CN111686018A - Formula and preparation method of anti-blue-light isolation emulsion - Google Patents
Formula and preparation method of anti-blue-light isolation emulsion Download PDFInfo
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Abstract
The invention discloses a formula and a preparation method of blue-light-resistant isolation milk, and relates to the technical field of skin care products. The material comprises the following raw material components in parts by weight: 6.0 to 10.0 percent of butanediol, 5.0 to 10.0 percent of cyclopentyldimethyl siloxane, 3.0 to 6.0 percent of butanediol dicaprylate/dicaprate, 1.5 to 3.5 percent of cetyl PEG/PPG-10/1 polydimethylsiloxane, 2.0 to 5.0 percent of isododecane, 0.3 to 1.5 percent of PEG-10 polydimethylsiloxane, 0.6 to 1.0 percent of sodium chloride, 2.0 to 10.0 percent of inorganic ultraviolet absorbent, 3.0 to 10.0 percent of organic ultraviolet absorbent, 0.1 to 0.8 percent of disteardimonium hectorite, 1.0 to 5.0 percent of hydrogenated polyisobutene, 0.5 to 2.0 percent of plant extraction and repair essence, 1.0 to 2.0 percent of stearyloxypolysiloxane/polydimethylsiloxane copolymer, 0.3 to 0.9 percent of dimethyl silylated silica, 0.05 to 0.3 percent of tocopherol acetate, 1.0 to 3.0 percent of ethanol, 0.5 to 0 percent of ethyl hexyl glycerol, and 0.6 to 0.6 percent of phenoxy glycerol, 0.01 to 0.1 percent of sodium hyaluronate, 1.0 to 5.0 percent of polydimethylsiloxane and 0.35 to 1.5 percent of blue light resistant plant extract component.
Description
Technical Field
The invention relates to the technical field of skin care products, in particular to a formula and a preparation method of blue light resistant isolation milk.
Background
Various sun-proof isolation products on the market are various, and mainly claim a sun-proof function, namely ultraviolet rays for preventing solar radiation in the daytime, and in addition, the sun-proof isolation products also have additional functions with skin care and maintenance effects of moisturizing, whitening, oil control and the like, and have sun protection of UVA and UVB wave bands, namely wave band protection of 275-400 nm wavelength. The products are subdivided with different SPF and PA values, and distinguished on top of the additional function of skin care. The frequency of use of electronic products with display screens in modern work and life is increasing, and besides natural sunlight radiating ultraviolet rays, people are also exposed to blue light radiated by the electronic products at a higher frequency.
Because blue light radiated by an electronic product display screen is very harmful to a human body, at present, fewer protective cosmetics specially applied to blue light radiation have good market prospects by combining multiple effects of sun protection in broad spectrum, radiation pollution isolation, skin repair, blemish hiding, skin color brightening and the like, and a design and development of an isolation emulsion for applying on the skin are needed to reduce or block the damage of the blue light radiated by the electronic display product to the human body and simultaneously provide more repair and maintenance effects for the skin.
Disclosure of Invention
Aiming at the defects of the prior art, the invention provides a formula and a preparation method of an anti-blue-light isolation milk, which aim to solve the problems in the background art.
In order to achieve the purpose, the invention provides the following technical scheme: the formula of the blue-light-resistant isolation milk comprises the following raw material components in parts by mass: 6.0 to 10.0 percent of butanediol, 5.0 to 10.0 percent of cyclopentyldimethyl siloxane, 3.0 to 6.0 percent of butanediol dicaprylate/dicaprate, 1.5 to 3.5 percent of cetyl PEG/PPG-10/1 polydimethylsiloxane, 2.0 to 5.0 percent of isododecane, 0.3 to 1.5 percent of PEG-10 polydimethylsiloxane, 0.6 to 1.0 percent of sodium chloride, 2.0 to 10.0 percent of inorganic ultraviolet absorbent, 3.0 to 10.0 percent of organic ultraviolet absorbent, 0.1 to 0.8 percent of disteardimonium hectorite, 1.0 to 5.0 percent of hydrogenated polyisobutene, 0.5 to 2.0 percent of plant extraction and repair essence, 1.0 to 2.0 percent of stearyloxypolysiloxane/polydimethylsiloxane copolymer, 0.3 to 0.9 percent of dimethyl silylated silica, 0.05 to 0.3 percent of tocopherol acetate, 1.0 to 3.0 percent of ethanol, 0.5 to 0 percent of ethyl hexyl glycerol, and 0.6 to 0.6 percent of phenoxy glycerol, 0.01-0.1 percent of sodium hyaluronate, 1.0-5.0 percent of polydimethylsiloxane, 0.35-1.5 percent of blue light resistant plant extract component, 0.01-0.05 percent of essence, 0.05-0.30 percent of ferric oxide and the balance of deionized water being 100 percent.
A preparation method of a formula of blue light resistant isolation milk comprises the following steps:
s1, grinding of the raw material I: weighing butanediol dicaprylate/dicaprate, PEG-10 polydimethylsiloxane, an inorganic ultraviolet absorbent, hydrogenated polyisobutene and ferric oxide in sequence according to the percentage, putting the mixture into a tank, uniformly stirring the mixture, and finely grinding the mixture for 30min by using a colloid mill to obtain a required raw material I for later use;
s2, dissolving a second raw material: sequentially weighing cyclopentadimethylsiloxane, cetyl PEG/PPG-10/1 polydimethylsiloxane, isododecane, organic ultraviolet absorbent, disteardimonium hectorite, stearyloxymethylsiloxane/polydimethylsiloxane copolymer, silica dimethyl silylate, tocopheryl acetate and polydimethylsiloxane according to the percentage, putting the materials into an emulsifying pot, heating to dissolve the materials, and uniformly stirring the materials to obtain a required raw material II for later use;
s3, preparing a mixture: putting the ground raw material I in the step S1 into the emulsifying pot in the step S2, and stirring and homogenizing again to obtain a required mixture;
s4, preparation of a raw material III: weighing butanediol, sodium chloride, sodium hyaluronate and deionized water in percentage in turn, putting into a water phase pot, heating for dissolving, and uniformly stirring to obtain a required raw material III for later use;
s5, first treatment of the mixture: stirring the emulsifying pot in the step S3 at a high speed of 800-1200rpm, and slowly pumping the dissolved solution in the step S4 into the emulsifying pot until no water is accumulated on the liquid surface of the complete package for later use;
s6, secondary treatment of the mixture: weighing the plant extraction repair essence and the blue-light resisting plant extraction components in percentage in sequence, putting into the emulsifying pot in the step S5, stirring uniformly, and stirring at high speed for 3min for later use;
s7, obtaining blue-light resistant isolation milk: and (5) stirring the emulsifying pot in the step (S6) and starting the first homogenization treatment, cooling, sequentially adding ethanol, phenoxyethanol & ethylhexyl glycerin and essence into the emulsifying pot, starting the second homogenization treatment, and continuously stirring for 10min to finish the preparation, thereby obtaining the required blue-light resistant isolation milk.
In order to further optimize the technical solution, the inorganic ultraviolet absorbent in step S1 is preferably one or a combination of nano titanium dioxide, nano zinc oxide, triethoxy octyl silane and nano cerium oxide.
In order to further optimize the technical solution, the organic ultraviolet absorbent in step S2 is preferably one or a combination of ethylhexyl methoxycinnamate, hexyl diethylamino-benzoylbenzoate, ethylhexyl salicylate, methylene bis-benzotriazolyl tetramethylbutylphenol, bis-ethylhexyloxyphenol methoxyphenyl triazine, and ethylhexyl triazone.
Further optimizing the technical scheme, the dissolving temperature in the step S2 is 80-85 ℃, the stirring homogenizing rotation speed in the step S3 is 3000rpm, and the stirring time is 20-30 min.
Further optimizing the technical scheme, the plant extraction and repair essence in the step S6 is a composition of dendrobium nobile extract, sophora flavescens root extract, echinacea purpurea extract, lycium barbarum fruit extract and aloe barbadensis extract.
Further optimizing the technical solution, the anti-blue-light plant extract component in step S6 is a combination of wild soybean oil, rice germ extract and rice extract.
Further optimizing the technical scheme, wherein the heating temperature of the water phase pot in the step S4 is 75-80 ℃.
Further optimizing the technical scheme, the rotation speed of the first homogenization treatment in the step S7 is 3000rpm, the time is 5min, the temperature after the temperature reduction treatment in the step S7 is 40-50 ℃, the rotation speed of the second homogenization treatment in the step S7 is 3000rpm, and the time is 5 min.
Compared with the prior art, the invention provides a formula and a preparation method of blue-light resistant isolation milk, and the blue-light resistant isolation milk has the following beneficial effects:
1. according to the formula and the preparation method of the anti-blue-light isolation emulsion, the organic ultraviolet absorbent, the inorganic absorbent and the anti-blue-light component extracted from plants are used in a matching manner, the synergistic effect is promoted, the damage of an ultraviolet blue-light waveband to skin is blocked, the stable and efficient absorbent with the UVA wavelength of 320 nm and 400nm and the nano cerium oxide are particularly screened and used in an accurate ratio, the comprehensive absorption capacity is provided for the blue-light waveband, and the blue-light resistance and the cell damage caused by the blue-light resistance are repaired.
2. The blue light resistant isolation milk is scientific in proportioning, good in light stability, efficient in absorption, low in dosage, low in irritation and high in safety coefficient, excellent blue light resistant application of the plant rice embryo extract component brings safer and milder guarantee for the product, and meanwhile, the preparation method is easy to realize and can realize large-scale mass production.
Drawings
FIG. 1 is a flow chart of a formula and a preparation method of the blue light resistant isolation milk provided by the invention.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The first embodiment is as follows: referring to fig. 1, the invention discloses a formula of blue light resistant isolation milk, which comprises the following raw material components in parts by weight: 7.0 percent of butanediol, 9.0 percent of cyclopentadimethylsiloxane, 3.0 percent of butanediol dicaprylate/dicaprate, 2.0 percent of cetyl PEG/PPG-10/1 polydimethylsiloxane, 2.0 percent of isododecane, 0.5 percent of PEG-10 polydimethylsiloxane, 0.8 percent of sodium chloride, 2.0 percent of inorganic ultraviolet absorbent, 10.0 percent of organic ultraviolet absorbent, 0.6 percent of disteardimonium hectorite, 2.0 percent of hydrogenated polyisobutene, 2.0% of plant extraction and repair essence, 2.0% of stearyloxypolysiloxane/polydimethylsiloxane copolymer, 0.6% of dimethyl silylated silica, 0.1% of tocopherol acetate, 2.0% of ethanol, 0.5% of phenoxyethanol & ethylhexyl glycerin, 0.02% of sodium hyaluronate, 1.0% of polydimethylsiloxane, 1.0% of blue light resistant plant extraction component, 0.02% of essence, 0.05% of ferric oxide and the balance of deionized water being 100%.
A preparation method of a formula of blue light resistant isolation milk comprises the following steps:
s1, grinding of the raw material I: weighing butanediol dicaprylate/dicaprate, PEG-10 polydimethylsiloxane, an inorganic ultraviolet absorbent, hydrogenated polyisobutene and ferric oxide in sequence according to the percentage, putting the mixture into a tank, uniformly stirring, and finely grinding the mixture for 30min by using a colloid mill to obtain a required raw material I, wherein the inorganic ultraviolet absorbent is preferably one of nano titanium dioxide for later use;
s2, dissolving a second raw material: sequentially weighing cyclopentadimethylsiloxane, cetyl PEG/PPG-10/1 polydimethylsiloxane, isododecane, organic ultraviolet absorbent, disteardimonium hectorite, stearyloxypolysiloxane/polydimethylsiloxane copolymer, silica dimethyl silylate, tocopheryl acetate and polydimethylsiloxane into an emulsifying pot according to the percentage, heating to dissolve at the temperature of 80 ℃, and uniformly stirring to obtain a required raw material II, wherein the organic ultraviolet absorbent is preferably a combination of ethylhexyl methoxycinnamate and diethyl aminohydroxybenzoate benzoylhexyl benzoate for later use;
s3, preparing a mixture: putting the ground raw material I in the step S1 into the emulsifying pot in the step S2, and stirring and homogenizing again at the rotating speed of 3000rpm for 20min to obtain a required mixture;
s4, preparation of a raw material III: weighing butanediol, sodium chloride, sodium hyaluronate and deionized water in percentage in turn, putting into a water phase pot, heating to dissolve, and stirring uniformly, wherein the heating temperature of the water phase pot is 75 ℃, so as to obtain the required raw material III for later use;
s5, first treatment of the mixture: stirring the emulsifying pot in the step S3 at a high speed of 1200rpm, slowly pumping the dissolved solution in the step S4 into the emulsifying pot until the liquid surface of the complete package is free from water accumulation for later use;
s6, secondary treatment of the mixture: weighing plant extraction and repair essence and blue light resisting plant extraction components in percentage in sequence, putting the mixture into an emulsifying pot in the step S5, uniformly stirring the mixture, and stirring the mixture at a high speed for 3min for later use, wherein the plant extraction and repair essence is a composition of dendrobium nobile extract, sophora flavescens root extract, echinacea purpurea extract, lycium barbarum fruit extract and aloe barbarum extract, and the blue light resisting plant extraction components are a composition of wild soybean oil, rice germ extract and rice extract;
s7, obtaining blue-light resistant isolation milk: and (5) stirring the emulsifying pot in the step (S6) and starting first homogenization treatment, cooling, wherein the temperature after cooling is 40 ℃, adding ethanol, phenoxyethanol & ethylhexyl glycerin and essence into the emulsifying pot in sequence, starting second homogenization treatment, stirring for 10min, and finishing preparation to obtain the required blue-light resistant isolation milk, wherein the rotation speed of the first homogenization treatment is 3000rpm, the time is 5min, and the rotation speed of the second homogenization treatment is 3000rpm, and the time is 5 min.
Example two: referring to fig. 1, the invention discloses a formula of blue light resistant isolation milk, which comprises the following raw material components in parts by weight: 7.0 percent of butanediol, 7.5 percent of cyclopentadimethylsiloxane, 3.0 percent of butanediol dicaprylate/dicaprate, 2.5 percent of cetyl PEG/PPG-10/1 polydimethylsiloxane, 4.0 percent of isododecane, 0.5 percent of PEG-10 polydimethylsiloxane, 0.8 percent of sodium chloride, 5.0 percent of inorganic ultraviolet absorbent, 6.0 percent of organic ultraviolet absorbent, 0.6 percent of disteardimonium hectorite, 2.0 percent of hydrogenated polyisobutene, 1.5% of plant extraction and repair essence, 2.0% of stearyloxypolysiloxane/polydimethylsiloxane copolymer, 0.3% of dimethyl silylated silica, 0.1% of tocopherol acetate, 1.0% of ethanol, 0.6% of phenoxyethanol & ethylhexylglycerin, 0.02% of sodium hyaluronate, 1.0% of polydimethylsiloxane, 1.0% of blue light resistant plant extraction component, 0.02% of essence, 0.1% of ferric oxide and 100% of deionized water.
A preparation method of a formula of blue light resistant isolation milk comprises the following steps:
s1, grinding of the raw material I: weighing butanediol dicaprylate/dicaprate, PEG-10 polydimethylsiloxane, an inorganic ultraviolet absorbent, hydrogenated polyisobutene and ferric oxide in sequence according to the percentage, putting the mixture into a tank, uniformly stirring, and finely grinding the mixture for 30min by using a colloid mill to obtain a required raw material I, wherein the inorganic ultraviolet absorbent is preferably a composition of nano zinc oxide and nano cerium oxide;
s2, dissolving a second raw material: sequentially weighing cyclopentadimethylsiloxane, cetyl PEG/PPG-10/1 polydimethylsiloxane, isododecane, organic ultraviolet absorbent, disteardimonium hectorite, stearyloxypolysiloxane/polydimethylsiloxane copolymer, silica dimethyl silylate, tocopheryl acetate and polydimethylsiloxane into an emulsifying pot according to the percentage, heating to dissolve at 81 ℃, and uniformly stirring to obtain a composition of a required raw material II, wherein the organic ultraviolet absorbent is preferably diethyl-hydroxy-benzoyl-benzoic hexyl benzoate and ethylhexyl salicylate for later use;
s3, preparing a mixture: putting the ground raw material I in the step S1 into the emulsifying pot in the step S2, and stirring and homogenizing again at the rotating speed of 3000rpm for 28min to obtain a required mixture;
s4, preparation of a raw material III: weighing butanediol, sodium chloride, sodium hyaluronate and deionized water in percentage in turn, putting into a water phase pot, heating to dissolve, and stirring uniformly, wherein the heating temperature of the water phase pot is 76 ℃ to obtain a required raw material III for later use;
s5, first treatment of the mixture: stirring the emulsifying pot in the step S3 at a high speed of 900rpm, slowly pumping the dissolved solution in the step S4 into the emulsifying pot until the liquid surface of the coating is completely coated and no water is accumulated for later use;
s6, secondary treatment of the mixture: sequentially weighing plant extraction and repair essence and blue light resistant plant extraction components according to the percentage, wherein the plant extraction and repair essence is a composition of dendrobium nobile extract, sophora flavescens root extract, echinacea purpurea extract, fructus lycii extract and aloe barbadensis extract, and the blue light resistant plant extraction components are a composition of wild soybean oil, rice germ extract and rice extract, putting the composition into the milk obtained in the step S5, dissolving the mixture in a pot, uniformly stirring the mixture, and stirring the mixture at a high speed for 3min for later use;
s7, obtaining blue-light resistant isolation milk: and (5) stirring the emulsifying pot in the step S6, starting first homogenization treatment, cooling, wherein the temperature after cooling is 43 ℃, adding ethanol, phenoxyethanol & ethylhexyl glycerin and essence into the emulsifying pot in sequence, starting second homogenization treatment, wherein the rotation speed of the first homogenization treatment is 3000rpm, the time is 5min, the rotation speed of the second homogenization treatment is 3000rpm, and the time is 5min, continuing stirring for 10min, and completing preparation to obtain the required blue-light resistant isolation milk.
Example three: referring to fig. 1, the invention discloses a formula of blue light resistant isolation milk, which comprises the following raw material components in parts by weight: 9.0 percent of butanediol, 7.5 percent of cyclopentadimethylsiloxane, 6.0 percent of butanediol dicaprylate/dicaprate, 3.5 percent of cetyl PEG/PPG-10/1 polydimethylsiloxane, 4.0 percent of isododecane, 1.0 percent of PEG-10 polydimethylsiloxane, 1.0 percent of sodium chloride, 6.0 percent of inorganic ultraviolet absorbent, 6.0 percent of organic ultraviolet absorbent, 0.5 percent of disteardimonium hectorite, 4.0 percent of hydrogenated polyisobutene, 1.5% of plant extraction and repair essence, 1.0% of stearyloxypolysiloxane/polydimethylsiloxane copolymer, 0.5% of dimethyl silylated silica, 0.1% of tocopherol acetate, 1.0% of ethanol, 0.6% of phenoxyethanol & ethylhexyl glycerin, 0.03% of sodium hyaluronate, 2.0% of polydimethylsiloxane, 0.35% of blue light resistant plant extraction component, 0.03% of essence, 0.2% of ferric oxide and the balance of deionized water being 100%.
A preparation method of a formula of blue light resistant isolation milk comprises the following steps:
s1, grinding of the raw material I: weighing butanediol dicaprylate/dicaprate, PEG-10 polydimethylsiloxane, an inorganic ultraviolet absorbent, hydrogenated polyisobutene and ferric oxide in sequence according to the percentage, putting the mixture into a tank, uniformly stirring, and finely grinding the mixture for 30min by using a colloid mill to obtain a required raw material I, wherein the inorganic ultraviolet absorbent is preferably a composition of nano titanium dioxide and triethoxyoctylsilane for later use;
s2, dissolving a second raw material: sequentially weighing cyclopentadimethylsiloxane, cetyl PEG/PPG-10/1 polydimethylsiloxane, isododecane, organic ultraviolet absorbent, disteardimonium hectorite, stearyloxypolydimethylsiloxane/polydimethylsiloxane copolymer, silica dimethyl silylate, tocopherol acetate and polydimethylsiloxane into an emulsifying pot according to the percentage, heating to dissolve at 82 ℃, and uniformly stirring to obtain a required raw material II, wherein the organic ultraviolet absorbent is preferably a composition of methylene bis-benzotriazolyl tetramethylbutyl phenol and bis-ethylhexyloxyphenol methoxyphenyl triazine;
s3, preparing a mixture: putting the ground raw material I in the step S1 into the emulsifying pot in the step S2, and stirring and homogenizing again at the rotating speed of 3000rpm for 26min to obtain a required mixture;
s4, preparation of a raw material III: weighing butanediol, sodium chloride, sodium hyaluronate and deionized water in percentage in turn, putting into a water phase pot, heating to dissolve, and stirring uniformly, wherein the heating temperature of the water phase pot is 78 ℃, so as to obtain the required raw material III for later use;
s5, first treatment of the mixture: stirring the emulsifying pot in the step S3 at a high speed of 1100rpm, slowly pumping the dissolved solution in the step S4 into the emulsifying pot until the liquid surface of the complete package is free from water accumulation for later use;
s6, secondary treatment of the mixture: weighing plant extraction and repair essence and blue light resisting plant extraction components in percentage in sequence, putting the mixture into an emulsifying pot in the step S5, uniformly stirring the mixture, and stirring the mixture at a high speed for 3min, wherein the plant extraction and repair essence is a composition of dendrobium nobile extract, sophora flavescens root extract, echinacea purpurea extract, lycium barbarum fruit extract and aloe barbadensis extract, and the blue light resisting plant extraction components are a composition of wild soybean oil, rice germ extract and rice extract for later use;
s7, obtaining blue-light resistant isolation milk: and (5) stirring the emulsifying pot in the step S6, starting first homogenization treatment, cooling, wherein the temperature after cooling is 48 ℃, sequentially adding ethanol, phenoxyethanol & ethylhexyl glycerin and essence into the emulsifying pot, starting second homogenization treatment, wherein the rotation speed of the first homogenization treatment is 3000rpm, the time is 5min, the rotation speed of the second homogenization treatment is 3000rpm, the time is 5min, and stirring is continued for 10min, so that the preparation is completed, and the required blue-light resistant isolation milk is obtained.
Example four: referring to fig. 1, the invention discloses a formula of blue light resistant isolation milk, which comprises the following raw material components in parts by weight: 9.0 percent of butanediol, 5.0 percent of cyclopentadimethylsiloxane, 3.0 to 6.0 percent of butanediol dicaprylate/dicaprate, 3.0 percent of cetyl PEG/PPG-10/1 polydimethylsiloxane, 5.0% of isododecane, 1.0% of PEG-10 polydimethylsiloxane, 1.0% of sodium chloride, 8.0% of inorganic ultraviolet absorbent, 4.0% of organic ultraviolet absorbent, 0.3% of disteardimonium hectorite, 5.0% of hydrogenated polyisobutene, 0.5% of plant extraction repair essence, 1.0% of stearyloxypolysiloxane/polydimethylsiloxane copolymer, 0.8% of silica dimethylsilylate, 0.2% of tocopherol acetate, 2.0% of ethanol, 0.6% of phenoxyethanol & ethylhexylglycerin, 0.05% of sodium hyaluronate, 5.0% of polydimethylsiloxane, 1.5% of anti-blue-light plant extraction component, 0.05% of essence, 0.2% of iron oxide and the balance of deionized water being 100%.
A preparation method of a formula of blue light resistant isolation milk comprises the following steps:
s1, grinding of the raw material I: weighing butanediol dicaprylate/dicaprate, PEG-10 polydimethylsiloxane, an inorganic ultraviolet absorbent, hydrogenated polyisobutene and ferric oxide in sequence according to the percentage, putting the mixture into a tank, uniformly stirring, finely grinding the mixture for 30min by using a colloid mill, and preferably selecting a composition of triethoxyoctylsilane and nano cerium oxide as the inorganic ultraviolet absorbent to obtain a required raw material I for later use;
s2, dissolving a second raw material: sequentially weighing cyclopentadimethylsiloxane, cetyl PEG/PPG-10/1 polydimethylsiloxane, isododecane, organic ultraviolet absorbent, disteardimonium hectorite, stearyloxypolysiloxane/polydimethylsiloxane copolymer, silica dimethyl silylate, tocopherol acetate and polydimethylsiloxane according to the percentage, putting the materials into an emulsifying pot, heating to dissolve at 84 ℃, and uniformly stirring to obtain a required raw material II, wherein the organic ultraviolet absorbent is one or the combination of bis-ethylhexyloxyphenol methoxyphenyl triazine and ethylhexyltriazone;
s3, preparing a mixture: putting the ground raw material I in the step S1 into the emulsifying pot in the step S2, and stirring and homogenizing again at the rotating speed of 3000rpm for 28min to obtain a required mixture;
s4, preparation of a raw material III: weighing butanediol, sodium chloride, sodium hyaluronate and deionized water in percentage in sequence, putting into a water phase pot, heating the water phase pot at 79 ℃, heating to dissolve, and uniformly stirring to obtain a required raw material III for later use;
s5, first treatment of the mixture: stirring the emulsifying pot in the step S3 at a high speed of 900rpm, slowly pumping the dissolved solution in the step S4 into the emulsifying pot until the liquid surface of the coating is completely coated and no water is accumulated for later use;
s6, secondary treatment of the mixture: weighing plant extraction and repair essence and blue light resisting plant extraction components in percentage in sequence, putting the mixture into an emulsifying pot in the step S5, uniformly stirring the mixture, and stirring the mixture at a high speed for 3min, wherein the plant extraction and repair essence is a composition of dendrobium nobile extract, sophora flavescens root extract, echinacea purpurea extract, lycium barbarum fruit extract and aloe barbadensis extract, and the blue light resisting plant extraction components are a composition of wild soybean oil, rice germ extract and rice extract for later use;
s7, obtaining blue-light resistant isolation milk: and (5) stirring the emulsifying pot in the step S6, starting first homogenization treatment, cooling, wherein the temperature after cooling is 49 ℃, sequentially adding ethanol, phenoxyethanol & ethylhexyl glycerin and essence into the emulsifying pot, starting second homogenization treatment, stirring for 10min, wherein the rotation speed of the first homogenization treatment is 3000rpm for 5min, the rotation speed of the second homogenization treatment is 3000rpm for 5min, and the time is 5min, so that the preparation is completed, and the required blue-light resistant isolation milk is obtained.
Example five: referring to fig. 1, the invention discloses a formula of blue light resistant isolation milk, which comprises the following raw material components in parts by weight: 8.0 percent of butanediol, 5.0 percent of cyclopentadimethylsiloxane, 5.0 percent of butanediol dicaprylate/dicaprate, 3.0 percent of cetyl PEG/PPG-10/1 polydimethylsiloxane, 5.0 percent of isododecane, 1.5 percent of PEG-10 polydimethylsiloxane, 1.0 percent of sodium chloride, 8.0 percent of inorganic ultraviolet absorbent, 3.0 percent of organic ultraviolet absorbent, 0.3 percent of disteardimonium hectorite, 5.0 percent of hydrogenated polyisobutene, 0.5% of plant extraction and repair essence, 1.0% of stearyloxypolysiloxane/polydimethylsiloxane copolymer, 0.8% of dimethyl silylated silica, 0.2% of tocopherol acetate, 3.0% of ethanol, 0.5% of phenoxyethanol & ethylhexyl glycerin, 0.05% of sodium hyaluronate, 5.0% of polydimethylsiloxane, 0.5% of blue-light-resistant plant extraction component, 0.05% of essence, 0.30% of ferric oxide and 100% of the balance of deionized water.
A preparation method of a formula of blue light resistant isolation milk comprises the following steps:
s1, grinding of the raw material I: weighing butanediol dicaprylate/dicaprate, PEG-10 polydimethylsiloxane, an inorganic ultraviolet absorbent, hydrogenated polyisobutene and ferric oxide in sequence according to the percentage, putting the mixture into a tank, uniformly stirring, finely grinding the mixture for 30min by using a colloid mill, and preferably selecting a composition of nano titanium dioxide, nano zinc oxide, triethoxyoctylsilane and nano cerium oxide as the inorganic ultraviolet absorbent to obtain a required raw material I for later use;
s2, dissolving a second raw material: sequentially weighing cyclopentadimethylsiloxane, cetyl PEG/PPG-10/1 polydimethylsiloxane, isododecane, an organic ultraviolet absorbent, disteardimonium hectorite, stearyloxypolysiloxane/polydimethylsiloxane copolymer, silica dimethyl silylate, tocopherol acetate and polydimethylsiloxane into an emulsifying pot, heating to dissolve at 85 ℃, and uniformly stirring to obtain a required raw material II, wherein the organic ultraviolet absorbent is preferably a composition of ethylhexyl methoxycinnamate, hexyl diethylcarbamoylbenzoate, ethylhexyl salicylate, methylene bis-benzotriazolyl tetramethylbutyl phenol, bis-ethylhexyloxyphenol methoxyphenyl triazine and ethylhexyl triazone for later use;
s3, preparing a mixture: putting the ground raw material I in the step S1 into the emulsifying pot in the step S2, and stirring and homogenizing again at the rotating speed of 3000rpm for 30min to obtain a required mixture;
s4, preparation of a raw material III: weighing butanediol, sodium chloride, sodium hyaluronate and deionized water in percentage in turn, putting into a water phase pot, heating the water phase pot at 80 ℃, heating to dissolve, and uniformly stirring to obtain a required raw material III for later use;
s5, first treatment of the mixture: stirring the emulsifying pot in the step S3 at a high speed of 1200rpm, slowly pumping the dissolved solution in the step S4 into the emulsifying pot until the liquid surface of the complete package is free from water accumulation for later use;
s6, secondary treatment of the mixture: weighing plant extraction and repair essence and blue light resisting plant extraction components in percentage in sequence, putting the mixture into an emulsifying pot in the step S5, uniformly stirring the mixture, and stirring the mixture at a high speed for 3min, wherein the plant extraction and repair essence is a composition of dendrobium nobile extract, sophora flavescens root extract, echinacea purpurea extract, lycium barbarum fruit extract and aloe barbadensis extract, and the blue light resisting plant extraction components are a composition of wild soybean oil, rice germ extract and rice extract for later use;
s7, obtaining blue-light resistant isolation milk: and (5) stirring the emulsifying pot in the step S6, starting first homogenization treatment, cooling, wherein the temperature after cooling is 50 ℃, sequentially adding ethanol, phenoxyethanol & ethylhexyl glycerin and essence into the emulsifying pot, starting second homogenization treatment, and stirring for 10min to finish preparation, wherein the rotation speed of the first homogenization treatment is 3000rpm and the time is 5min, and the rotation speed of the second homogenization treatment is 3000rpm and the time is 5min to obtain the required blue-light resistant isolation milk.
Table 1 below is a table of numerical variations for each example:
note: table 1 blue light resistant isolation emulsion formula (the total of all raw materials of the formula is 100%)
The invention has the beneficial effects that: according to the formula and the preparation method of the anti-blue-light isolation emulsion, the organic ultraviolet absorbent, the inorganic absorbent and the anti-blue-light component extracted from plants are used in a matching manner, the synergistic effect is promoted, the damage of an ultraviolet blue-light waveband to skin is blocked, the stable and efficient absorbent with the UVA wavelength of 320 nm and 400nm and the nano cerium oxide are particularly screened and used in an accurate ratio, the comprehensive absorption capacity is provided for the blue-light waveband, and the blue-light resistance and the cell damage caused by the blue-light resistance are repaired; the isolation milk prepared by the invention is scientific in proportioning, good in light stability, efficient in absorption, low in dosage, low in irritation and high in safety factor, and the excellent blue light resistance application of the isolation milk from plant rice embryo extract components brings safer and milder guarantee to the isolation milk, and meanwhile, the preparation method is easy to realize and can realize large-scale mass production.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (9)
1. The formula of the blue-light-resistant isolation milk is characterized by comprising the following raw material components in parts by mass: 6.0 to 10.0 percent of butanediol, 5.0 to 10.0 percent of cyclopentyldimethyl siloxane, 3.0 to 6.0 percent of butanediol dicaprylate/dicaprate, 1.5 to 3.5 percent of cetyl PEG/PPG-10/1 polydimethylsiloxane, 2.0 to 5.0 percent of isododecane, 0.3 to 1.5 percent of PEG-10 polydimethylsiloxane, 0.6 to 1.0 percent of sodium chloride, 2.0 to 10.0 percent of inorganic ultraviolet absorbent, 3.0 to 10.0 percent of organic ultraviolet absorbent, 0.1 to 0.8 percent of disteardimonium hectorite, 1.0 to 5.0 percent of hydrogenated polyisobutene, 0.5 to 2.0 percent of plant extraction and repair essence, 1.0 to 2.0 percent of stearyloxypolysiloxane/polydimethylsiloxane copolymer, 0.3 to 0.9 percent of dimethyl silylated silica, 0.05 to 0.3 percent of tocopherol acetate, 1.0 to 3.0 percent of ethanol, 0.5 to 0 percent of ethyl hexyl glycerol, and 0.6 to 0.6 percent of phenoxy glycerol, 0.01-0.1 percent of sodium hyaluronate, 1.0-5.0 percent of polydimethylsiloxane, 0.35-1.5 percent of blue light resistant plant extract component, 0.01-0.05 percent of essence, 0.05-0.30 percent of ferric oxide and the balance of deionized water being 100 percent.
2. The preparation method of the formula of the blue-light resistant isolation milk is characterized by comprising the following steps:
s1, grinding of the raw material I: weighing butanediol dicaprylate/dicaprate, PEG-10 polydimethylsiloxane, an inorganic ultraviolet absorbent, hydrogenated polyisobutene and ferric oxide in sequence according to the percentage, putting the mixture into a tank, uniformly stirring the mixture, and finely grinding the mixture for 30min by using a colloid mill to obtain a required raw material I for later use;
s2, dissolving a second raw material: sequentially weighing cyclopentadimethylsiloxane, cetyl PEG/PPG-10/1 polydimethylsiloxane, isododecane, organic ultraviolet absorbent, disteardimonium hectorite, stearyloxymethylsiloxane/polydimethylsiloxane copolymer, silica dimethyl silylate, tocopheryl acetate and polydimethylsiloxane according to the percentage, putting the materials into an emulsifying pot, heating to dissolve the materials, and uniformly stirring the materials to obtain a required raw material II for later use;
s3, preparing a mixture: putting the ground raw material I in the step S1 into the emulsifying pot in the step S2, and stirring and homogenizing again to obtain a required mixture;
s4, preparation of a raw material III: weighing butanediol, sodium chloride, sodium hyaluronate and deionized water in percentage in turn, putting into a water phase pot, heating for dissolving, and uniformly stirring to obtain a required raw material III for later use;
s5, first treatment of the mixture: stirring the emulsifying pot in the step S3 at a high speed of 800-1200rpm, and slowly pumping the dissolved solution in the step S4 into the emulsifying pot until no water is accumulated on the liquid surface of the complete package for later use;
s6, secondary treatment of the mixture: weighing the plant extraction repair essence and the blue-light resisting plant extraction components in percentage in sequence, putting into the emulsifying pot in the step S5, stirring uniformly, and stirring at high speed for 3min for later use;
s7, obtaining blue-light resistant isolation milk: and (5) stirring the emulsifying pot in the step (S6) and starting the first homogenization treatment, cooling, sequentially adding ethanol, phenoxyethanol & ethylhexyl glycerin and essence into the emulsifying pot, starting the second homogenization treatment, and continuously stirring for 10min to finish the preparation, thereby obtaining the required blue-light resistant isolation milk.
3. The method for preparing the formulation of blue light resistant barrier milk according to claim 2, wherein the inorganic ultraviolet absorbent in step S1 is preferably one or a combination of nano titanium dioxide, nano zinc oxide, triethoxyoctylsilane and nano cerium oxide.
4. The method for preparing the formulation of blue light resistant barrier milk according to claim 2, wherein the organic UV absorber in step S2 is preferably one or a combination of ethylhexyl methoxycinnamate, hexyl diethylamino hydroxybenzoyl benzoate, ethylhexyl salicylate, methylene bis-benzotriazolyl tetramethylbutyl phenol, bis-ethylhexyloxyphenol methoxyphenyl triazine, and ethylhexyl triazone.
5. The method for preparing the formulation of blue light resistant barrier milk according to claim 2, wherein the dissolution temperature in step S2 is 80-85 ℃, the stirring homogenization speed in step S3 is 3000rpm, and the stirring time is 20-30 min.
6. The method for preparing the formula of the blue-light resistant barrier milk according to claim 2, wherein the plant extraction and repair essence in step S6 is a combination of dendrobium nobile lindl extract, sophora flavescens ait root extract, echinacea purpurea extract, lycium barbarum fruit extract and aloe barbadensis extract.
7. The method of claim 2, wherein the blue-light resistant plant extract component of step S6 is a combination of wild soybean oil, rice germ extract, and rice extract.
8. The method for preparing the formula of the blue-light resistant barrier milk according to claim 2, wherein the heating temperature of the water phase pot in the step S4 is 75-80 ℃.
9. The method for preparing the formulation of blue-light resistant barrier milk according to claim 2, wherein the rotation speed of the first homogenization treatment in step S7 is 3000rpm for 5min, the temperature after the temperature reduction treatment in step S7 is 40-50 ℃, and the rotation speed of the second homogenization treatment in step S7 is 3000rpm for 5 min.
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Application publication date: 20200922 |