CN111902385A - 改进的制备卤化烷烃的方法 - Google Patents

改进的制备卤化烷烃的方法 Download PDF

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Publication number
CN111902385A
CN111902385A CN201980022005.5A CN201980022005A CN111902385A CN 111902385 A CN111902385 A CN 111902385A CN 201980022005 A CN201980022005 A CN 201980022005A CN 111902385 A CN111902385 A CN 111902385A
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CN
China
Prior art keywords
combination
halogenated
reactor
reaction mixture
olefin
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201980022005.5A
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English (en)
Chinese (zh)
Inventor
J·D·迈尔斯
M·泰勒维乔乔
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Blue Cube Intellectual Property Co ltd
Original Assignee
Blue Cube Intellectual Property Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Blue Cube Intellectual Property Co ltd filed Critical Blue Cube Intellectual Property Co ltd
Publication of CN111902385A publication Critical patent/CN111902385A/zh
Pending legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C19/00—Acyclic saturated compounds containing halogen atoms
    • C07C19/01—Acyclic saturated compounds containing halogen atoms containing chlorine
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/26—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton
    • C07C17/272—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions
    • C07C17/275—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions of hydrocarbons and halogenated hydrocarbons
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053—Details of the reactor
    • B01J19/0066—Stirrers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1812—Tubular reactors
    • B01J19/1818—Tubular reactors in series
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/72—Copper
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/74—Iron group metals
    • B01J23/745—Iron
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/18—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes containing nitrogen, phosphorus, arsenic or antimony as complexing atoms, e.g. in pyridine ligands, or in resonance therewith, e.g. in isocyanide ligands C=N-R or as complexed central atoms
    • B01J31/1845—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes containing nitrogen, phosphorus, arsenic or antimony as complexing atoms, e.g. in pyridine ligands, or in resonance therewith, e.g. in isocyanide ligands C=N-R or as complexed central atoms the ligands containing phosphorus
    • B01J31/185—Phosphites ((RO)3P), their isomeric phosphonates (R(RO)2P=O) and RO-substitution derivatives thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00162—Controlling or regulating processes controlling the pressure
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C19/00—Acyclic saturated compounds containing halogen atoms
    • C07C19/01—Acyclic saturated compounds containing halogen atoms containing chlorine
    • C07C19/03—Chloromethanes
    • C07C19/041—Carbon tetrachloride

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CN201980022005.5A 2018-04-03 2019-04-02 改进的制备卤化烷烃的方法 Pending CN111902385A (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201862652033P 2018-04-03 2018-04-03
US62/652,033 2018-04-03
PCT/US2019/025332 WO2019195247A1 (en) 2018-04-03 2019-04-02 Improved processes for preparing halogenated alkanes

Publications (1)

Publication Number Publication Date
CN111902385A true CN111902385A (zh) 2020-11-06

Family

ID=66223835

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201980022005.5A Pending CN111902385A (zh) 2018-04-03 2019-04-02 改进的制备卤化烷烃的方法

Country Status (5)

Country Link
US (1) US11192841B2 (https=)
EP (1) EP3774702B1 (https=)
JP (1) JP2021520379A (https=)
CN (1) CN111902385A (https=)
WO (1) WO2019195247A1 (https=)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2022115151A1 (en) * 2020-11-30 2022-06-02 Blue Cube Ip Llc Method for treating a heavy byproduct stream from chlorinated propane production
CN116535287B (zh) * 2023-07-04 2023-09-05 山东澳帆新材料有限公司 一种1,1,1,3,3-五氯丙烷的合成方法
CN116986966B (zh) * 2023-09-21 2023-12-12 淄博澳帆化工有限公司 一种1,1,1,3,3-五氯丙烷连续制备的方法

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1199387A (zh) * 1995-08-14 1998-11-18 联合讯号公司 用于制造卤代烷烃的方法
US6300532B1 (en) * 1998-12-15 2001-10-09 Alliedsignal Inc. Process for addition of haloalkanes to alkenes catalyzed by an organophosphite compound
US6313360B1 (en) * 2000-09-29 2001-11-06 Vulcan Materials Company Process for the manufacture of 1, 1, 1, 3, 3-pentachloropropane
JP2012254950A (ja) * 2011-06-08 2012-12-27 Tokuyama Corp ポリクロロプロパンの製造方法
CN105026346A (zh) * 2013-02-04 2015-11-04 霍尼韦尔国际公司 1，1，2，3-四氯丙烯的合成
CN107001191A (zh) * 2014-10-16 2017-08-01 化学和冶金生产联合体股份公司 方法

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4650914A (en) 1983-07-06 1987-03-17 Monsanto Company Process for producing 1,1,2,3-tetrachloropropene
US6720466B2 (en) * 2002-04-17 2004-04-13 Vulcan Chemicals, a division of Vulcan Materials Company 1,1,1,3,3-pentachloropropane process purge stream concentration using a secondary refluxed evaporator and secondary product recovery
US8835702B2 (en) * 2011-06-03 2014-09-16 Honeywell International Inc. Method for mitigating the formation of by-products during the production of haloalkane compounds
US8722946B2 (en) * 2011-06-03 2014-05-13 Honeywell International Inc. Method for avoiding the generation of by-products during the production of haloalkane compounds
JP6173908B2 (ja) * 2013-12-27 2017-08-02 株式会社トクヤマ クロロ高次アルケンの製造方法
TWI702202B (zh) * 2014-10-16 2020-08-21 捷克商史波克專業化學杭尼維洛普合股公司 用於製備高純度1,1,1,2,3-五氯丙烷產物之方法

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1199387A (zh) * 1995-08-14 1998-11-18 联合讯号公司 用于制造卤代烷烃的方法
US6300532B1 (en) * 1998-12-15 2001-10-09 Alliedsignal Inc. Process for addition of haloalkanes to alkenes catalyzed by an organophosphite compound
US6313360B1 (en) * 2000-09-29 2001-11-06 Vulcan Materials Company Process for the manufacture of 1, 1, 1, 3, 3-pentachloropropane
JP2012254950A (ja) * 2011-06-08 2012-12-27 Tokuyama Corp ポリクロロプロパンの製造方法
CN105026346A (zh) * 2013-02-04 2015-11-04 霍尼韦尔国际公司 1，1，2，3-四氯丙烯的合成
CN107001191A (zh) * 2014-10-16 2017-08-01 化学和冶金生产联合体股份公司 方法

Also Published As

Publication number Publication date
EP3774702A1 (en) 2021-02-17
JP2021520379A (ja) 2021-08-19
EP3774702B1 (en) 2022-04-27
US20210107849A1 (en) 2021-04-15
WO2019195247A1 (en) 2019-10-10
US11192841B2 (en) 2021-12-07

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