embodiment, the antimicrobial agent is formed by mixing an organic metal compound, licorice, mint and water.
In the embodiment, the antibacterial agent comprises the following components in parts by weight: 10 parts of organic metal compound, 12 parts of liquorice, 8 parts of mint and 30 parts of water.
In this embodiment, the organometallic compound is an organic copper compound, an organic zinc compound, or an organic mercury compound.
Example 3
Silver ion anti-fading silk pantyhose comprise the following components in parts by weight: 35 parts of polyester yarn, 35 parts of nylon yarn, 70 parts of nylon yarn, 15 parts of silver ion solution, 11 parts of 3-hydroxybenzoic acid, 7 parts of plant saponin, 7 parts of fatty acid salt amphoteric antistatic agent, 9 parts of muscovite powder, 2 parts of antibacterial agent, 7 parts of anti-fading auxiliary agent and 7 parts of anti-mosquito emulsion.
In this embodiment, the anti-decoloring auxiliary agent is prepared by mixing AES, starch transaminase, dimethyl phenyl acetate, an AES partner thickener, polyethylene glycol, ramination, sodium octadecyl benzene sulfonate, sodium oleate, a cationic agglomerate, and water.
In this embodiment, the anti-discoloration auxiliary comprises the following components in parts by weight: AES17 parts, 8 parts of starch transaminase, 8 parts of dimethyl phenyl acetate, 4 parts of AES mate thickener, 25 parts of polyethylene glycol, 4 parts of Ramipron, 10 parts of sodium octadecyl benzene sulfonate, 3 parts of sodium oleate, 2 parts of cation agglomerate and 50 parts of water.
In the embodiment, AES, starch transaminase, dimethylacetophenone and an AES mate thickener are fully and uniformly mixed, then polyethylene glycol, ramination, sodium oleate and cation agglomerates are added, water is added, a stirrer is used for fully stirring and dissolving, and finally sodium octadecylbenzene sulfonate is added for thickening.
In the embodiment, the mosquito-proof emulsion is prepared by mixing methyl salicylate, argy wormwood leaf oil, eucalyptus citriodora oil, amomum villosum leaf oil, base oil and a volatile auxiliary agent.
In the embodiment, the mosquito-proof emulsion comprises the following components in parts by weight: 8 parts of methyl salicylate, 9 parts of argyi leaf oil, 7 parts of lemon eucalyptus oil, 13 parts of villous amomum leaf oil, 6 parts of base oil and 4 parts of volatile auxiliary agent.
In this embodiment, the antimicrobial agent is formed by mixing an organic metal compound, licorice, mint and water.
In the embodiment, the antibacterial agent comprises the following components in parts by weight: 8 parts of organic metal compound, 11 parts of liquorice, 7 parts of mint and 25 parts of water.
In this embodiment, the organometallic compound is an organic copper compound, an organic zinc compound, or an organic mercury compound.
Example 4
Silver ion anti-fading silk pantyhose comprise the following components in parts by weight: 35 parts of polyester yarn, 35 parts of nylon yarn, 70 parts of nylon yarn, 11 parts of 3-hydroxybenzoic acid, 7 parts of plant saponin, 7 parts of fatty acid salt amphoteric antistatic agent, 9 parts of muscovite powder, 2 parts of antibacterial agent, 7 parts of anti-fading auxiliary agent and 7 parts of anti-mosquito emulsion.
In this embodiment, the anti-decoloring auxiliary agent is prepared by mixing AES, starch transaminase, dimethyl phenyl acetate, an AES partner thickener, polyethylene glycol, ramination, sodium octadecyl benzene sulfonate, sodium oleate, a cationic agglomerate, and water.
In this embodiment, the anti-discoloration auxiliary comprises the following components in parts by weight: AES17 parts, 8 parts of starch transaminase, 8 parts of dimethyl phenyl acetate, 4 parts of AES mate thickener, 25 parts of polyethylene glycol, 4 parts of Ramipron, 10 parts of sodium octadecyl benzene sulfonate, 3 parts of sodium oleate, 2 parts of cation agglomerate and 50 parts of water.
In the embodiment, AES, starch transaminase, dimethylacetophenone and an AES mate thickener are fully and uniformly mixed, then polyethylene glycol, ramination, sodium oleate and cation agglomerates are added, water is added, a stirrer is used for fully stirring and dissolving, and finally sodium octadecylbenzene sulfonate is added for thickening.
In the embodiment, the mosquito-proof emulsion is prepared by mixing methyl salicylate, argy wormwood leaf oil, eucalyptus citriodora oil, amomum villosum leaf oil, base oil and a volatile auxiliary agent.
In the embodiment, the mosquito-proof emulsion comprises the following components in parts by weight: 8 parts of methyl salicylate, 9 parts of argyi leaf oil, 7 parts of lemon eucalyptus oil, 13 parts of villous amomum leaf oil, 6 parts of base oil and 4 parts of volatile auxiliary agent.
In this embodiment, the antimicrobial agent is formed by mixing an organic metal compound, licorice, mint and water.
In the embodiment, the antibacterial agent comprises the following components in parts by weight: 8 parts of organic metal compound, 11 parts of liquorice, 7 parts of mint and 25 parts of water.
In this embodiment, the organometallic compound is an organic copper compound, an organic zinc compound, or an organic mercury compound.
Example 5
Silver ion anti-fading silk pantyhose comprise the following components in parts by weight: 35 parts of polyester yarn, 35 parts of nylon yarn, 70 parts of nylon yarn, 15 parts of silver ion solution, 11 parts of 3-hydroxybenzoic acid, 7 parts of plant saponin, 7 parts of fatty acid salt amphoteric antistatic agent, 9 parts of muscovite powder, 7 parts of anti-fading auxiliary agent and 7 parts of anti-mosquito emulsion.
In this embodiment, the anti-decoloring auxiliary agent is prepared by mixing AES, starch transaminase, dimethyl phenyl acetate, an AES partner thickener, polyethylene glycol, ramination, sodium octadecyl benzene sulfonate, sodium oleate, a cationic agglomerate, and water.
In this embodiment, the anti-discoloration auxiliary comprises the following components in parts by weight: AES17 parts, 8 parts of starch transaminase, 8 parts of dimethyl phenyl acetate, 4 parts of AES mate thickener, 25 parts of polyethylene glycol, 4 parts of Ramipron, 10 parts of sodium octadecyl benzene sulfonate, 3 parts of sodium oleate, 2 parts of cation agglomerate and 50 parts of water.
In the embodiment, AES, starch transaminase, dimethylacetophenone and an AES mate thickener are fully and uniformly mixed, then polyethylene glycol, ramination, sodium oleate and cation agglomerates are added, water is added, a stirrer is used for fully stirring and dissolving, and finally sodium octadecylbenzene sulfonate is added for thickening.
In the embodiment, the mosquito-proof emulsion is prepared by mixing methyl salicylate, argy wormwood leaf oil, eucalyptus citriodora oil, amomum villosum leaf oil, base oil and a volatile auxiliary agent.
In the embodiment, the mosquito-proof emulsion comprises the following components in parts by weight: 8 parts of methyl salicylate, 9 parts of argyi leaf oil, 7 parts of lemon eucalyptus oil, 13 parts of villous amomum leaf oil, 6 parts of base oil and 4 parts of volatile auxiliary agent.
In this embodiment, the antimicrobial agent is formed by mixing an organic metal compound, licorice, mint and water.
In the embodiment, the antibacterial agent comprises the following components in parts by weight: 8 parts of organic metal compound, 11 parts of liquorice, 7 parts of mint and 25 parts of water.
In this embodiment, the organometallic compound is an organic copper compound, an organic zinc compound, or an organic mercury compound.
A preparation process of silver ion anti-discoloration silk pantyhose specifically comprises the following steps:
the method comprises the following steps: soaking polyester yarns, nylon yarns and nylon yarns in a silver ion solution for 1-2 days, drying by using an air heater, melting the polyester yarns, the nylon yarns and the nylon yarns, and then mutually bonding to prepare the reticular anti-drop core-spun yarns;
step two: cutting the prepared short fibers, uniformly mixing, carrying out coarse carding and fine carding by a carding machine, and then carrying out drawing and fine carding;
step three: taking one chemical fiber filament as a core filament, twisting the other chemical fiber filament to form a coating yarn of the chemical fiber filament, preparing a composite yarn, and finally performing warp and weft weaving on the composite yarn;
step four: weaving a waist of trousers, weaving a left leg, weaving a right leg and weaving a crotch part, wherein the left leg comprises an upper trousers body and a lower sock cylinder, and the right leg comprises an upper trousers body and a lower sock cylinder to prepare a semi-finished silk pantyhose;
step five: immersing the semi-finished silk pantyhose again in the silver ion solution for 2-3 h, then uniformly mixing 3-hydroxybenzoic acid, plant saponin, a fatty acid salt amphoteric antistatic agent, muscovite powder and an antibacterial agent, adding the mixture into the silver ion solution, controlling the temperature to be 20-30 ℃, and immersing for 1-2 h;
step six: spraying an anti-mosquito emulsion and a silver ion solution on the surface of the semi-finished silk stockings at the temperature of 30-40 ℃, and performing air drying treatment to obtain dry blanks;
step seven: controlling the temperature at 80-90 ℃ and the pH value at 7-9, fixing the finished dried blank, dyeing, and adding an anti-decoloration auxiliary agent in the dyeing process to obtain a silk pantyhose blank;
step eight: and (3) washing the dyed semi-finished silk pantyhose for 20-30 min, and heating, drying and shaping by adopting steam at 220-280 ℃ to obtain the finished silk pantyhose.
Experiment one: the tests of antibacterial ability were carried out on the silk pantyhose prepared in the above examples 1, 2, 3, 4, 5 and on the silk pantyhose of the prior art: the method is mainly evaluated by three indexes, namely minimum antibacterial mass concentration (MIC), minimum bactericidal mass concentration (MBC) and bactericidal rate (%); the test data indices are shown in the following table:
Figure BDA0002596475930000111
Figure BDA0002596475930000121
the experimental results are as follows: the antimicrobial capacity of the silk pantyhose prepared in example 1, example 2, example 3 and example 5 was the same and significantly higher than the antimicrobial capacity of the silk pantyhose of example 4 and the prior art.
Experiment two: the silk pantyhose prepared in examples 1, 2, 3, 4, 5 above and the silk pantyhose of the prior art were subjected to an anti-splitting non-raveling performance test: the prepared pantyhose were placed in a stirring device and the time h required to crack the loose filaments for the first time was observed.
Figure BDA0002596475930000122
The experimental results are as follows: the silk stockings prepared in the examples 1, 2, 3, 4 and 5 have the anti-cracking and non-loosing silk performance which is obviously higher than that of the silk stockings in the prior art.
Compared with the prior art, the invention has the beneficial effects that: silver ions are positive cations formed by silver atoms losing one or more electrons, such as Ag +, Ag2+, Ag3+ and the like; the antibacterial and antibacterial pantyhose can inhibit the reproduction of fungi to prevent and treat tinea pedis and smelly feet by preparing the pantyhose from silver-plated fibers; when a trace amount of silver ions reach the cell membrane of the microorganism, the silver ions are charged with negative charges and are firmly adsorbed by coulomb attraction, penetrate through the cell wall to enter the cell and react with SH groups to solidify proteins, destroy the activity of cell synthetase, and the cell loses division and proliferation capacity to die. According to the silver ion anti-fading silk pantyhose and the production process thereof, after the polyester yarns, the polyamide yarns and the nylon yarns are soaked in the silver ion solution for 1-2 d, an air heater is used for drying, the polyester yarns, the polyamide yarns and the nylon yarns are subjected to melting treatment and then are bonded with one another to prepare the netted anti-fading core-spun yarns, and the netted anti-fading core-spun yarns are combined with the fatty acid salt amphoteric antistatic agent to reduce static electricity generated among the polyester yarns, the polyamide yarns and the nylon yarns and achieve the better technical effect of anti-cracking and non-loosing yarns. The silver ion anti-fading silk stockings and the production process thereof are woven by silk threads dyed with anti-mosquito emulsion, and the anti-mosquito emulsion is prepared by emulsifying anti-mosquito liquid consisting of methyl salicylate, argy wormwood leaf oil, lemon eucalyptus oil, amomum villosum leaf oil, base oil and volatile auxiliary agents. The prepared mosquito-proof silk stockings can effectively protect the leg skin of cool women wearing in summer and prevent mosquito bites.
It will be apparent to those skilled in the art that various changes and modifications may be made in the present invention without departing from the spirit and scope of the invention. Thus, if such modifications and variations of the present invention fall within the scope of the claims of the present invention and their equivalents, the present invention is also intended to include such modifications and variations.

Claims (10)

1. The utility model provides a silver ion anticreep silk panty hose which characterized in that: the composition comprises the following components in parts by weight: 30-40 parts of polyester yarn, 30-40 parts of nylon yarn, 60-80 parts of nylon yarn, 10-20 parts of silver ion solution, 10-12 parts of 3-hydroxybenzoic acid, 6-10 parts of plant saponin, 6-8 parts of fatty acid salt amphoteric antistatic agent, 8-10 parts of muscovite powder, 1-3 parts of antibacterial agent, 5-9 parts of anti-fading auxiliary agent and 6-8 parts of anti-mosquito emulsion.
2. The silver ion depigmenting pantyhose according to claim 1, wherein: the anti-decoloration auxiliary agent is prepared by mixing AES, starch transaminase, dimethyl phenyl acetate, AES mate thickener, polyethylene glycol, ramination, sodium octadecyl benzene sulfonate, sodium oleate, cation agglomerate and water.
3. The silver ion depigmenting pantyhose according to claim 2, wherein: the anti-fading auxiliary agent comprises the following components in parts by weight: the modified anion exchange resin comprises, by weight, 15-20 parts of AES, 6-10 parts of starch transaminase, 6-10 parts of dimethyl phenyl acetate, 3-5 parts of AES mate thickener, 20-30 parts of polyethylene glycol, 3-5 parts of Ramipron, 8-12 parts of sodium octadecyl benzene sulfonate, 2-3 parts of sodium oleate, 1-2 parts of cation agglomerate and 40-60 parts of water.
4. The silver ion depigmenting pantyhose according to claim 2, wherein: the method comprises the steps of fully and uniformly mixing AES, starch transaminase, dimethyl phenyl acetate and AES mate thickener, adding polyethylene glycol, ramine, sodium oleate and cation agglomerate, adding water, fully stirring and dissolving by using a stirrer, and finally adding sodium octadecylbenzene sulfonate for thickening.
5. The silver ion depigmenting pantyhose according to claim 1, wherein: the mosquito-proof emulsion is prepared by mixing methyl salicylate, argy wormwood leaf oil, eucalyptus citriodora oil, villous amomum leaf oil, base oil and volatile auxiliary agents.
6. The silver ion depigmenting pantyhose according to claim 5, wherein: the mosquito-proof emulsion comprises the following components in parts by weight: 6-10 parts of methyl salicylate, 8-10 parts of argyi leaf oil, 6-8 parts of eucalyptus citriodora oil, 12-14 parts of amomum villosum leaf oil, 4-8 parts of base oil and 2-6 parts of volatile auxiliary agents.
7. The silver ion depigmenting pantyhose according to claim 1, wherein: the antibacterial agent is prepared by mixing organic metal compound, liquorice, mint and water.
8. The silver ion depigmenting pantyhose according to claim 7, wherein: the antibacterial agent comprises the following components in parts by weight: 6-10 parts of organic metal compound, 10-12 parts of liquorice, 6-8 parts of mint and 20-30 parts of water.
9. The silver ion depigmenting pantyhose according to claim 8, wherein: the organic metal compound is an organic copper compound, an organic zinc compound or an organic mercury compound.
10. A preparation process of silver ion anti-discoloration silk pantyhose is characterized by comprising the following steps: the method specifically comprises the following steps:
the method comprises the following steps: soaking polyester yarns, nylon yarns and nylon yarns in a silver ion solution for 1-2 days, drying by using an air heater, melting the polyester yarns, the nylon yarns and the nylon yarns, and then mutually bonding to prepare the reticular anti-drop core-spun yarns;
step two: cutting the prepared short fibers, uniformly mixing, carrying out coarse carding and fine carding by a carding machine, and then carrying out drawing and fine carding;
step three: taking one chemical fiber filament as a core filament, twisting the other chemical fiber filament to form a coating yarn of the chemical fiber filament, preparing a composite yarn, and finally performing warp and weft weaving on the composite yarn;
step four: weaving a waist of trousers, weaving a left leg, weaving a right leg and weaving a crotch part, wherein the left leg comprises an upper trousers body and a lower sock cylinder, and the right leg comprises an upper trousers body and a lower sock cylinder to prepare a semi-finished silk pantyhose;
step five: immersing the semi-finished silk pantyhose again in the silver ion solution for 2-3 h, then uniformly mixing 3-hydroxybenzoic acid, plant saponin, a fatty acid salt amphoteric antistatic agent, muscovite powder and an antibacterial agent, adding the mixture into the silver ion solution, controlling the temperature to be 20-30 ℃, and immersing for 1-2 h;
step six: spraying an anti-mosquito emulsion and a silver ion solution on the surface of the semi-finished silk stockings at the temperature of 30-40 ℃, and performing air drying treatment to obtain dry blanks;
step seven: controlling the temperature at 80-90 ℃ and the pH value at 7-9, fixing the finished dried blank, dyeing, and adding an anti-decoloration auxiliary agent in the dyeing process to obtain a silk pantyhose blank;
step eight: and (3) washing the dyed semi-finished silk pantyhose for 20-30 min, and heating, drying and shaping by adopting steam at 220-280 ℃ to obtain the finished silk pantyhose.
CN202010710799.9A 2020-07-22 2020-07-22 Silver ion anti-discoloration silk pantyhose and production process thereof Pending CN111962288A (en)

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