CN111841314A - Ionized negative ion spray and preparation method thereof - Google Patents
Ionized negative ion spray and preparation method thereof Download PDFInfo
- Publication number
- CN111841314A CN111841314A CN202010822378.5A CN202010822378A CN111841314A CN 111841314 A CN111841314 A CN 111841314A CN 202010822378 A CN202010822378 A CN 202010822378A CN 111841314 A CN111841314 A CN 111841314A
- Authority
- CN
- China
- Prior art keywords
- parts
- negative ion
- solution
- ionized
- titanium
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/74—General processes for purification of waste gases; Apparatus or devices specially adapted therefor
- B01D53/86—Catalytic processes
- B01D53/8668—Removing organic compounds not provided for in B01D53/8603 - B01D53/8665
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
- A01N25/04—Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
- A01N25/06—Aerosols
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/16—Heavy metals; Compounds thereof
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2255/00—Catalysts
- B01D2255/80—Type of catalytic reaction
- B01D2255/802—Photocatalytic
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2258/00—Sources of waste gases
- B01D2258/06—Polluted air
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Dentistry (AREA)
- Environmental & Geological Engineering (AREA)
- Plant Pathology (AREA)
- Pest Control & Pesticides (AREA)
- Agronomy & Crop Science (AREA)
- Dispersion Chemistry (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Toxicology (AREA)
- Biomedical Technology (AREA)
- Analytical Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Disinfection, Sterilisation Or Deodorisation Of Air (AREA)
Abstract
An ionized negative ion spray is prepared from the following materials in parts by weight: 5-10 parts of tourmaline negative ion powder, 2-5 parts of nano silver-titanium powder, 5-10 parts of plant extract and 900 parts of water. The nano silver-titanium powder is prepared by adopting a coprecipitation method, and the ionized negative ion spray can sterilize, decompose peculiar smell, remove formaldehyde, decompose bacteria and viruses and remove harmful gases.
Description
Technical Field
The invention belongs to the technical field of air purification, and particularly relates to ionized negative ion spray and a preparation method thereof.
Background
At present, PM2.5 and PM10 particles are caused to the environment by industrial development, harmful substances such as TVOC (total volatile organic compound), ammonia, benzene, formaldehyde and the like in indoor air are threatened to the life safety of human bodies by indoor environment decorations, and meanwhile, the texture of the decorations can be kept.
The nano-titanium silver particles, the plant liquid and the deionized water can decompose harmful substances by photocatalysis, oxidize and decompose bacteria and viruses, remove formaldehyde in a special effect, thoroughly decompose peculiar smell, and protect decorations and ionize negative oxygen ions while removing harmful substance gas.
In view of the above background, there is a need to develop a series of spray products for decomposing odor, ionizing negative oxygen ions, removing formaldehyde, decomposing bacteria and viruses, and protecting ornaments, in order to improve the quality of life and ensure the safety of daily life.
Disclosure of Invention
The invention aims to provide an ionized negative ion spray and a preparation method thereof, wherein the ionized negative ion spray has the effects of sterilizing, decomposing peculiar smell, removing formaldehyde, decomposing bacteria and viruses and removing harmful gas by using tourmaline, nano silver-titanium and plant essence, so that the final performance of the product meets the requirement. The key point of the project is that the novel tourmaline and the nano silver-titanium react with the water in the air to generate biological performance, and are neutral, not corroded and not left in different proportions, so that the safety, the stability and the durability of the final product which is used and accords with food grade are ensured.
The ionization negative ion spray is prepared from the following materials in parts by weight:
5-10 parts of tourmaline negative ion powder, 2-5 parts of nano silver-titanium powder, 5-10 parts of plant extract and 900 parts of water.
The tourmaline negative ion powder contains silicate substances with ring structure of aluminum, sodium, iron and lithium, which contains boron.
The preparation method of the nano silver-titanium powder comprises the following steps:
(1) taking 1mol/L metatitanic acid aqueous solution with a certain volume according to a metering ratio, and dropwise adding 10% ammonia water until the pH value is 7 to prepare solution A;
(2) 1mol/L silver nitrate with a certain volume is taken according to a metering ratio, and 0.5mol/L sodium carbonate solution is dripped to the pH value of 7.5 to prepare a solution B;
(3) dropwise adding the solution B obtained in the step (2) into the solution A obtained in the step (1) at 70 ℃ under stirring, continuously stirring for 3 hours, cooling to room temperature, standing for 2 hours, performing suction filtration, and washing with absolute ethyl alcohol; drying at 120 ℃ for one day, heating to 450 ℃ in air at the speed of 2 ℃/min, roasting for 5 hours, and finally preparing the nano silver-titanium material by a mechanical grinding method; wherein the molar ratio of titanium to silver is 5-10: 1.
The preparation method of the plant extract comprises the following steps:
(1) putting 10 parts of mint, 10 parts of cactus and 10 parts of cactus into 50-60 parts of pure water, smashing the mixture into pulp by a beating machine, adding an active carbon decolorant and stirring for 20 minutes; and (2) filtering by using a centrifugal filter to obtain filtrate.
Wherein the mint, the cactus and the cactus have synergistic effect on removing formaldehyde.
The preparation method of the ionized negative ion spray comprises the following steps:
(1) blending tourmaline negative ion powder and nano silver-titanium powder in a nanometer way, then adding one fifth of the total amount of water, adopting a constant temperature turbine stirring technology, filtering by a filter element with extremely fine diameter, and forming a liquid phase mixed solution which is uniformly dispersed, wherein the particle diameter of the dispersed nano material is between 3 and 5nm, and the nano material is in a spherical shape;
(2) adding the plant essence and the rest water, and uniformly mixing to obtain the ionized negative ion spray.
The ionized negative ion spray has the following beneficial effects: can sterilize, decompose peculiar smell, remove formaldehyde, decompose bacteria and viruses, and remove harmful gas.
Detailed Description
The present invention will be specifically described below by way of examples.
Example 1
7 parts of tourmaline negative ion powder, 4 parts of nano silver-titanium powder, 6 parts of plant extract and 850 parts of water.
The preparation method of the nano silver-titanium powder comprises the following steps:
(1) taking 1mol/L metatitanic acid aqueous solution with a certain volume according to a metering ratio, and dropwise adding 10% ammonia water until the pH value is 7 to prepare solution A;
(2) 1mol/L silver nitrate with a certain volume is taken according to a metering ratio, and 0.5mol/L sodium carbonate solution is dripped to the pH value of 7.5 to prepare a solution B;
(3) dropwise adding the solution B obtained in the step (2) into the solution A obtained in the step (1) at 70 ℃ under stirring, continuously stirring for 3 hours, cooling to room temperature, standing for 2 hours, performing suction filtration, and washing with absolute ethyl alcohol; drying at 120 ℃ for one day, heating to 450 ℃ in air at the speed of 2 ℃/min, roasting for 5 hours, and finally preparing the nano silver-titanium material by a mechanical grinding method; wherein the molar ratio of titanium to silver is 8: 1.
The preparation method of the plant extract comprises the following steps:
(1) putting 10 parts of mint, 10 parts of cactus and 10 parts of cactus into 60 parts of pure water, smashing the mixture into pulp by a beating machine, adding an active carbon decolorant and stirring for 20 minutes; and (2) filtering by using a centrifugal filter to obtain filtrate.
The preparation method of the ionized negative ion spray comprises the following steps:
(1) blending tourmaline negative ion powder and nano silver-titanium powder in a nanometer way, then adding one fifth of the total amount of water, adopting a constant temperature turbine stirring technology, filtering by a filter element with extremely fine diameter, and forming a liquid phase mixed solution which is uniformly dispersed, wherein the particle size of the dispersed nano material is between 3nm and 5nm, and the nano material is in a spherical shape;
(2) adding the plant essence and the rest water, and uniformly mixing to obtain the ionized negative ion spray.
The ionized negative ion spray is uniformly sprayed in a newly bought great wall automobile, and the effect of the embodiment 1 is as follows:
1) removing formaldehyde; not less than 90%
2) Removing staphylococcus aureus: not less than 99.9%;
3) removing escherichia coli: not less than 99.9 percent
4) Removing candida albicans: not less than 99.9%;
5) removing pseudomonas aeruginosa; not less than 99.9 percent
6) Ionizing negative ions: not less than 3000
7) The characteristics are as follows: high formaldehyde eliminating effect, high bacteria and virus decomposing effect, high oxygen resistance, and lasting creep resistance and strength.
8) Appearance: no crystal point, no impurity, transparency and no peculiar smell.
Comparative example 1
The plant extract was prepared by using only 30 parts of peppermint, and the formaldehyde removal rate was only 83% under the same use conditions as in example 1.
Comparative example 2
The plant extract was prepared by using only 30 parts of cacumen biotae, and the formaldehyde removal rate was only 84% under the same conditions as in example 1.
Comparative example 3
The plant extract was prepared by using 30 parts of cactus, and the formaldehyde removal rate was only 88% under the same conditions as in example 1.
Comparative example 4
The same as example 1 except that the nano silver and the nano titanium dioxide are directly mixed, under the same using conditions, the formaldehyde removal rate is only 88%, and the removal rate of staphylococcus aureus is only 89%, which indicates that the sterilization and formaldehyde removal rates are good when the silver and the titanium dioxide are in close contact, and the respective dispersion state effects are poor.
Claims (4)
1. The ionized negative ion spray is characterized by being prepared from the following materials in parts by weight: 5-10 parts of tourmaline negative ion powder, 2-5 parts of nano silver-titanium powder, 5-10 parts of plant extract and 900 parts of water.
2. The ionized negative ion spray of claim 1, wherein the nano silver-titanium powder is prepared by the following steps:
(1) taking 1mol/L metatitanic acid aqueous solution with a certain volume according to a metering ratio, and dropwise adding 10% ammonia water until the pH value is 7 to prepare solution A;
(2) 1mol/L silver nitrate with a certain volume is taken according to a metering ratio, and 0.5mol/L sodium carbonate solution is dripped to the pH value of 7.5 to prepare a solution B;
(3) dropwise adding the solution B obtained in the step (2) into the solution A obtained in the step (1) at 70 ℃ under stirring, continuously stirring for 3 hours, cooling to room temperature, standing for 2 hours, performing suction filtration, and washing with absolute ethyl alcohol; drying at 120 ℃ for one day, heating to 450 ℃ in air at the speed of 2 ℃/min, roasting for 5 hours, and finally preparing the nano silver-titanium material by a mechanical grinding method; wherein the molar ratio of titanium to silver is 5-10: 1.
3. The ionized negative ion spray of claim 1, wherein the plant extract is prepared by the following method:
(1) putting 10 parts of mint, 10 parts of cactus and 10 parts of cactus into 50-60 parts of pure water, smashing the mixture into pulp by a beating machine, adding an active carbon decolorant and stirring for 20 minutes; and (2) filtering by using a centrifugal filter to obtain filtrate.
4. The method for preparing the ionized anion spray according to claim 1, which is characterized in that (1) tourmaline anion powder and nano silver-titanium powder are blended in a nanometer mode, one fifth of the total amount of water is added, a constant-temperature turbine stirring technology is adopted, and after the mixture is filtered by a filter element with an extremely fine diameter, a uniformly dispersed liquid phase mixed solution is formed, wherein the particle size of the dispersed nano material is between 3 and 5nm, and the nano material is in a spherical shape;
(2) adding the plant essence and the rest water, and mixing to obtain the ionized anion spray.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010822378.5A CN111841314A (en) | 2020-08-17 | 2020-08-17 | Ionized negative ion spray and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010822378.5A CN111841314A (en) | 2020-08-17 | 2020-08-17 | Ionized negative ion spray and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN111841314A true CN111841314A (en) | 2020-10-30 |
Family
ID=72969059
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202010822378.5A Withdrawn CN111841314A (en) | 2020-08-17 | 2020-08-17 | Ionized negative ion spray and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN111841314A (en) |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5935608A (en) * | 1996-04-15 | 1999-08-10 | Nittetsu Mining Co., Ltd. | Antibacterial titania and process for producing the same |
| CN101300982A (en) * | 2008-06-27 | 2008-11-12 | 中南大学 | Method for preparing silver-carrying nano titanic oxide |
| CN103190442A (en) * | 2013-02-28 | 2013-07-10 | 陈自金 | Composite antibacterial anion air cleanser and preparation method thereof |
| CN105998637A (en) * | 2016-05-11 | 2016-10-12 | 保护伞环保科技成都有限公司 | Long-acting air purification spray |
| CN107955426A (en) * | 2017-12-06 | 2018-04-24 | 杭州诗杭新材料科技有限公司 | One kind is except formaldehyde spray liniment and preparation method thereof |
| CN109603524A (en) * | 2018-12-27 | 2019-04-12 | 秦皇岛威曼斯环保工程集团有限公司 | A kind of negative oxygen ion photocatalyst Formaldehyde decomposition liquid and preparation method thereof |
-
2020
- 2020-08-17 CN CN202010822378.5A patent/CN111841314A/en not_active Withdrawn
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5935608A (en) * | 1996-04-15 | 1999-08-10 | Nittetsu Mining Co., Ltd. | Antibacterial titania and process for producing the same |
| CN101300982A (en) * | 2008-06-27 | 2008-11-12 | 中南大学 | Method for preparing silver-carrying nano titanic oxide |
| CN103190442A (en) * | 2013-02-28 | 2013-07-10 | 陈自金 | Composite antibacterial anion air cleanser and preparation method thereof |
| CN105998637A (en) * | 2016-05-11 | 2016-10-12 | 保护伞环保科技成都有限公司 | Long-acting air purification spray |
| CN107955426A (en) * | 2017-12-06 | 2018-04-24 | 杭州诗杭新材料科技有限公司 | One kind is except formaldehyde spray liniment and preparation method thereof |
| CN109603524A (en) * | 2018-12-27 | 2019-04-12 | 秦皇岛威曼斯环保工程集团有限公司 | A kind of negative oxygen ion photocatalyst Formaldehyde decomposition liquid and preparation method thereof |
Non-Patent Citations (4)
| Title |
|---|
| 冯强: "《实用生活法宝大全》", 30 November 2014, 北方妇女儿童出版社 * |
| 彭春生等: "《一粒种子的幸福生活 人气多肉香草在家玩》", 31 July 2015, 青岛出版社 * |
| 武杰: "《新型果蔬食品加工工艺与配方》", 31 January 2001, 科学技术文献出版社 * |
| 田景振等: "《抗病毒中草药的研究与应用》", 30 April 2019, 山东科学技术出版社 * |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN110951303A (en) | Plant antibacterial water paint capable of decomposing formaldehyde and releasing negative ions | |
| CN106560243B (en) | A kind of antibacterial metal ions/titanium supported hydroxyapatite nano-photocatalyst and preparation method thereof | |
| CN109224878A (en) | A kind of air cleaning composite antibacterial film and preparation method | |
| CN113652110B (en) | Monoatomic antibacterial antiviral formaldehyde-removing paint additive suitable for interior wall paint and preparation method thereof | |
| CN108244145A (en) | Triple effect all-weather light catalyst indoor air purification agent and preparation method and application | |
| JP2017025383A (en) | Manufacturing method of metal nanoparticle composition, metal nanoparticle composition, antibacterial agent, and dye | |
| Bapat et al. | Surface-modified water hyacinth (Eichhornia crassipes) over activated carbon for wastewater treatment: a comparative account | |
| CN106345218A (en) | Antibacterial air purifying material and preparing method thereof | |
| CN107754584A (en) | A kind of spray liniment for indoor harmful substance of degrading and preparation method thereof | |
| CN111097279A (en) | Environment-friendly indoor environment purifying agent and preparation method thereof | |
| CN107008055A (en) | A kind of air purifier environment-friendly high-efficiency material for core and preparation method thereof | |
| CN102872473A (en) | Environment-friendly air purifying preparation and method for manufacturing same | |
| CN105478075A (en) | Air-purifying modified nano-composite material for aqueous system | |
| CN111841314A (en) | Ionized negative ion spray and preparation method thereof | |
| CN112844004A (en) | Spray type air purifying agent and preparation method thereof | |
| CN104474814A (en) | Air purifying agent and preparation method thereof | |
| CN115245176A (en) | Synthetic method for preparing antibacterial agent containing nano silver powder and having antibacterial property | |
| CN111040477A (en) | Dry powder coating with lasting antibacterial and mildew-proof effects and preparation method thereof | |
| CN106689201B (en) | Nano silver antibacterial agent and preparation method thereof | |
| CN110917838B (en) | Light/oxygen catalyst purifying agent and preparation method and application thereof | |
| CN109603921A (en) | A kind of nano photo-catalytic composite material and preparation method and application | |
| CN110882625A (en) | Environment-friendly aldehyde-removing smell-cleaning agent and preparation method thereof | |
| CN113521100A (en) | Nano silver ion disinfectant and preparation method and application thereof | |
| Faruruwa et al. | Green synthesis, characterization and antibacterial activity of zinc oxide and titanium dioxide nanoparticles using Terminalia catappa and Cymbopogon citratus leaf extract | |
| CN113265169A (en) | Antibacterial antiviral formaldehyde-removing antifouling agent and preparation method thereof, glazed tile and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20201030 |